CN109329318A - A kind of municipal administration gardens insecticide and preparation method thereof - Google Patents
A kind of municipal administration gardens insecticide and preparation method thereof Download PDFInfo
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- CN109329318A CN109329318A CN201811307051.3A CN201811307051A CN109329318A CN 109329318 A CN109329318 A CN 109329318A CN 201811307051 A CN201811307051 A CN 201811307051A CN 109329318 A CN109329318 A CN 109329318A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N41/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom
- A01N41/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom containing a sulfur-to-oxygen double bond
- A01N41/10—Sulfones; Sulfoxides
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N51/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds having the sequences of atoms O—N—S, X—O—S, N—N—S, O—N—N or O-halogen, regardless of the number of bonds each atom has and with no atom of these sequences forming part of a heterocyclic ring
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N55/00—Biocides, pest repellants or attractants, or plant growth regulators, containing organic compounds containing elements other than carbon, hydrogen, halogen, oxygen, nitrogen and sulfur
- A01N55/08—Biocides, pest repellants or attractants, or plant growth regulators, containing organic compounds containing elements other than carbon, hydrogen, halogen, oxygen, nitrogen and sulfur containing boron
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
- A01N57/10—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds
- A01N57/14—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds containing aromatic radicals
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/06—Aluminium; Calcium; Magnesium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/26—Phosphorus; Compounds thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/14—Celastraceae [Staff-tree or Bittersweet family], e.g. spindle tree, bittersweet or thunder god vine
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/20—Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/32—Ranunculaceae [Buttercup family], e.g. hepatica, hydrastis or goldenseal
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The present invention relates to gardens protection technique fields, disclose a kind of municipal gardens insecticide, including below according to the raw material of parts by weight: 10-20 parts of Dalmatian chrysanthemum, 15-25 parts of Chinese tallowtree leaf, 6-12 parts of cordate houttuynia, 10-15 parts of frutus cnidii, 7-11 parts of lilac daphne, 3-7 parts of the root of Chinese clematis, 5-10 parts of fish pelargonium, 6-11 parts of tripterygium wilfordii, 15-21 parts of derris root, 7-12 parts of Eupatorium adenophorum, 3-8 parts of calamus, 3-7 parts of Chinese ephedra, 3, 4-8 parts of 5- dimethylphenyl boronic acid, 1-2 parts of phosmet, 0.8-1.6 parts of tetradiphon, 2-4 parts of imidacloprid, 1.6-2.2 parts of phoxim, 1-3 parts of epsom salt, 30-50 parts of solvent.The invention also discloses the municipal gardens method for producing insecticide.It is strong that insecticide of the present invention kills pest pest ability, has preferable insect killing effect to different types of pest.
Description
Technical field
The present invention relates to gardens protection technique field, specifically a kind of municipal administration gardens insecticide and preparation method thereof.
Background technique
Garden-like cities are to organize and construct art uply city space using a certain amount of greening as basic organic tie
Each fundamental, so that urban physical environment is had optimal aesthetics and ecological effect." garden-like cities " bias toward city
Urban Landscape Construction take public lawn per capita, ratio of green space, forest coverage rate as the basic index of competition.Garden-like cities be unable to do without
The decoration of plant, therefore plant is protected, prevent pest from destroying just particularly important.
The use of insecticide is a kind of means for killing pest, plant can be protected, existing insecticide is to pest
Insect killing effect it is not good enough, often there is specific aim, it is pervasive only to killing certain type of pest with preferable insect killing effect
Property is not strong, and insecticide duration of efficacy is not grown, and after a period of time, pest can breed again again, be unfavorable for plant into
Row extended protection.
Summary of the invention
The purpose of the present invention is to provide a kind of municipal gardens insecticides, to solve mentioned above in the background art ask
Topic.
