CN111803422B - Oil control composition and application thereof - Google Patents
Oil control composition and application thereof Download PDFInfo
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- CN111803422B CN111803422B CN202010825397.3A CN202010825397A CN111803422B CN 111803422 B CN111803422 B CN 111803422B CN 202010825397 A CN202010825397 A CN 202010825397A CN 111803422 B CN111803422 B CN 111803422B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4953—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom containing pyrimidine ring derivatives, e.g. minoxidil
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/008—Preparations for oily hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/10—General cosmetic use
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The invention provides an oil control composition which comprises the following raw materials in parts by weight: 0.01-5 parts of ectoin, 1-10 parts of spiraea ulmaria extract and 0.01-10 parts of 10-hydroxydecanoic acid. The oil control composition can be applied to an external oil control product, and the addition amount of the oil control composition in the external oil control product is 1-20%. The external oil control product can be a cosmetic such as astringent, essence, cream or emulsion. The oil control composition of the invention reduces the problem of system instability caused by spiraea ulmaria extract. The skin care product has the advantages of being used in functional skin care products, having excellent function of controlling grease secretion, being capable of rapidly eliminating oily light and greasy feeling, bringing fresh feeling to skin, being capable of gradually balancing skin water and oil composition after long-term use, helping repair skin barrier and being capable of showing continuous oil control effect after being used. In addition, the combination of the three has better improvement effect on the condition of reddening of the face.
Description
Technical Field
The invention belongs to the field of cosmetics, and relates to an oil control composition and application thereof.
Background
People who mix skin or oily skin rise year by year due to bad living habits such as work and rest, irregular diet and the like, internal causes such as endocrine disturbance, psychological stress and the like, and objective factors such as environmental pollution and the like, and once oily skin is formed, the people are difficult to improve rapidly, and the appearance of individuals is influenced, so that the problem is plagued by more and more people. Oily skin is formed due to vigorous secretion of skin grease, which causes skin to be shiny and oily, oily look and feel, and poor skin problems such as acne and seborrheic dermatitis. In addition, the skin barrier function of people with oily skin is often unbalanced, pores are enlarged by accumulated grease, and the skin gradually loses elasticity.
At present, the existing oil control cosmetics on the market mainly comprise oil absorption powder such as silicon dioxide, titanium dioxide, talcum or plant extracts, the former is characterized in that powdery particles are used for rapidly filling pores to absorb excessive grease, so that the problem of skin oil is improved, the problem of skin oil can only be temporarily lightened, both symptoms and root causes cannot be treated, even excessive addition can cause the problem of pore blockage and the like, and plant extracts such as calendula, aloe, viola yedoensis and the like have small side effects, but the problems of slow effect, easiness in repetition and the like are unavoidable.
CN 101874768A discloses an oil-controlling cosmetic composition, the formulation comprises the following components in weight percentage: 0.01-10% of water-soluble zinc salt, 0.1-8% of oil-absorbing powder, 0.1-15% of royal jelly extract and 0.1-10% of natural Chinese herbal medicine extract. The composition can reduce oil secretion and absorb skin oil. However, the product has no effect of repairing skin barrier, can not continuously maintain water-oil balance of skin after being stopped, and does not solve the problem of more facial red blood filaments.
CN 106661676A discloses a plant extract for controlling oil and shrinking pores, and preparation method and application thereof, the raw materials components include: 15-25 parts of rice fermentation liquid, 35-35 parts of calendula extract, 15-25 parts of aloe extract and 25-35 parts of Mao Ruilv fruit oil. The composition has good effect of inhibiting oil secretion, but has no mention of repairing skin barrier and continuously controlling oil, and has no mention of reducing facial redness.
Disclosure of Invention
Aiming at the problems that the existing oil control cosmetics cannot continuously maintain the water-oil balance of skin and have no effect of repairing skin barriers, the invention provides an oil control composition which can continuously control oil, repair skin barriers and reduce the problem of facial redness.
Another object of the present invention is to provide a cosmetic use of the above oil control composition.
In order to achieve the above purpose, the present invention adopts the following technical scheme.
An oil control composition comprises the following raw materials in parts by weight: 0.01-5 parts of ectoin, 1-10 parts of spiraea ulmaria extract and 0.01-10 parts of 10-hydroxydecanoic acid.
