CN107021634A - A kind of red glaze of an ancient unit of weight - Google Patents

A kind of red glaze of an ancient unit of weight Download PDF

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Publication number
CN107021634A
CN107021634A CN201710375686.6A CN201710375686A CN107021634A CN 107021634 A CN107021634 A CN 107021634A CN 201710375686 A CN201710375686 A CN 201710375686A CN 107021634 A CN107021634 A CN 107021634A
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China
Prior art keywords
parts
weight
glaze
ancient unit
red
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CN201710375686.6A
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Chinese (zh)
Inventor
张占领
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Yuzhou City Jun Artifact Co Ltd
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Yuzhou City Jun Artifact Co Ltd
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Priority to CN201710375686.6A priority Critical patent/CN107021634A/en
Publication of CN107021634A publication Critical patent/CN107021634A/en
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    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • C03C8/14Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
    • C03C8/20Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions containing titanium compounds; containing zirconium compounds
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2204/00Glasses, glazes or enamels with special properties
    • C03C2204/04Opaque glass, glaze or enamel
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2209/00Compositions specially applicable for the manufacture of vitreous glazes
    • C03C2209/02Compositions specially applicable for the manufacture of vitreous glazes to produce non-uniformly coloured glazes

Abstract

A kind of red glaze of an ancient unit of weight, it is prepared from by the raw material of following parts by weight:37 43 parts of melilite, 13 19 parts of quartz, 10 16 parts of calcite, blue or green 4.5 5.5 parts of alkali, 12 18 parts of frit, 0.5 1.5 parts of bovine bone powder, 2.5 3.5 parts of tin oxide, 3.5 4.5 parts of zinc oxide, 23 parts of talcum, 0.25 0.75 parts of cupric oxide.Compared with prior art, by scientific and reasonable raw material proportioning and control burning process, not only glaze colours is bright in colour for the red glaze of an ancient unit of weight prepared by the present invention, glossiness is good, and mobility is moderate and has fine cracks, and glaze colours is abundant, on the basis of with an ancient unit of weight red for mass-tone, occur in that transition is bright and clear between yellow, blue, purple multiple color, color, clear and natural, high yield rate, up to more than 75%, having filled up the red glaze of an ancient unit of weight does not have the blank of many colored glazes, is that the red glaze pottery of an ancient unit of weight adds a new varieties.

