CN107417071B - 制造含孔隙的不透明石英玻璃的方法 - Google Patents
制造含孔隙的不透明石英玻璃的方法 Download PDFInfo
- Publication number
- CN107417071B CN107417071B CN201710373815.8A CN201710373815A CN107417071B CN 107417071 B CN107417071 B CN 107417071B CN 201710373815 A CN201710373815 A CN 201710373815A CN 107417071 B CN107417071 B CN 107417071B
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- Prior art keywords
- sio
- particles
- bet
- slip
- quartz glass
- Prior art date
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Links
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title claims abstract description 136
- 239000011148 porous material Substances 0.000 title claims abstract description 33
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 31
- 239000002245 particle Substances 0.000 claims abstract description 259
- 238000000034 method Methods 0.000 claims abstract description 103
- 229910052906 cristobalite Inorganic materials 0.000 claims abstract description 78
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 78
- 229910052681 coesite Inorganic materials 0.000 claims abstract description 77
- 229910052682 stishovite Inorganic materials 0.000 claims abstract description 77
- 229910052905 tridymite Inorganic materials 0.000 claims abstract description 77
- 230000008569 process Effects 0.000 claims abstract description 48
- 238000000280 densification Methods 0.000 claims abstract description 35
- 239000008187 granular material Substances 0.000 claims abstract description 31
- 239000007921 spray Substances 0.000 claims abstract description 27
- 239000006185 dispersion Substances 0.000 claims abstract description 26
- 239000011361 granulated particle Substances 0.000 claims abstract description 10
- 238000007493 shaping process Methods 0.000 claims abstract description 5
- 238000009826 distribution Methods 0.000 claims description 32
- 238000005469 granulation Methods 0.000 claims description 30
- 230000003179 granulation Effects 0.000 claims description 26
- 239000011164 primary particle Substances 0.000 claims description 17
- 238000001179 sorption measurement Methods 0.000 claims description 14
- 238000005054 agglomeration Methods 0.000 claims description 9
- 239000007788 liquid Substances 0.000 claims description 8
- 239000000460 chlorine Substances 0.000 claims description 6
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 5
- 238000006243 chemical reaction Methods 0.000 claims description 5
- 229910052801 chlorine Inorganic materials 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 5
- 238000007569 slipcasting Methods 0.000 abstract description 5
- 238000005245 sintering Methods 0.000 description 18
- 238000000227 grinding Methods 0.000 description 17
- 230000015572 biosynthetic process Effects 0.000 description 12
- 239000004071 soot Substances 0.000 description 11
- 239000000463 material Substances 0.000 description 10
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 9
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- 238000002360 preparation method Methods 0.000 description 6
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- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- 238000003786 synthesis reaction Methods 0.000 description 4
- 239000002585 base Substances 0.000 description 3
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- 239000008367 deionised water Substances 0.000 description 3
- 229910021641 deionized water Inorganic materials 0.000 description 3
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- 238000010438 heat treatment Methods 0.000 description 3
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- 239000013067 intermediate product Substances 0.000 description 3
- 229910052742 iron Inorganic materials 0.000 description 3
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- 239000004065 semiconductor Substances 0.000 description 3
