CN107375180B - Skin care product composition, facial mask and preparation method of facial mask - Google Patents
Skin care product composition, facial mask and preparation method of facial mask Download PDFInfo
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- CN107375180B CN107375180B CN201710686258.5A CN201710686258A CN107375180B CN 107375180 B CN107375180 B CN 107375180B CN 201710686258 A CN201710686258 A CN 201710686258A CN 107375180 B CN107375180 B CN 107375180B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/10—General cosmetic use
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/522—Antioxidants; Radical scavengers
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Abstract
The invention provides a skin care composition, which comprises: 0.001-1 part by weight of folic acid and/or folic acid derivatives; 0-5 parts by weight of sturgeon caviar extract; 0-8 parts of pearl extract; 0-15 parts by weight of caprylic/capric triglyceride; and the content of the sturgeon caviar extract, the content of the pearl extract and the content of the caprylic/capric triglyceride are not 0 at the same time. Compared with the prior art, the folic acid and/or the derivatives thereof are combined with one or more of the sturgeon caviar extract, the pearl extract and the caprylic/capric triglyceride, so that the obtained composition not only can synergize in effect and improve whitening and anti-aging effects on skin, but also has the effects of scavenging free radicals and filtering ultraviolet rays due to the sturgeon caviar extract, the pearl extract and the caprylic/capric triglyceride, so that the light and heat stability of folic acid is enhanced, the content of folic acid is kept stable, and the action time of the skin care composition is prolonged.
Description
Technical Field
The invention relates to the technical field of daily necessities, in particular to a skin care product composition, a mask and a preparation method thereof.
Background
Folic acid is an efficient skin care component, can combine water which is 5000 times of the self weight of the folic acid, has good moisturizing performance, and can promote the generation of natural moisturizing factors NMF in skin cutin, thereby forming a protective film, reducing the water loss of the skin under the condition of not changing sebum secretion, and leading the skin to recover the moisture, the tenderness and the smoothness. In addition, folic acid has strong promotion effect on physiological processes such as DNA synthesis, cell metabolism and the like, and can promote DNA chain scission to be recombined, so that skin injury caused by ultraviolet rays is effectively repaired, and the skin is restored to be smooth and soft and elastic. Moreover, the red blood cells in the human body are renewed about once every four months, and if folic acid is lacked, the generation of the red blood cells is disturbed, so that the volume of the red blood cells is increased and decreased, and the symptoms of pale face and the like are further caused. In conclusion, folic acid can be added into skin care products such as facial masks, face creams, body lotions and the like to moisten and nourish the skin, thereby achieving the effect of improving the skin quality.
However, folic acid is an unstable B-group vitamin, and is easily oxidized by environmental factors such as light and heat, thereby losing activity and causing a reduction in skin care effect.
Disclosure of Invention
In view of the above, the technical problem to be solved by the present invention is to provide a skin care composition, a facial mask and a preparation method thereof, wherein the folic acid content of the skin care composition provided by the present invention is stable.
The invention provides a skin care composition, which comprises:
and the content of the sturgeon caviar extract, the content of the pearl extract and the content of the caprylic/capric triglyceride are not 0 at the same time.
Preferably, the folic acid derivative is selected from tetrahydrofolic acid, 5-methyltetrahydrofolic acid, 6-S-5-methyltetrahydrofolic acid, leucovorin, calcium folinate or calcium levofolinate.
The invention also provides an application of the composition in preparing cosmetics.
The invention also provides a cosmetic comprising the composition.
Preferably, the cosmetic is a mask, cream or milk.
The invention also provides a mask, which comprises a solvent and the following components:
and the content of the sturgeon caviar extract, the content of the pearl extract and the content of the caprylic/capric triglyceride are not 0 at the same time.
Preferably, the skin conditioning agent is selected from one or more of ulmus pumila root extract, p-hydroxyacetophenone, dipotassium glycyrrhizinate, creatine, polyglycerol-10 oleate, allantoin, shea butter, hydrogenated lecithin, and amaranthus caucasicus seed extract.
