CN106214579B - A kind of beautiful ferment Whitening sunscreen cream of promise and preparation method thereof - Google Patents
A kind of beautiful ferment Whitening sunscreen cream of promise and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/78—Enzyme modulators, e.g. Enzyme agonists
- A61K2800/782—Enzyme inhibitors; Enzyme antagonists
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
Abstract
The present invention proposes a kind of beautiful ferment Whitening sunscreen cream of promise and preparation method thereof, and count by weight percentage, formula composition includes：Tristerin, 16/18 natural fatty alcohols, caprylic/capric triglyceride, isononyl isononanoate, jojoba oil, dimethyl silicone polymer, sterol ester, vitamin E, methyl hydroxybenzoate, propylben, glycerine, amino acid humectant, allantoin, lauryl alcohol, the beautiful ferment of promise and deionized water.The beautiful ferment Whitening sunscreen cream of promise proposed by the present invention has significant free radical scavenging ability, effectively inhibits melanin growth, good to ultraviolet radiation absorption effect, realizes the effect of whitening sun protection skin care, preparation method is simple to operation, and production cost is relatively low.
Description
Technical field
The present invention relates to cosmetic technical field, more particularly to a kind of beautiful ferment Whitening sunscreen cream of promise and preparation method thereof.
Background technology
The cosmetics on Cosmetic Market contain essence, preservative, fungicide at present.Consumer is similar in long-time service
After product, skin is it is possible that allergic reaction, or even induces other diseases.Therefore, it is necessary to a kind of cosmetics, not only have good
Good using effect, and do not have side effect, the health of consumer will not be damaged.Influence human skin health because
In element, maximum two killers are melanin and aging, and wherein whitening cosmetics market becomes more and more active in recent years, sales volume
Rapid growth.
Nuo Li (Noni) also known as Morinda, morinda citrifolia, four seasons fruit etc., genus rubia section Morinda plant.The plant master
It is distributed in the South Sea Islands small island, such as Philippine, Australia.Existing China is mainly distributed on the heat such as Hainan, the Xisha Islands
Band area, has been carried out large-scale plantation.Nuo Li has stronger functional character, and root, stem, leaf, flower and fruit can be used as medicine.
Root can get the dyestuff of yellow or red for contaminating clothes, and edible fruit is used, as food-grade health products.Nuo Li is as a kind of generation
Boundary medicinal plant new lover, caused food, medicine researcher extensive concern, therefrom separation identifies and carrys out about 200 compounds, main
To include the composition of the ingredients such as anthraquinone, flavones, cumarin, glucosides, triterpenes, Middle East scopola pavilion, rutin, malol, tannin
Card is considered as the effective active composition during promise is beautiful.In addition promise it is beautiful rich in unsaturated fatty acid, it is vitamin, minerals, anti-oxidant
Agent, rare element and celo peaceful original, the peaceful invertase of celo etc..Bioactivity research beautiful to promise at present focus primarily upon antibacterial,
Pre- preventing tumor removes free radical and anti-oxidant and other functional characteristics.Due to the beautiful unique functional characteristic of promise, be the whole world most
One of health-oriented products salable, the existing market demand beautiful to promise are increased with annual 50% speed, and government is also increasing to promise
Beautiful exploitation and development.Flavone compound and phenolic compound have inhibiting effect to tyrosinase according to the literature, can press down
Melanin processed increases.Find that there are many phenolic compounds in Noni fruit zymotic fluid in we study.
Invention content
For mirror with this, it is an object of the invention to propose a kind of beautiful ferment Whitening sunscreen cream of promise and preparation method thereof, it is intended to solve
There are certain side effect, stimulation skins to cause allergy, the ineffective problem of whitening sun protection for certainly existing Whitening sunscreen cream.
The technical proposal of the invention is realized in this way：
A kind of beautiful ferment Whitening sunscreen cream of promise, count by weight percentage, formula composition includes：Tristerin 1
~1.5%, 16/18 natural fatty alcohols 0.5~1%, caprylic/capric triglyceride 2~3%, isononyl isononanoate 3~
5%, jojoba oil 1~1.2%, dimethyl silicone polymer 0.5~1%, sterol ester 0.8~1%, vitamin E 0.5~1%,
Methyl hydroxybenzoate 0.1~0.2%, propylben 0.1%, glycerine 3~5%, amino acid humectant 2~3%, allantoin 0.1
~0.3%, lauryl alcohol 0.8~1% and the beautiful ferment 0.2~0.3% of promise, surplus is deionized water.