- 239000007858 starting material Substances 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 238000004017 vitrification Methods 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 238000004438 BET method Methods 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 238000005299 abrasion Methods 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
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- 229910052783 alkali metal Inorganic materials 0.000 description 2
- 150000001340 alkali metals Chemical class 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- 238000000149 argon plasma sintering Methods 0.000 description 2
- 229910052791 calcium Inorganic materials 0.000 description 2
- 238000009690 centrifugal atomisation Methods 0.000 description 2
- 229910052804 chromium Inorganic materials 0.000 description 2
- 238000005056 compaction Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
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- 238000001125 extrusion Methods 0.000 description 2
- 238000009483 freeze granulation Methods 0.000 description 2
- 229910002804 graphite Inorganic materials 0.000 description 2
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- 229910052744 lithium Inorganic materials 0.000 description 2
- 229910052749 magnesium Inorganic materials 0.000 description 2
- 229910052748 manganese Inorganic materials 0.000 description 2
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 2
- 229910052753 mercury Inorganic materials 0.000 description 2
- 229910052750 molybdenum Inorganic materials 0.000 description 2
- 229910052759 nickel Inorganic materials 0.000 description 2
- 238000005457 optimization Methods 0.000 description 2
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- 229910052700 potassium Inorganic materials 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
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- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical class [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 206010041662 Splinter Diseases 0.000 description 1
- WGKMWBIFNQLOKM-UHFFFAOYSA-N [O].[Cl] Chemical compound [O].[Cl] WGKMWBIFNQLOKM-UHFFFAOYSA-N 0.000 description 1
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- 238000004458 analytical method Methods 0.000 description 1
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- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 238000001095 inductively coupled plasma mass spectrometry Methods 0.000 description 1
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- XZWYZXLIPXDOLR-UHFFFAOYSA-N metformin Chemical compound CN(C)C(=N)NC(N)=N XZWYZXLIPXDOLR-UHFFFAOYSA-N 0.000 description 1
- 238000005121 nitriding Methods 0.000 description 1
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- 238000010422 painting Methods 0.000 description 1
- JTJMJGYZQZDUJJ-UHFFFAOYSA-N phencyclidine Chemical class C1CCCCN1C1(C=2C=CC=CC=2)CCCCC1 JTJMJGYZQZDUJJ-UHFFFAOYSA-N 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
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- QZPQZTGNWBSSQP-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O.O[Si](O)(O)O QZPQZTGNWBSSQP-UHFFFAOYSA-N 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
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Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B19/00—Other methods of shaping glass
- C03B19/10—Forming beads
- C03B19/108—Forming porous, sintered or foamed beads
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B19/00—Other methods of shaping glass
- C03B19/06—Other methods of shaping glass by sintering, e.g. by cold isostatic pressing of powders and subsequent sintering, by hot pressing of powders, by sintering slurries or dispersions not undergoing a liquid phase reaction