To achieve the above object, the invention provides the following technical scheme:
A kind of municipal administration gardens insecticide, including below according to the raw material of parts by weight: 10-20 parts of Dalmatian chrysanthemum, Chinese tallowtree leaf 15-
25 parts, 6-12 parts of cordate houttuynia, 10-15 parts of frutus cnidii, 7-11 parts of lilac daphne, 3-7 parts of the root of Chinese clematis, 5-10 parts of fish pelargonium, tripterygium wilfordii 6-
11 parts, 15-21 parts of derris root, 7-12 parts of Eupatorium adenophorum, 3-8 parts of calamus, 3-7 parts of Chinese ephedra, 4-8 parts of 3,5- dimethylphenyl boronic acid,
As a further solution of the present invention: including below according to the raw material of parts by weight: 12-18 parts of Dalmatian chrysanthemum, Chinese tallowtree leaf
17-22 parts, 8-10 parts of cordate houttuynia, 11-14 parts of frutus cnidii, 8-10 parts of lilac daphne, 4-6 parts of the root of Chinese clematis, 6-9 parts of fish pelargonium, tripterygium wilfordii
7-10 parts, 16-20 parts of derris root, 8-11 parts of Eupatorium adenophorum, 5-7 parts of calamus, 4-6 parts of Chinese ephedra, 3,5- dimethylphenyl boronic acid 5-7
Part, 1.2-1.8 parts of phosmet, 1-1.4 parts of tetradiphon, 2.5-3.5 parts of imidacloprid, 1.8-2.1 parts of phoxim, seven water sulphur
Sour magnesium 1.5-2.5 parts, 35-45 parts of solvent.
As further scheme of the invention: including below according to the raw material of parts by weight: 15 parts of Dalmatian chrysanthemum, Chinese tallowtree leaf 20
Part, 9 parts of cordate houttuynia, 12 parts of frutus cnidii, 9 parts of lilac daphne, 5 parts of the root of Chinese clematis, 7 parts of fish pelargonium, 8 parts of tripterygium wilfordii, 18 parts of derris root, purple stem
10 parts of Herba Lycopi, 6 parts of calamus, 5 parts of Chinese ephedra, 6 parts of 3,5- dimethylphenyl boronic acid, 1.5 parts of phosmet, 1.2 parts of tetradiphon, pyrrole
3 parts of worm quinoline, 2 parts of phoxim, 2 parts of epsom salt, 40 parts of solvent.
As further scheme of the invention: the solvent is the ethanol solution of concentration 80-90%.
Municipal administration gardens method for producing insecticide, steps are as follows:
1) by Dalmatian chrysanthemum, Chinese tallowtree leaf, cordate houttuynia, frutus cnidii, lilac daphne, the root of Chinese clematis, fish pelargonium, tripterygium wilfordii, derris root, purple stem
It is crushed after Herba Lycopi, calamus, Chinese ephedra clean dry, crosses 100-200 mesh, obtain particulate matter:
2) solvent is added in the particulate matter obtained to step 1), impregnates 3-6h, is warming up to 60-80 DEG C, it is auxiliary by ultrasonic wave
It helps and extracts 5-10min, filter after the completion, obtain filtrate I and filter residue I；
3) distilled water of 5-8 times of parts by weight is added in the filter residue obtained to step 2), continues to decoct 30-50min after boiling,
It filters after the completion, obtains filtrate II and filter residue II；
4) filtrate II that the filtrate I obtained step 2) and step 3) obtain mixes, and 3,5- dimethylphenyl boronic acid, Asia is added
Amine sulphur phosphorus, tetradiphon, imidacloprid, phoxim, epsom salt, stir 3- under 600-800r/min speed conditions
5min stands 1-2h, takes supernatant liquid after removing surface offscum.
As further scheme of the invention: ultrasonic frequency described in step 2) is 40-60KHz.
Above-mentioned insecticide is preparing the application in herbicide.