Further, the beautiful ferment of the promise is made by following steps：
It takes fresh Noni fruit to shred, distilled water is added and sucrose, mixing sterilize through high-pressure sterilizing pot, ferment is added after cooling
Female bacterium, standing for fermentation, it is the beautiful ferment of promise that zymotic fluid, which is obtained by filtration,.
Further, in the preparation process of the beautiful ferment of the promise, the adding proportion of Noni fruit, distilled water and sucrose is：Often
100mL distilled water and 4g sucrose is added in 100g Noni fruits.
Further, in the preparation process of the beautiful ferment of the promise, fermentation time is 30~40 days.
A kind of preparation method of the beautiful ferment Whitening sunscreen cream of promise, includes the following steps：
S1, A phases and B phases are taken respectively, heating stirring is to 80~90 DEG C in homogeneous；
S2, when A phases and B phase temperature differences are not more than 5 DEG C, while persistently stirring, B slowly is added in A phase oil solutions
It is thoroughly mixed to two-phase in phase aqueous solution, starts homogenizer, obtain stable and glossiness lotion；
S3, when emulsion temperature is down to 60~70 DEG C be added C phases, start again homogenizer until lotion be uniformly mixed, wait for
D phases are added when temperature is down to 40~45 DEG C, persistently stirs lotion and is down to room temperature, close blender, stand 5~12h to get；
Wherein, A phases include tristerin, 16/18 natural fatty alcohols, caprylic/capric triglyceride, isononanoic acid
Different nonyl ester, jojoba oil, dimethyl silicone polymer, sterol ester, vitamin E, methyl hydroxybenzoate and propylben；B phases include
Glycerine, amino acid humectant, allantoin and deionized water；C phases include lauryl alcohol；D phases include the beautiful ferment of promise.
Compared with prior art, beneficial effects of the present invention are：
The beautiful ferment Whitening sunscreen cream of promise proposed by the present invention has significant free radical scavenging ability, effectively inhibits tyrosine
The activity of enzyme inhibits melanin growth, good to ultraviolet radiation absorption effect, realizes the effect of whitening sun protection skin care, preparation method
Simple to operation, production cost is relatively low.In addition, the beautiful ferment Whitening sunscreen cream of promise proposed by the present invention may be directly applied to skin care U.S.
In vain, can also be applied to prepare other skin-lightening cosmetics or skin care item product.
Specific implementation mode
For the technical solution in the present invention is clearly and completely described in conjunction with the embodiments, it is clear that inventor says
It is bright, but it is only a part of the embodiment of the present invention that following embodiment is described, instead of all the embodiments.Based on the present invention
In embodiment, every other implementation obtained by those of ordinary skill in the art without making creative efforts
Example, shall fall within the protection scope of the present invention.
Embodiment 1
A kind of beautiful ferment Whitening sunscreen cream of promise, formula composition are as shown in table 1：
Table 1
The beautiful ferment of promise in above-mentioned Whitening sunscreen cream is prepared by following steps：
It takes the fresh Noni fruit of 500g to shred and is positioned over clean 2L wide-mouth bottles, 500mL distilled water and 20g sucrose is added,
Mixing sterilizes through high-pressure sterilizing pot, and saccharomycete is added after cooling, is stored at room temperature fermentation 30~40 days, zymotic fluid is obtained by filtration i.e.
For the beautiful ferment of promise.Wherein, the adding proportion of Noni fruit, distilled water and sucrose is, be added per 100g Noni fruits 100mL distilled water and
4g sucrose, nutritional agents of the sucrose as yeast, the energy is provided for fermentation process, and ferment effect is preferable under the conditions of the adding proportion.
The preparation method of the beautiful ferment Whitening sunscreen cream of promise proposed by the present invention, includes the following steps：
S1, the 150mL beakers after two sterilizing-dryings are taken, is separately added into A phases and B phases, heating stirring is in 80~90 DEG C
Homogeneously.
S2, the temperature of aqueous solution (i.e. B phases) are more slightly higher than oil solution (i.e. A phases), when two-phase temperature difference is not more than 5 DEG C
When, while persistently stirring, slowly A phase oil solutions are added in B phase aqueous solutions and are thoroughly mixed to two-phase, homogenizer is started, obtains
Obtain stable and glossiness lotion.
S3, when emulsion temperature is down to 60~70 DEG C be added C phases, start again homogenizer until lotion after mixing,
D is added when its temperature is down to 40~45 DEG C, persistently stirs lotion and is down to room temperature, close blender, 5~12h is stood, after bottling
Suncream can be obtained.