The pH value regulator is selected from one or more of tromethamine, sodium hydroxide, potassium hydroxide, arginine and triethanolamine;
the chelating agent is selected from one or more of trisodium EDTA, disodium EDTA and tetrasodium EDTA;
the humectant is selected from one or more of 1, 2-hexanediol, butanediol, glycerol, methyl propylene glycol, betaine, glyceryl polyether-26, sodium hyaluronate, propylene glycol, polyglycerol-10 and luba gum oil;
the surfactant is selected from PEG-60 hydrogenated castor oil and/or acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer;
the aromatic is selected from essence and/or essential oil;
the thickening agent is selected from one or more of xanthan gum, hydroxyethyl cellulose and carbomer;
the solvent is water.
The invention also provides a preparation method of the facial mask, which comprises the following steps:
s1) mixing and heating the thickening agent, the humectant, the solvent and the chelating agent to obtain a phase A;
mixing and heating raw materials which need to be added under high temperature condition in the skin conditioning agent and caprylic/capric triglyceride to obtain a phase B;
s2) mixing the phase A and the phase B with a surfactant, homogenizing, cooling, adding a pH regulator, folic acid and/or folic acid derivatives, sturgeon roe paste extract, pearl extract, and raw materials to be added in a skin conditioner at a low temperature, and mixing with an aromatic agent under stirring to obtain the facial mask.
Preferably, the temperature of the phase A is 80-90 ℃; the temperature of the phase B is 80-90 ℃.
Preferably, the step S2) is specifically: mixing the phase A and the phase B with a surfactant, homogenizing, cooling to 50-60 ℃, adding a pH regulator, then continuously cooling to 40-50 ℃, adding folic acid and/or folic acid derivatives, sturgeon roe sauce extract, pearl extract, raw materials which need to be added in a skin conditioner under a low temperature condition, and an aromatic agent, mixing and stirring to obtain the mask.
Compared with the prior art, the invention provides a skin care product composition, which comprises the following components: 0.001-1 part by weight of folic acid and/or folic acid derivatives; 0-5 parts by weight of sturgeon caviar extract; 0-8 parts of pearl extract; 0-15 parts by weight of caprylic/capric triglyceride; and the content of the sturgeon caviar extract, the content of the pearl extract and the content of the caprylic/capric triglyceride are not 0 at the same time. According to the invention, folic acid and/or derivatives thereof are combined with one or more of sturgeon caviar extract, pearl extract and caprylic/capric triglyceride, so that the obtained composition not only has synergistic effect in effect and improves whitening and anti-aging effects on skin, but also has the effects of scavenging free radicals and filtering ultraviolet rays due to the sturgeon caviar extract, the pearl extract and the caprylic/capric triglyceride, so that the light and heat stability of folic acid is enhanced, the content of folic acid is kept stable, and the action time of the skin care composition is prolonged.
Detailed Description
The invention provides a skin care composition, which comprises:
and the content of the sturgeon caviar extract, the content of the pearl extract and the content of the caprylic/capric triglyceride are not 0 at the same time.
The skin care composition provided by the invention comprises 0.001-1 part by weight of folic acid and/or folic acid derivatives, preferably 0.01-0.5 part by weight of folic acid and/or folic acid derivatives, and more preferably 0.01-0.2 part by weight of folic acid and/or folic acid derivatives; in some embodiments provided herein, the folic acid and/or folic acid derivatives are preferably present in an amount of 0.001 parts by weight; in some embodiments provided herein, the folic acid and/or folic acid derivatives are preferably present in an amount of 0.01 parts by weight; in other embodiments provided herein, the folic acid and/or folic acid derivatives are preferably present in an amount of 0.02 parts by weight; in some embodiments provided herein, the folic acid and/or folic acid derivatives are preferably present in an amount of 0.1 parts by weight; in other embodiments provided herein, the folic acid and/or folic acid derivatives are preferably present in an amount of 0.2 parts by weight; in other embodiments provided herein, the folic acid and/or folic acid derivatives are preferably present in an amount of 1 part by weight; the folic acid derivative is not particularly limited as long as it is a folic acid derivative known to those skilled in the art, but in the present invention, tetrahydrofolic acid, 5-methyltetrahydrofolic acid, 6-S-5-methyltetrahydrofolic acid, leucovorin, calcium folinate, or calcium levofolinate is preferable.
