CN107549220A - A kind of gardens synergy compound plant source pesticide and preparation method thereof - Google Patents

A kind of gardens synergy compound plant source pesticide and preparation method thereof Download PDF

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CN107549220A
CN107549220A CN201710894903.2A CN201710894903A CN107549220A CN 107549220 A CN107549220 A CN 107549220A CN 201710894903 A CN201710894903 A CN 201710894903A CN 107549220 A CN107549220 A CN 107549220A
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parts
root
chinese
raw
gardens
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林愿
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林愿
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

Abstract

The invention discloses a kind of gardens synergy compound plant source pesticide and preparation method thereof, it is prepared by the raw material of following parts by weight:16 25 parts of eucalyptol mother liquor, 8 14 parts of wartwort, 6 11 parts of tripterygium wilfordii, 7 11 parts of lilac daphne, 35 parts of chilli oil, 47 parts of root of Chinese clematis herb, 26 parts of baeckea frutescen, 15 21 parts of derris root, 7 12 parts of Eupatorium adenophorum, 6 12 parts of hairyvein agrimony.The present invention is using eucalyptol mother liquor, wartwort, tripterygium wilfordii, lilac daphne, chilli oil, root of Chinese clematis herb, baeckea frutescen, derris root, Eupatorium adenophorum, hairyvein agrimony, effective proportioning of raw material, insecticide is made, feedstock capture cost is low, make simple and convenient, there is good insecticidal effect to ethanol water rice, vegetables, fruit tree, tea tree etc., and it is environmentally safe, meet the requirement of green production;Seedling can be protected well, can effectively be killed off the insect pests, and small toxicity itself, nursery stock and human body will not be impacted.

Description

A kind of gardens synergy compound plant source pesticide and preparation method thereof
Technical field
The present invention relates to a kind of insecticide, and in particular to a kind of gardens synergy compound plant source pesticide and its preparation side Method.
Background technology
Agricultural insect management is the non-environmental pollution control of the important step that high yield increases income in agricultural production, especially subterranean pest-insect It is always the emphasis of agricultural plant protection circle concern, the technology and product of nontoxic, efficient, safe preventing and treating subterranean pest-insect are complete for many years The craving of ball agricultural community.
The species of subterranean pest-insect mainly has:Nemata, grub, cutworm, wireworm and some flies, the larva of mosquito class are each Kind ground maggot etc..The insecticide that preventing and treating to these insects allows to use is chemical synthetic pesticide AVM, phoxim, poisoned with poison A small amount of products such as tick, the matrine of fosthiazate and plant extract, nimbin, also dazomet, calcium cyanamide, vikane etc. are complete in addition Killing property fumigant.Wherein AVM, the prevention effect of chlopyrifos are several and be widely used better than other, but actually should In, the AVM lasting period is short, prevents and treats only 15 days or so vegetables Meloidogyne incognita lasting period.Chlopyrifos category poisoning agriculture Medicine, it is higher to fish and aquatic toxicity, it is poisonous to honeybee, and also its safety interval is longer.Some areas also often use
Fumigant realizes complete killing property, but fumigant is used and wasted time and energy, and cost is very high.
Also occur some botanical pesticides in the market, because composition is single, prevention effect is not good enough, the lasting period is short, peace Numerous reasons such as full interval length, therefore cannot be widely popularized in actual applications.What is more, is preferably killed to reach Worm effect, yield is improved, indivedual illegal hypertoxic insecticides disabled using national explicit order in area, causes malicious vegetables, malicious melon and fruit to show As happening occasionally, huge injury is brought to consumer.
The content of the invention
To solve the above problems, the invention provides a kind of gardens synergy compound plant source pesticide and its preparation side Method.