Description

A kind of red glaze of an ancient unit of weight
Technical field
The present invention relates to a kind of glaze, and in particular to a kind of red glaze of an ancient unit of weight.
Background technology
Pottery is one of five big kiln porcelain of China's Song Dynasty, the treasure in Chinese tradition technology in producing porcelain, with unique transmutation Art and be renown far and wide in generation, be the exclusive national treasure porcelain in Henan Province Xuchang Yuzhou City god Hou towns." rough flambe " in pottery is brilliant with it Jade-like stone is bright, it is uniform famous to moisten, and the red glaze of an ancient unit of weight moistens as one kind in rough flambe, its appearance uniform, and entire body is pure bright-coloured Red, has certain mobility and does not take off mouth, glaze is furnished with fine and closely woven crackle, bright and clean bright, but the existing firing red glaze of an ancient unit of weight The red glaze glaze face color of an ancient unit of weight that glaze formula and firing process burn out is single, and yield rate is relatively low.
The content of the invention
The purpose of the present invention is that provides a kind of an ancient unit of weight red glaze to solve the deficiencies in the prior art.
The purpose of the present invention is realized with following technical proposals:
A kind of red glaze of an ancient unit of weight, it is prepared from by the raw material of following parts by weight:37-43 parts of melilite, 13-19 parts of quartz, Fang Xie 10-16 parts of stone, blue or green 4.5-5.5 parts of alkali, 12-18 parts of frit, 0.5-1.5 parts of bovine bone powder, 2.5-3.5 parts of tin oxide, zinc oxide 3.5-4.5 parts, 2-3 parts of talcum, 0.25-0.75 parts of cupric oxide.
It is prepared from by the raw material of following parts by weight:40 parts of melilite, 16 parts of quartz, 13 parts of calcite, blue or green alkali 5 Part, 15 parts of frit, 1 part of bovine bone powder, 3 parts of tin oxide, 4 parts of zinc oxide, 2.5 parts of talcum, 0.5 part of cupric oxide.
The preparation method of the red glaze of an ancient unit of weight as described above, comprises the following steps:
(1)Above-mentioned raw materials are added water mixing, ball milling obtains glaze slip;
(2)Glazing;
(3)Burn till, firing temperature is 1250-1280 DEG C.
Step(3)Middle firing process specifically includes following steps:1. pre-burning phase:Base substrate after glazing is put into kiln, is made Temperature rises to 540-580 DEG C in 2-3h from room temperature;2. heat of oxidation:Under oxidizing atmosphere, temperature is set to be ramped up in 3-4h 1000-1030℃;3. reduction period:Under reducing atmosphere, temperature is made to be ramped up 1250-1280 DEG C in 5-6h;4. natural cooling To room temperature, it is made.
The air door of kiln is opened during the reduction period.
The present invention is using melilite as primary solvent, and melilite compares for example white feldspar of other feldspars, red feldspar, silicon, iron content It is higher, the glossiness of the red glaze of pottery an ancient unit of weight can be improved, calcite plays hydrotropy, and quartz can improve the mobility of glaze, and blue or green alkali is A kind of trona stone of Yuzhou, belongs to kaolinite class clay mineral, and silicon, aluminium content are higher, and outward appearance is in cyan, can be reduced Firing temperature, promotes to melt other raw mineral materials, makes base substrate quality fine and close, and outward appearance has translucence, and containing less amount of The nonferrous metal oxides such as iron oxide and titanium oxide, make the glaze burnt out have certain milk yellow;Frit is cosolvent, preferably For zinc frit, the main calcic of bovine bone powder and phosphorus can improve the opacity of glaze, talcum is natural hydrous magnesium silicate mineral, is glaze Cosolvent, by increasing capacitance it is possible to increase the opaque of chun glaze;Zinc oxide during high-temperature firing as glaze cosolvent and assistant toner, The firing temperature of glaze is reduced, contributes to the color development of glaze and causes glaze rich in change, while the opaque effect of glaze colours can be increased, Tin oxide is assistant toner;Cupric oxide is photoghraphic coupler, and copper ion shows copper red color, as an ancient unit of weight in reducing atmosphere as the colouring agent of glaze It is red.After above-mentioned raw materials are used cooperatively, moisture in glaze is first excluded, then under oxygen atmosphere, by the relatively low component of fusing point in glaze Melt, glaze is melted into liquid phase from solid phase, then open the air door of kiln, lead into kiln such as high temperature hair in cold wind, with kiln After raw collision, glaze is formed fine and closely woven crackle, and under reducing atmosphere, carry out " transmutation ".