The skin care product composition provided by the invention comprises 0-5 parts by weight of sturgeon caviar extract, more preferably 0.5-5 parts by weight of sturgeon caviar extract, and further preferably 0.5-3 parts by weight of sturgeon caviar extract; in some embodiments provided herein, the sturgeon caviar extract is preferably present in an amount of 0 parts by weight; in some embodiments provided herein, the sturgeon caviar extract is preferably present in an amount of 0.5 parts by weight; in some embodiments provided herein, the sturgeon caviar extract is preferably present in an amount of 0.8 parts by weight; in some embodiments provided herein, the sturgeon caviar extract is preferably present in an amount of 1 part by weight; in some embodiments provided herein, the sturgeon caviar extract is preferably present in an amount of 1.01 parts by weight; in some embodiments provided herein, the sturgeon caviar extract is preferably present in an amount of 1.5 parts by weight; in some embodiments provided herein, the sturgeon caviar extract is preferably present in an amount of 2.011 parts by weight; in some embodiments provided herein, the sturgeon caviar extract is preferably present in an amount of 2.3 parts by weight; in some embodiments provided herein, the sturgeon caviar extract is preferably present in an amount of 2.5 parts by weight; in some embodiments provided herein, the sturgeon caviar extract is preferably present in an amount of 3 parts by weight; in some embodiments provided herein, the sturgeon caviar extract is preferably present in an amount of 5 parts by weight.
The skin care composition provided by the invention comprises 0-8 parts by weight of pearl extract, preferably 0.5-8 parts by weight of pearl extract, and more preferably 0.5-6 parts by weight of pearl extract; in some embodiments provided herein, the pearl extract is preferably present in an amount of 0 parts by weight; in some embodiments provided herein, the pearl extract is preferably present in an amount of 2.5 parts by weight; in some embodiments provided herein, the pearl extract is preferably present in an amount of 2 parts by weight; in some embodiments provided herein, the pearl extract is preferably present in an amount of 5 parts by weight; in some embodiments provided herein, the pearl extract is preferably present in an amount of 1 part by weight; in some embodiments provided herein, the pearl extract is preferably present in an amount of 8 parts by weight; in some embodiments provided herein, the pearl extract is preferably present in an amount of 4 parts by weight; in some embodiments provided herein, the pearl extract is preferably present in an amount of 0.5 parts by weight; in some embodiments provided herein, the pearl extract is preferably present in an amount of 1.5 parts by weight; in other embodiments provided herein, the pearl extract is preferably present in an amount of 6 parts by weight.
According to the invention, the content of caprylic/capric triglyceride in the skin care product extract is preferably 2-15 parts by weight, and more preferably 2.5-10 parts by weight; in some embodiments provided herein, the caprylic/capric triglyceride is preferably present in an amount of 0 parts by weight; in some embodiments provided herein, the caprylic/capric triglyceride is preferably present in an amount of 5 parts by weight; in some embodiments provided herein, the caprylic/capric triglyceride is preferably present in an amount of 2.5 parts by weight; in some embodiments provided herein, the caprylic/capric triglyceride is preferably present in an amount of 15 parts by weight; in some embodiments provided herein, the caprylic/capric triglyceride is preferably present in an amount of 4.001 parts by weight; in some embodiments provided herein, the caprylic/capric triglyceride is preferably present in an amount of 10 parts by weight; in some embodiments provided herein, the caprylic/capric triglyceride is preferably present in an amount of 2 parts by weight; in some embodiments provided herein, the caprylic/capric triglyceride is preferably present in an amount of 8 parts by weight; in some embodiments provided herein, the caprylic/capric triglyceride is preferably present in an amount of 8.5 parts by weight; in some embodiments provided herein, the caprylic/capric triglyceride is preferably present in an amount of 11 parts by weight; in other embodiments provided herein, the caprylic/capric triglyceride is preferably present in an amount of 3 parts by weight.
The skin care composition provided by the invention can also comprise auxiliary materials acceptable in skin care products, or comprise other components and auxiliary agents which are well known by the technical personnel in the field and can be used for skin care; preferably, the composition also comprises 0-2 parts by weight of sodium bicarbonate, more preferably 0.1-2 parts by weight of sodium bicarbonate, and still more preferably 0.5-1 part by weight of sodium bicarbonate; according to the invention, the emulsion also comprises 0-5 parts by weight of emulsifier, more preferably 1-4 parts by weight of emulsifier, and further preferably 2-3 parts by weight of emulsifier; the emulsifier is not particularly limited as long as it is well known to those skilled in the art, and self-emulsifying monoglyceride is preferred in the present invention.
