CN106868876A - 抗紫外线防泼水环保伞布的制作方法 - Google Patents

抗紫外线防泼水环保伞布的制作方法 Download PDF

Info

Publication number
CN106868876A
CN106868876A CN201710098332.1A CN201710098332A CN106868876A CN 106868876 A CN106868876 A CN 106868876A CN 201710098332 A CN201710098332 A CN 201710098332A CN 106868876 A CN106868876 A CN 106868876A
Authority
CN
China
Prior art keywords
spill resistant
uvioresistant
umbrella cloth
base fabric
drying
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710098332.1A
Other languages
English (en)
Inventor
张小玲
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CN201710098332.1A priority Critical patent/CN106868876A/zh
Publication of CN106868876A publication Critical patent/CN106868876A/zh
Pending legal-status Critical Current

Links

Classifications

    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/0002—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the substrate
    • D06N3/0015—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the substrate using fibres of specified chemical or physical nature, e.g. natural silk
    • D06N3/0036—Polyester fibres
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
    • D06M13/188—Monocarboxylic acids; Anhydrides, halides or salts thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
    • D06M13/207—Substituted carboxylic acids, e.g. by hydroxy or keto groups; Anhydrides, halides or salts thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/46—Compounds containing quaternary nitrogen atoms
    • D06M13/463—Compounds containing quaternary nitrogen atoms derived from monoamines
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/244—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of halogenated hydrocarbons
    • D06M15/256—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of halogenated hydrocarbons containing fluorine
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/53—Polyethers
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/0056—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the compounding ingredients of the macro-molecular coating
    • D06N3/0063—Inorganic compounding ingredients, e.g. metals, carbon fibres, Na2CO3, metal layers; Post-treatment with inorganic compounds
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/04—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/12—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins
    • D06N3/128—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins with silicon polymers
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/12—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins
    • D06N3/14—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins with polyurethanes
    • D06N3/142—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins with polyurethanes mixture of polyurethanes with other resins in the same layer
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16—Synthetic fibres, other than mineral fibres
    • D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M2101/32—Polyesters
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/10—Repellency against liquids
    • D06M2200/12—Hydrophobic properties
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/50—Modified hand or grip properties; Softening compositions
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N2209/00—Properties of the materials
    • D06N2209/10—Properties of the materials having mechanical properties
    • D06N2209/103—Resistant to mechanical forces, e.g. shock, impact, puncture, flexion, shear, compression, tear
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N2209/00—Properties of the materials
    • D06N2209/12—Permeability or impermeability properties
    • D06N2209/126—Permeability to liquids, absorption
    • D06N2209/128—Non-permeable
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N2209/00—Properties of the materials
    • D06N2209/16—Properties of the materials having other properties
    • D06N2209/1664—Releasability
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N2209/00—Properties of the materials
    • D06N2209/16—Properties of the materials having other properties
    • D06N2209/1678—Resistive to light or to UV

Landscapes

  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

本发明涉及一种抗紫外线防泼水环保伞布的制作方法，属于伞布技术领域。该制作方法包括步骤一，基布处理；步骤二，柔软整理；步骤三，一次烘干定型；步骤四，防泼水整理；步骤五，二次烘干定型；步骤六，防水抗紫外线处理，经干燥后即得所述抗紫外线防泼水环保伞布。本发明通过对涤纶基布进行柔软整理、一次烘干定型处理、防泼水整理、二次烘干定型及防水抗紫外线处理，尤其在柔软整理、防泼水整理及防水抗紫外线处理中配合相应的整理液及胶料，对涤纶基布进行特殊处理，使制得的涤纶伞布具有优异的抗紫外性、防水性和防泼水性；本发明在制作过程中使用环保助剂对涤纶基布进行处理，对人体和环境友好。

