CN105560156A - Mask and preparation method thereof - Google Patents

Mask and preparation method thereof Download PDF

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Publication number
CN105560156A
CN105560156A CN201410530870.XA CN201410530870A CN105560156A CN 105560156 A CN105560156 A CN 105560156A CN 201410530870 A CN201410530870 A CN 201410530870A CN 105560156 A CN105560156 A CN 105560156A
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CN
China
Prior art keywords
agent
add
facial film
skin conditioning
cooled
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201410530870.XA
Other languages
Chinese (zh)
Inventor
冯博洋
谷陟欣
刘浩
陈诗圣
袁莉
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jiuzhitang Co Ltd
Original Assignee
Jiuzhitang Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jiuzhitang Co Ltd filed Critical Jiuzhitang Co Ltd
Priority to CN201410530870.XA priority Critical patent/CN105560156A/en
Publication of CN105560156A publication Critical patent/CN105560156A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a mask and a preparation method thereof. The mask is prepared from water, a humectant, a skin conditioning agent, a thickening agent and a solubilizer as raw materials. The mask has good moisture retention and nourishing effects, is safe, does not produce irritation and can be used for a long time.

Description

A kind of facial film and preparation method thereof
Technical field
The present invention relates to a kind of facial film, be specifically related to a kind of to there is facial film of the effect such as nourishing, moisturizing and preparation method thereof.
Background technology
Facial film is a cosmetics that modern society is subject to consumers very much, but the action effect of portioned product does not very obviously even have some side effect, therefore develops the facial film that a kind of beauty functions is better, side effect is extremely low very important.
Summary of the invention
The object of the present invention is to provide a kind of facial film, be achieved through the following technical solutions:
A kind of facial film, is characterized in that the raw material comprising following parts by weight:
Water 80-90 part
Wetting agent:
Butanediol 4-6 part
Hyaluronate sodium 0.1-0.3 part
Skin conditioning agent:
Collagen 1-3 part
Silk gum albumen 1-3 part
Tremella extract 0.05-0.1 part
Thickening agent:
Hydroxyethyl-cellulose 0.2-0.4 part
Carbomer 0.1-0.3 part
PH adjusting agent:
Triethanolamine 0.2-0.3 part
Solubilizing agent:
Cremophor RH40 0.03-0.05 part
Natrulon H-10 myristinate 0.06-0.1 part.
On the raw material composition basis of this facial film, can adding portion pH conditioner, wetting agent again:
(1) described facial film, can also contain skin conditioning agent (Chondrus crispus extract 0.1-0.3 part) and/or (nicotiamide 1-2 part, betanin 1-2 part);
(2) on (1) gained facial film raw material composition basis, further also containing skin conditioning agent saccharide isomers 0.7-1 part, hydrolyzed pearl 0.1-0.2 part, hydrolysis avenin 0.1-0.2 part;
(3) further again, on the facial film raw material composition basis of (2) gained, also containing skin conditioning agent methyl-monosilane alcohol hydroxyproline ester aspartate 0.8-1.2 part, allantoin 0.2-0.4 part;
(4) further, on the facial film raw material composition basis of (3) gained, also containing wetting agent propylene glycol 0.8-1.4 part and/or glycerol polymethacrylates 0.7-1.2 part.
The preparation method of facial film of the present invention, comprises the steps:
(1) take pure water successively, wetting agent, thickening agent add in stirred tank, rapid stirring, is warming up to 80-85 DEG C gradually, insulation 10-15 minute.
(2) when stirring is cooled to 48 DEG C-55 DEG C, add skin conditioning agent, stir and make it to be uniformly dissolved completely.
(3) stir limit and be cooled to 40-45 DEG C, add pH adjusting agent, solubilizing agent stirs, discharging.
Facial film of the present invention can directly apply on the face, also can fully infiltrate in mask carriers, and used carrier is non-woven fabrics, silk fabric, cotton, wood pulp cloth etc.
