CN109431941A - One kind, which is releived, repairs multiple-effect facial mask and preparation method thereof - Google Patents
One kind, which is releived, repairs multiple-effect facial mask and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/645—Proteins of vegetable origin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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- A61Q19/08—Anti-ageing preparations
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
It releives the invention discloses one kind and repairs multiple-effect facial mask and preparation method thereof.This, which is releived, repairs multiple-effect facial mask, by weight percentage, including the following raw material: propylene glycol 2~10%, glycerol 5~20%, wheat bran extract 0.1~10%, thickener 0.1~1%, oat polypeptide 0.5~5%, glycerol polymethacrylates 0.2~2%, arginine ferulate 0.2~3%, polyglutamic acid sodium 0.2~3%, strawflower flower extract 0.01~1%, Sodium Hyaluronate 0.01~0.1%, disodium ethylene diamine tetraacetate 0.05~0.5%, dipotassium glycyrrhizinate 0.01~0.1%, Cremophor RH40 0.05~0.5%, peppermint leaf oil 0~0.1%, water surplus.Maintenance multiple-effect facial mask provided by the invention of releiving is safe and non-stimulating, and skin sensitivity person is suitble to use；Other effect components in two kinds of plant extract components and formula act synergistically, and have facial mask and repair skin, anti-wrinkle, moisturizing, moist effect well.
Description
Technical field
The present invention relates to cosmetic technical fields, in particular to one kind, which is releived, repairs multiple-effect facial mask and preparation method thereof.
Background technique
Facial mask is a kind of cosmetics and skincare product for spreading on face, and facial mask is temporarily isolating using the of short duration time for being covered on face
Extraneous air and pollution, improves skin temperature, and the pore expansion of skin promotes sweat gland secretion and metabolism, makes skin
Oxygen content rises, and is conducive to skin and excludes the product of epidermal cell metabolism and the oil substances of accumulation, the water in facial mask
Divide the cuticula for penetrating into epidermis, skin becomes soft, and skin is naturally bright flexible.Present facial mask has become numerous women that like to be beautiful
One of essential skin care item, therefore facial mask in the market is also more and more, and type emerges one after another, price also costly, however city
Most of facial mask all contains various harmful additives, such as hormone, heavy metal, fluorescer etc. on face, can make some after
Skin is stimulated, and generates uncomfortable reaction.In addition facial mask in the market is substantially that performance is more single before, only the function in terms of certain
Effect, cannot solve the problems, such as that skin occurs various, is not able to satisfy the demand of current consumer simultaneously.
Summary of the invention
The purpose of the present invention, which is intended to provide one kind, releives and repairs multiple-effect facial mask and preparation method thereof, is asked with solving above-mentioned technology
Topic.
To achieve the goals above, the technical solution of the present invention is as follows:
In a first aspect, one kind provided by the invention, which is releived, repairs multiple-effect facial mask, by weight percentage, including it is following former
Material: propylene glycol 2~10%, glycerol 5~20%, wheat bran extract 0.1~10%, thickener 0.1~1%, oat polypeptide 0.5
~5%, glycerol polymethacrylates 0.2~2%, arginine ferulate 0.2~3%, polyglutamic acid sodium 0.2~3%, wax
Chrysanthemum extract 0.01~1%, Sodium Hyaluronate 0.01~0.1%, disodium ethylene diamine tetraacetate 0.05~0.5%, glycyrrhizic acid
Dipotassium 0.01~0.1%, Cremophor RH40 0.05~0.5%, peppermint leaf oil 0~0.1%, water surplus.
Preferably, described releive repairs multiple-effect facial mask, by weight percentage, including the following raw material: propylene glycol 2~8%,
Glycerol 7~15%, wheat bran extract 0.5~2%, thickener 0.1~0.5%, oat polypeptide 1~2%, the poly- methyl-prop of glycerol
Olefin(e) acid ester 0.2~1%, arginine ferulate 0.2~1%, polyglutamic acid sodium 0.2~1%, strawflower flower extract 0.05~
0.2%, Sodium Hyaluronate 0.02~0.08%, disodium ethylene diamine tetraacetate 0.05~0.2%, dipotassium glycyrrhizinate 0.02~
0.08%, Cremophor RH40 0.05~0.2%, peppermint leaf oil 0.001~0.005%, water surplus.
