CN107417105A - A kind of pottery moon white glaze - Google Patents
A kind of pottery moon white glaze Download PDFInfo
- Publication number
- CN107417105A CN107417105A CN201710375286.5A CN201710375286A CN107417105A CN 107417105 A CN107417105 A CN 107417105A CN 201710375286 A CN201710375286 A CN 201710375286A CN 107417105 A CN107417105 A CN 107417105A
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- China
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- parts
- glaze
- pottery
- white glaze
- moon white
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
Abstract
A kind of pottery moon white glaze, it is prepared by the raw material of following parts by weight：37 43 parts of melilite, 9 15 parts of this medicine, 19 25 parts of quartz, 7 13 parts of Copper Ores, 9 15 parts of calcite, 1.5 2.5 parts of bovine bone powder, 1.5 2.5 parts of tin oxide.The present invention is compared with prior art, by scientific and reasonable raw material proportioning and control burning process, overcome the easy sootiness occurred during moon white glaze tradition is fired, go out the defects of glaze eye, yield rate is promoted to more than 90%, and the moon white glaze glaze colours that firing obtains is pure, texture is gentle.
Description
Technical field
The present invention relates to a kind of glaze, and in particular to a kind of pottery moon white glaze.
Background technology
Pottery is one of five big kiln porcelain of China's Song Dynasty, the treasure in Chinese tradition technology in producing porcelain, with the transmutation of uniqueness
Art and be renown far and wide in generation, be the exclusive national treasure porcelain in Henan Province Xuchang Yuzhou City god Hou towns." moon white glaze " its glaze colours in an ancient unit of weight kiln
Thin compared with celeste glaze, pure white clear just as moonlight, enamel is bright and clean moist, when tradition is fired with Yuzhou ore such as feldspar,
Quartz, calcite are primary raw material, the easy sootiness of glaze colours, go out glaze eye, and yield rate is low, only 40% or so.
The content of the invention
The purpose of the present invention be that for solve the deficiencies in the prior art provide it is a kind of fire easily, an ancient unit of weight of high yield rate
The porcelain moon white glaze.
The purpose of the present invention is realized with following technical proposals：
A kind of pottery moon white glaze, it is prepared by the raw material of following parts by weight：Melilite 37-43 parts, this medicine 9-15 parts, stone
English 19-25 parts, Copper Ores 7-13 parts, calcite 9-15 parts, bovine bone powder 1.5-2.5 parts, tin oxide 1.5-2.5 parts.
Preferably, it is prepared by the raw material of following parts by weight：40 parts of melilite, 12 parts of this medicine, quartzy 22 parts, copper
10 parts of ore, 12 parts of calcite, 2 parts of bovine bone powder, 2 parts of tin oxide.
The preparation method of pottery moon white glaze as described above, comprises the following steps：
（1）Above-mentioned raw materials plus water are mixed, ball milling, obtain glaze slip；
（2）Glazing；
（3）Burn till, firing temperature is 1280-1300 DEG C.
Step（3）Middle firing process specifically comprises the following steps：1. the heat of oxidation：Base substrate after glazing is put into kiln,
Fired under oxidizing atmosphere, temperature is ramped up 1000-1050 DEG C in 3-4h；2. under reducing atmosphere, make temperature equal in 5-7h
It is ramped up 1280-1300 DEG C；3. 2-3h under reducing atmosphere, is kept under the conditions of 1280-1300 DEG C；4. being cooled to room temperature, make
.
The present invention compared with prior art, by scientific and reasonable raw material proportioning and control burning process, overcomes bluish white
Easy sootiness that glaze tradition occurs in firing, go out the defects of glaze eye, yield rate is promoted to more than 90%, and fire the obtained moon
White glaze glaze colours is pure, and texture is gentle.
Brief description of the drawings
Fig. 1 is the moon white glaze schematic diagram that the embodiment of the present invention 2 obtains.
Embodiment
Embodiment 1
A kind of pottery moon white glaze, is prepared by the raw material of following parts by weight：Melilite 37-43 parts, this medicine 9-15 parts, quartz
19-25 parts, Copper Ores 7-13 parts, calcite 9-15 parts, bovine bone powder 1.5-2.5 parts, tin oxide 1.5-2.5 parts.
The preparation method of above-mentioned pottery moon white glaze, comprises the following steps：
（1）Above-mentioned raw materials plus water are mixed, ball milling, obtain glaze slip；
（2）Glazing；
（3）Burn till, firing temperature is 1280-1300 DEG C；
Firing process specifically comprises the following steps：1. the heat of oxidation：Base substrate after glazing is put into kiln, is burnt under oxidizing atmosphere
System, makes temperature be ramped up 1000-1050 DEG C in 3-4h；2. under reducing atmosphere, temperature is set to be ramped up 1280- in 5-7h
1300℃；3. 2-3h under reducing atmosphere, is kept under the conditions of 1280-1300 DEG C；4. being cooled to room temperature, it is made.
