CN107001190A - 方法 - Google Patents

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Publication number
CN107001190A
CN107001190A CN201580068826.4A CN201580068826A CN107001190A CN 107001190 A CN107001190 A CN 107001190A CN 201580068826 A CN201580068826 A CN 201580068826A CN 107001190 A CN107001190 A CN 107001190A
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CN
China
Prior art keywords
less
reactant mixture
100ppm
tetra
500ppm
Prior art date
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Pending
Application number
CN201580068826.4A
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English (en)
Chinese (zh)
Inventor
兹德涅克·昂德鲁斯
帕维尔·库比切克
卡雷尔·菲拉斯
彼得·斯拉德切克
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Spolek Pro Chemickou A Hutni Vyrobu Narodni Podnik Unite
Original Assignee
Spolek Pro Chemickou A Hutni Vyrobu Narodni Podnik Unite
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Application filed by Spolek Pro Chemickou A Hutni Vyrobu Narodni Podnik Unite filed Critical Spolek Pro Chemickou A Hutni Vyrobu Narodni Podnik Unite
Publication of CN107001190A publication Critical patent/CN107001190A/zh
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/013Preparation of halogenated hydrocarbons by addition of halogens
    • C07C17/02Preparation of halogenated hydrocarbons by addition of halogens to unsaturated hydrocarbons
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/07Preparation of halogenated hydrocarbons by addition of hydrogen halides
    • C07C17/087Preparation of halogenated hydrocarbons by addition of hydrogen halides to unsaturated halogenated hydrocarbons
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/013Preparation of halogenated hydrocarbons by addition of halogens
    • C07C17/04Preparation of halogenated hydrocarbons by addition of halogens to unsaturated halogenated hydrocarbons
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/093Preparation of halogenated hydrocarbons by replacement by halogens
    • C07C17/20Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/25Preparation of halogenated hydrocarbons by splitting-off hydrogen halides from halogenated hydrocarbons
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/26Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/263Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by condensation reactions
    • C07C17/266Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by condensation reactions of hydrocarbons and halogenated hydrocarbons
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/26Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/272Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions
    • C07C17/275Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions of hydrocarbons and halogenated hydrocarbons
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/38Separation; Purification; Stabilisation; Use of additives
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/38Separation; Purification; Stabilisation; Use of additives
    • C07C17/383Separation; Purification; Stabilisation; Use of additives by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00Acyclic saturated compounds containing halogen atoms
    • C07C19/01Acyclic saturated compounds containing halogen atoms containing chlorine
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C21/00Acyclic unsaturated compounds containing halogen atoms
    • C07C21/02Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
    • C07C21/04Chloro-alkenes
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/582Recycling of unreacted starting or intermediate materials

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
CN201580068826.4A 2014-10-16 2015-10-15 方法 Pending CN107001190A (zh)

Applications Claiming Priority (7)

Application Number Priority Date Filing Date Title
CZ2014706 2014-10-16
CZPV2014-705 2014-10-16
CZ2014707 2014-10-16
CZ2014705 2014-10-16
CZPV2014-706 2014-10-16
CZPV2014-707 2014-10-16
PCT/CZ2015/000123 WO2016058569A1 (en) 2014-10-16 2015-10-15 Process

Publications (1)

Publication Number Publication Date
CN107001190A true CN107001190A (zh) 2017-08-01

Family

ID=54540761

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201580068826.4A Pending CN107001190A (zh) 2014-10-16 2015-10-15 方法

Country Status (7)

Country Link
US (2) US9840448B2 (de)
EP (1) EP3207007B1 (de)
JP (2) JP7168321B2 (de)
CN (1) CN107001190A (de)
CZ (1) CZ309310B6 (de)
TW (2) TWI702202B (de)
WO (1) WO2016058569A1 (de)