Compared with prior art, the beneficial effects of the present invention are:
For insecticide prepared by the present invention under the common mating reaction of various raw materials, insecticide kills pest pest ability
By force, there is preferable insect killing effect to different types of pest；Pest can be quickly killed, to carry out to the plant in gardens
Protection；And the insect killing effect duration is long, can effectively contain the procreation of pest, to carry out digital preservation to ornamental plant.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described,
Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention
Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
Embodiment 1
A kind of municipal administration gardens insecticide, including below according to the raw material of parts by weight: 10 parts of Dalmatian chrysanthemum, 15 parts of Chinese tallowtree leaf,
6 parts of cordate houttuynia, 10 parts of frutus cnidii, 7 parts of lilac daphne, 3 parts of the root of Chinese clematis, 5 parts of fish pelargonium, 6 parts of tripterygium wilfordii, 15 parts of derris root, purple stem pool
Blue 7 parts, 3 parts of calamus, 3 parts of Chinese ephedra, 4 parts of 3,5- dimethylphenyl boronic acid, 1 part of phosmet, 0.8 part of tetradiphon, imidacloprid 2
Part, 1.6 parts of phoxim, 1 part of epsom salt, 30 parts of solvent.
Wherein, the solvent is the ethanol solution of concentration 80%.
In the present embodiment, municipal administration gardens method for producing insecticide, steps are as follows:
1) by Dalmatian chrysanthemum, Chinese tallowtree leaf, cordate houttuynia, frutus cnidii, lilac daphne, the root of Chinese clematis, fish pelargonium, tripterygium wilfordii, derris root, purple stem
It crushes, sieves with 100 mesh sieve after Herba Lycopi, calamus, Chinese ephedra clean dry, obtain particulate matter:
2) solvent is added in the particulate matter obtained to step 1), impregnates 3h, is warming up to 60 DEG C, passes through ultrasonic wave assisted extraction
5min is filtered after the completion, obtains filtrate I and filter residue I；
3) distilled water of 5 times of parts by weight is added in the filter residue obtained to step 2), continues to decoct 30min after boiling, complete
After filter, obtain filtrate II and filter residue II；
4) filtrate II that the filtrate I obtained step 2) and step 3) obtain mixes, and 3,5- dimethylphenyl boronic acid, Asia is added
Amine sulphur phosphorus, tetradiphon, imidacloprid, phoxim, epsom salt stir 3min under 600r/min speed conditions, stand
1h takes supernatant liquid after removing surface offscum.
Wherein, ultrasonic frequency described in step 2) is 40KHz.
Embodiment 2
A kind of municipal administration gardens insecticide, including below according to the raw material of parts by weight: 12 parts of Dalmatian chrysanthemum, 17 parts of Chinese tallowtree leaf,
8 parts of cordate houttuynia, 11 parts of frutus cnidii, 8 parts of lilac daphne, 4 parts of the root of Chinese clematis, 6 parts of fish pelargonium, 7 parts of tripterygium wilfordii, 16 parts of derris root, purple stem pool
Blue 8 parts, 5 parts of calamus, 4 parts of Chinese ephedra, 7 parts of 3,5- dimethylphenyl boronic acid, 1.8 parts of phosmet, 1.4 parts of tetradiphon, pyrrole worm
3.5 parts of quinoline, 2.1 parts of phoxim, 2.5 parts of epsom salt, 45 parts of solvent.
Wherein, the solvent is the ethanol solution of concentration 85%.
In the present embodiment, municipal administration gardens method for producing insecticide, steps are as follows:
1) by Dalmatian chrysanthemum, Chinese tallowtree leaf, cordate houttuynia, frutus cnidii, lilac daphne, the root of Chinese clematis, fish pelargonium, tripterygium wilfordii, derris root, purple stem
It is crushed after Herba Lycopi, calamus, Chinese ephedra clean dry, crosses 150 meshes, obtain particulate matter:
2) solvent is added in the particulate matter obtained to step 1), impregnates 4.5h, is warming up to 70 DEG C, mentioned by ultrasonic wave auxiliary
7min is taken, is filtered after the completion, filtrate I and filter residue I are obtained；
3) distilled water of 6 times of parts by weight is added in the filter residue obtained to step 2), continues to decoct 40min after boiling, complete
After filter, obtain filtrate II and filter residue II；
4) filtrate II that the filtrate I obtained step 2) and step 3) obtain mixes, and 3,5- dimethylphenyl boronic acid, Asia is added
Amine sulphur phosphorus, tetradiphon, imidacloprid, phoxim, epsom salt stir 4min under 700r/min speed conditions, stand
1.5h takes supernatant liquid after removing surface offscum.