The present invention compared with prior art, by scientific and reasonable raw material proportioning and control burning process, an ancient unit of weight prepared Not only glaze colours is bright in colour for red glaze, and glossiness is good, and mobility is moderate and has fine cracks, and glaze colours is abundant, red with an ancient unit of weight On the basis of mass-tone, occur in that transition is bright and clear between yellow, blue, purple multiple color, color, clear and natural, high yield rate is reachable More than 75%, having filled up the red glaze of an ancient unit of weight does not have the blank of many colored glazes, is that the red glaze pottery of an ancient unit of weight adds a new varieties.
Brief description of the drawings
Fig. 1 is the red glaze schematic diagram of pottery an ancient unit of weight that the embodiment of the present invention 2 is obtained.
Embodiment
Embodiment 1
A kind of red glaze of an ancient unit of weight, is prepared from by the raw material of following parts by weight:37-43 parts of melilite, 13-19 parts of quartz, calcite 10- 16 parts, blue or green 4.5-5.5 parts of alkali, 12-18 parts of frit, 0.5-1.5 parts of ox bone, 2.5-3.5 parts of tin oxide, 3.5-4.5 parts of zinc oxide, 2-3 parts of talcum, 0.25-0.75 parts of cupric oxide.
The preparation method of above-mentioned pottery month white glaze, comprises the following steps:
(1)Take the raw material of above-mentioned parts by weight to add water and be put into ball milling in ball mill, cross 250 mesh sieves, obtain glaze slip;
(2)The glazing by the way of leaching glaze on base substrate after biscuiting;
(3)Burn till, firing temperature is 1250-1280 DEG C;
Firing process specifically includes following steps:1. pre-burning phase:Base substrate after glazing is put into kiln, make temperature in 2-3h from Room temperature rises to 540-580 DEG C;2. heat of oxidation:Under oxidizing atmosphere, temperature is set to be ramped up 1000-1030 DEG C in 3-4h;3. also The former phase:When temperature rises to 1000-1030 DEG C, the air door of kiln is opened, cold wind is passed through into kiln, and under reducing atmosphere, make Temperature is ramped up 1250-1280 DEG C in 5-6h;4. room temperature is naturally cooled to, is made.
Melilite, quartz, calcite, blue or green alkali originate from Yuzhou in the present embodiment.
Embodiment 2
A kind of red glaze of an ancient unit of weight, is prepared from by the raw material of following parts by weight:40 parts of melilite, 16 parts of quartz, 13 parts of calcite, blue or green alkali 5 parts, 15 parts of frit, 1 part of ox bone, 3 parts of tin oxide, 4 parts of zinc oxide, 2.5 parts of talcum, 0.5 part of cupric oxide.
The preparation method of the above-mentioned red glaze of an ancient unit of weight, comprises the following steps:
(1)Take the raw material of above-mentioned parts by weight to add water and be put into ball milling in ball mill, cross 250 mesh sieves, obtain glaze slip;
(2)The glazing by the way of leaching glaze on base substrate after biscuiting;
(3)Burn till, firing temperature is 1270 DEG C;
Firing process specifically includes following steps:1. pre-burning phase:Base substrate after glazing is put into kiln, make temperature in 2.5h from Room temperature rises to 560 DEG C;2. heat of oxidation:Under oxidizing atmosphere, temperature is set to be ramped up 1020 DEG C in 3.5h;3. reduction period:Work as temperature When degree rises to 1020 DEG C, the air door of kiln is opened, cold wind is passed through into kiln, and under reducing atmosphere, make temperature uniform in 5.5h Rise to 1265 DEG C;4. room temperature is naturally cooled to, is made.
The red glaze glaze of an ancient unit of weight obtained using said ratio and method is as shown in figure 1, its glaze colours is bright in colour, and glossiness is good, Mobility is moderate and has fine cracks, and glaze colours is abundant, on the basis of with an ancient unit of weight red for mass-tone, occurs in that yellow, blue, purple many Plant transition between color, color bright and clear, clear and natural, high yield rate, up to more than 75%.
Embodiment 3
A kind of red glaze of an ancient unit of weight, is prepared from by the raw material of following parts by weight:40 parts of melilite, 16 parts of quartz, 13 parts of calcite, blue or green alkali 5 parts, 15 parts of frit, 1 part of ox bone, 3 parts of tin oxide, 4 parts of zinc oxide, 2.5 parts of talcum, 0.5 part of cupric oxide.
(1)Take the raw material of above-mentioned parts by weight to add water and be put into ball milling in ball mill, cross 250 mesh sieves, obtain glaze slip;
(2)The glazing by the way of leaching glaze on base substrate after biscuiting;
(3)Burn till, firing temperature is 1250 DEG C;
Firing process specifically includes following steps:1. pre-burning phase:Base substrate after glazing is put into kiln, makes temperature in 3h from room Temperature rise is to 540 DEG C;2. heat of oxidation:Under oxidizing atmosphere, temperature is set to be ramped up 1030 DEG C in 3h;3. reduction period:When temperature liter During to 1030 DEG C, the air door of kiln is opened, cold wind is passed through into kiln, and under reducing atmosphere, temperature is ramped up in 5h 1250℃;4. room temperature is naturally cooled to, is made.