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109232173A (zh) * 2018-07-26 2019-01-18 浙江巨化技术中心有限公司 一种1,1,1,2,3-五氯丙烷的连续制备方法
CN110511112A (zh) * 2019-08-16 2019-11-29 浙江巨化技术中心有限公司 一种1,1,2,3-四氯丙烯的制备方法
CN111604041A (zh) * 2020-06-18 2020-09-01 大连九信精细化工有限公司 一种γ-氧化铝改性催化剂、其制备方法及在合成1,1,3-三氯丙烯中的应用
CN111712479A (zh) * 2018-03-07 2020-09-25 阿科玛法国公司 2,3,3,3-四氟丙烯的生产工艺
CN111757863A (zh) * 2018-03-07 2020-10-09 阿科玛法国公司 2-氯-3,3,3-三氟丙烯的生产工艺
CN111770908A (zh) * 2018-03-07 2020-10-13 阿科玛法国公司 2,3,3,3-四氟丙烯的生产工艺
CN112334436A (zh) * 2018-04-03 2021-02-05 蓝立方知识产权有限责任公司 使用吸收器-反应器组合生产卤化烷烃的方法
CN112384490A (zh) * 2018-07-09 2021-02-19 科慕埃弗西有限公司 用于整合式2,3,3,3-四氟丙烯制造工艺的组合物和方法

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20190127303A1 (en) * 2016-04-13 2019-05-02 Arkema France Process for the manufacture of 2,3,3,3-tetrafluoropropene
CZ309472B6 (cs) * 2016-09-02 2023-02-08 Spolek Pro Chemickou A Hutní Výrobu, Akciová Společnost Způsob výroby tetrachlormethanu
US10717662B2 (en) * 2018-02-07 2020-07-21 Honeywell International Inc. Process for the removal of iron and phosphate ions from a chlorinated hydrocarbon waste stream
EP3774702B1 (de) * 2018-04-03 2022-04-27 Blue Cube IP LLC Verbesserte verfahren zur herstellung von halogenierten alkanen
WO2019195258A1 (en) * 2018-04-03 2019-10-10 Blue Cube Ip Llc Improved process for preparing chloroalkanes and/or chlorofluoroalkanes
US10773192B1 (en) * 2019-04-09 2020-09-15 Bitfury Ip B.V. Method and apparatus for recovering dielectric fluids used for immersion cooling
EP4251599A1 (de) * 2020-11-30 2023-10-04 Blue Cube IP LLC Verfahren zur behandlung eines schweren nebenproduktstroms aus der herstellung von chloriertem propan
CN115108882B (zh) * 2022-06-07 2024-04-12 浙江衢化氟化学有限公司 一种1,1,1,2,3-五氯丙烷的连续制备方法

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0131560A1 (de) * 1983-07-06 1985-01-16 Monsanto Company Verfahren zur Herstellung von 1,1,2,3-Tetrachloropropen
CN102177116A (zh) * 2009-06-24 2011-09-07 株式会社德山 氯化烃的制备方法
JP2012056920A (ja) * 2010-09-13 2012-03-22 Tokuyama Corp クロロプロパンの製造方法
CN102405202A (zh) * 2009-04-23 2012-04-04 大金工业株式会社 制备2-氯-3,3,3-三氟丙烯的方法
CN103717560A (zh) * 2011-07-26 2014-04-09 大金工业株式会社 用于制备2,3,3,3-四氟丙烯的方法
WO2014130436A1 (en) * 2013-02-19 2014-08-28 Honeywell International Inc. Methods for the dehydrochlorination of 1,1,1,3-tetrachloropropane to 1,1,3-trichloropeopene
CN104058925A (zh) * 2013-03-22 2014-09-24 中化蓝天集团有限公司 1,1,1,2,3-五氯丙烷的连续制备方法