Preferably, the oil control composition comprises the following raw materials in parts by weight: 1 part of ectoin, 1 part of spiraea ulmaria extract and 3 parts of 10-hydroxydecanoic acid. When the preferable proportion is adopted, the performance of the obtained product in all aspects is better.
In the above oil control composition, the use of elm, elm spiraea extract and 10-hydroxydecanoic acid are commercially available.
The oil control composition is simple and convenient to prepare, and is obtained by directly mixing or weighing a certain amount of ectoin, spiraea ulmaria extract and 10-hydroxydecanoic acid in distilled water, fully stirring to ensure that the components are uniformly dispersed and dissolved, and freeze-drying.
An application of the oil control composition in an external oil control product.
The oil control composition can be added with conventional auxiliary materials in the field, and processed into various common cosmetic formulations such as cosmetic water, essence, emulsion, cream type cosmetics, shampoo and hair care products and the like by a conventional method for controlling excessive secretion of facial or head skin grease.
An external oil control product comprising the above oil control composition.
The addition amount of the oil control composition in the external oil control product is 1-20%, preferably 3-15%, and more preferably 10%. The addition amount of the oil control composition can be selected according to the dosage form of the external oil control product.
The mechanism/synergy of the present invention is as follows:
exodeine is derived from high halophilic bacteriaHalomonas Elongata) Is a natural small molecular amino acid derivative. Under the extreme conditions of high salt, high temperature and high ultraviolet radiation, the ectoine can protect halophilic bacteria from being damaged by severe environment. It can be said that ectoin is a compatible solute produced in cells by salt-tolerant organisms to maintain osmotic pressure balance, to regulate intracellular and extracellular osmotic pressure balance. Thus, the method is characterized by the following stepsHas osmotic pressure regulating effect, stable protein hydration layer, inhibiting UV induced cell injury (mitochondrial gene mutation and cell nucleus DNA injury, etc.), and protecting cell membrane structure. Are often used in cosmetic applications to prevent photodamage to the skin, to resist haze, etc. 10-hydroxydecanoic acid (10-HDAA) can reduce the number of active sebaceous glands, effectively inhibit grease secretion, has excellent antibacterial activity and inhibits various pathogenic microorganisms, so that inflammatory response caused by the vigorous grease secretion can be reduced. Both the ectoine and the 10-HDAA are compatible with the exterior and the interior, so that the problems of face oil-making, oily appearance and the like are solved from inside to outside.
The spiraea ulmaria extract is a natural product extracted from the flower buds of spiraea ulmaria, effectively astringes large pores, inhibits abnormal oil production of hair follicles, and effectively regulates sebaceous glands of human bodies. Inhibit bacterial reproduction and prevent acne, thereby achieving the effect of conditioning skin. However, the plant extract is used as a plant extract, and is influenced by temperature, and the properties of the plant extract are changed, so that the color of the product is deepened when the plant extract is added into a formula, and the application range and the addition amount of the plant extract are greatly influenced. The composition can avoid the problem of color change of the spiraea ulmaria extract in the use of the formula, and the three components are mutually cooperated to greatly improve the high-temperature stability of the spiraea ulmaria extract and the product.
The invention has the following advantages:
the composition of the invention consists of the elm extract, the elm spiraea extract and 10-hydroxydecanoic acid (10-HDAA), and the use of the composition with a specific proportion in a formula reduces the problem of system instability caused by the elm spiraea extract. The skin care product has the advantages of being used in functional skin care products, having excellent function of controlling grease secretion, being capable of rapidly eliminating oily light and greasy feeling, bringing fresh feeling to skin, being capable of gradually balancing skin water and oil composition after long-term use, helping repair skin barrier and being capable of showing continuous oil control effect after being used. In addition, the combination of the three has better improvement effect on the condition of reddening of the face.
Drawings
FIG. 1 shows the color comparison of application example 1 and application example 13 after storage at a constant temperature of 55℃for 10 days.
Detailed Description
The present invention will be further described with reference to examples and drawings, but the present invention is not limited to the examples.