Compared with prior art, beneficial effect of the present invention is:
1, compared with blank group, product moisturizing effect of the present invention is obvious, the moisturizing of energy long-acting lock water;
2, product of the present invention extracts silkworm silk, Tremella, donkey-hide gelatin essence, is rich in the multiple nourishing composition useful to skin, improves skin dark and gloomy, and desalination microgroove, increases skin elasticity, and skin smooth is moistened;
3, product of the present invention is tested by antiallergic, safe and non-stimulating, can life-time service.
Detailed description of the invention
Embodiment 1
Raw material is composed as follows:
80 parts, water
Wetting agent:
Butanediol 4 parts
Hyaluronate sodium 0.3 part
Skin conditioning agent:
Collagen 1 part
3 parts, silk gum albumen
Tremella extract 0.1 part
Thickening agent:
Hydroxyethyl-cellulose 0.2 part
Carbomer 0.2 part
PH adjusting agent:
Triethanolamine 0.2 part
Solubilizing agent:
Cremophor RH40 0.03 part
Natrulon H-10 myristinate 0.08 part.
Preparation method:
(1) take pure water successively, wetting agent, thickening agent add in stirred tank, rapid stirring, is warming up to 80-85 DEG C gradually, is incubated 10 minutes.
(2) when stirring is cooled to 48 DEG C-50 DEG C, add skin conditioning agent, stir and make it to be uniformly dissolved completely.
(3) stir limit and be cooled to 40-42 DEG C, add pH adjusting agent, solubilizing agent stirs, discharging.
Embodiment 2
Raw material is composed as follows:
90 parts, water
Wetting agent:
Butanediol 6 parts
Hyaluronate sodium 0.1 part
Skin conditioning agent:
Collagen 3 parts
1 part, silk gum albumen
Tremella extract 0.05 part
Thickening agent:
Hydroxyethyl-cellulose 0.4 part
Carbomer 0.1 part
PH adjusting agent:
Triethanolamine 0.3 part
Solubilizing agent:
Cremophor RH40 0.03 part
Natrulon H-10 myristinate 0.1 part.
Preparation method:
(1) take pure water successively, wetting agent, thickening agent add in stirred tank, rapid stirring, is warming up to 80-85 DEG C gradually, is incubated 15 minutes.
(2) when stirring is cooled to 52 DEG C-55 DEG C, add skin conditioning agent, stir and make it to be uniformly dissolved completely.
(3) stir limit and be cooled to 42-45 DEG C, add pH adjusting agent, solubilizing agent stirs, discharging.
Embodiment 3
Raw material is composed as follows:
88 parts, water
Wetting agent:
Butanediol 6 parts
Hyaluronate sodium 0.2 part
Chondrus crispus extract 0.1 part
Skin conditioning agent:
Collagen 2.5 parts
2.5 parts, silk gum albumen
Tremella extract 0.05 part
Thickening agent:
Hydroxyethyl-cellulose 0.25 part
Carbomer 0.15 part
PH adjusting agent:
Triethanolamine 0.25 part
Solubilizing agent:
Cremophor RH40 0.04 part
Natrulon H-10 myristinate 0.09 part
Preparation method:
(1) take pure water successively, wetting agent, thickening agent add in stirred tank, rapid stirring, is warming up to 82-85 DEG C gradually, is incubated 12 minutes.
(2) when stirring is cooled to 52 DEG C-54 DEG C, add skin conditioning agent, stir and make it to be uniformly dissolved completely.
(3) stir limit and be cooled to 42-44 DEG C, add pH adjusting agent, solubilizing agent stirs, discharging.
Embodiment 5
Raw material is composed as follows:
85 parts, water
Wetting agent:
Butanediol 5.5 parts
Hyaluronate sodium 0.3 part
Chondrus crispus extract 0.15 part
Skin conditioning agent:
Thickening agent:
Hydroxyethyl-cellulose 0.25 part
Carbomer 0.25 part
PH adjusting agent:
Triethanolamine 0.25 part
Solubilizing agent:
Cremophor RH40 0.05 part
Natrulon H-10 myristinate 0.09 part
Preparation method:
(1) take pure water successively, wetting agent, thickening agent add in stirred tank, rapid stirring, is warming up to 82-85 DEG C gradually, is incubated 14 minutes.
(2) when stirring is cooled to 52 DEG C-54 DEG C, add skin conditioning agent, stir and make it to be uniformly dissolved completely.
(3) stir limit and be cooled to 42-45 DEG C, add pH adjusting agent, solubilizing agent stirs, discharging.
Embodiment 5
Raw material is composed as follows:
86 parts, water
Wetting agent:
Butanediol 5.5 parts
Hyaluronate sodium 0.25 part
Chondrus crispus extract 0.15 part
Skin conditioning agent:
Thickening agent:
Hydroxyethyl-cellulose 0.25 part
Carbomer 0.25 part
PH adjusting agent:
Triethanolamine 0.25 part
Solubilizing agent:
Cremophor RH40 0.05 part
Natrulon H-10 myristinate 0.09 part
Preparation method:
(1) take pure water successively, wetting agent, thickening agent add in stirred tank, rapid stirring, is warming up to 82-85 DEG C gradually, is incubated 12 minutes.
(2) when stirring is cooled to 52 DEG C-54 DEG C, add skin conditioning agent, stir and make it to be uniformly dissolved completely.
(3) stir limit and be cooled to 42-44 DEG C, add pH adjusting agent, solubilizing agent stirs, discharging.
Embodiment 6
Raw material is composed as follows:
86 parts, water
Wetting agent:
Butanediol 5.5 parts
Hyaluronate sodium 0.25 part
Chondrus crispus extract 0.15 part
Skin conditioning agent:
Methyl-monosilane alcohol hydroxyproline ester aspartate 1 part
Allantoin 0.2 part
Thickening agent:
Hydroxyethyl-cellulose 0.25 part
Carbomer 0.25 part
PH adjusting agent:
Triethanolamine 0.25 part
Solubilizing agent:
Cremophor RH40 0.05 part
Natrulon H-10 myristinate 0.09 part
Preparation method:
(1) take pure water successively, wetting agent, thickening agent add in stirred tank, rapid stirring, is warming up to 80-84 DEG C gradually, is incubated 12 minutes.
(2) when stirring is cooled to 50 DEG C-54 DEG C, add skin conditioning agent, stir and make it to be uniformly dissolved completely.
(3) stir limit and be cooled to 40-42 DEG C, add pH adjusting agent, solubilizing agent stirs, discharging.
Embodiment 7
Raw material is composed as follows:
85 parts, water
Wetting agent:
Butanediol 4.5 parts
Hyaluronate sodium 0.25 part
Chondrus crispus extract 0.25 part
Propylene glycol 0.8 part
Skin conditioning agent:
Methyl-monosilane alcohol hydroxyproline ester aspartate 1.1 parts
Allantoin 0.3 part
Thickening agent:
Hydroxyethyl-cellulose 0.2 part
Carbomer 0.3 part
PH adjusting agent:
Triethanolamine 0.25 part
Solubilizing agent:
Cremophor RH40 0.04 part
Natrulon H-10 myristinate 0.08 part
Preparation method:
(1) take pure water successively, wetting agent, thickening agent add in stirred tank, rapid stirring, is warming up to 80-84 DEG C gradually, is incubated 15 minutes.
(2) when stirring is cooled to 50 DEG C-54 DEG C, add skin conditioning agent, stir and make it to be uniformly dissolved completely.
(3) stir limit and be cooled to 40-42 DEG C, add pH adjusting agent, solubilizing agent stirs, discharging.
The facial film moisturizing and nourishing efficacy test of embodiment 1-7 and safety testing
If 7 experimental grouies, often organize 20 people, be women, age distribution is 25-45 year.
Experiment facial film: the facial film prepared by embodiment 1-7 fully infiltrates on mask carriers cotton, the blank facial film (namely only having the facial film that purified water infiltrates) of another standby equivalent amount.
The left face of each experimental group experimenter applies and applies facial film of the present invention (namely No. 1 experimental group applies facial film prepared by embodiment 1, and No. 2 experimental grouies apply the facial film of embodiment 2 preparation, the like) respectively, and right face applies blank facial film, and application is torn after 20 minutes facial film.
Experimenter before by face mask film, use after facial film after 1 hour, 4 hours, 6 hours, test its moisture content of skin, moisture content of skin test is used cM825 measures, and often group gets its meansigma methods.
Experimenter applied a facial film every 3 days, the same experimental design, left face applies facial film of the present invention, right face applies blank facial film, after face mask film 5 times, the skin gloss of observation experiment person left and right sides face, elasticity, smoothness, carry out the scoring of skin integrated status (according to degree from low to high, successively from 1-10 marking), often group gets its meansigma methods.In this experimentation, observe each experimenter's skin allergy situation simultaneously.
Experimental result refers to following form:
Table 1 moisture-keeping efficacy contrast test
The contrast of table 2 skin integrated status and safety testing result