Family Cites Families (32)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB920855A (en) 1960-05-08 1963-03-13 Aharon Katchalsky A process for the preparation of telomers or adducts
DE1902843C3 (de) 1969-01-21 1974-04-25 Wacker-Chemie Gmbh, 8000 Muenchen Verfahren zur Anlagerung von Chlor an Olefine
US3927131A (en) 1974-06-10 1975-12-16 Dow Chemical Co Dehydrohalogenation of halogenated hydrocarbons
EP0247215A1 (de) 1986-05-26 1987-12-02 Halocarbon Products Corporation Verfahren zur Herstellung von 1,1,1,3-Tetrachlorpropan
EP0094527B1 (de) 1982-05-14 1987-08-19 Stauffer Chemical Company Verfahren zur Behandlung von Abfällen von flüssigen chlorierten Kohlenwasserstoffen, die Eisen enthalten
ATE22877T1 (de) 1983-07-06 1986-11-15 Monsanto Co Verfahren zur herstellung von monoaddukten von olefinen und damit reagierfaehigen telogenen.
CA1244481A (en) 1984-05-24 1988-11-08 Angelo J. Magistro Catalytic dehydrohalogenation process
JPH0821984B2 (ja) * 1988-08-09 1996-03-04 松下電器産業株式会社 集合住宅電話システム
US6187978B1 (en) 1999-05-12 2001-02-13 Alliedsignal Inc. Continuous process for manufacturing halogenated compounds
US20040225166A1 (en) 2003-05-05 2004-11-11 Vulcan Chemicals A Business Group Of Vulcan Materials Company Method for producing 1,1,1,3-tetrachloropropane and other haloalkanes with iron catalyst
US20050049443A1 (en) 2003-08-28 2005-03-03 Vulcan Chemicals A Business Group Of Vulcan Materials Company Method for producing 1,1,1,3-tetrachloropropane and other haloalkanes using a copper catalyst
US8952208B2 (en) 2006-01-03 2015-02-10 Honeywell International Inc. Method for prolonging a catalyst's life during hydrofluorination
US9738577B2 (en) * 2006-10-11 2017-08-22 Honeywell International Inc. Process for the manufacture of 1,1,1,3,3-pentachloropropane
US8563789B2 (en) 2007-06-27 2013-10-22 Arkema Inc. Process for the manufacture of hydrofluoroolefins
US8846990B2 (en) 2007-07-06 2014-09-30 Honeywell International Inc. Process for producing 2,3,3,3-tetrafluoropropene
PL2687504T3 (pl) 2007-12-19 2016-04-29 Occidental Chem Co Sposoby wytwarzania chlorowanych węglowodorów
GB0806419D0 (en) 2008-04-09 2008-05-14 Ineos Fluor Holdings Ltd Process
US8987535B2 (en) 2008-11-19 2015-03-24 Arkema Inc. Process for the manufacture of hydrochlorofluoroolefins
JP2010248104A (ja) 2009-04-14 2010-11-04 Tokuyama Corp 1,1,1,2,3−ペンタクロロプロパンの製造方法
WO2010131766A2 (en) 2009-05-13 2010-11-18 Daikin Industries, Ltd. Process for preparing chlorine-containing fluorocarbon compound
KR100935113B1 (ko) 2009-06-26 2010-01-06 주식회사 평산 중공관 형상의 열처리물 급속 에어냉각장치
JP5532131B2 (ja) * 2009-11-27 2014-06-25 ダイキン工業株式会社 1,1,2,3−テトラクロロプロペンの製造方法
US8586804B2 (en) 2010-12-01 2013-11-19 E. I. Du Pont De Nemours And Company Synthesis of 1,1,3-trichloro-1-propene
ES2609975T3 (es) 2011-01-21 2017-04-25 Arkema France Procedimiento para la fabricación de 2,3,3,3-tetrafluoropropeno mediante fluoración en fase gaseosa de pentacloropropano
EP2766331B1 (de) * 2011-10-14 2021-01-06 Honeywell International, Inc. Verfahren zur herstellung von 2,3,3,3-tetrafluorpropen
WO2013086262A1 (en) 2011-12-09 2013-06-13 Dow Global Technologies, Llc Process for the production of chlorinated propanes
KR20140134651A (ko) 2012-02-10 2014-11-24 하이유 왕 2,3,3,3-테트라플루오로프로펜의 개선된 제조 방법
US8907147B2 (en) * 2013-02-04 2014-12-09 Honeywell International Inc. Synthesis of 1,1,2,3-tetrachloropropene
US9067858B2 (en) 2013-02-12 2015-06-30 Occidental Chemical Corporation Methods for recovering 1,1,1,2,3-pentachloropropane
US8889929B2 (en) 2013-02-19 2014-11-18 Honeywell International Inc. Process to make 1,1,2,3-tetrachloropropene from 1,1,3-trichloropropene and/or 3,3,3-trichloropropene
US8889927B2 (en) 2013-03-12 2014-11-18 Honeywell International Inc. Method to reduce the formation of high boiling compounds during the dehydrochlorination of 1,1,1,3-tetrachloropropane
US9663425B2 (en) * 2014-03-31 2017-05-30 Honeywell International Inc. Method to produce 1,1,2,3-tetrachloropropene with high yield