Example 1 preparation of oil control composition
Respectively weighing the exendin, the spiraea ulmaria extract and the 10-hydroxydecanoic acid according to the components of the samples 1-6 and the comparative samples 1-5 in the following table 1 (g), adding distilled water to completely disperse and dissolve, fully stirring and uniformly mixing, and freeze-drying to obtain an oil control composition; the control samples 6-8 were taken directly.
Table 1 formulation of different oil control compositions
EXAMPLE 2 inhibition of sebaceous gland secretion by different products
The oil control effect of the experimental and comparative examples was investigated by examining the synthesis of neutral lipids from human sebaceous cells during cell culture:
SZ95 human sebaceous gland cells cultured in vitro are selected, the cells are cultured in a Sebomed basal medium, and 10% fetal bovine serum, 5 mug/L epidermal growth factor, 100U/ml penicillin and 100 mug/ml streptomycin are added. Placing at 37deg.C, 5% CO 2 In the incubator, the culture medium was replaced every 2 days. Cells were seeded in 96-well plates, samples 1-6 and controls 1-8 of the same mass were added the next day, the supernatant was discarded after 48h, washed twice with PBS, and after repeated pipetting, divided into two portions, one portion was added with PBS-diluted Nile red dye (1 mg/ml in acetone, stored at-20 ℃ C.) to a final concentration of 10. Mu.g/ml, and one portion was added with PBS-diluted Fluorescein Diacetate (FDA) (5 mg/ml in DMSO, stored at-20 ℃ C.) to a final concentration of 15. Mu.g/ml. Detecting fluorescence intensity of different samples, detecting emission wavelength at 565nm by using 485nm as excitation wavelength, and detecting emission wavelength at 523nm by using 494nm as excitation wavelength by FDA, wherein the fluorescence intensity is calculated according to the following formula: intracellular neutral lipid percentage (%) =nile red fluorescence intensity/FDA fluorescence intensity×100%. ExperimentThe data are as follows:
TABLE 2
The different letters in the table represent significant differences at the 5% level (p < 0.05).
From the above table data, the composition has the least neutral lipid content of 10-hydroxydecanoic acid and the most neutral lipid content of ectoin, indicating that 10-hydroxydecanoic acid is optimal for oil control and ectoin is the worst. For the two-by-two combination of the three components, the combination of the spiraea ulmaria extract and the 10-hydroxydecanoic acid is significantly better than the spiraea ulmaria extract alone, while the combination of the spiraea ulmaria extract and the ectoin is not significantly different from the neutral lipid content of the spiraea ulmaria extract alone. The neutral lipid content of the composition mixed according to the proportion of 1-10 parts by weight of spiraea ulmaria extract, 0.01-5 parts by weight of ectoin and 0.01-10 parts by weight of 10-hydroxydecanoic acid is lower, and the neutral lipid content after the three components are combined is obviously better than that of the composition used in a pairwise combined way, so that the three components in the composition have the effect of synergistically inhibiting the secretion of neutral lipids of cells. The too low proportion of spiraea ulmaria extract compared with the optimal proportion of sample 1, the neutral lipid content of the comparison samples 3-5 when 10-hydroxydecanoic acid or exendin is excessive, is significantly increased, which indicates that the effect of inhibiting the secretion of neutral lipids of cells can be best only when the spiraea ulmaria extract, 10-hydroxydecanoic acid and exendin are in proper proportion.
Example 3 preparation of oil control emulsion
The oil control emulsion was prepared by conventional methods according to the following table raw material formulation, and the numbers prepared for samples 1 to 6 were application examples 1 to 6, and the numbers prepared for comparative samples 1 to 8 were application examples 8 to 15.
TABLE 3 Table 3
The preparation method of the oil control emulsion comprises the steps of adding purified water into an emulsifying tank, sequentially adding xanthan gum, betaine, glycerol, methylparaben and propylparaben into the emulsifying tank, stirring and heating to 75-80 ℃, sequentially adding cetostearyl glucoside, cetostearyl alcohol, dioctyl carbonate, isononyl isononanoate and VE acetate into an oil phase tank, heating to 75-80 ℃, pumping into the emulsifying tank, homogenizing for several minutes, cooling to 40-45 ℃, sequentially adding the oil control composition prepared in the embodiment 1 and phenoxyethanol, stirring until all materials are completely dissolved, and cooling to normal temperature to obtain the oil control emulsion.