Claims (9)

1. a facial film, is characterized in that the raw material comprising following parts by weight:
Water 80-90 part
Wetting agent:
Butanediol 4-6 part
Hyaluronate sodium 0.1-0.3 part
Skin conditioning agent:
Collagen 1-3 part
Silk gum albumen 1-3 part
Tremella extract 0.05-0.1 part
Thickening agent:
Hydroxyethyl-cellulose 0.2-0.4 part
Carbomer 0.1-0.3 part
PH adjusting agent:
Triethanolamine 0.2-0.3 part
Solubilizing agent:
Cremophor RH40 0.03-0.05 part
Natrulon H-10 myristinate 0.06-0.1 part.
2. facial film as claimed in claim 1, is characterized in that also containing wetting agent Chondrus crispus extract 0.1-0.3 part.
3. facial film as claimed in claim 1 or 2, is characterized in that also containing skin conditioning agent nicotiamide 1-2 part, betanin 1-2 part.
4. facial film as claimed in claim 3, is characterized in that also containing skin conditioning agent saccharide isomers 0.7-1 part, hydrolyzed pearl 0.1-0.2 part, hydrolysis avenin 0.1-0.2 part.
5. facial film as claimed in claim 4, is characterized in that also containing skin conditioning agent methyl-monosilane alcohol hydroxyproline ester aspartate 0.8-1.2 part, allantoin 0.2-0.4 part.
6. facial film as claimed in claim 5, is characterized in that also containing wetting agent propylene glycol 0.8-1.4 part and/or glycerol polymethacrylates 0.7-1.2 part.
7., as the preparation method of facial film according to claim 1 or claim 2, it is characterized in that comprising the steps:
(1) take pure water successively, wetting agent, thickening agent add in stirred tank, rapid stirring, is warming up to 80-85 DEG C gradually, insulation 10-15 minute.
(2) when stirring is cooled to 48 DEG C-55 DEG C, add skin conditioning agent, stir and make it to be uniformly dissolved completely.
(3) stir limit and be cooled to 40-45 DEG C, add pH adjusting agent, solubilizing agent stirs, discharging.
8. the preparation method of facial film as claimed in claim 3, is characterized in that comprising the steps:
(1) take pure water successively, wetting agent, thickening agent add in stirred tank, rapid stirring, is warming up to 80-85 DEG C gradually, insulation 10-15 minute.
(2) when stirring is cooled to 48 DEG C-55 DEG C, add skin conditioning agent, stir and make it to be uniformly dissolved completely.
(3) stir limit and be cooled to 40-45 DEG C, add pH adjusting agent, solubilizing agent stirs, discharging.
9. the preparation method of the facial film as described in claim as arbitrary in claim 4-6, is characterized in that comprising the steps:
(1) take pure water successively, wetting agent, thickening agent add in stirred tank, rapid stirring, is warming up to 80-85 DEG C gradually, insulation 10-15 minute.
(2) when stirring is cooled to 48 DEG C-55 DEG C, add skin conditioning agent, stir and make it to be uniformly dissolved completely.
(3) stir limit and be cooled to 40-45 DEG C, add pH adjusting agent, solubilizing agent stirs, discharging.
CN201410530870.XA 2014-10-10 2014-10-10 Mask and preparation method thereof Pending CN105560156A (en)