It is further preferred that described releive repairs multiple-effect facial mask, by weight percentage, including the following raw material: propylene glycol
5.5%, glycerol 10%, wheat bran extract 1%, thickener 0.24%, oat polypeptide 1.5%, glycerol polymethacrylates
0.5%, arginine ferulate 0.5%, polyglutamic acid sodium 0.5%, strawflower flower extract 0.1%, Sodium Hyaluronate 0.05%,
Disodium ethylene diamine tetraacetate 0.1%, dipotassium glycyrrhizinate 0.05%, Cremophor RH40 0.1%, peppermint leaf oil 0.003%,
Water surplus.
It is further preferred that described releive repairs multiple-effect facial mask, by weight percentage, including the following raw material: propylene glycol
8%, glycerol 7%, wheat bran extract 0.5%, thickener 0.1%, oat polypeptide 2%, glycerol polymethacrylates 1%,
Arginine ferulate 0.2%, polyglutamic acid sodium 0.2%, strawflower flower extract 0.2%, Sodium Hyaluronate 0.02%, ethylenediamine
Tetraacethyl disodium 0.05%, dipotassium glycyrrhizinate 0.08%, Cremophor RH40 0.2%, peppermint leaf oil 0.005%, more than water
Amount.
It is further preferred that described releive repairs multiple-effect facial mask, by weight percentage, including the following raw material: propylene glycol
2%, glycerol 15%, wheat bran extract 2%, thickener 0.5%, oat polypeptide 1%, glycerol polymethacrylates 0.2%,
Arginine ferulate 1%, polyglutamic acid sodium 1%, strawflower flower extract 0.05%, Sodium Hyaluronate 0.08%, ethylenediamine tetraacetic
Acetic acid disodium 0.2%, dipotassium glycyrrhizinate 0.02%, Cremophor RH40 0.05%, peppermint leaf oil 0.001%, water surplus.
Preferably, the thickener is selected from least one of hydroxyethyl cellulose and xanthan gum.
Preferably, the wheat bran extract be using Microwave Extraction side, ultrasonic extraction, continuous phase transistion extracting method,
It is any obtained in soxhlet extraction methods.
Preferably, the strawflower flower extract be using Microwave Extraction side, ultrasonic extraction, continuous phase transistion extracting method,
It is any obtained in soxhlet extraction methods.
Second aspect, a kind of releiving and repair the preparation method of multiple-effect facial mask as described in relation to the first aspect provided by the invention,
Include the following steps:
(1) propylene glycol, glycerol, glycerol polymethacrylates, Sodium Hyaluronate, Cremophor RH40 and water are added
Enter in blender, revolving speed 30~60min of stirring under conditions of 80~85 DEG C with 2000~4000rpm is equal to each component mixing
It is even；
(2) after being cooled to not higher than 45 DEG C, by wheat bran extract, thickener, oat polypeptide, arginine ferulate,
Polyglutamic acid sodium, strawflower flower extract, Sodium Hyaluronate, disodium ethylene diamine tetraacetate, dipotassium glycyrrhizinate are added in blender, with
It is uniformly mixed to each component that the revolving speed of 2000~4000rpm stirs 30~60min；
(3) peppermint leaf oil is added in blender, stirs evenly, obtains releiving and repair multiple-effect facial mask.
Compared with prior art, the beneficial effects of the present invention are:
Maintenance multiple-effect facial mask provided by the invention of releiving is safe and non-stimulating, and skin sensitivity person is suitble to use；Wheat in formula
Bran extract controls inflammation the release of substance, reduces the generation of various inflammation interleukins；Strawflower flower extract is rich in triterpenes chemical combination
Object can enhance the resistance of capillary, inhibit capillary permeability and have anti-inflammatory effect；Free radical can be eliminated simultaneously,
There is inoxidizability, has and alleviate aging effect；Also there is certain inhibiting effect to melanocyte, so there is certain whitening spot-removing
The effect of；Other components (such as Sodium Hyaluronate, oat polypeptide) in formula have effects that significant moisturizing and moist, can
Soften skin, lock moisture of skin, assigns skin and moisten, accelerate cell Proliferation and metabolism；Two kinds of plant extract components with
Other effect components synergistic effect in formula, has facial mask and repairs skin, anti-wrinkle, moisturizing, moist effect well.
Specific embodiment
Specific embodiments of the present invention will be further explained below.It should be noted that for these implementations
The explanation of mode is used to help understand the present invention, but and does not constitute a limitation of the invention.In addition, invention described below
Technical characteristic involved in each embodiment can be combined with each other as long as they do not conflict with each other.