The pottery yield rate that said ratio and method are obtained is used for 71% or so.
Embodiment 4
A kind of red glaze of an ancient unit of weight, is prepared from by the raw material of following parts by weight:40 parts of melilite, 16 parts of quartz, 13 parts of calcite, blue or green alkali 5 parts, 15 parts of frit, 1 part of ox bone, 3 parts of tin oxide, 4 parts of zinc oxide, 2.5 parts of talcum, 0.5 part of cupric oxide.
1)Take the raw material of above-mentioned parts by weight to add water and be put into ball milling in ball mill, cross 250 mesh sieves, obtain glaze slip;
(2)The glazing by the way of leaching glaze on base substrate after biscuiting;
(3)Burn till, firing temperature is 1280 DEG C;
Firing process specifically includes following steps:1. pre-burning phase:Base substrate after glazing is put into kiln, makes temperature in 2h from room Temperature rise is to 580 DEG C;2. heat of oxidation:Under oxidizing atmosphere, temperature is set to be ramped up 1000 DEG C in 2.5h;3. reduction period:Work as temperature When rising to 1000 DEG C, the air door of kiln is opened, cold wind is passed through into kiln, and under reducing atmosphere, temperature is ramped up in 6h 1270℃;;4. room temperature is naturally cooled to, is made.
The pottery yield rate that said ratio and method are obtained is used for 73% or so.
Embodiment 5
A kind of red glaze of an ancient unit of weight, is prepared from by the raw material of following parts by weight:43 parts of melilite, 18 parts of quartz, 12 parts of calcite, blue or green alkali 5 parts, 15 parts of frit, 1 part of ox bone, 3 parts of tin oxide, 4 parts of zinc oxide, 2.5 parts of talcum, 0.5 part of cupric oxide.Its preparation method is with real Apply example 2.
The pottery yield rate that said ratio and method are obtained is used for 70% or so.
Embodiment 6
A kind of red glaze of an ancient unit of weight, is prepared from by the raw material of following parts by weight:40 parts of melilite, 16 parts of quartz, 13 parts of calcite, blue or green alkali 3 parts, 15 parts of frit, 1 part of ox bone, 2.5 parts of tin oxide, 4.3 parts of zinc oxide, 2.5 parts of talcum, 0.7 part of cupric oxide.
The pottery yield rate that said ratio and method are obtained is used for 74% or so.
Comparative example 1
A kind of red glaze of an ancient unit of weight, is prepared from by the raw material of following parts by weight:40 parts of melilite, 16 parts of quartz, 13 parts of calcite, frit 15 parts, 1 part of ox bone, 3 parts of tin oxide, 2.5 parts of talcum, 0.5 part of cupric oxide.Preparation method be the same as Example 2.This example and embodiment 2 Compare, green grass or young crops alkali and zinc oxide is not used, the glaze colours color and luster burnt out is not bright-coloured, glaze colours more than 90% is that an ancient unit of weight is red, only very little portion Separate transition between existing milk yellow and blueness, and color to obscure, yield rate is only 30%.
Comparative example 2
A kind of red glaze of an ancient unit of weight, is prepared from by the raw material of following parts by weight:40 parts of melilite, 16 parts of quartz, 13 parts of calcite, blue or green alkali 5 parts, 15 parts of frit, 1 part of ox bone, 3 parts of tin oxide, 4 parts of zinc oxide, 2.5 parts of talcum, 0.5 part of cupric oxide.
The preparation method of the above-mentioned red glaze of an ancient unit of weight, comprises the following steps:
(1)Take the raw material of above-mentioned parts by weight to add water and be put into ball milling in ball mill, cross 250 mesh sieves, obtain glaze slip;
(2)The glazing by the way of leaching glaze on base substrate after biscuiting;
(3)Burn till, firing temperature is 1270 DEG C;
Firing process specifically includes following steps:1. pre-burning phase:Base substrate after glazing is put into kiln, make temperature in 2.5h from Room temperature rises to 560 DEG C;2. heat of oxidation:Under oxidizing atmosphere, temperature is set to be ramped up 1020 DEG C in 3.5h;3. reduction period:Also Under Primordial Qi atmosphere, temperature is set to be ramped up 1265 DEG C in 5.5h;4. room temperature is naturally cooled to, is made.
This example compared with Example 2, in reduction period, when temperature rises to 1020 DEG C, is not switched on the air door of kiln, fires Although the glaze colours gone out enriches, glaze does not occur crackle, and yield rate is more than 75%.
Comparative example 3
A kind of red glaze of an ancient unit of weight, is prepared from by the raw material of following parts by weight:40 parts of melilite, 16 parts of quartz, 13 parts of calcite, blue or green alkali 5 parts, 15 parts of frit, 1 part of ox bone, 3 parts of tin oxide, 4 parts of zinc oxide, 2.5 parts of talcum, 0.5 part of cupric oxide.Preparation method is with implementation Example 2.Compared with Example 2, frit is not used in this example, and the glaze burnt out is rough, and glaze pinprick defect, gloss is bad, finished product Rate is 50%.
The red glaze formula of an ancient unit of weight that 7-26 of the embodiment of the present invention is provided is shown in Table 1-3.