Inhibit the active testing of tyrosinase
Contain tyrosinase in potato extracting solution, tyrosinase is a kind of oxidoreducing enzyme, and tyrosinase oxidation can promote
Melanin is generated into l-tyrosine, during tyrosine forms melanin, tyrosinase can promote l-tyrosine to produce L-
DOPA and further effect make L-3,4 dihydroxyphenylalanine form bar quinone, and DOPA quinone ultimately generates melanin.
The calculation formula of inhibiting rate：[1- (T2-T1)/(C2-C1)] * 100%
C1 is the absorbance value of the mixed liquor of buffer solution and potato extracting solution, C2 be buffer solution, potato extracting solution and
The absorbance value of the mixed liquor of tyrosine is C2-C1 using the C1 absorbance values for surveying C2 as reference, indicates deducting potato extraction
The absorbance value of the melanin generated after the absorbance of liquid.T1 is the mixed of the beautiful ferment sample of promise, potato extracting solution and buffer solution
The absorbance value of liquid is closed, T2 is the absorbance of the mixed liquor of the beautiful ferment sample of promise, buffer solution, potato extracting solution and tyrosine
Value is similarly that reference surveys the absorbance value of T2 and obtains T2-T1 using T1, is indicated in deduction sample and potato extracting solution absorbance
Under the influence of, the absorbance value of the melanin after the inhibition of the beautiful ferment sample of promise.It keeps under identical test condition, measures real
The Whitening sunscreen cream in example 1 is applied to the inhibiting effect of tyrosinase, the results are shown in Table 9：
Inhibiting effect of 9 Whitening sunscreen cream of table to tyrosinase
As shown in Table 9, the beautiful ferment Whitening sunscreen cream of promise of the present invention can effectively inhibit the activity of tyrosinase, inhibit black
Element growth.
Absorb ultraviolet light test
It weighs the Whitening sunscreen cream that 0.06g embodiments 1 obtain uniformly to be applied on the glass slide with medical adhesive tape, with not
The glass slide for smearing suncream is blank control product, after timebase, scan sample and reference substance UVA (320~420nm),
UV absorption average value in UVB (275~320nm), UVC (200~275nm) wave band, comparative sample suncream and control are anti-
Frost is shone to ultraviolet radiation absorption situation, the results are shown in Table 10.
10 Whitening sunscreen cream ultraviolet absorption value of table
As can be known from Table 10, the beautiful ferment Whitening sunscreen cream of promise proposed by the present invention is good to ultraviolet radiation absorption effect, has one
Fixed sun-proof function.
ABTS free radical scavenging abilities measure
This experimental applications ABTS measures free radical scavenging activity.Compound concentration is the ABTS's and 2.45mmol/L of 7mmol/L
Potassium peroxydisulfate mixed solution, room temperature are protected from light 10~16h of standing, are diluted with water, make its light absorption value at 734nm be 0.7 ±
0.02 (is denoted as A0)；1 sample 1mg, ABTS working solution 1.5mL of embodiment is added in ABTS working solution test tubes；Blank group is steamed
Distilled water replaces sample solution；Control group replaces ABTS working solutions with distilled water.The above each group room temperature avoid light place 1h, in 734nm
Lower its light absorption value (being denoted as A) of measurement, ascorbic acid does positive control.
Clearance rate (%)=(A0-A)/A0* 100%.
Clearance rate measurement result such as table in the ABTS free radical scavenging abilities measurement for the Whitening sunscreen cream that embodiment 1 obtains
Shown in 11：
The free radical scavenging activity of 11 Whitening sunscreen cream of table
| Embodiment | Embodiment 1 |
| Clearance rate (%) | 81.26 |
As can be known from Table 11, the beautiful ferment Whitening sunscreen cream of promise proposed by the present invention has significant free radical scavenging ability,
Has good whitening and skin-protecting effect.
In conclusion the application the present invention relates to a kind of beautiful ferment of promise in cosmetics, the beautiful ferment whitening of promise provided is anti-
It shines frost and can be applied to cosmetic industry whitening nursing field.The beautiful ferment of promise is by fresh Noni fruit and sucrose in saccharomycetes to make fermentation
Under the conditions of extract and obtain, there is the beautiful ferment of the promise extracted preferable whitening nursing efficacy, Whitening sunscreen cream obtained to have
Significant free radical scavenging ability effectively inhibits the activity of tyrosinase, inhibits melanin growth, to ultraviolet radiation absorption effect
It is good, it realizes the effect of whitening sun protection skin care, and side effect is not present, also finds no the phenomenon that stimulation skin causes allergy.This
Invention preparation method is simple to operation, and equipment requirement is low, and production cost is low, energy conservation and environmental protection, is suitble to produce in enormous quantities.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
With within principle, any modification, equivalent replacement, improvement and so on should all be included in the protection scope of the present invention god.