In a first aspect, one kind provided by the invention, which is releived, repairs multiple-effect facial mask, by weight percentage, including it is following former
Material: propylene glycol 2~10%, glycerol 5~20%, wheat bran extract 0.1~10%, thickener 0.1~1%, oat polypeptide 0.5
~5%, glycerol polymethacrylates 0.2~2%, arginine ferulate 0.2~3%, polyglutamic acid sodium 0.2~3%, wax
Chrysanthemum extract 0.01~1%, Sodium Hyaluronate 0.01~0.1%, disodium ethylene diamine tetraacetate 0.05~0.5%, glycyrrhizic acid
Dipotassium 0.01~0.1%, Cremophor RH40 0.05~0.5%, peppermint leaf oil 0~0.1%, water surplus.
In embodiments of the present invention, described releive repairs multiple-effect facial mask, by weight percentage, including the following raw material:
Propylene glycol 2~8%, glycerol 7~15%, wheat bran extract 0.5~2%, thickener 0.1~0.5%, oat polypeptide 1~
2%, glycerol polymethacrylates 0.2~1%, arginine ferulate 0.2~1%, polyglutamic acid sodium 0.2~1%, strawflower
Flower extract 0.05~0.2%, Sodium Hyaluronate 0.02~0.08%, disodium ethylene diamine tetraacetate 0.05~0.2%, glycyrrhizic acid
Dipotassium 0.02~0.08%, Cremophor RH40 0.05~0.2%, peppermint leaf oil 0.001~0.005%, water surplus.
Further, described releive repairs multiple-effect facial mask, by weight percentage, including the following raw material: propylene glycol
5.5%, glycerol 10%, wheat bran extract 1%, thickener 0.24%, oat polypeptide 1.5%, glycerol polymethacrylates
0.5%, arginine ferulate 0.5%, polyglutamic acid sodium 0.5%, strawflower flower extract 0.1%, Sodium Hyaluronate 0.05%,
Disodium ethylene diamine tetraacetate 0.1%, dipotassium glycyrrhizinate 0.05%, Cremophor RH40 0.1%, peppermint leaf oil 0.003%,
Water surplus.
Further, described releive repairs multiple-effect facial mask, by weight percentage, including the following raw material: propylene glycol 8%,
Glycerol 7%, wheat bran extract 0.5%, thickener 0.1%, oat polypeptide 2%, glycerol polymethacrylates 1%, smart ammonia
Sour ferulate 0.2%, polyglutamic acid sodium 0.2%, strawflower flower extract 0.2%, Sodium Hyaluronate 0.02%, ethylenediamine tetrem
Acid disodium 0.05%, dipotassium glycyrrhizinate 0.08%, Cremophor RH40 0.2%, peppermint leaf oil 0.005%, water surplus.
Further, described releive repairs multiple-effect facial mask, by weight percentage, including the following raw material: propylene glycol 2%,
Glycerol 15%, wheat bran extract 2%, thickener 0.5%, oat polypeptide 1%, glycerol polymethacrylates 0.2%, smart ammonia
Sour ferulate 1%, polyglutamic acid sodium 1%, strawflower flower extract 0.05%, Sodium Hyaluronate 0.08%, ethylenediamine tetra-acetic acid
Disodium 0.2%, dipotassium glycyrrhizinate 0.02%, Cremophor RH40 0.05%, peppermint leaf oil 0.001%, water surplus.
In embodiments of the present invention, the thickener is selected from least one of hydroxyethyl cellulose and xanthan gum.
In embodiments of the present invention, the wheat bran extract is using Microwave Extraction side, ultrasonic extraction, continuous phase
It is any obtained in change extracting method, soxhlet extraction methods.
In embodiments of the present invention, the wheat bran extract is to be made using following methods:
It after wheat bran raw material drying, is fitted into the continuous phase transistion extraction kettle for filling extractant, in consistently lower than extractant
Critical pressure and critical-temperature under conditions of, by extractant boil down to liquid, in 60~75 DEG C of extraction temperature, extracting pressure
Under conditions of 0.3~2Mpa, extraction kettle is flowed through with the flow velocity of 80~100L/h, 50~120min of continuous extraction extracts tea polyphenols
Afterwards, it flows through in extraction-container, 70~90 DEG C of resolution temperature, parses 0.08~0.5Mpa of pressure, extractant passes through heating, decompression phase transformation
For gas, then by compressing immediately, becomes liquid and pass through extraction kettle, material is extracted again, so circulation repeatedly, obtains small
Wheat bran extracting solution, then vacuum freeze drying obtains wheat bran extract；Wherein, the extractant is the aqueous solution of ethyl alcohol, institute
The mass concentration for stating ethyl alcohol described in the aqueous solution of ethyl alcohol is 70~80%.