According to the invention, folic acid and/or derivatives thereof are combined with one or more of sturgeon caviar extract, pearl extract and caprylic/capric triglyceride, so that the obtained composition not only has synergistic effect in effect and improves whitening and anti-aging effects on skin, but also has the effects of scavenging free radicals and filtering ultraviolet rays due to the sturgeon caviar extract, the pearl extract and the caprylic/capric triglyceride, so that the light and heat stability of folic acid is enhanced, the content of folic acid is kept stable, and the action time of the skin care composition is prolonged.
The invention provides application of the skin care product composition in any one of the technical schemes in preparation of cosmetics.
The invention also provides a cosmetic comprising the skin care composition in any one of the technical schemes.
Preferably, the cosmetic is a mask, cream or milk.
Wherein the cream is preferably a facial cream; the milk is preferably body milk.
While specific bases for creams and body milks may be well known to those skilled in the art, the inventors are not limited thereto.
The invention provides a facial mask, which comprises a solvent and the following components:
and the content of the sturgeon caviar extract, the content of the pearl extract and the content of the caprylic/capric triglyceride are not 0 at the same time.
Wherein the folic acid and/or folic acid derivatives, sturgeon caviar extract, pearl extract and caprylic/capric triglyceride are the same as above, and are not repeated herein.
In the mask provided by the invention, the content of folic acid and/or folic acid derivatives is preferably 0.01-0.1 part by weight; the content of the sturgeon caviar extract is preferably 0.5-3 parts by weight; the content of the pearl extract is preferably 0-1.5 parts by weight; the content of the caprylic/capric triglyceride is preferably 0 to 2 parts by weight.
According to the present invention, the skin conditioner is preferably contained in an amount of 2 to 25 parts by weight, more preferably 2 to 20 parts by weight, still more preferably 2 to 10 parts by weight, still more preferably 3 to 6 parts by weight, still more preferably 4 to 6 parts by weight, and most preferably 5.85 parts by weight; the skin conditioner is not particularly limited as long as it is well known to those skilled in the art, and in the present invention, one or more of ulmus pumila root extract, p-hydroxyacetophenone, dipotassium glycyrrhizinate, creatine, polyglycerol-10 oleate, allantoin, shea butter, hydrogenated lecithin, and amaranthus caucasicus seed extract are preferable.
Wherein the polyglycerol-10 oleate, the shea butter and the hydrogenated lecithin need to be added at high temperature in the preparation process, and the chunshigen extract, the p-hydroxyacetophenone, the caucasian amaranth seed extract, the allantoin, the dipotassium glycyrrhizinate and the creatine need to be added at low temperature in the preparation process.
The content of the pH regulator is preferably 0.05 to 4 parts by weight, more preferably 0.1 to 3 parts by weight, still more preferably 0.1 to 1 part by weight, still more preferably 0.1 to 0.5 part by weight, and most preferably 0.12 to 0.3 part by weight; the pH adjuster is not particularly limited as long as it is well known to those skilled in the art, and in the present invention, one or more of tromethamine, sodium hydroxide, potassium hydroxide, arginine, and triethanolamine are preferable.
The content of the chelating agent is preferably 0.05-0.08 weight part, and more preferably 0.05-0.06 weight part; the chelating agent is not particularly limited as long as it is a chelating agent well known to those skilled in the art, and in the present invention, one or more of trisodium EDTA, disodium EDTA, and tetrasodium EDTA are preferable.
The content of the humectant is preferably 5-20 parts by weight, more preferably 10-20 parts by weight, still more preferably 13-16 parts by weight, and most preferably 15-15.52 parts by weight; the humectant is not particularly limited as long as it is known to those skilled in the art, and in the present invention, one or more of 1, 2-hexanediol, butylene glycol, glycerin, methyl propylene glycol, betaine, glyceryl polyether-26, sodium hyaluronate, propylene glycol, polyglycerol-10, and luba gum oil are preferable.
The content of the surfactant is preferably 0.1-2 parts by weight, more preferably 0.1-1 part by weight, still more preferably 0.2-0.5 part by weight, and most preferably 0.4-0.5 part by weight; the surfactant is not particularly limited as long as it is well known to those skilled in the art, and PEG-60 hydrogenated castor oil and/or acrylic/C10-30 alkanol acrylate crosspolymer is preferred in the present invention.