- C03B19/066—Other methods of shaping glass by sintering, e.g. by cold isostatic pressing of powders and subsequent sintering, by hot pressing of powders, by sintering slurries or dispersions not undergoing a liquid phase reaction for the production of quartz or fused silica articles
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B20/00—Processes specially adapted for the production of quartz or fused silica articles, not otherwise provided for
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/06—Glass compositions containing silica with more than 90% silica by weight, e.g. quartz
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B2201/00—Type of glass produced
- C03B2201/02—Pure silica glass, e.g. pure fused quartz
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2201/00—Glass compositions
- C03C2201/02—Pure silica glass, e.g. pure fused quartz
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2204/00—Glasses, glazes or enamels with special properties
- C03C2204/04—Opaque glass, glaze or enamel
- C03C2204/06—Opaque glass, glaze or enamel opacified by gas
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/50—Glass production, e.g. reusing waste heat during processing or shaping
- Y02P40/57—Improving the yield, e-g- reduction of reject rates
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Dispersion Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Silicon Compounds (AREA)
- Glass Melting And Manufacturing (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP16171047.0A EP3248950B1 (de) | 2016-05-24 | 2016-05-24 | Verfahren zur herstellung eines poren enthaltenden, opaken quarzglases |
| EP16171047.0 | 2016-05-24 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107417071A CN107417071A (zh) | 2017-12-01 |
| CN107417071B true CN107417071B (zh) | 2021-08-17 |
Family
ID=56080293
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710373815.8A Active CN107417071B (zh) | 2016-05-24 | 2017-05-24 | 制造含孔隙的不透明石英玻璃的方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US10358373B2 (enExample) |
| EP (1) | EP3248950B1 (enExample) |
| JP (1) | JP6698585B2 (enExample) |
| KR (1) | KR102123925B1 (enExample) |
| CN (1) | CN107417071B (enExample) |
| TW (1) | TWI705045B (enExample) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BR112017027426A2 (pt) * | 2015-11-04 | 2018-09-04 | Unimin Corp | pó de quartzo purificado modificado para revestir cabo de fibra ótica e método de modificar um pó de quartzo altamente purificado |
| CN108563615B (zh) * | 2018-04-09 | 2022-04-01 | 清华大学深圳研究生院 | 支柱绝缘子聚氨酯孔泡的评估方法 |
| JP7157932B2 (ja) * | 2019-01-11 | 2022-10-21 | 株式会社Sumco | シリカガラスルツボの製造装置および製造方法 |
| JP6751822B1 (ja) * | 2019-06-03 | 2020-09-09 | 東ソー・クォーツ株式会社 | 不透明石英ガラス及びその製造方法 |
| CN115279705A (zh) * | 2020-02-28 | 2022-11-01 | Ａｇｃ株式会社 | 二氧化硅玻璃、使用有二氧化硅玻璃的高频装置、以及二氧化硅玻璃的制造方法 |
| CN111233308A (zh) * | 2020-03-17 | 2020-06-05 | 江苏亨通智能科技有限公司 | 一种不透明石英玻璃锭及其制备方法 |
| JPWO2022215662A1 (enExample) * | 2021-04-07 | 2022-10-13 | ||
| EP4108641A1 (de) * | 2021-06-24 | 2022-12-28 | Heraeus Quarzglas GmbH & Co. KG | Formkörper aus opakem quarzglas sowie verfahren zur herstellung desselben |
| CN116375315B (zh) * | 2022-11-29 | 2024-11-22 | 湖北菲利华石英玻璃股份有限公司 | 一种掺钛合成石英砂的制备方法 |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN87107444A (zh) * | 1986-12-11 | 1988-06-22 | 美国电话电报公司 | 制造具有高纯石英玻璃体的制品的方法和用该方法生产的制品 |
| DE10243953A1 (de) * | 2002-09-21 | 2004-04-08 | Heraeus Quarzglas Gmbh & Co. Kg | Verfahren für die Herstellung eines Bauteils aus opakem Quarzglas |
| CN1200896C (zh) * | 1999-12-22 | 2005-05-11 | 赫罗伊斯石英玻璃股份有限两合公司 | 石英玻璃的制造方法及所用的颗粒和由其构成的部件 |
| CN104671670A (zh) * | 2013-11-28 | 2015-06-03 | 赫罗伊斯石英玻璃股份有限两合公司 | 制造透明或不透明熔融二氧化硅的涂覆部件的方法 |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4042361A (en) | 1976-04-26 | 1977-08-16 | Corning Glass Works | Method of densifying metal oxides |