Wherein, ultrasonic frequency described in step 2) is 50KHz.
Embodiment 3
A kind of municipal administration gardens insecticide, including below according to the raw material of parts by weight: 15 parts of Dalmatian chrysanthemum, 20 parts of Chinese tallowtree leaf,
9 parts of cordate houttuynia, 12 parts of frutus cnidii, 9 parts of lilac daphne, 5 parts of the root of Chinese clematis, 7 parts of fish pelargonium, 8 parts of tripterygium wilfordii, 18 parts of derris root, purple stem pool
Blue 10 parts, 6 parts of calamus, 5 parts of Chinese ephedra, 6 parts of 3,5- dimethylphenyl boronic acid, 1.5 parts of phosmet, 1.2 parts of tetradiphon, pyrrole worm
3 parts of quinoline, 2 parts of phoxim, 2 parts of epsom salt, 40 parts of solvent.
Wherein, the solvent is the ethanol solution of concentration 85%.
In the present embodiment, municipal administration gardens method for producing insecticide, steps are as follows:
1) by Dalmatian chrysanthemum, Chinese tallowtree leaf, cordate houttuynia, frutus cnidii, lilac daphne, the root of Chinese clematis, fish pelargonium, tripterygium wilfordii, derris root, purple stem
It is crushed after Herba Lycopi, calamus, Chinese ephedra clean dry, crosses 150 meshes, obtain particulate matter:
2) solvent is added in the particulate matter obtained to step 1), impregnates 4.5h, is warming up to 70 DEG C, mentioned by ultrasonic wave auxiliary
7min is taken, is filtered after the completion, filtrate I and filter residue I are obtained；
3) distilled water of 6 times of parts by weight is added in the filter residue obtained to step 2), continues to decoct 40min after boiling, complete
After filter, obtain filtrate II and filter residue II；
4) filtrate II that the filtrate I obtained step 2) and step 3) obtain mixes, and 3,5- dimethylphenyl boronic acid, Asia is added
Amine sulphur phosphorus, tetradiphon, imidacloprid, phoxim, epsom salt stir 4min under 700r/min speed conditions, stand
1.5h takes supernatant liquid after removing surface offscum.
Wherein, ultrasonic frequency described in step 2) is 50KHz.
Embodiment 4
A kind of municipal administration gardens insecticide, including below according to the raw material of parts by weight: 18 parts of Dalmatian chrysanthemum, 22 parts of Chinese tallowtree leaf,
10 parts of cordate houttuynia, 14 parts of frutus cnidii, 10 parts of lilac daphne, 6 parts of the root of Chinese clematis, 9 parts of fish pelargonium, 10 parts of tripterygium wilfordii, 20 parts of derris root, purple stem
11 parts of Herba Lycopi, 7 parts of calamus, 6 parts of Chinese ephedra, 5 parts of 3,5- dimethylphenyl boronic acid, 1.2 parts of phosmet, 1 part of tetradiphon, pyrrole worm
2.5 parts of quinoline, 1.8 parts of phoxim, 1.5 parts of epsom salt, 35 parts of solvent.
Wherein, the solvent is the ethanol solution of concentration 85%.
In the present embodiment, municipal administration gardens method for producing insecticide, steps are as follows:
1) by Dalmatian chrysanthemum, Chinese tallowtree leaf, cordate houttuynia, frutus cnidii, lilac daphne, the root of Chinese clematis, fish pelargonium, tripterygium wilfordii, derris root, purple stem
It is crushed after Herba Lycopi, calamus, Chinese ephedra clean dry, crosses 150 meshes, obtain particulate matter:
2) solvent is added in the particulate matter obtained to step 1), impregnates 4.5h, is warming up to 70 DEG C, mentioned by ultrasonic wave auxiliary
7min is taken, is filtered after the completion, filtrate I and filter residue I are obtained；
3) distilled water of 6 times of parts by weight is added in the filter residue obtained to step 2), continues to decoct 40min after boiling, complete
After filter, obtain filtrate II and filter residue II；
4) filtrate II that the filtrate I obtained step 2) and step 3) obtain mixes, and 3,5- dimethylphenyl boronic acid, Asia is added
Amine sulphur phosphorus, tetradiphon, imidacloprid, phoxim, epsom salt stir 4min under 700r/min speed conditions, stand
1.5h takes supernatant liquid after removing surface offscum.