In embodiments of the present invention, the strawflower flower extract is using Microwave Extraction side, ultrasonic extraction, continuous phase
It is any obtained in change extracting method, soxhlet extraction methods.
In embodiments of the present invention, the strawflower flower extract is to be made using following methods:
It after the Flowers of Helichrysum bracteatum raw material drying, crushing, is fitted into the continuous phase transistion extraction kettle for filling extractant, extracts being consistently lower than
Under conditions of taking the critical pressure and critical-temperature of agent, by extractant boil down to liquid, in 70~80 DEG C of extraction temperature, extraction pressure
Under conditions of 0.3~2Mpa of power, extraction kettle is flowed through with the flow velocity of 80~120L/h, it is more to extract tea by 50~120min of continuous extraction
It after phenol, flows through in extraction-container, 80~90 DEG C of resolution temperature, parses 0.08~0.5Mpa of pressure, extractant passes through heating, decompression phase
Become gas, then by compressing immediately, becomes liquid and pass through extraction kettle, material is extracted again, so circulation repeatedly, obtains
The Flowers of Helichrysum bracteatum extracting solution, then vacuum freeze drying obtains strawflower flower extract；Wherein, the extractant is water.
Second aspect, a kind of releiving and repair the preparation method of multiple-effect facial mask as described in relation to the first aspect provided by the invention,
Include the following steps:
(1) propylene glycol, glycerol, glycerol polymethacrylates, Sodium Hyaluronate, Cremophor RH40 and water are added
Enter in blender, revolving speed 30~60min of stirring under conditions of 80~85 DEG C with 2000~4000rpm is equal to each component mixing
It is even；
(2) after being cooled to not higher than 45 DEG C, by wheat bran extract, thickener, oat polypeptide, arginine ferulate,
Polyglutamic acid sodium, strawflower flower extract, Sodium Hyaluronate, disodium ethylene diamine tetraacetate, dipotassium glycyrrhizinate are added in blender, with
It is uniformly mixed to each component that the revolving speed of 2000~4000rpm stirs 30~60min；
(3) peppermint leaf oil is added in blender, stirs evenly, obtains releiving and repair multiple-effect facial mask.
Embodiment is described further below.
Wheat bran extract in following embodiment and comparative example is to be made using following methods:
It after wheat bran raw material drying, is fitted into the continuous phase transistion extraction kettle for filling extractant, in consistently lower than extractant
Critical pressure and critical-temperature under conditions of, by extractant boil down to liquid, in 70 DEG C of extraction temperature, extracting pressure 1.5Mpa
Under conditions of, extraction kettle is flowed through with the flow velocity of 90L/h, continuous extraction 60min is flowed through in extraction-container after extracting tea polyphenols, is parsed
80 DEG C of temperature, pressure 0.32Mpa is parsed, extractant mutually becomes gas by heating, decompression, then by compressing immediately, becomes liquid
Body passes through extraction kettle, extracts again to material, and so circulation repeatedly, obtains wheat bran extracting solution, then vacuum freeze drying
Obtain wheat bran extract；Wherein, the extractant is the aqueous solution of ethyl alcohol, the matter of ethyl alcohol described in the aqueous solution of the ethyl alcohol
Measuring concentration is 75%.
Strawflower flower extract in following embodiment and comparative example is to be made using following methods:
It after the Flowers of Helichrysum bracteatum raw material drying, crushing, is fitted into the continuous phase transistion extraction kettle for filling extractant, extracts being consistently lower than
Under conditions of taking the critical pressure and critical-temperature of agent, by extractant boil down to liquid, in 75 DEG C of extraction temperature, extracting pressure
Under conditions of 1.2Mpa, extraction kettle is flowed through with the flow velocity of 100L/h, continuous extraction 80min flows through extraction-container after extracting tea polyphenols
In, 85 DEG C of resolution temperature, pressure 0.25Mpa is parsed, extractant mutually becomes gas by heating, decompression, then by compressing immediately,
Become liquid and pass through extraction kettle, material is extracted again, so circulation repeatedly, obtains the Flowers of Helichrysum bracteatum extracting solution, then vacuum is cold
Jelly is dried to obtain strawflower flower extract；Wherein, the extractant is water.