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0131560A1 (de) * 1983-07-06 1985-01-16 Monsanto Company Verfahren zur Herstellung von 1,1,2,3-Tetrachloropropen
US4535194A (en) * 1983-07-06 1985-08-13 Monsanto Co. Process for producing 1,1,2,3-tetrachloropropene
CN102405202A (zh) * 2009-04-23 2012-04-04 大金工业株式会社 制备2-氯-3,3,3-三氟丙烯的方法
CN102177116A (zh) * 2009-06-24 2011-09-07 株式会社德山 氯化烃的制备方法
JP2012056920A (ja) * 2010-09-13 2012-03-22 Tokuyama Corp クロロプロパンの製造方法
CN103717560A (zh) * 2011-07-26 2014-04-09 大金工业株式会社 用于制备2,3,3,3-四氟丙烯的方法
WO2014130436A1 (en) * 2013-02-19 2014-08-28 Honeywell International Inc. Methods for the dehydrochlorination of 1,1,1,3-tetrachloropropane to 1,1,3-trichloropeopene
CN105050989A (zh) * 2013-02-19 2015-11-11 霍尼韦尔国际公司 用于使1,1,1,3-四氯丙烷脱氯化氢为1,1,3-三氯丙烯的方法
CN104058925A (zh) * 2013-03-22 2014-09-24 中化蓝天集团有限公司 1,1,1,2,3-五氯丙烷的连续制备方法

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111712479A (zh) * 2018-03-07 2020-09-25 阿科玛法国公司 2,3,3,3-四氟丙烯的生产工艺
CN111757863A (zh) * 2018-03-07 2020-10-09 阿科玛法国公司 2-氯-3,3,3-三氟丙烯的生产工艺
CN111770908A (zh) * 2018-03-07 2020-10-13 阿科玛法国公司 2,3,3,3-四氟丙烯的生产工艺
CN112334436A (zh) * 2018-04-03 2021-02-05 蓝立方知识产权有限责任公司 使用吸收器-反应器组合生产卤化烷烃的方法
CN112384490A (zh) * 2018-07-09 2021-02-19 科慕埃弗西有限公司 用于整合式2,3,3,3-四氟丙烯制造工艺的组合物和方法
CN109232173A (zh) * 2018-07-26 2019-01-18 浙江巨化技术中心有限公司 一种1,1,1,2,3-五氯丙烷的连续制备方法
CN109232173B (zh) * 2018-07-26 2021-12-14 浙江巨化技术中心有限公司 一种1,1,1,2,3-五氯丙烷的连续制备方法
CN110511112A (zh) * 2019-08-16 2019-11-29 浙江巨化技术中心有限公司 一种1,1,2,3-四氯丙烯的制备方法
CN111604041A (zh) * 2020-06-18 2020-09-01 大连九信精细化工有限公司 一种γ-氧化铝改性催化剂、其制备方法及在合成1,1,3-三氯丙烯中的应用
CN111604041B (zh) * 2020-06-18 2023-04-07 大连九信精细化工有限公司 一种γ-氧化铝改性催化剂、其制备方法及在合成1,1,3-三氯丙烯中的应用

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TW202039406A (zh) 2020-11-01
US20180118641A1 (en) 2018-05-03
EP3207007B1 (de) 2021-12-15
JP7139393B2 (ja) 2022-09-20
WO2016058569A1 (en) 2016-04-21
US9840448B2 (en) 2017-12-12
TWI770558B (zh) 2022-07-11
WO2016058569A9 (en) 2016-06-30
JP2021006541A (ja) 2021-01-21
CZ309310B6 (cs) 2022-08-17
CZ2016126A3 (cs) 2016-08-10
JP7168321B2 (ja) 2022-11-09
TWI702202B (zh) 2020-08-21
JP2017532380A (ja) 2017-11-02
US10611707B2 (en) 2020-04-07
EP3207007A1 (de) 2017-08-23
US20160107956A1 (en) 2016-04-21
TW201619101A (zh) 2016-06-01

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