Wherein, ultrasonic frequency described in step 2) is 50KHz.
Embodiment 5
A kind of municipal administration gardens insecticide, including below according to the raw material of parts by weight: 20 parts of Dalmatian chrysanthemum, 25 parts of Chinese tallowtree leaf,
12 parts of cordate houttuynia, 15 parts of frutus cnidii, 11 parts of lilac daphne, 7 parts of the root of Chinese clematis, 10 parts of fish pelargonium, 11 parts of tripterygium wilfordii, 21 parts of derris root, purple
12 parts of stem Herba Lycopi, 8 parts of calamus, 7 parts of Chinese ephedra, 3,8 parts of dimethylphenyl boronic acid, 2 parts of phosmet, 1.6 parts of tetradiphon, pyrrole worm
4 parts of quinoline, 2.2 parts of phoxim, 3 parts of epsom salt, 50 parts of solvent.
Wherein, the solvent is the ethanol solution of concentration 90%.
In the present embodiment, municipal administration gardens method for producing insecticide, steps are as follows:
1) by Dalmatian chrysanthemum, Chinese tallowtree leaf, cordate houttuynia, frutus cnidii, lilac daphne, the root of Chinese clematis, fish pelargonium, tripterygium wilfordii, derris root, purple stem
It is crushed after Herba Lycopi, calamus, Chinese ephedra clean dry, crosses 200 meshes, obtain particulate matter:
2) solvent is added in the particulate matter obtained to step 1), impregnates 6h, is warming up to 80 DEG C, passes through ultrasonic wave assisted extraction
10min is filtered after the completion, obtains filtrate I and filter residue I；
3) distilled water of 8 times of parts by weight is added in the filter residue obtained to step 2), continues to decoct 50min after boiling, complete
After filter, obtain filtrate II and filter residue II；
4) filtrate II that the filtrate I obtained step 2) and step 3) obtain mixes, and 3,5- dimethylphenyl boronic acid, Asia is added
Amine sulphur phosphorus, tetradiphon, imidacloprid, phoxim, epsom salt stir 5min under 800r/min speed conditions, stand
2h takes supernatant liquid after removing surface offscum.
Wherein, ultrasonic frequency described in step 2) is 60KHz.
Comparative example 1
Compared with Example 3,3,5- dimethylphenyl boronic acid is free of, other are same as Example 3.
Comparative example 2
Compared with Example 3, epsom salt is free of, other are same as Example 3.
Comparative example 3
Compared with Example 3,3,5- dimethylphenyl boronic acid and epsom salt are free of, other are same as Example 3.
Insecticide prepared by embodiment 1-5 and comparative example 1-3 is tested for the property, test result is as shown in table 1.
Insecticide application method: insecticide sprays after mixing with water by weight 1:500, obtains data and insecticide spraying
Preceding comparison.
Table 1
From can be seen that insecticide prepared by the present invention in result above under the common mating reaction of various raw materials, kill
It is strong that pest pest ability is killed in worm agent, has preferable insect killing effect to different types of pest；Pest can be quickly killed, from
And the plant in gardens is protected；And the insect killing effect duration is long, can effectively contain the procreation of pest, thus to garden
Woods plant carries out digital preservation.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (7)
1. a kind of municipal administration gardens insecticide, which is characterized in that including below according to the raw material of parts by weight: 10-20 parts of Dalmatian chrysanthemum,
15-25 parts of Chinese tallowtree leaf, 6-12 parts of cordate houttuynia, 10-15 parts of frutus cnidii, 7-11 parts of lilac daphne, 3-7 parts of the root of Chinese clematis, 5-10 parts of fish pelargonium,
6-11 parts of tripterygium wilfordii, 15-21 parts of derris root, 7-12 parts of Eupatorium adenophorum, 3-8 parts of calamus, 3-7 parts of Chinese ephedra, 3,5- dimethyl benzene boron
4-8 parts sour, 1-2 parts of phosmet, 0.8-1.6 parts of tetradiphon, 2-4 parts of imidacloprid, 1.6-2.2 parts of phoxim, seven water sulphur
Sour magnesium 1-3 parts, 30-50 parts of solvent.