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Application Number Priority Date Filing Date Title
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Application Number Priority Date Filing Date Title
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Cited By (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105833332A (en) * 2016-06-01 2016-08-10 北京汉氏联合生物技术股份有限公司 Composite external use dressing rich in collagen and hyaluronic acid
CN106074315A (en) * 2016-08-24 2016-11-09 广东芭薇生物科技股份有限公司 A kind of facial mask liquid with multiple skin-care effect and preparation method thereof
CN106551868A (en) * 2016-11-28 2017-04-05 益科路博(天津)科技有限公司 A kind of resveratrol multi-effect compound facial film and preparation method thereof
CN106551890A (en) * 2016-11-26 2017-04-05 无锡市汉方八珍科技有限公司 A kind of facial film
CN106691962A (en) * 2016-12-14 2017-05-24 珍尔姿(广州)化妆品有限公司 Functional mask with effects of whitening skin and removing freckles
CN106726880A (en) * 2016-11-26 2017-05-31 无锡市汉方八珍科技有限公司 A kind of facial mask base fluid for repairing facial wound
CN106726699A (en) * 2016-12-23 2017-05-31 惠州市七分妆化妆品有限公司 A kind of facial mask liquid
CN106798693A (en) * 2017-02-14 2017-06-06 石家庄市中医院 A kind of Chinese medicine Face-protecting mask
CN107050055A (en) * 2017-04-20 2017-08-18 陈溢民 A kind of donkey-hide gelatin microcapsules dermalaxia film and preparation method
CN107184466A (en) * 2017-05-26 2017-09-22 佛山市迭蓓生物科技有限公司 A kind of no added facial mask and preparation method thereof
CN107260607A (en) * 2017-06-29 2017-10-20 龚国华 The plant mask and its processing technology of a kind of natural health
CN107375180A (en) * 2017-08-11 2017-11-24 北京斯利安药业有限公司 A kind of composite skin care product, facial mask and preparation method thereof
CN107898679A (en) * 2017-10-10 2018-04-13 广州柏俐臣化妆品有限公司 A kind of water light moisturizing stoste and preparation method thereof
CN108553364A (en) * 2018-06-01 2018-09-21 广州澳希亚实业有限公司 A kind of skin replenishing water and preserving moisture composition with smooth skin and its application in skin care item
CN108853000A (en) * 2018-08-17 2018-11-23 广州皓雨投资有限公司 Have effects that moisture-keeping crease-shedding restores the composition of elasticity of skin, facial mask and preparation method thereof
CN108888539A (en) * 2018-08-17 2018-11-27 广东丸美生物技术股份有限公司 Organic skin care matrix and its preparation method and application and organic cosmetics
CN109044906A (en) * 2018-08-28 2018-12-21 广州皓雨投资有限公司 A kind of moisturizing is releived anti-wrinkle composition, facial mask and preparation method thereof
CN109044945A (en) * 2018-07-19 2018-12-21 北京润熙怡和科技有限公司 It is a kind of to have effects that moisten and repair the composite skin care product of dry impaired skin
CN110327263A (en) * 2019-08-09 2019-10-15 汉西(厦门)科技有限公司 It is a kind of for improving the graphene facial mask and preparation method of dry skin problem of rough
CN110368349A (en) * 2019-09-02 2019-10-25 苏州榭睿迦医疗科技发展有限公司 A kind of nourishing and moisturizing reparation facial mask and preparation method thereof for after fitness training
CN110368334A (en) * 2019-05-27 2019-10-25 河南大学淮河医院 Chinese-medicinal skin-protecting product with crease-resistant skin lightening effect
CN113018201A (en) * 2021-04-13 2021-06-25 东晟源研究院(广州)有限公司 Skin-beautifying nourishing ice film
CN113332222A (en) * 2021-07-23 2021-09-03 衢州市衢江区廿里镇养和残疾人之家 Whitening anti-inflammatory moisturizing mask and preparation method thereof

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CN103989615A (en) * 2014-05-28 2014-08-20 广州市洁宝日用品有限公司 Skin repair mask composition used before and after make-up and preparation method thereof

Patent Citations (1)

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Publication number Priority date Publication date Assignee Title
CN103989615A (en) * 2014-05-28 2014-08-20 广州市洁宝日用品有限公司 Skin repair mask composition used before and after make-up and preparation method thereof