The content of the aromatic is preferably 0 to 0.3 part by weight, more preferably 0.1 to 0.2 part by weight, and still more preferably 0.1 part by weight; the aromatic may be one known to those skilled in the art, and is not particularly limited, and in the present invention, essence and/or essential oil is preferable.
The content of the thickener is preferably 0.05 to 3 parts by weight, more preferably 0.1 to 2 parts by weight, still more preferably 0.1 to 1 part by weight, still more preferably 0.1 to 0.5 part by weight, and most preferably 0.15 to 0.25 part by weight; the thickener is not particularly limited as long as it is well known to those skilled in the art, and in the present invention, one or more of xanthan gum, hydroxyethyl cellulose and carbomer are preferable.
The solvent is not particularly limited as long as it is well known to those skilled in the art, and in the present invention, water is preferred; the amount of the solvent is preferably to make up 100 parts by weight with other components.
According to the mask provided by the invention, folic acid and/or derivatives thereof are combined with one or more of sturgeon caviar extract, pearl extract and caprylic/capric triglyceride, so that the obtained mask not only can be synergistic in effect and improve skin whitening and anti-aging effects, but also has the effects of scavenging free radicals and filtering ultraviolet rays due to the sturgeon caviar extract, the pearl extract and the caprylic/capric triglyceride, so that the light and heat stability of folic acid is enhanced, the content of folic acid is kept stable, and the action time of the mask is prolonged.
The invention also provides a preparation method of the facial mask, which comprises the following steps: s1) mixing and heating the thickening agent, the humectant, the solvent and the chelating agent to obtain a phase A; mixing and heating the raw material added into the skin conditioning agent under the condition of high temperature and caprylic/capric triglyceride to obtain a phase B; s2) mixing the phase A and the phase B with a surfactant, homogenizing, cooling, adding a pH regulator, folic acid and/or folic acid derivatives, sturgeon roe paste extract, pearl extract, and raw materials to be added in a skin conditioner at a low temperature, and mixing with an aromatic agent under stirring to obtain the facial mask.
Wherein the thickener, humectant, chelating agent, solvent, skin conditioning agent, surfactant, pH regulator, folic acid and/or folic acid derivatives, sturgeon caviar extract, pearl extract, caprylic/capric triglyceride and fragrance are the same as above, and are not repeated herein.
Mixing and heating a thickening agent, a humectant, a solvent and a chelating agent to obtain a phase A; preferably, the thickening agent and the humectant are mixed firstly, then the water and the chelating agent are added, and the mixture is mixed and heated; the heating temperature is preferably 80 ℃ to 90 ℃.
Mixing and heating the raw material added into the skin conditioning agent under the condition of high temperature and caprylic/capric triglyceride, preferably heating to 80-90 ℃ to obtain phase B. In the present invention, the preparation of the phase A and the phase B is not ordered.
Mixing the A phase and the B phase with a surfactant, preferably adding the B phase into the A phase, then adding the B phase into the surfactant, and homogenizing.
Homogenizing, cooling, preferably to 50-60 deg.C, adding pH regulator, folic acid and/or folic acid derivatives, sturgeon roe sauce extract, Margarita extract, and skin conditioner, mixing with aromatic, and stirring; more preferably, after adding the pH regulator, continuously cooling to 40-50 ℃, then adding folic acid and/or folic acid derivatives, sturgeon roe sauce extract, pearl extract, raw materials which need to be added under the low temperature condition in the skin conditioner, and the aromatic, mixing and stirring to obtain the facial mask.
The evaluation method of the skin care composition in the examples of the present invention mainly proceeds as follows:
the skin care composition and the evaluation of the effect of the skin care product comprising the composition in the examples were carried out by human trial test:
(1) skin whitening effect measurement:
and selecting the crowds with dark skin color, sunburn, chloasma and acne marks to participate in the test of the whitening effect of the skin care sample. The skin care samples in the examples and the comparative examples were used for each group of 20 persons, and the average value of variations in ITA and the average value of variations in the number of spots before and after 4 weeks of continuous use of the skin care samples were measured and calculated using the individual type angle of ITA.