Comparative example 1
According to CN 101874768A, an oil-controlling cosmetic composition is disclosed, comprising the following specific components:
TABLE 4 Table 4
A control ointment was prepared according to the usual method and the number is application example 7.
Example 4 oil control effect of different products
100 healthy subjects were enrolled in a self-control method, randomly divided into 5 groups, the left half face was used with a matrix containing no oil control composition, the right half face was used with application examples 1, 7, 9, 13, 14, respectively, and then the oil control efficacy of the product was evaluated by measuring the fat content of the forehead of the left and right half faces (using an apparatus of a multi-probe skin test system MPA 580 (daily+khazaka, germany; oil distribution test kit).
The specific implementation mode is as follows: the subjects were cleaned with mild cleanser for 30 minutes after face cleansing, then left and right half faces were used with equal amounts of matrix and different samples, each of the morning and evening, and the indexes were detected 1h, 6h, 3d, 7d, 14d, 28d after the first morning (first time) use, and then were detected again at 14d (test 42 d), and the rate of change of grease for the right face versus the left face was calculated, as grease rate (%) = (right face grease content-left face grease content)/left face grease content x 100%, with lower values indicating more grease reduction.
TABLE 5 oil control effect (% oil change) for different products
The different letters in the table represent that at the same time the difference in the 5% level was significant for the different samples (p < 0.05).
As can be seen from the above table, compared with the prior art in application example 7, application example 1 was significantly improved in both the instantaneous oil control effect at 1h and 6h and the long-term oil control effect at 28d, and was also significantly superior to application example 13 using spiraea ulmaria extract alone and application example 14 using 10-hydroxydecanoic acid alone in the same period, demonstrating that the compositions of the present invention have synergistic oil control effects with each other. As can be seen by comparing the rates of change of the subject's oils after 28d and 14d (trial 42 d), example 1 containing exendin was significantly better than application example 9 without exendin, demonstrating that application example 1 of the present invention can provide long lasting oil control.
Example 5 effects of different products on repairing skin Barrier and improving Red blood Silk
50 healthy subjects were enrolled using the self-control method, the left half face using the matrix without the oil control composition, and the right half face using application examples 1, 8, 13, 14, and 15, respectively. The skin moisture loss content of the left and right half-face forehead was detected by using a skin moisture loss tester tewatter TM300 (courage+khazaka, germany), and the restoration efficacy of the product to skin barrier was evaluated; the proportion of red blood streaks on the skin of the left and right half-face apple muscles was detected by using a facial image analyzer VISIA-CR (Canfield, USA), and the efficacy of the product in removing red blood streaks was evaluated.
The specific implementation mode is as follows: the subjects cleaned the face with the mild facial cleanser for 30 minutes, then the left and right half faces respectively use the same amount of matrix and different samples, and then use the same amount of matrix and different samples once in the morning and evening, use the samples for 28 days continuously, and detect water loss 1h, 6h, 3d, 7d, 14d and 28d after the first morning (first time); the moisture content was measured 3d, 7d, 14d, 28d after use and 14d after stopping use (test 42 d), respectively, and the proportion of red blood streaks in the skin was measured. Then, the moisture content change rate and the red blood streak change rate of the right face to the left face were calculated, respectively, and the moisture content change rate (%) = (right face moisture content-left face moisture content)/left face moisture content×100%. Lower values indicate stronger barrier repair efficacy. Red blood streak change rate (%) = (right-face red blood streak ratio-left-face red blood streak ratio)/left-face red blood streak ratio x 100%, the lower the value, the stronger the red blood streak improvement ability.
TABLE 6 skin barrier repair effects (moisture content Change Rate) for different products
The different letters in the table represent that at the same time the difference in level of 5% was significant for the different samples (p < 0.05)
As can be seen from the above table, the instantaneous skin moisture change after 6 hours of use, the short-term skin moisture change after 7 days of use and the long-term skin moisture change after 28 days of use of application example 1 are significantly better than the application examples 13 to 15 in which the three components were used alone and the application example 8 in which the ectoin was used in combination with the spiraea ulmaria extract, which demonstrates that the combined use of the three components of the present invention has a synergistic effect for the instantaneous moisturizing and long-term skin barrier repair effects. Application example 1 was still significantly better than application examples 8, 13-15 in terms of skin moisture change after 14 days of inactivity (test 42 d), demonstrating that long term use of the oil control composition of the present invention can improve skin function, enhance its barrier effect, and prevent moisture loss.