Description

抗紫外线防泼水环保伞布的制作方法
技术领域
本发明属于伞布技术领域，具体涉及一种抗紫外线防泼水环保伞布的制作方法。
背景技术
涤纶，又称聚酯纤维，具有强度高、弹性好、耐磨性好、耐腐蚀性佳等优点，涤纶的应用极为广泛，被广泛应用于服饰制造、日用品制造及工业制品的制造中。对涤纶基布进行后整理，以赋予其新的特殊功能，是目前改善涤纶面料性能常用的手段。
目前，涤纶因其较低的成本，在伞用面料中的应用较广，其质地较厚实，反光性较强，色彩鲜艳，通常会对涤纶面料进行后处理，将其用作伞布，晴雨两用伞布主要进行防水处理和防紫外线处理，以使涤纶面料具有较稳定的防紫外线性能和防水性能，防水和防紫外线处理主要有两种方式：功能性处理液浸轧处理和涂层处理。但是由于涤纶面料自身具有易出现折痕的特点，折痕不易还原，涂覆在其上的涂层附着力较差，容易脱落，因此现有的涤纶伞布的抗紫外线效果不佳，同时，由于目前对伞用涤纶面料的防水处理不成熟，导致涤纶伞布的防水效果较差；此外防泼水也是雨伞布的一个重要指标，一般还会对雨伞用涤纶面料进行防泼水处理，但其防泼水效果仍较其他较高档次的伞用面料差。
针对上述不足，申请人对涤纶基布的后整理工艺进行了研究，以期得到一种具有优异抗紫外线性能，并同时具有优异防泼水和防水性能的晴雨两用环保伞布。
发明内容
本发明的目的是为了解决现有技术的不足，而提供一种抗紫外线防泼水环保伞布的制作方法，该方法制作的涤纶伞布具有优异的抗紫外线性、极强的防水性和防泼水性。
本发明采用如下技术方案：
抗紫外线防泼水环保伞布的制作方法，包括如下步骤：
步骤一，基布处理：取涤纶基布，除去基布表面的灰尘杂质，水洗后烘干定型；
步骤二，柔软整理：缸内入水，按照水量计，将12.5-14.8g/L柔软剂、30-35g/L乙醇加入水中，以2℃/min的速率升温至50-60℃，搅拌均匀后，再加入4-6g/L柠檬酸，恒温搅拌均匀，冷却，将步骤一所得涤纶基布浸入其中，一浸一轧，轧余率80％；
步骤三，一次烘干定型：将步骤二经过柔软整理的涤纶基布烘干定型；
步骤四，防泼水整理：缸内入水，按照水量计，依次加入50-70g/L全氟防泼水剂、5-9g/L乙酸和15-20g/L脂肪醇聚氧乙烯醚，混合搅拌均匀，将步骤三经过烘干定型的涤纶基布以20-30m/min的车速入缸，二浸二轧，轧余率75％；
步骤五，二次烘干定型：将步骤四经过防泼水整理的涤纶基布烘干定型；
步骤六，防水抗紫外线处理：按照质量份数计，将60-80份水性聚氨酯乳液、5-9份水性有机硅树脂乳液(可通过东莞俊怡化工科技有限公司购买，型号JY8452)加入100-150份水中，搅拌均匀，再依次加入10-15份防水剂、12-14份聚乙烯吡咯烷酮，搅拌均匀，得混合液Ⅰ，将4-8份紫外线吸收剂加入10-15份丁酮中，搅拌均匀，得混合液Ⅱ，将混合液Ⅱ加入混合液Ⅰ中，升温至40-50℃，加入5-8份纳米二氧化钛，搅拌均匀，自然冷却，得防水抗紫外线胶，将防水抗紫外线胶刮涂于经过二次烘干定型的涤纶基布的表面，湿涂量20-30g/m2，干燥后即得所述抗紫外线防泼水环保伞布。
更进一步地，步骤二中所述柔软剂为十六烷基磺基甜菜碱(cas号：2281-11-0)。
更进一步地，步骤三中所述一次烘干定型时的温度为120-135℃，车速为30-40m/min，时间1-3min。