Embodiment 1
A kind of releive provided in this embodiment repairs the preparation method of multiple-effect facial mask, includes the following steps:
Raw material is weighed according to the following weight percentages: propylene glycol 5.5%, glycerol 10%, wheat bran extract 1%, ethoxy
Cellulose 0.12%, xanthan gum 0.12%, oat polypeptide 1.5%, glycerol polymethacrylates 0.5%, arginine ferulic acid
Salt 0.5%, polyglutamic acid sodium 0.5%, strawflower flower extract 0.1%, Sodium Hyaluronate 0.05%, disodium ethylene diamine tetraacetate
0.1%, dipotassium glycyrrhizinate 0.05%, Cremophor RH40 0.1%, peppermint leaf oil 0.003%, water surplus.
Propylene glycol, glycerol, glycerol polymethacrylates, Sodium Hyaluronate, Cremophor RH40 and water are added
In blender, it is uniformly mixed under conditions of 82 DEG C with the revolving speed stirring 45min of 2000rpm to each component；It is cooled to and is not higher than
After 45 DEG C, by wheat bran extract, thickener, oat polypeptide, arginine ferulate, polyglutamic acid sodium, strawflower flower extract,
Sodium Hyaluronate, disodium ethylene diamine tetraacetate, dipotassium glycyrrhizinate are added in blender, extremely with the revolving speed stirring 50min of 2500rpm
Each component is uniformly mixed；Peppermint leaf oil is added in blender, is stirred evenly, is obtained releiving and repair multiple-effect facial mask.
Embodiment 2
A kind of releive provided in this embodiment repairs the preparation method of multiple-effect facial mask, includes the following steps:
Weigh raw material according to the following weight percentages: propylene glycol 8%, glycerol 7%, wheat bran extract 0.5%, ethoxy are fine
Tie up plain 0.05%, xanthan gum 0.05%, oat polypeptide 2%, glycerol polymethacrylates 1%, arginine ferulate
0.2%, polyglutamic acid sodium 0.2%, strawflower flower extract 0.2%, Sodium Hyaluronate 0.02%, disodium ethylene diamine tetraacetate
0.05%, dipotassium glycyrrhizinate 0.08%, Cremophor RH40 0.2%, peppermint leaf oil 0.005%, water surplus.According to this
The similar preparation method of inventive embodiments 1, which is made to releive, repairs multiple-effect facial mask.
Embodiment 3
A kind of releive provided in this embodiment repairs the preparation method of multiple-effect facial mask, includes the following steps:
Weigh raw material according to the following weight percentages: propylene glycol 2%, glycerol 15%, wheat bran extract 2%, ethoxy are fine
Tie up plain 0.25%, xanthan gum 0.25%, oat polypeptide 1%, glycerol polymethacrylates 0.2%, arginine ferulate
1%, polyglutamic acid sodium 1%, strawflower flower extract 0.05%, Sodium Hyaluronate 0.08%, disodium ethylene diamine tetraacetate 0.2%,
Dipotassium glycyrrhizinate 0.02%, Cremophor RH40 0.05%, peppermint leaf oil 0.001%, water surplus.According to real with the present invention
It applies obtained releive of the similar preparation method of example 1 and repairs multiple-effect facial mask.
Embodiment 4
It is made to releive according to the preparation method similar with the embodiment of the present invention 1 and repairs multiple-effect facial mask；The present embodiment and implementation
The difference of example 1 is only that the dosage of wheat bran extract is different, and the dosage of wheat bran extract used by the present embodiment is
0.1%.
Embodiment 5
It is made to releive according to the preparation method similar with the embodiment of the present invention 1 and repairs multiple-effect facial mask；The present embodiment and implementation
The difference of example 1 is only that the dosage of wheat bran extract is different, and the dosage of wheat bran extract used by the present embodiment is
5%.
Embodiment 6
It is made to releive according to the preparation method similar with the embodiment of the present invention 1 and repairs multiple-effect facial mask；The present embodiment and implementation
The difference of example 1 is only that the dosage of wheat bran extract is different, and the dosage of wheat bran extract used by the present embodiment is
10%.
Embodiment 7
It is made to releive according to the preparation method similar with the embodiment of the present invention 1 and repairs multiple-effect facial mask；The present embodiment and implementation
The difference of example 1 is only that the dosage of strawflower flower extract is different, and the dosage of strawflower flower extract used by the present embodiment is
0.01%.
Embodiment 8
It is made to releive according to the preparation method similar with the embodiment of the present invention 1 and repairs multiple-effect facial mask；The present embodiment and implementation
The difference of example 1 is only that the dosage of strawflower flower extract is different, and the dosage of strawflower flower extract used by the present embodiment is
0.5%.
Embodiment 9
It is made to releive according to the preparation method similar with the embodiment of the present invention 1 and repairs multiple-effect facial mask；The present embodiment and implementation
The difference of example 1 is only that the dosage of strawflower flower extract is different, and the dosage of strawflower flower extract used by the present embodiment is
1%.