To achieve the above object, the technical scheme taken of the present invention is:
A kind of gardens synergy compound plant source pesticide, is prepared by the raw material of following parts by weight:
Eucalyptol mother liquor 16-25 parts, wartwort 8-14 parts, tripterygium wilfordii 6-11 parts, lilac daphne 7-11 parts, chilli oil 3-5 parts, the root of Chinese clematis are complete Careless 4-7 parts, baeckea frutescen 2-6 parts, derris root 15-21 parts, Eupatorium adenophorum 7-12 parts, hairyvein agrimony 6-12 parts, Chinese Stellera Root 1-4 parts, hardship Melon 3-8 parts, Chinese ephedra 1-7 parts, calamus 2-8 parts, ginger 2-8 parts, euphorbia lunulata 5-10 parts, emulsifying agent 6-11 parts, remaining is ethanol water Solution.
Further, a kind of gardens synergy compound plant source pesticide, is prepared by the raw material of following parts by weight:
Eucalyptol mother liquor 17-24 parts, wartwort 9-13 parts, tripterygium wilfordii 7-10 parts, lilac daphne 8-10 parts, chilli oil 4-5 parts, the root of Chinese clematis are complete Careless 4-6 parts, baeckea frutescen 3-5 parts, derris root 16-20 parts, Eupatorium adenophorum 8-11 parts, hairyvein agrimony 7-11 parts, Chinese Stellera Root 2-4 parts, hardship Melon 4-7 parts, Chinese ephedra 2-6 parts, calamus 3-7 parts, ginger 3-7 parts, euphorbia lunulata 6-9 parts, emulsifying agent 7-10 parts, remaining is that ethanol is water-soluble Liquid.
Further, a kind of gardens synergy compound plant source pesticide, is prepared by the raw material of following parts by weight:
19 parts of eucalyptol mother liquor, 11 parts of wartwort, 8 parts of tripterygium wilfordii, 9 parts of lilac daphne, 4 parts of chilli oil, 4 parts of root of Chinese clematis herb, baeckea frutescen 4 Part, 17 parts of derris root, 9 parts of Eupatorium adenophorum, 8 parts of hairyvein agrimony, 3 parts of Chinese Stellera Root, 5 parts of balsam pear, 5 parts of Chinese ephedra, 6 parts of calamus, ginger 5 Part, 9 parts of euphorbia lunulata, 8 parts of emulsifying agent, remaining is ethanol water.
Further, the preparation method of a kind of gardens synergy compound plant source pesticide, it is characterised in that by following step Suddenly it is made:
S1, crush:By eucalyptol mother liquor 17-24 parts, wartwort 9-13 parts, tripterygium wilfordii 7-10 parts, lilac daphne 8-10 parts, chilli oil 4-5 Part, root of Chinese clematis herb 4-6 parts, baeckea frutescen 3-5 parts, derris root 16-20 parts, Eupatorium adenophorum 8-11 parts, hairyvein agrimony 7-11 parts, winter daphne wolf Malicious 2-4 parts, balsam pear 4-7 parts, Chinese ephedra 2-6 parts, calamus 3-7 parts, ginger 3-7 parts, euphorbia lunulata 6-9 part raw materials, after being cleaned It is broken, and cross 40-50 mesh sieves;
S2, immersion:Take above-mentioned raw materials mix after with ethanol by 1:2 part by weight immersion with 68% ethanol, being in temperature Soaked one day at 40-80 DEG C, filter and remove residue, the pH value for adjusting leaching liquor is 7 mixing filtrate;
S3, concentration extraction:The mixing filtrate that step S2 is obtained is concentrated under reduced pressure, it is the dense of 1.3g/m3 that density, which is made, Contracting liquid;Then extracted with ether organic solvent, obtain raw material mixed biologic alkali;
S4, crystallization extraction:Propyl alcohol organic solvent is slowly added into step S3 raw material mixed biologic alkali, is occurred in liquid surface During crystal settling, stop extraction operation, add emulsifying agent 7-10 parts, stir and produce this product.
Further, the emulsifying agent is ethoxylated dodecyl alcohol, iso-octyl APEO and fatty amine polyoxy second One or more in alkene ether.