TABLE 7 improvement of Red blood streak effect by different products
From the above table, application example 1 showed very significant improvement effect on facial red blood streaks, and the effect was still significant after the shutdown, the red blood streaks were reduced by 13.52% from the initial ones, whereas application examples 8, 13, 14, 15 showed no improvement or no significant improvement on facial red blood streaks.
Example 6 product stability
The application examples 1, 5, 6, 9 and 13 were packaged in transparent glass sample bottles, respectively placed in a constant temperature experimental box at 55 ℃, respectively observed for 1d, 3d and 10d, and the samples were cooled to room temperature before observation.
TABLE 8 high temperature stability of different products
As is clear from the above data and fig. 1, application examples 9 and 13 turned to pale yellow brown on the 3 rd day of storage, compared with the milky white of application examples 1, 5 and 6 after storage at high temperature. This suggests that the spiraea ulmaria extract undergoes a color change at high temperature without addition of ectoin and 10-hydroxydecanoic acid, thereby affecting the color and stability of the product.
Example 7 preparation of oil control composition and cosmetic
1. Toning lotion
The raw materials comprise: 1% of oil control composition (1 part by weight of elm spiraea extract, 1 part by weight of 10-hydroxydecanoic acid 2 parts by weight of elm spiraea extract), 1% of glycerol 2%, 1% of betaine, 0.2% of allantoin and 0.6% of phenoxyethanol, and supplementing 100% of water;
the preparation method comprises the following steps: mixing glycerol, betaine and allantoin, and stirring to obtain a mixture A; adding the oil control composition and phenoxyethanol into the mixture A, and uniformly mixing and stirring to obtain the toning lotion.
2. Essence liquid
The raw materials comprise: 3% of oil control composition (1 part by weight of elm spiraea extract, 1 part by weight of 10-hydroxydecanoic acid, 4 parts by weight of elm spiraea extract), 40.8% of poloxamer, 8% of glycerol, 5% of sorbitol, 2% of betaine, 0.2% of allantoin, 0.5% of chitosan and 1% of beta-glucan; pentanediol 2%, octanoyl hydroxamic acid 1%; triethanolamine 0.1% and water to 100%;
the preparation method comprises the following steps: taking a proper amount of glycerol and sorbitol to wet poloxamer and an oil control composition; adding purified water into the mixture, homogenizing in a high-pressure homogenizer for 2 times at 12000rpm/min for 3 minutes each time; then adding other components, adjusting the pH value to about 6.5, and stirring until the components are uniformly mixed to obtain the essence.
3. Oil control cream
The raw materials comprise: 15% of oil control composition (1.5 parts by weight of elm spiraea extract, 1 part by weight of 10-hydroxydecanoic acid, 3 parts by weight of 10-hydroxydecanoic acid), 5% of glyceryl stearate, 10% of caprylic/capric triglyceride, 5% of shea butter, 3% of glycerol, 2% of sorbitol, 2% of betaine, 0.05% of allantoin, 0.5% of chitosan, 0.8% of beta-glucan, 0.2% of sodium polyglutamate, 0.6% of phenoxyethanol and 100% of water;
the preparation method comprises the following steps: weighing glycerol stearate, caprylic/capric triglyceride and shea butter according to a proportion, mixing and heating to 70-75 ℃ to obtain a mixture A; taking a proper amount of glycerol and sorbitol, fully dispersing and dissolving the oil control composition, continuously adding a proper amount of water, stirring to add other components, uniformly mixing, and heating to 70-75 ℃ to obtain a mixture B; mixing A, B, homogenizing for 5-8 min, stirring to 45-40deg.C, adding antiseptic and acid-base regulator, and mixing to obtain oil control cream.