Comparative example 1
Beneficial effect in order to further illustrate the present invention, this comparative example weigh following raw materials by weight percentage:
Propylene glycol 5.5%, glycerol 10%, hydroxyethyl cellulose 0.12%, xanthan gum 0.12%, oat polypeptide 1.5%, the poly- methyl of glycerol
Acrylate 0.5%, arginine ferulate 0.5%, polyglutamic acid sodium 0.5%, strawflower flower extract 1.1%, hyaluronic acid
Sodium 0.05%, disodium ethylene diamine tetraacetate 0.1%, dipotassium glycyrrhizinate 0.05%, Cremophor RH40 0.1%, dried peppermint leaf
Oily 0.003%, water surplus.It is made to releive according to the preparation method similar with the embodiment of the present invention 1 and repairs multiple-effect facial mask.
Comparative example 2
Beneficial effect in order to further illustrate the present invention, this comparative example weigh following raw materials by weight percentage:
Propylene glycol 5.5%, glycerol 10%, wheat bran extract 1.1%, hydroxyethyl cellulose 0.12%, xanthan gum 0.12%, oat are more
Peptide 1.5%, glycerol polymethacrylates 0.5%, arginine ferulate 0.5%, polyglutamic acid sodium 0.5%, hyaluronic acid
Sodium 0.05%, disodium ethylene diamine tetraacetate 0.1%, dipotassium glycyrrhizinate 0.05%, Cremophor RH40 0.1%, dried peppermint leaf
Oily 0.003%, water surplus.
1 skin irritation test of effect example
New zealand rabbit, half male and half female are chosen, weight 2.5Kg is randomly divided into 11 groups, and every group 10, each group is smeared respectively
Product obtained by corresponding embodiment and comparative example.New zealand rabbit back backbone side is lost hair or feathers in first 24 hours of test, unhairing range
Right side 3cm × 3cm.Going through whether skin of unhairing is damaged because of unhairing before to given the test agent, the skin haveing damage is not
Preferably tested.Tested new zealand rabbit is fixed in rabbit fixed bin, it is plucked to be applied to right side with 0.5g test material
On skin, application area is 2.5cm × 2.5cm, is smeared daily once, continuous to smear 14 days, since the 2nd day, is smeared every time
Before answer cropping, clear up remaining given the test agent with warm water, observation is as a result, and carry out skin wound repair Scoring System after 1 hour.
(1) standards of grading of skin wound repair are as follows: 1. without erythema: 0 point；2. slight erythema (visible reluctantly): 1 point；
3. moderate erythema (clearly visible): 2 points；4. severe erythema: 3 points；5. aubergine erythema is formed to slight eschar: 4 points；6. water
It is swollen: 0 point；7. Mild edema (visible reluctantly): 1 point；8. intermediate edema (obvious protuberance): 2 points；9. severe edema's (cutaneous protuberance
1mm, clear-cut): 3 points；10. Severe edema (cutaneous protuberance is more than 1mm, and has expansion): 4 points.
(2) grade scale of skin irritatin intensity is as follows: 1. skin irritation index is 0~0.49: nonirritant；2. skin
Stimulus index is 0.5~1.99: slight stimulation；3. skin irritation index is 2.0~5.99: moderate irritation；4. skin pierces
Swashing index is 6.0~8.0: severe irritation.
(3) test result is as shown in table 1:
Table 1, which is respectively releived, repairs the skin irritation test result of multiple-effect facial mask
| Group | Rule of origin | Skin irritatin scoring | Skin irritatin strength grading |
| 1 | Embodiment 1 | 0 | It is nonirritant |
| 2 | Embodiment 2 | 0 | It is nonirritant |
| 3 | Embodiment 3 | 0 | It is nonirritant |
| 4 | Embodiment 4 | 0 | It is nonirritant |
| 5 | Embodiment 5 | 0 | It is nonirritant |
| 6 | Embodiment 6 | 0 | It is nonirritant |
| 7 | Embodiment 7 | 0 | It is nonirritant |
| 8 | Embodiment 8 | 0 | It is nonirritant |
| 9 | Embodiment 9 | 0 | It is nonirritant |
| 10 | Comparative example 1 | 0 | It is nonirritant |
| 11 | Comparative example 2 | 0 | It is nonirritant |
Interpretation of result: the test result of table 1 shows that product property provided by the embodiment of the present invention and comparative example is mild,
It is highly-safe without skin irritation.