The present invention using eucalyptol mother liquor, wartwort, tripterygium wilfordii, lilac daphne, chilli oil, root of Chinese clematis herb, baeckea frutescen, derris root, Eupatorium adenophorum, hairyvein agrimony, Chinese Stellera Root, balsam pear, Chinese ephedra, calamus, effective proportioning of ginger raw material, are made insecticide, and raw material is adopted It is low to collect cost, making is simple and convenient, has good insecticidal effect to ethanol water rice, vegetables, fruit tree, tea tree etc., and right Environmental nonpollution, meet the requirement of green production;Seedling can be protected well, can effectively be killed off the insect pests, and Small toxicity itself, nursery stock and human body will not be impacted.
The present invention uses plant material, pure natural, nuisanceless, makees extractant using water or alcohol, simplifies production technology, reduces Production cost, the agricultural insecticide that the plant component that this technology is extracted makes is free of or contains organic solvent less, residual after processing Slag can do the carrier of this product, can also do organic fertilizer raw material, the discharge of three wastes material, clean manufacturing, green;User Just, application method is directly pouring, and can be to be used simultaneously with fertilizer before transplanting, time saving province convenient and swift compared with fumigating insecticide Power, reduce human cost.
Vegetable insecticide component of the present invention is simple, safe and convenient to use, noresidue pollution-free to food and cash crops, to people and animals Toxicity is low;Good disinsection effect, insect are not likely to produce the resistance to the action of a drug, and desinsection wide spectrum, had to the various pests of a variety of pesticide meridian crops Preventing and treating and killing effect.
Embodiment
In order that objects and advantages of the present invention are more clearly understood, the present invention is carried out with reference to embodiments further detailed Explanation.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not intended to limit the present invention.
A kind of gardens synergy compound plant source pesticide, is prepared by the raw material of following parts by weight:
Eucalyptol mother liquor 16-25 parts, wartwort 8-14 parts, tripterygium wilfordii 6-11 parts, lilac daphne 7-11 parts, chilli oil 3-5 parts, the root of Chinese clematis are complete Careless 4-7 parts, baeckea frutescen 2-6 parts, derris root 15-21 parts, Eupatorium adenophorum 7-12 parts, hairyvein agrimony 6-12 parts, Chinese Stellera Root 1-4 parts, hardship Melon 3-8 parts, Chinese ephedra 1-7 parts, calamus 2-8 parts, ginger 2-8 parts, euphorbia lunulata 5-10 parts, emulsifying agent 6-11 parts, remaining is ethanol water Solution.
A kind of gardens synergy compound plant source pesticide, is prepared by the raw material of following parts by weight:
Eucalyptol mother liquor 17-24 parts, wartwort 9-13 parts, tripterygium wilfordii 7-10 parts, lilac daphne 8-10 parts, chilli oil 4-5 parts, the root of Chinese clematis are complete Careless 4-6 parts, baeckea frutescen 3-5 parts, derris root 16-20 parts, Eupatorium adenophorum 8-11 parts, hairyvein agrimony 7-11 parts, Chinese Stellera Root 2-4 parts, hardship Melon 4-7 parts, Chinese ephedra 2-6 parts, calamus 3-7 parts, ginger 3-7 parts, euphorbia lunulata 6-9 parts, emulsifying agent 7-10 parts, remaining is that ethanol is water-soluble Liquid.
A kind of gardens synergy compound plant source pesticide, is prepared by the raw material of following parts by weight:
19 parts of eucalyptol mother liquor, 11 parts of wartwort, 8 parts of tripterygium wilfordii, 9 parts of lilac daphne, 4 parts of chilli oil, 4 parts of root of Chinese clematis herb, baeckea frutescen 4 Part, 17 parts of derris root, 9 parts of Eupatorium adenophorum, 8 parts of hairyvein agrimony, 3 parts of Chinese Stellera Root, 5 parts of balsam pear, 5 parts of Chinese ephedra, 6 parts of calamus, ginger 5 Part, 9 parts of euphorbia lunulata, 8 parts of emulsifying agent, remaining is ethanol water.