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CN105833332A (en) * 2016-06-01 2016-08-10 北京汉氏联合生物技术股份有限公司 Composite external use dressing rich in collagen and hyaluronic acid
CN106074315A (en) * 2016-08-24 2016-11-09 广东芭薇生物科技股份有限公司 A kind of facial mask liquid with multiple skin-care effect and preparation method thereof
CN106551890A (en) * 2016-11-26 2017-04-05 无锡市汉方八珍科技有限公司 A kind of facial film
CN106726880A (en) * 2016-11-26 2017-05-31 无锡市汉方八珍科技有限公司 A kind of facial mask base fluid for repairing facial wound
CN106551868A (en) * 2016-11-28 2017-04-05 益科路博(天津)科技有限公司 A kind of resveratrol multi-effect compound facial film and preparation method thereof
CN106691962A (en) * 2016-12-14 2017-05-24 珍尔姿(广州)化妆品有限公司 Functional mask with effects of whitening skin and removing freckles
CN106726699A (en) * 2016-12-23 2017-05-31 惠州市七分妆化妆品有限公司 A kind of facial mask liquid
CN106798693A (en) * 2017-02-14 2017-06-06 石家庄市中医院 A kind of Chinese medicine Face-protecting mask
CN107050055A (en) * 2017-04-20 2017-08-18 陈溢民 A kind of donkey-hide gelatin microcapsules dermalaxia film and preparation method
CN107184466A (en) * 2017-05-26 2017-09-22 佛山市迭蓓生物科技有限公司 A kind of no added facial mask and preparation method thereof
CN107260607A (en) * 2017-06-29 2017-10-20 龚国华 The plant mask and its processing technology of a kind of natural health
CN107375180A (en) * 2017-08-11 2017-11-24 北京斯利安药业有限公司 A kind of composite skin care product, facial mask and preparation method thereof
CN107375180B (en) * 2017-08-11 2020-10-16 北京斯利安药业有限公司 Skin care product composition, facial mask and preparation method of facial mask
CN107898679A (en) * 2017-10-10 2018-04-13 广州柏俐臣化妆品有限公司 A kind of water light moisturizing stoste and preparation method thereof
CN108553364A (en) * 2018-06-01 2018-09-21 广州澳希亚实业有限公司 A kind of skin replenishing water and preserving moisture composition with smooth skin and its application in skin care item
CN109044945A (en) * 2018-07-19 2018-12-21 北京润熙怡和科技有限公司 It is a kind of to have effects that moisten and repair the composite skin care product of dry impaired skin
CN108853000A (en) * 2018-08-17 2018-11-23 广州皓雨投资有限公司 Have effects that moisture-keeping crease-shedding restores the composition of elasticity of skin, facial mask and preparation method thereof
CN108888539A (en) * 2018-08-17 2018-11-27 广东丸美生物技术股份有限公司 Organic skin care matrix and its preparation method and application and organic cosmetics
CN109044906A (en) * 2018-08-28 2018-12-21 广州皓雨投资有限公司 A kind of moisturizing is releived anti-wrinkle composition, facial mask and preparation method thereof
CN110368334A (en) * 2019-05-27 2019-10-25 河南大学淮河医院 Chinese-medicinal skin-protecting product with crease-resistant skin lightening effect
CN110368334B (en) * 2019-05-27 2022-08-16 河南大学淮河医院 Chinese herbal medicine skin care product with anti-wrinkle and skin brightening effects
CN110327263A (en) * 2019-08-09 2019-10-15 汉西(厦门)科技有限公司 It is a kind of for improving the graphene facial mask and preparation method of dry skin problem of rough
CN110368349A (en) * 2019-09-02 2019-10-25 苏州榭睿迦医疗科技发展有限公司 A kind of nourishing and moisturizing reparation facial mask and preparation method thereof for after fitness training
CN110368349B (en) * 2019-09-02 2020-02-18 苏州榭睿迦医疗科技发展有限公司 Nutrition, moisture retention and repair mask used after body building training and preparation method thereof
CN113018201A (en) * 2021-04-13 2021-06-25 东晟源研究院(广州)有限公司 Skin-beautifying nourishing ice film
CN113332222A (en) * 2021-07-23 2021-09-03 衢州市衢江区廿里镇养和残疾人之家 Whitening anti-inflammatory moisturizing mask and preparation method thereof

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