Effect example 2
Have the function of reparation, moist, moisturizing and anti-wrinkle to show that multiple-effect facial mask is repaired in of the invention releiving, it will be above-mentioned
The product of embodiment and comparative example preparation carries out following clinical trial:
110 female volunteers are chosen, the age 20~50 years old, are uniformly divided into 11 groups, respectively to Examples 1 to 9 and comparison
The product prepared in example 1~2 is tried out, and it is best result that every using effect total score, which is 5 points: 5 points, indicates fine；4 points for compared with
It is good；3 points are that can receive；2 points are bad；1 point is that cannot receive.The following are every average, result on trial refers to table
2。
Table 2, which is respectively releived, repairs the result on trial of multiple-effect facial mask
Interpretation of result: available to draw a conclusion from above-mentioned test result: multiple-effect is repaired in releiving for the embodiment of the present invention 1~3
Facial mask has good service performance and stability, while having reparation and anti-wrinkle, is much better than the resulting facial mask of comparative example 1~2,
This illustrates wheat bran extract and strawflower flower extract
There is more significant effect for bright color, test carries out the 7th day, and skin brightness improves 11.3% or more；
Test carries out the 14th day, and skin brightness improves 26.3% or more；Test carries out the 28th day, and skin brightness improves
30.2% or more；Test carries out 28 days, using Examples 1 to 4 releive repair the tester of multiple-effect facial mask skin brightness it is flat
Increase 39%.
Above the embodiments of the present invention are described in detail, but the present invention is not limited to described embodiments.It is right
For those skilled in the art, in the case where not departing from the principle of the invention and spirit, these embodiments are carried out more
Kind change, modification, replacement and modification, still fall in protection scope of the present invention.
Claims (9)
1. one kind, which is releived, repairs multiple-effect facial mask, which is characterized in that by weight percentage, including the following raw material: propylene glycol 2~
10%, glycerol 5~20%, wheat bran extract 0.1~10%, thickener 0.1~1%, oat polypeptide 0.5~5%, glycerol are poly-
Methacrylate 0.2~2%, arginine ferulate 0.2~3%, polyglutamic acid sodium 0.2~3%, strawflower flower extract
0.01~1%, Sodium Hyaluronate 0.01~0.1%, disodium ethylene diamine tetraacetate 0.05~0.5%, dipotassium glycyrrhizinate 0.01~
0.1%, Cremophor RH40 0.05~0.5%, peppermint leaf oil 0~0.1%, water surplus.
2. according to claim 1 releive repairs multiple-effect facial mask, which is characterized in that described releive repairs multiple-effect facial mask, presses
Weight percent meter, including the following raw material: propylene glycol 2~8%, glycerol 7~15%, wheat bran extract 0.5~2%, thickening
Agent 0.1~0.5%, oat polypeptide 1~2%, glycerol polymethacrylates 0.2~1%, arginine ferulate 0.2~
1%, polyglutamic acid sodium 0.2~1%, strawflower flower extract 0.05~0.2%, Sodium Hyaluronate 0.02~0.08%, ethylenediamine
Tetraacethyl disodium 0.05~0.2%, dipotassium glycyrrhizinate 0.02~0.08%, Cremophor RH40 0.05~0.2%, peppermint
Leaf oil 0.001~0.005%, water surplus.
3. according to claim 2 releive repairs multiple-effect facial mask, which is characterized in that described releive repairs multiple-effect facial mask, presses
Weight percent meter, including the following raw material: propylene glycol 5.5%, glycerol 10%, wheat bran extract 1%, thickener 0.24%,
Oat polypeptide 1.5%, glycerol polymethacrylates 0.5%, arginine ferulate 0.5%, polyglutamic acid sodium 0.5%, wax
Chrysanthemum extract 0.1%, Sodium Hyaluronate 0.05%, disodium ethylene diamine tetraacetate 0.1%, dipotassium glycyrrhizinate 0.05%, PEG-
40 rilanit specials 0.1%, peppermint leaf oil 0.003%, water surplus.
4. according to claim 2 releive repairs multiple-effect facial mask, which is characterized in that described releive repairs multiple-effect facial mask, presses
Weight percent meter, including the following raw material: propylene glycol 8%, glycerol 7%, wheat bran extract 0.5%, thickener 0.1%, swallow
Wheat polypeptide 2%, glycerol polymethacrylates 1%, arginine ferulate 0.2%, polyglutamic acid sodium 0.2%, the Flowers of Helichrysum bracteatum mention
Take object 0.2%, Sodium Hyaluronate 0.02%, disodium ethylene diamine tetraacetate 0.05%, dipotassium glycyrrhizinate 0.08%, PEG-40 hydrogenation
Castor oil 0.2%, peppermint leaf oil 0.005%, water surplus.