(2) And (3) determining the anti-aging effect:
and selecting a population with consistent skin types and working outdoors to take the test of the anti-aging effect of the skin care sample. Grouping according to the number of test samples, wherein 20 persons are used in each group, the skin care samples in the examples and the comparative examples are used in each group, and after 4 weeks, the humidity of the skin and the roughness of the skin are measured by a skin tester, and the average values are calculated respectively; wherein the humidity test parameters and the roughness test parameters are shown in the following table.
Table 1 humidity test parameters
TABLE 2 roughness test parameters
Determination of folic acid stability:
and (3) placing the skin care product sample at 45 ℃ under the illumination condition, measuring the folic acid content in the skin care product sample on days 0, 5, 15, 30, 60 and 90, and calculating the attenuation rate. The determination method is carried out according to the detection method of folic acid in pharmacopoeia.
In order to further illustrate the present invention, the skin care composition, the mask and the preparation method thereof provided by the present invention are described in detail below with reference to examples.
Examples 1 to 7 and comparative examples 1 to 3
A skin care composition.
(1) Formulation of
(2) The preparation method comprises the following steps: mixing the rest 0.5g of sodium bicarbonate and 2g of self-emulsifying monoglyceride, and diluting to 100ml with distilled water, and mixing to obtain the skin care composition.
(3) Effect testing
The whitening effect and the anti-photoaging effect are compared:
decay of folate content over time:
examples 8 to 10 and comparative examples 4 to 5
Skin care composition
(1) Formulation of
(2) The preparation method comprises the following steps: mixing the above components with 0.5g sodium bicarbonate and 2g self-emulsifying monoglyceride, and diluting to 100ml with distilled water to obtain skin care composition.
(3) Comparison of effects
Examples 11 to 13 and comparative examples 6 to 8
A facial mask is provided.
(1) Formulation of
(2) The preparation method comprises the following steps:
phase A: xanthan gum, carbomer, hydroxyethyl cellulose, sodium hyaluronate, glycerol, butanediol, methyl propylene glycol, 1, 2-hexanediol, betaine and glyceryl polyether-26 are uniformly dispersed, water and EDTA trisodium are added, and the mixture is stirred and heated to 85 ℃.
Phase B: weighing oil phases such as shea butter, polyglycerol-10 oleate, hydrogenated lecithin, caprylic/capric triglyceride and the like, and heating to 85 ℃.
Adding phase B into phase A, adding PEG-60 hydrogenated castor oil, and homogenizing.
Slowly stirring and cooling to 55 ℃, and adding tromethamine.
Cooling to 45 deg.C, adding folic acid, sturgeon caviar extract, Margarita extract, Amaranthus caudatus (Amaranthus caudatus) seed extract, Ulmus DAVIDIANA (Ulmus DAVIDIANA) root extract, p-hydroxyacetophenone, allantoin, dipotassium glycyrrhizinate, creatine, and essence. Stirring evenly, and discharging.
(3) Effect testing
Comparison of whitening and anti-photoaging effects
Decay of folate content over time
Examples 14 to 16 and comparative examples 9 to 11
A body lotion.
(1) Formulation of
(2) The preparation method comprises the following steps:
phase A: mixing water, glycerol and xanthan gum, stirring, and heating to 85 deg.C.
Phase B: mixing caprylic/capric acid glycerol, stearyl alcohol, isopropyl palmitate, oleum Hippophae, isooctyl palmitate, PS-100, isopropyl myristate, Brij 721, Brij 72, and shea butter, stirring, and heating to 85 deg.C.
Phase B was added to phase A, stirred and homogenized for 5 minutes.
Cooling to 45 deg.C, adding folic acid, sturgeon caviar extract, Margarita extract, methylisothiazolinone/iodopropynyl butylcarbamate, creatine, and essence. Discharging.
(3) Effect testing
Comparison of whitening and anti-photoaging effects
Decay of folate content over time
Examples 17 to 19 and comparative examples 12 to 14
A facial cream.
(1) Formulation of
(2) The preparation method comprises the following steps:
phase A: adding water, carbomer 940 (carbomer), EDTA-Na, glycerol and propylene glycol into water phase pot, stirring and heating to 85 deg.C.
Phase B: adding caprylic/capric triglyceride, beeswax, C16-18 alcohol, shea butter, self-emulsifying monoglyceride A165, synthetic squalane, and DC 345 into oil phase pot, stirring and heating to 85 deg.C, and stirring to dissolve.