Claims (5)

1. a kind of red glaze of an ancient unit of weight, it is characterised in that:It is prepared from by the raw material of following parts by weight:37-43 parts of melilite, quartz 13-19 parts, 10-16 parts of calcite, blue or green 4.5-5.5 parts of alkali, 12-18 parts of frit, 0.5-1.5 parts of bovine bone powder, tin oxide 2.5-3.5 Part, 3.5-4.5 parts of zinc oxide, 2-3 parts of talcum, 0.25-0.75 parts of cupric oxide.
2. the red glaze of an ancient unit of weight as claimed in claim 1, it is characterised in that:It is prepared from by the raw material of following parts by weight:Huang is long 40 parts of stone, 16 parts of quartz, 13 parts of calcite, blue or green 5 parts of alkali, 15 parts of frit, 1 part of bovine bone powder, 3 parts of tin oxide, 4 parts of zinc oxide, cunning 2.5 parts of stone, 0.5 part of cupric oxide.
3. the preparation method of the red glaze of an ancient unit of weight as described in claim any one of 1-2, it is characterised in that comprise the following steps:
(1)Above-mentioned raw materials are added water mixing, ball milling obtains glaze slip;
(2)Glazing;
(3)Burn till, firing temperature is 1250-1280 DEG C.
4. the preparation method of the red glaze of an ancient unit of weight as claimed in claim 3, it is characterised in that step(3)Middle firing process specifically include as Lower step:1. pre-burning phase:Base substrate after glazing is put into kiln, temperature is risen to 540-580 DEG C from room temperature in 2-3h;2. oxygen The change phase:Under oxidizing atmosphere, temperature is set to be ramped up 1000-1030 DEG C in 3-4h;3. reduction period:Under reducing atmosphere, temperature is made Degree is ramped up 1250-1280 DEG C in 5-6h;4. room temperature is naturally cooled to, is made.
5. the preparation method of the red glaze of an ancient unit of weight as claimed in claim 4, it is characterised in that in the reduction period by the air door of kiln Open.
CN201710375686.6A 2017-05-24 2017-05-24 A kind of red glaze of an ancient unit of weight Withdrawn CN107021634A (en)

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Cited By (8)

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Publication number Priority date Publication date Assignee Title
CN107540216A (en) * 2017-09-30 2018-01-05 浙江工业大学之江学院 A kind of yellowish-brown colour glaze and the method for firing yellowish-brown color glaze
CN107572817A (en) * 2017-11-06 2018-01-12 张韶璞 A kind of method for cooking of red pottery glaze
CN107599722A (en) * 2017-10-27 2018-01-19 禹州市正玉钧窑有限公司 The preparation method of the pottery handicraft of horse stepping on a swallow moulding
CN107963812A (en) * 2017-10-18 2018-04-27 禹州市锦丰源瓷业有限公司 A kind of pottery hacking yellowish pea green glaze and preparation method thereof
CN108585506A (en) * 2018-07-30 2018-09-28 赵红刚 A kind of red chun glaze and preparation method thereof
CN108640648A (en) * 2018-06-16 2018-10-12 李德汉 A kind of production method of kwan-yin pottery craftwork
CN109384478A (en) * 2018-12-19 2019-02-26 禹州市正玉钧窑有限公司 A kind of red glaze of band spot an ancient unit of weight
CN111410425A (en) * 2020-03-31 2020-07-14 景德镇市乐陶陶瓷原料有限公司 Medium-temperature bright red glaze and preparation method thereof

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CN106007380A (en) * 2016-05-27 2016-10-12 高根长 Red glaze and preparation method thereof
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Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107540216A (en) * 2017-09-30 2018-01-05 浙江工业大学之江学院 A kind of yellowish-brown colour glaze and the method for firing yellowish-brown color glaze
CN107540216B (en) * 2017-09-30 2021-01-05 浙江工业大学之江学院 Brown glaze and method for firing brown glaze
CN107963812A (en) * 2017-10-18 2018-04-27 禹州市锦丰源瓷业有限公司 A kind of pottery hacking yellowish pea green glaze and preparation method thereof
CN107599722A (en) * 2017-10-27 2018-01-19 禹州市正玉钧窑有限公司 The preparation method of the pottery handicraft of horse stepping on a swallow moulding
CN107572817A (en) * 2017-11-06 2018-01-12 张韶璞 A kind of method for cooking of red pottery glaze
CN108640648A (en) * 2018-06-16 2018-10-12 李德汉 A kind of production method of kwan-yin pottery craftwork
CN108585506A (en) * 2018-07-30 2018-09-28 赵红刚 A kind of red chun glaze and preparation method thereof
CN109384478A (en) * 2018-12-19 2019-02-26 禹州市正玉钧窑有限公司 A kind of red glaze of band spot an ancient unit of weight
CN111410425A (en) * 2020-03-31 2020-07-14 景德镇市乐陶陶瓷原料有限公司 Medium-temperature bright red glaze and preparation method thereof

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