A kind of gardens preparation method of synergy compound plant source pesticide, is made up of following steps:
S1, crush:By eucalyptol mother liquor 17-24 parts, wartwort 9-13 parts, tripterygium wilfordii 7-10 parts, lilac daphne 8-10 parts, chilli oil 4-5 Part, root of Chinese clematis herb 4-6 parts, baeckea frutescen 3-5 parts, derris root 16-20 parts, Eupatorium adenophorum 8-11 parts, hairyvein agrimony 7-11 parts, winter daphne wolf Malicious 2-4 parts, balsam pear 4-7 parts, Chinese ephedra 2-6 parts, calamus 3-7 parts, ginger 3-7 parts, euphorbia lunulata 6-9 part raw materials, after being cleaned It is broken, and cross 40-50 mesh sieves;
S2, immersion:Take above-mentioned raw materials mix after with ethanol by 1:2 part by weight immersion with 68% ethanol, being in temperature Soaked one day at 40-80 DEG C, filter and remove residue, the pH value for adjusting leaching liquor is 7 mixing filtrate;
S3, concentration extraction:The mixing filtrate that step S2 is obtained is concentrated under reduced pressure, it is the dense of 1.3g/m3 that density, which is made, Contracting liquid;Then extracted with ether organic solvent, obtain raw material mixed biologic alkali;
S4, crystallization extraction:Propyl alcohol organic solvent is slowly added into step S3 raw material mixed biologic alkali, is occurred in liquid surface During crystal settling, stop extraction operation, add emulsifying agent 7-10 parts, stir and produce this product.
The emulsifying agent is one in ethoxylated dodecyl alcohol, iso-octyl APEO and aliphatic amine polyoxyethylene ether Kind is a variety of.
Embodiment 1
A kind of gardens preparation method of synergy compound plant source pesticide, is made up of following steps:
S1, crush:By 19 parts of eucalyptol mother liquor, 9 parts of tripterygium wilfordii, 9 parts of lilac daphne, 4 parts of chilli oil, 5 parts of root of Chinese clematis herb, baeckea frutescen 3 Part, 18 parts of derris root, 9 parts of Eupatorium adenophorum, 9 parts of hairyvein agrimony, 3 parts of Chinese Stellera Root, 7 parts of balsam pear, 7 parts of euphorbia lunulata, 4 parts of Chinese ephedra, Chang 6 parts of 5 parts of Pu, ginger raw materials, crushed after being cleaned, and cross 45 mesh sieves;
S2, immersion:Take above-mentioned raw materials mix after with ethanol by 1:2 part by weight immersion with 68% ethanol, being in temperature Soaked one day at 45 DEG C, filter and remove residue, the pH value for adjusting leaching liquor is 7 mixing filtrate;
S3, concentration extraction:The mixing filtrate that step S2 is obtained is concentrated under reduced pressure, it is the dense of 1.3g/m3 that density, which is made, Contracting liquid;Then extracted with ether organic solvent, obtain raw material mixed biologic alkali;
S4, crystallization extraction:Propyl alcohol organic solvent is slowly added into step S3 raw material mixed biologic alkali, is occurred in liquid surface During crystal settling, stop extraction operation, add 9 parts of emulsifying agent, stir and produce this product.