The present invention is using melilite as primary solvent, and melilite is compared to for example white feldspar of other feldspars, red feldspar, silicon, iron content
It is higher, the glossiness of moon white glaze can be improved, calcite plays hydrotropy, and quartz can improve the mobility of glaze, and this medicine is Yuzhou
A kind of local natural feldspar, iron-holder is higher, and Copper Ores are also made in addition to being used as cosolvent with certain coloring
With the main calcic of bovine bone powder and phosphorus, the opacity of glaze being improved, improve texture, tin oxide coordinates Copper Ores to use, to help color
Agent；After above-mentioned raw materials are used cooperatively, first under oxidizing atmosphere, moisture in glaze is excluded, then under reducing atmosphere, glaze paint starts
Melt glassing, " transmutation " starts, and after reaching firing temperature, glaze paint reaches bright, smoothly, is burnt by rational proportion and control
Into atmosphere and temperature, the problem of reducing sootiness and go out glaze eye, the yield rate of moon white glaze is greatly improved.It is yellow long in the present invention
Stone, this medicine, calcite, quartz, Copper Ores originate from Yuzhou.
Embodiment 2
A kind of pottery moon white glaze, is prepared by the raw material of following parts by weight：40 parts of melilite, 12 parts of this medicine, quartzy 22 parts, copper
10 parts of ore, 12 parts of calcite, 2 parts of bovine bone powder, 2 parts of tin oxide.
The preparation method of above-mentioned pottery moon white glaze, comprises the following steps：
（1）Above-mentioned raw materials plus water are mixed, ball milling, cross 250 mesh sieves, obtain glaze slip；
（2）Glazing；
（3）Burn till, specifically comprise the following steps：1. the heat of oxidation：Base substrate after glazing is put into kiln, is burnt under oxidizing atmosphere
System, makes temperature be ramped up 1030 DEG C in 3.5h；2. temperature under reducing atmosphere, is set to be ramped up 1280 DEG C in 6h；3. also
Under Primordial Qi atmosphere, 2.5h is kept under the conditions of 1280 DEG C；4. being cooled to room temperature, it is made.
The bluish white glaze paint of pottery obtained using said ratio and method as shown in figure 1, its color and luster is pure white pure, moisten by texture
Pool, and yield rate reaches more than 95%.
Embodiment 3
A kind of pottery moon white glaze, is prepared by the raw material of following parts by weight：40 parts of melilite, 12 parts of this medicine, quartzy 22 parts, copper
10 parts of ore, 12 parts of calcite, 2 parts of bovine bone powder, 2 parts of tin oxide.
The preparation method of above-mentioned pottery moon white glaze, comprises the following steps：
（1）Above-mentioned raw materials plus water are mixed, ball milling, cross 250 mesh sieves, obtain glaze slip；
（2）Glazing；
（3）Burn till, specifically comprise the following steps：1. the heat of oxidation：Base substrate after glazing is put into kiln, is burnt under oxidizing atmosphere
System, makes temperature be ramped up 1050 DEG C in 3h；2. temperature under reducing atmosphere, is set to be ramped up 1300 DEG C in 5h；3. reducing
Under atmosphere, 3h is kept under the conditions of 1300 DEG C；4. being cooled to room temperature, it is made.
The pottery yield rate that said ratio and method obtain is used as 90% or so.
Embodiment 4
A kind of pottery moon white glaze, is prepared by the raw material of following parts by weight：40 parts of melilite, 12 parts of this medicine, quartzy 22 parts, copper
10 parts of ore, 12 parts of calcite, 2 parts of bovine bone powder, 2 parts of tin oxide.
The preparation method of above-mentioned pottery moon white glaze, comprises the following steps：
（1）Above-mentioned raw materials plus water are mixed, ball milling, cross 250 mesh sieves, obtain glaze slip；
（2）Glazing；
（3）Burn till, specifically comprise the following steps：1. the heat of oxidation：Base substrate after glazing is put into kiln, is burnt under oxidizing atmosphere
System, makes temperature be ramped up 1020 DEG C in 4h；2. temperature under reducing atmosphere, is set to be ramped up 1290 DEG C in 7h；3. reducing
Under atmosphere, 2.5h is kept under the conditions of 1290 DEG C；4. being cooled to room temperature, it is made.
The pottery yield rate that said ratio and method obtain is used as 90% or so.