Claims (2)
1. a kind of beautiful ferment Whitening sunscreen cream of promise, which is characterized in that count by weight percentage, formula composition includes：It is stearic
1~4.5%, 16/18 natural fatty alcohol 0.5~4% of acid glyceride, caprylic/capric triglyceride 2~8%, isononanoic acid are different
Nonyl ester 3~11%, jojoba oil 1~2.4%, dimethyl silicone polymer 0.5~4%, sterol ester 0.8~2.5%, vitamin E
0.5~4%, methyl hydroxybenzoate 0.1~0.4%, propylben 0.1%, glycerine 3~16%, amino acid humectant 2~6%,
Allantoin 0.1~0.3%, lauryl alcohol 0.8~2.2% and the beautiful ferment 0.2~1.2% of promise, surplus is deionized water；
The beautiful ferment of promise is made by following steps：It takes fresh Noni fruit to shred, distilled water and sucrose, mixing, through high pressure is added
Autoclave sterilizes, and saccharomycete is added after cooling, is stored at room temperature fermentation 30~40 days, it is the beautiful ferment of promise that zymotic fluid, which is obtained by filtration,；
Wherein, the adding proportion of Noni fruit, distilled water and sucrose is：100mL distilled water and 4g sucrose is added per 100g Noni fruits.
2. the beautiful ferment Whitening sunscreen cream of a kind of promise according to claim 1, which is characterized in that including following preparation process：
S1, A phases and B phases are taken respectively, heating stirring is to 80~90 DEG C in homogeneous；
S2, when A phases and B phase temperature differences are not more than 5 DEG C, while persistently stirring, B phase water slowly is added in A phase oil solutions
It is thoroughly mixed to two-phase in solution, starts homogenizer, obtain stable and glossiness lotion；
S3, when emulsion temperature is down to 60~70 DEG C be added C phases, start again homogenizer until lotion be uniformly mixed, wait for temperature
D phases are added when being down to 40~45 DEG C, persistently stirs lotion and is down to room temperature, close blender, stand 5~12h to get；
Wherein, A phases include tristerin, 16/18 natural fatty alcohols, caprylic/capric triglyceride, the different nonyl of isononanoic acid
Ester, jojoba oil, dimethyl silicone polymer, sterol ester, vitamin E, methyl hydroxybenzoate and propylben；B phases include glycerine,
Amino acid humectant, allantoin and deionized water；C phases include lauryl alcohol；D phases include the beautiful ferment of promise.
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| CN106860163A (en) * | 2017-02-24 | 2017-06-20 | 长沙协浩吉生物工程有限公司 | A kind of compound method of ferment anti-acne suncream |
| CN107412073A (en) * | 2017-08-30 | 2017-12-01 | 上海应用技术大学 | A kind of composition containing peach gum hydrolysate and its preparation method and application |
| CN109199953B (en) * | 2018-10-22 | 2021-11-16 | 海南师范大学 | Noni enzyme eye mask and preparation method thereof |
| CN109364007A (en) * | 2018-12-04 | 2019-02-22 | 天津尚美化妆品有限公司 | Plant enzyme face cleaning condensation |
| CN110511969A (en) * | 2019-09-06 | 2019-11-29 | 上海应用技术大学 | Natural peach gum fermentation prepares the method for peach gum extract and its applies in cosmetics |
| CN115364019B (en) * | 2021-05-21 | 2023-07-04 | 海南师范大学 | Millettia speciosa-dendrobe-noni composite enzyme, preparation method thereof and application thereof as sun-screening agent |
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| CN104207293A (en) * | 2014-08-08 | 2014-12-17 | 宋如珍 | Processing method of Noni enzyme |
| CN104207997A (en) * | 2014-09-18 | 2014-12-17 | 深圳朶妃生物科技有限公司 | Deep revitalizing facial mask containing morinda citrifolia stock extract liquid and preparation method thereof |
| CN104586741A (en) * | 2015-02-05 | 2015-05-06 | 上海昊淼生物科技有限公司 | Bubble enzyme facial mask |
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