Embodiment 2
A kind of gardens preparation method of synergy compound plant source pesticide, is made up of following steps:
S1, crush:By 24 parts of eucalyptol mother liquor, 10 parts of tripterygium wilfordii, 10 parts of lilac daphne, 5 parts of chilli oil, 6 parts of root of Chinese clematis herb, baeckea frutescen 5 parts, 20 parts of derris root, 11 parts of Eupatorium adenophorum, 11 parts of hairyvein agrimony, 4 parts of Chinese Stellera Root, 7 parts of balsam pear, 9 parts of euphorbia lunulata, 6 parts of Chinese ephedra, 7 parts of 7 parts of calamus, ginger raw materials, crushed after being cleaned, and cross 40 mesh sieves;
S2, immersion:Take above-mentioned raw materials mix after with ethanol by 1:2 part by weight immersion with 68% ethanol, being in temperature Soaked one day at 40 DEG C, filter and remove residue, the pH value for adjusting leaching liquor is 7 mixing filtrate;
S3, concentration extraction:The mixing filtrate that step S2 is obtained is concentrated under reduced pressure, it is the dense of 1.3g/m3 that density, which is made, Contracting liquid;Then extracted with ether organic solvent, obtain raw material mixed biologic alkali;
S4, crystallization extraction:Propyl alcohol organic solvent is slowly added into step S3 raw material mixed biologic alkali, is occurred in liquid surface During crystal settling, stop extraction operation, add 7 parts of emulsifying agent, stir and produce this product.
Embodiment 3
A kind of gardens preparation method of synergy compound plant source pesticide, is made up of following steps:
S1, crush:By 17 parts of eucalyptol mother liquor, 7 parts of tripterygium wilfordii, 8 parts of lilac daphne, 4 parts of chilli oil, 4 parts of root of Chinese clematis herb, baeckea frutescen 3 Part, 16 parts of derris root, 8 parts of Eupatorium adenophorum, 7 parts of hairyvein agrimony, 2 parts of Chinese Stellera Root, 4 parts of balsam pear, 6 parts of euphorbia lunulata, 2 parts of Chinese ephedra, Chang 3 parts of 3 parts of Pu, ginger raw materials, crushed after being cleaned, and cross 50 mesh sieves;
S2, immersion:Take above-mentioned raw materials mix after with ethanol by 1:2 part by weight immersion with 68% ethanol, being in temperature Soaked one day at 80 DEG C, filter and remove residue, the pH value for adjusting leaching liquor is 7 mixing filtrate;
S3, concentration extraction:The mixing filtrate that step S2 is obtained is concentrated under reduced pressure, it is the dense of 1.3g/m3 that density, which is made, Contracting liquid;Then extracted with ether organic solvent, obtain raw material mixed biologic alkali;
S4, crystallization extraction:Propyl alcohol organic solvent is slowly added into step S3 raw material mixed biologic alkali, is occurred in liquid surface During crystal settling, stop extraction operation, add 10 parts of emulsifying agent, stir and produce this product.
The present invention using eucalyptol mother liquor, wartwort, tripterygium wilfordii, lilac daphne, chilli oil, root of Chinese clematis herb, baeckea frutescen, derris root, Eupatorium adenophorum, hairyvein agrimony, Chinese Stellera Root, balsam pear, Chinese ephedra, calamus, effective proportioning of ginger raw material, are made insecticide, and raw material is adopted It is low to collect cost, making is simple and convenient, has good insecticidal effect to ethanol water rice, vegetables, fruit tree, tea tree etc., and right Environmental nonpollution, meet the requirement of green production;Seedling can be protected well, can effectively be killed off the insect pests, and Small toxicity itself, nursery stock and human body will not be impacted.
Described above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art For member, under the premise without departing from the principles of the invention, some improvements and modifications can also be made, these improvements and modifications also should It is considered as protection scope of the present invention.

Claims (5)

1. a kind of gardens synergy compound plant source pesticide, it is characterised in that be prepared by the raw material of following parts by weight:
Eucalyptol mother liquor 16-25 parts, wartwort 8-14 parts, tripterygium wilfordii 6-11 parts, lilac daphne 7-11 parts, chilli oil 3-5 parts, the root of Chinese clematis are complete Careless 4-7 parts, baeckea frutescen 2-6 parts, derris root 15-21 parts, Eupatorium adenophorum 7-12 parts, hairyvein agrimony 6-12 parts, Chinese Stellera Root 1-4 parts, hardship Melon 3-8 parts, Chinese ephedra 1-7 parts, calamus 2-8 parts, ginger 2-8 parts, euphorbia lunulata 5-10 parts, emulsifying agent 6-11 parts, remaining is ethanol water Solution.