Embodiment 5
A kind of pottery moon white glaze, is prepared by the raw material of following parts by weight：37 parts of melilite, 12 parts of this medicine, quartzy 25 parts, copper
10 parts of ore, 11 parts of calcite, 2 parts of bovine bone powder, 2 parts of tin oxide.Its preparation method is the same as embodiment 2.
The pottery yield rate that said ratio and method obtain is used as 92% or so.
Comparative example 1
A kind of pottery moon white glaze, is prepared by the raw material of following parts by weight：Red 40 parts of feldspar, 12 parts of this medicine, quartzy 22 parts, copper
10 parts of ore, 12 parts of calcite, 2 parts of tin oxide.Preparation method is the same as embodiment 2.Compared with Example 2, ox bone is not used in this example
Powder, and melilite is changed to red feldspar, the glaze that red feldspar makes easily precipitates, and firing glaze paint texture is poor, and yield rate only has 60%
Left and right.
Comparative example 2
A kind of pottery moon white glaze, is prepared by the raw material of following parts by weight：40 parts of melilite, 12 parts of this medicine, quartzy 22 parts, copper
10 parts of ore, 12 parts of calcite, 2 parts of bovine bone powder.Preparation method is the same as embodiment 2.Compared with Example 2, oxidation is not used in this example
Tin, fires glaze paint color and luster yellowing, and yield rate only has 72% or so.
Comparative example 3
A kind of pottery moon white glaze, is prepared by the raw material of following parts by weight：45 parts of melilite, 7 parts of this medicine, quartzy 12 parts, copper
10 parts of ore, 12 parts of calcite, 2 parts of bovine bone powder, 2 parts of tin oxide.Preparation method is the same as embodiment 2.This example compared with Example 2,
This medicine, quartz content are reduced, the increase of melilite content, and pinprick easily occurs in glaze paint in sintering procedure, and yield rate only has 65% left side
It is right.
The bluish white glaze formula of pottery that 6-18 of the embodiment of the present invention is provided is shown in Table 1-2.
Claims (4)
- A kind of 1. pottery moon white glaze, it is characterised in that：It is prepared by the raw material of following parts by weight：Melilite 37-43 parts, This medicine 9-15 parts, quartzy 19-25 parts, Copper Ores 7-13 parts, calcite 9-15 parts, bovine bone powder 1.5-2.5 parts, tin oxide 1.5- 2.5 part.
- 2. pottery moon white glaze as claimed in claim 1, it is characterised in that：It is prepared by the raw material of following parts by weight： 40 parts of melilite, 12 parts of this medicine, 22 parts of quartz, 10 parts of Copper Ores, 12 parts of calcite, 2 parts of bovine bone powder, 2 parts of tin oxide.
- 3. as described in claim any one of 1-2 the pottery moon white glaze preparation method, it is characterised in that comprise the following steps：（1）Above-mentioned raw materials plus water are mixed, ball milling, obtain glaze slip；（2）Glazing；（3）Burn till, firing temperature is 1280-1300 DEG C.
- 4. the preparation method of pottery moon white glaze as claimed in claim 3, it is characterised in that step（3）Middle firing process specifically wraps Include following steps：1. the heat of oxidation：Base substrate after glazing is put into kiln, is fired under oxidizing atmosphere, makes temperature uniform in 3-4h Rise to 1000-1050 DEG C；2. under reducing atmosphere, temperature is set to be ramped up 1280-1300 DEG C in 5-7h；3. in reducing atmosphere Under, 2-3h is kept under the conditions of 1280-1300 DEG C；4. being cooled to room temperature, it is made.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710375286.5A CN107417105A (en) | 2017-05-24 | 2017-05-24 | A kind of pottery moon white glaze |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710375286.5A CN107417105A (en) | 2017-05-24 | 2017-05-24 | A kind of pottery moon white glaze |
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| CN201710375286.5A Withdrawn CN107417105A (en) | 2017-05-24 | 2017-05-24 | A kind of pottery moon white glaze |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109369016A (en) * | 2018-12-13 | 2019-02-22 | 禹州市神后镇永春瓷业有限公司 | A kind of month white glaze and preparation method thereof |
| CN115504763A (en) * | 2022-09-05 | 2022-12-23 | 李胜强 | Jun porcelain concentric circle and non-concentric circle manufacturing and traceless firing process |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109369016A (en) * | 2018-12-13 | 2019-02-22 | 禹州市神后镇永春瓷业有限公司 | A kind of month white glaze and preparation method thereof |
| CN115504763A (en) * | 2022-09-05 | 2022-12-23 | 李胜强 | Jun porcelain concentric circle and non-concentric circle manufacturing and traceless firing process |
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Application publication date: 20171201 |