| GB8627735D0 (en) * | 1986-11-20 | 1986-12-17 | Tsl Group Plc | Vitreous silica |
| DE3814863A1 (de) * | 1988-05-02 | 1989-11-16 | Siemens Ag | Verfahren zum herstellen von vielschichtenkeramik auf silikatbasis |
| DE10019693B4 (de) | 2000-04-20 | 2006-01-19 | Heraeus Quarzglas Gmbh & Co. Kg | Verfahren zur Herstellung eines Bauteils aus opakem, synthetischen Quarzglas, nach dem Verfahren hergestelltes Quarzglasrohr, sowie Verwendung desselben |
| EP1328482A1 (en) * | 2000-09-28 | 2003-07-23 | Corning Incorporated | Optical glass silica soot particles and method of making same |
| DE10114484C2 (de) * | 2001-03-24 | 2003-10-16 | Heraeus Quarzglas | Verfahren für die Herstellung eines Komposit-Werkstoffs mit einem SiO¶2¶-Gehalt von mindestens 99 Gew.-%, und Verwendung des nach dem Verfahren erhaltenen Komposit-Werkstoffs |
| DE10262015B3 (de) * | 2002-09-20 | 2004-07-15 | Heraeus Quarzglas Gmbh & Co. Kg | Verfahren für die Herstellung eines opaken Quarzglas-Kompositwerkstoffs |
| DE10243954B3 (de) * | 2002-09-20 | 2004-07-08 | Heraeus Quarzglas Gmbh & Co. Kg | Verfahren für die Herstellung eines opaken Quarzglas-Kompositwerkstoffs sowie Verwendung desselben |
| FR2858611B1 (fr) * | 2003-08-07 | 2006-11-24 | Saint Gobain Ct Recherches | Procede de fabrication d'une piece en silice amorphe frittee, moule et barbotine mis en oeuvre dans ce procede |
| JP2005097103A (ja) * | 2003-09-22 | 2005-04-14 | Heraeus Quarzglas Gmbh & Co Kg | 複合材料からキャスティングを製造する方法とセラミックもしくはガラス質の複合材料のキャスティング |
| DE102006052512A1 (de) * | 2006-11-06 | 2008-05-08 | Heraeus Quarzglas Gmbh & Co. Kg | Verfahren zur Herstellung von opakem Quarzglas, nach dem Verfahren erhaltenes Halbzeug sowie daraus hergestelltes Bauteil |
| DE102007030698B4 (de) * | 2007-06-30 | 2009-06-10 | Heraeus Quarzglas Gmbh & Co. Kg | Verfahren zur Herstellung eines Verbundkörpers aus einem Basiskörper aus opakem Quarzglas und einer dichten Versiegelungsschicht sowie Verwendung des Verbundkörpers |
| JP2011207719A (ja) * | 2010-03-30 | 2011-10-20 | Mitsubishi Materials Corp | 合成非晶質シリカ粉末とその製造方法 |
| CN102167500B (zh) * | 2011-01-10 | 2013-01-09 | 圣戈班石英（锦州）有限公司 | 一种不透明石英实验室器皿的制备方法 |
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| EP3000790B2 (de) * | 2014-09-29 | 2023-07-26 | Heraeus Quarzglas GmbH & Co. KG | Verfahren für die Herstellung von Bauteilen aus synthetischem Quarzglas aus SiO2-Granulat |
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2016
- 2016-05-24 EP EP16171047.0A patent/EP3248950B1/de active Active
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2017
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- 2017-05-23 US US15/602,919 patent/US10358373B2/en active Active
- 2017-05-24 KR KR1020170064377A patent/KR102123925B1/ko active Active
- 2017-05-24 CN CN201710373815.8A patent/CN107417071B/zh active Active
- 2017-05-24 JP JP2017102707A patent/JP6698585B2/ja active Active
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| CN87107444A (zh) * | 1986-12-11 | 1988-06-22 | 美国电话电报公司 | 制造具有高纯石英玻璃体的制品的方法和用该方法生产的制品 |
| CN1200896C (zh) * | 1999-12-22 | 2005-05-11 | 赫罗伊斯石英玻璃股份有限两合公司 | 石英玻璃的制造方法及所用的颗粒和由其构成的部件 |
| DE10243953A1 (de) * | 2002-09-21 | 2004-04-08 | Heraeus Quarzglas Gmbh & Co. Kg | Verfahren für die Herstellung eines Bauteils aus opakem Quarzglas |
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Also Published As
| Publication number | Publication date |
|---|---|
| CN107417071A (zh) | 2017-12-01 |
| US10358373B2 (en) | 2019-07-23 |
| JP2017210403A (ja) | 2017-11-30 |
| TW201741256A (zh) | 2017-12-01 |
| KR20170132696A (ko) | 2017-12-04 |
| EP3248950B1 (de) | 2020-08-05 |
| TWI705045B (zh) | 2020-09-21 |
| US20170341968A1 (en) | 2017-11-30 |
| EP3248950A1 (de) | 2017-11-29 |
| JP6698585B2 (ja) | 2020-05-27 |
| KR102123925B1 (ko) | 2020-06-18 |
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