2. a kind of gardens synergy compound plant source pesticide according to claim 1, it is characterised in that by following weight The raw material of part is prepared:
Eucalyptol mother liquor 17-24 parts, wartwort 9-13 parts, tripterygium wilfordii 7-10 parts, lilac daphne 8-10 parts, chilli oil 4-5 parts, the root of Chinese clematis are complete Careless 4-6 parts, baeckea frutescen 3-5 parts, derris root 16-20 parts, Eupatorium adenophorum 8-11 parts, hairyvein agrimony 7-11 parts, Chinese Stellera Root 2-4 parts, hardship Melon 4-7 parts, Chinese ephedra 2-6 parts, calamus 3-7 parts, ginger 3-7 parts, euphorbia lunulata 6-9 parts, emulsifying agent 7-10 parts, remaining is that ethanol is water-soluble Liquid.
3. a kind of gardens synergy compound plant source pesticide according to claim 1, it is characterised in that by following weight The raw material of part is prepared:
19 parts of eucalyptol mother liquor, 11 parts of wartwort, 8 parts of tripterygium wilfordii, 9 parts of lilac daphne, 4 parts of chilli oil, 4 parts of root of Chinese clematis herb, baeckea frutescen 4 Part, 17 parts of derris root, 9 parts of Eupatorium adenophorum, 8 parts of hairyvein agrimony, 3 parts of Chinese Stellera Root, 5 parts of balsam pear, 5 parts of Chinese ephedra, 6 parts of calamus, ginger 5 Part, 9 parts of euphorbia lunulata, 8 parts of emulsifying agent, remaining is ethanol water.
A kind of 4. preparation method of gardens synergy compound plant source pesticide according to claim 1, it is characterised in that It is made up of following steps:
S1, crush:By eucalyptol mother liquor 17-24 parts, wartwort 9-13 parts, tripterygium wilfordii 7-10 parts, lilac daphne 8-10 parts, chilli oil 4-5 Part, root of Chinese clematis herb 4-6 parts, baeckea frutescen 3-5 parts, derris root 16-20 parts, Eupatorium adenophorum 8-11 parts, hairyvein agrimony 7-11 parts, winter daphne wolf Malicious 2-4 parts, balsam pear 4-7 parts, Chinese ephedra 2-6 parts, calamus 3-7 parts, ginger 3-7 parts, euphorbia lunulata 6-9 part raw materials, after being cleaned It is broken, and cross 40-50 mesh sieves;
S2, immersion:Take above-mentioned raw materials mix after with ethanol by 1:2 part by weight immersion with 68% ethanol, being in temperature Soaked one day at 40-80 DEG C, filter and remove residue, the pH value for adjusting leaching liquor is 7 mixing filtrate;
S3, concentration extraction:The mixing filtrate that step S2 is obtained is concentrated under reduced pressure, it is the dense of 1.3g/m3 that density, which is made, Contracting liquid;Then extracted with ether organic solvent, obtain raw material mixed biologic alkali;
S4, crystallization extraction:Propyl alcohol organic solvent is slowly added into step S3 raw material mixed biologic alkali, is occurred in liquid surface During crystal settling, stop extraction operation, add emulsifying agent 7-10 parts, stir and produce this product.
A kind of 5. gardens synergy compound plant source pesticide according to claim 3, it is characterised in that the emulsifying agent For the one or more in ethoxylated dodecyl alcohol, iso-octyl APEO and aliphatic amine polyoxyethylene ether.
CN201710894903.2A 2017-09-28 2017-09-28 A kind of gardens synergy compound plant source pesticide and preparation method thereof Pending CN107549220A (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109329318A (en) * 2018-11-05 2019-02-15 孙同娟 A kind of municipal administration gardens insecticide and preparation method thereof

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