2. municipal administration gardens according to claim 1 insecticide, which is characterized in that including below according to the original of parts by weight
Material: 12-18 parts of Dalmatian chrysanthemum, 17-22 parts of Chinese tallowtree leaf, 8-10 parts of cordate houttuynia, 11-14 parts of frutus cnidii, 8-10 parts of lilac daphne, root of Chinese clematis 4-
6 parts, 6-9 parts of fish pelargonium, 7-10 parts of tripterygium wilfordii, 16-20 parts of derris root, 8-11 parts of Eupatorium adenophorum, 5-7 parts of calamus, Chinese ephedra 4-6
Part, 5-7 parts of 3,5- dimethylphenyl boronic acid, 1.2-1.8 parts of phosmet, 1-1.4 parts of tetradiphon, 2.5-3.5 parts of imidacloprid,
1.8-2.1 parts of phoxim, 1.5-2.5 parts of epsom salt, 35-45 parts of solvent.
3. municipal administration gardens according to claim 2 insecticide, which is characterized in that including below according to the original of parts by weight
Material: 15 parts of Dalmatian chrysanthemum, 20 parts of Chinese tallowtree leaf, 9 parts of cordate houttuynia, 12 parts of frutus cnidii, 9 parts of lilac daphne, 5 parts of the root of Chinese clematis, 7 parts of fish pelargonium, thunder
8 parts of public rattan, 18 parts of derris root, 10 parts of Eupatorium adenophorum, 6 parts of calamus, 5 parts of Chinese ephedra, 6 parts of 3,5- dimethylphenyl boronic acid, phosmet
1.5 parts, 1.2 parts of tetradiphon, 3 parts of imidacloprid, 2 parts of phoxim, 2 parts of epsom salt, 40 parts of solvent.
4. municipal administration gardens according to claim 1 insecticide, which is characterized in that the solvent is the second of concentration 80-90%
Alcoholic solution.
5. a kind of municipal gardens method for producing insecticide as described in claim 1-4 is any, which is characterized in that including with
Lower step:
1) by Dalmatian chrysanthemum, Chinese tallowtree leaf, cordate houttuynia, frutus cnidii, lilac daphne, the root of Chinese clematis, fish pelargonium, tripterygium wilfordii, derris root, purple stem pool
It is crushed after orchid, calamus, Chinese ephedra clean dry, crosses 100-200 mesh, obtain particulate matter:
2) solvent is added in the particulate matter obtained to step 1), impregnates 3-6h, is warming up to 60-80 DEG C, mentioned by ultrasonic wave auxiliary
5-10min is taken, is filtered after the completion, filtrate I and filter residue I are obtained；
3) distilled water of 5-8 times of parts by weight is added in the filter residue obtained to step 2, continues to decoct 30-50min after boiling, complete
After filter, obtain filtrate II and filter residue II；
4) filtrate I that step 2 obtains and the filtrate II that step 3) obtains are mixed, 3,5- dimethylphenyl boronic acid, imines sulphur is added
Phosphorus, tetradiphon, imidacloprid, phoxim, epsom salt stir 3-5min under 600-800r/min speed conditions, quiet
1-2h is set, takes supernatant liquid after removing surface offscum.
6. municipal administration gardens according to claim 5 method for producing insecticide, which is characterized in that described in step 2
Ultrasonic frequency is 40-60KHz.
7. a kind of insecticide as described in claim 1-4 is any is in the application prepared in herbicide.
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| CN106332921A (en) * | 2016-08-22 | 2017-01-18 | 吉林大学 | Botanical insecticide and preparation method and application thereof |
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Application publication date: 20190215 |