4. Shampoo liquid
The raw materials comprise: 20% of an oil control composition (0.5 part by weight of elm spiraea extract, 1 part by weight of 10-hydroxydecanoic acid, 3% by weight of ammonium lauryl sulfate, 12% of sodium laureth sulfate, 25% of laureth, 10.2% of polyquaternium, 22.5% of polyquaternium, 0.5% of guar hydroxypropyl trimethylammonium chloride, 5% of potassium laurylphosphate, 5% of cocamidopropyl betaine, 4% of cocomonoethanolamide, 3% of PEG-7 glycerol cocoate, 1% of ethylene glycol distearate, 1% of betaine, 0.05% of styrene acrylate copolymer, 0.05% of coco glucoside, 0.1% of disodium EDTA, 0.03% of methyl chloroisoquinoline ketone, 0.01% of methyl isoquinoline ketone, 0.01% of magnesium chloride, 1.5% of sodium chloride, 1% of zinc pyrithione, 0.5% of zinc sulfate, 0.3% of essence, and 100% of water;
the preparation method comprises the following steps: slowly adding polyquaternium-10 and guar hydroxypropyl trimethylammonium chloride into a proper amount of water, dispersing and stirring uniformly to obtain a phase A; adding ammonium laurylsulfate, sodium laurylsulfate, laureth-25, polyquaternium-22 and disodium EDTA into a proper amount of water, mixing, heating to 50-55deg.C, stirring to dissolve, adding phase A, stirring, heating to 75-80deg.C, and stirring for 1 hr; cooling to 55-60deg.C, adding cocamidopropyl betaine, cocamidoethanamide, and zinc pyrithione, and stirring; and continuously cooling to 40-45 ℃, adding the oil control composition, betaine, PEG-7 glycerol cocoate, glycol distearate, methyl chloroisoquinoline ketone, methyl isoquinoline ketone, essence, magnesium chloride, sodium chloride and zinc sulfate, and stirring until the mixture is uniform to obtain the shampoo.
Claims (9)
1. The oil control composition is characterized by comprising the following raw materials in parts by weight: 0.1-1 part of ectoine, 1-10 parts of spiraea ulmaria extract and 0.1-3 parts of 10-hydroxydecanoic acid.
2. The oil control composition according to claim 1, comprising the following raw materials in parts by weight: 1 part of ectoin, 1 part of spiraea ulmaria extract and 3 parts of 10-hydroxydecanoic acid.
3. Use of the oil control composition according to claim 1 or 2 in an external oil control product.
4. The use according to claim 3, wherein the external oil control product is in a form selected from the group consisting of lotions, essences, creams and emulsions.
5. The use according to claim 3, wherein the external oil control product is applied to facial skin or head skin.
6. A topical oil control product comprising the oil control composition of claim 1 or 2.
7. The external oil control product according to claim 6, wherein the oil control composition is added to the external oil control product in an amount of 1 to 20%.
8. The external oil control product according to claim 6, wherein the oil control composition is added to the external oil control product in an amount of 3 to 15%.
9. The external oil control product according to claim 6, wherein the oil control composition is added to the external oil control product in an amount of 10%.
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| CN112870136A (en) * | 2021-01-12 | 2021-06-01 | 吴维碧 | Shampoo for patients with seborrheic dermatitis and preparation method thereof |
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| JP2004123614A (en) * | 2002-10-03 | 2004-04-22 | Arysta Lifescience Corp | Skin care preparation for external use |
| DE102006020382A1 (en) * | 2006-04-28 | 2007-10-31 | Henkel Kgaa | Cosmetic oil-in-water emulsion, useful e.g. to treat skin, comprises oil or fat phase comprising a component e.g. branched saturated alkanol, water, a cosmetically active substance e.g. monomer and a polysaccharide |
| US20180085297A1 (en) * | 2016-05-31 | 2018-03-29 | L'oreal | Anti-acne compositions and methods of use |
| CN107789308A (en) * | 2017-11-06 | 2018-03-13 | 诺斯贝尔化妆品股份有限公司 | A kind of gentle oil control and acne removal elite |
| CN107951823A (en) * | 2017-12-06 | 2018-04-24 | 懿奈(上海)生物科技有限公司 | It is a kind of that there is the composition of oil-control and its application |
| CN109091433A (en) * | 2018-10-22 | 2018-12-28 | 广州智尚生物科技有限公司 | A kind of composition of oil control and acne removal and its application in cosmetics |
| CN111281832B (en) * | 2020-04-02 | 2022-06-14 | 广州一一生物技术有限公司 | Skin barrier repair compound, toning lotion and preparation method thereof |
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2020
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