Stirring phase A, adding phase B and homogenizing for 5 min. The temperature is reduced to 65 ℃, acrylic polymer (305) is added, and the mixture is homogenized for 2 minutes after being stirred.
Cooling to 60 deg.C, adding triethanolamine, and stirring.
Cooling to 45 deg.C, adding folic acid, sturgeon caviar extract, Margarita extract, antiseptic, and essence, and discharging.
(3) Effect testing
Comparison of whitening and anti-photoaging effects
Decay of folate content over time
The foregoing is only a preferred embodiment of the present invention, and it should be noted that, for those skilled in the art, various modifications and decorations can be made without departing from the principle of the present invention, and these modifications and decorations should also be regarded as the protection scope of the present invention.
Claims (9)
1. A skin care composition is characterized by comprising the following components:
2. the skin care composition of claim 1, wherein the folic acid derivative is selected from the group consisting of tetrahydrofolic acid, 5-methyltetrahydrofolic acid, 6-S-5-methyltetrahydrofolic acid, leucovorin, calcium folinate, and calcium levofolinate.
3. Use of a composition according to any one of claims 1 to 2 for the preparation of a cosmetic product.
4. A cosmetic comprising the composition according to any one of claims 1 to 2.
5. The cosmetic according to claim 4, which is a mask, cream or milk.
6. The mask is characterized by comprising a solvent and the following components:
the skin conditioner is selected from one or more of radix Ulmi Pumilae extract, p-hydroxyacetophenone, dipotassium glycyrrhizinate, creatine, polyglycerol-10 oleate, allantoin, shea butter, hydrogenated lecithin and Amaranthus caudatus seed extract;
the pH value regulator is selected from one or more of tromethamine, sodium hydroxide, potassium hydroxide, arginine and triethanolamine;
the chelating agent is selected from one or more of trisodium EDTA, disodium EDTA and tetrasodium EDTA;
the humectant is selected from one or more of 1, 2-hexanediol, butanediol, glycerol, methyl propylene glycol, betaine, glyceryl polyether-26, sodium hyaluronate, propylene glycol, polyglycerol-10 and luba gum oil;
the surfactant is selected from PEG-60 hydrogenated castor oil and/or acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer;
the aromatic is selected from essence and/or essential oil;
the thickening agent is selected from one or more of xanthan gum, hydroxyethyl cellulose and carbomer;
the solvent is water.
7. A method for preparing the mask pack of claim 6, comprising:
s1) mixing and heating the thickening agent, the humectant, the solvent and the chelating agent to obtain a phase A;
mixing and heating the raw material added into the skin conditioning agent under the condition of high temperature and caprylic/capric triglyceride to obtain a phase B;
s2) mixing the phase A and the phase B with a surfactant, homogenizing, cooling, adding a pH regulator, folic acid and/or folic acid derivatives, sturgeon roe paste extract, pearl extract, and a skin conditioner, mixing the raw materials which need to be added at low temperature with an aromatic, and stirring to obtain the facial mask.
8. The method according to claim 7, wherein the temperature of the phase A is 80 ℃ to 90 ℃; the temperature of the phase B is 80-90 ℃.
9. The preparation method according to claim 8, wherein the step S2) is specifically: mixing the phase A and the phase B with a surfactant, homogenizing, cooling to 50-60 ℃, adding a pH regulator, then continuously cooling to 40-50 ℃, adding folic acid and/or folic acid derivatives, sturgeon roe sauce extract, pearl extract, raw materials which need to be added under a low temperature condition in a skin conditioner, and an aromatic agent, mixing and stirring to obtain the mask.
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| CH713170B1 (en) | 2017-05-22 | 2018-05-31 | La Prairie Group Ag | Cosmetic or dermatological preparation containing an aqueous and a lipophilic fish extract. |
| CH713169B1 (en) * | 2017-05-22 | 2018-05-31 | La Prairie Group Ag | Cosmetic or dermatological preparation containing a fish extract. |
| CN108309909A (en) * | 2018-03-30 | 2018-07-24 | 广州科盈化妆品有限公司 | A kind of moisturizing essence and preparation method thereof containing deep-sea sturgeon seed |
| CN109172422B (en) * | 2018-10-31 | 2021-06-15 | 成都珂萝瑞诗化妆品有限公司 | Hyaluronic acid mask liquid and preparation method thereof |
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