5. according to claim 2 releive repairs multiple-effect facial mask, which is characterized in that described releive repairs multiple-effect facial mask, presses
Weight percent meter, including the following raw material: propylene glycol 2%, glycerol 15%, wheat bran extract 2%, thickener 0.5%, oat
Polypeptide 1%, glycerol polymethacrylates 0.2%, arginine ferulate 1%, polyglutamic acid sodium 1%, strawflower flower extract
0.05%, Sodium Hyaluronate 0.08%, disodium ethylene diamine tetraacetate 0.2%, dipotassium glycyrrhizinate 0.02%, PEG-40 hydrogenated castor
Oily 0.05%, peppermint leaf oil 0.001%, water surplus.
6. according to claim 1 releive repairs multiple-effect facial mask, which is characterized in that the thickener is selected from hydroxy ethyl fiber
At least one of element and xanthan gum.
7. according to claim 1 releive repairs multiple-effect facial mask, which is characterized in that the wheat bran extract is using micro-
Wave extraction side, ultrasonic extraction, continuous phase transistion extracting method, any in soxhlet extraction methods are made.
8. according to claim 1 releive repairs multiple-effect facial mask, which is characterized in that the strawflower flower extract is using micro-
Wave extraction side, ultrasonic extraction, continuous phase transistion extracting method, any in soxhlet extraction methods are made.
9. a kind of as according to any one of claims 1 to 8 releive repairs the preparation method of multiple-effect facial mask, which is characterized in that
Include the following steps:
(1) addition of propylene glycol, glycerol, glycerol polymethacrylates, Sodium Hyaluronate, Cremophor RH40 and water is stirred
It mixes in machine, is uniformly mixed under conditions of 80~85 DEG C with revolving speed 30~60min of stirring of 2000~4000rpm to each component；
(2) after being cooled to not higher than 45 DEG C, by wheat bran extract, thickener, oat polypeptide, arginine ferulate, poly- paddy
Propylhomoserin sodium, strawflower flower extract, Sodium Hyaluronate, disodium ethylene diamine tetraacetate, dipotassium glycyrrhizinate are added in blender, with 2000
It is uniformly mixed to each component that the revolving speed of~4000rpm stirs 30~60min；
(3) peppermint leaf oil is added in blender, stirs evenly, obtains releiving and repair multiple-effect facial mask.
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| CN201811584494.7A CN109431941A (en) | 2018-12-24 | 2018-12-24 | One kind, which is releived, repairs multiple-effect facial mask and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811584494.7A CN109431941A (en) | 2018-12-24 | 2018-12-24 | One kind, which is releived, repairs multiple-effect facial mask and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110051602A (en) * | 2019-05-14 | 2019-07-26 | 东方爱堡(北京)母婴健康科技有限公司 | A kind of moisturizing moisturizing repair latex and preparation method thereof |
| CN110623888A (en) * | 2019-11-04 | 2019-12-31 | 菲朗生物科技(湖北)有限公司 | Herbal soothing essence and preparation method thereof |
| CN113712860A (en) * | 2021-08-24 | 2021-11-30 | 广州市科能化妆品科研有限公司 | After-sun soothing frozen film and preparation method thereof |
-
2018
- 2018-12-24 CN CN201811584494.7A patent/CN109431941A/en active Pending
Non-Patent Citations (2)
| Title |
|---|
| 上海企骋生物科技有限公司: "理玑泉 安肤活颜修护霜", 《国产非特殊用途化妆品备案信息服务平台》 * |
| 广州仙施生物科技有限公司: "Aujimy水嫩净透修护面膜", 《国产非特殊用途化妆品备案信息服务平台》 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110051602A (en) * | 2019-05-14 | 2019-07-26 | 东方爱堡(北京)母婴健康科技有限公司 | A kind of moisturizing moisturizing repair latex and preparation method thereof |
| CN110051602B (en) * | 2019-05-14 | 2021-11-26 | 东方爱堡(北京)母婴健康科技有限公司 | Skin moistening, moisturizing and repairing emulsion and preparation method thereof |
| CN110623888A (en) * | 2019-11-04 | 2019-12-31 | 菲朗生物科技(湖北)有限公司 | Herbal soothing essence and preparation method thereof |
| CN113712860A (en) * | 2021-08-24 | 2021-11-30 | 广州市科能化妆品科研有限公司 | After-sun soothing frozen film and preparation method thereof |
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Application publication date: 20190308 |