更进一步地，步骤四中所述全氟防泼水剂为iHeir-666水性全氟防泼水剂。
更进一步地，步骤五中所述二次烘干定型时的温度为160-170℃，车速为10-20m/min，时间为60-70s。
更进一步地，步骤六中所述紫外线吸收剂为苯并三唑类紫外线吸收剂。
更进一步地，步骤六中所述紫外线吸收剂为紫外线吸收剂HTUV160(可通过赫特集团购买得到)。
更进一步地，步骤六中所述防水剂为十六烷基三乙氧基硅烷(cas号：16415-13-7)。
更进一步地，步骤二中所述搅拌的速度为200-300r/min，步骤四中所述搅拌的速度为200-300r/min，步骤五中所述搅拌的速度为100-200r/min。
本发明与现有技术相比，其有益效果为：
第一：本发明通过对涤纶基布进行柔软整理、一次烘干定型处理、防泼水整理、二次烘干定型及防水抗紫外线处理等工艺处理，尤其在柔软整理、防泼水整理及防水抗紫外线处理中配合相应的整理液及胶料，对涤纶基布进行特殊处理，使制得的涤纶伞布具有优异的抗紫外性、防水性和防泼水性；
第二：本发明通过对涤纶基布进行柔软整理和防泼水整理，有效提升了涤纶基布与防水抗紫外线胶层的附着力，不会出现胶层脱落现象，保证了伞布的防水性和抗紫外线性，同时，本发明得到的伞布的耐折性也得到了有效改善升；
第三：本发明在制作过程中使用环保助剂对涤纶基布进行处理，对人体和环境友好，同时本发明的制作方法简便易行，应用前景广阔。
具体实施方式
下面结合实施例对本发明作进一步的详细描述。
本领域技术人员将会理解，下列实施例仅用于说明本发明，而不应视为限定本发明的范围。本发明中所用试剂原料，如无特别说明，均可通过购买得到。
实施例1
抗紫外线防泼水环保伞布的制作方法，包括如下步骤：
步骤一，基布处理：取涤纶基布，除去基布表面的灰尘杂质，水洗后烘干定型；
步骤二，柔软整理：缸内入水，按照水量计，将13.2g/L十六烷基磺基甜菜碱、33g/L乙醇加入水中，以2℃/min的速率升温至55℃，于250r/min下搅拌均匀后，再加入5g/L柠檬酸，于250r/min下恒温搅拌均匀，冷却，将步骤一所得涤纶基布浸入其中，一浸一轧，轧余率80％；
步骤三，一次烘干定型：将步骤二经过柔软整理的涤纶基布于温度130℃，车速35m/min下烘干定型2min；
步骤四，防泼水整理：缸内入水，按照水量计，依次加入60g/L iHeir-666水性全氟防泼水剂、7g/L乙酸和18g/L脂肪醇聚氧乙烯醚，于250r/min下混合搅拌均匀，将步骤三经过烘干定型的涤纶基布以25m/min的车速入缸，二浸二轧，轧余率75％；
步骤五，二次烘干定型：将步骤四经过防泼水整理的涤纶基布于温度165℃，车速15m/min下时间烘干定型65s；
步骤六，防水抗紫外线处理：按照质量份数计，将70份水性聚氨酯乳液、7份水性有机硅树脂乳液加入125份水中，于150r/min下搅拌均匀，再依次加入12份十六烷基三乙氧基硅烷、13份聚乙烯吡咯烷酮，于150r/min下搅拌均匀，得混合液Ⅰ，将6份紫外线吸收剂HTUV160加入12份丁酮中，于150r/mi n下搅拌均匀，得混合液Ⅱ，将混合液Ⅱ加入混合液Ⅰ中，升温至45℃，加入6.5份纳米二氧化钛，于150r/min下搅拌均匀，自然冷却，得防水抗紫外线胶，将防水抗紫外线胶刮涂于经过二次烘干定型的涤纶基布的表面，湿涂量25g/m2，干燥后即得所述抗紫外线防泼水环保伞布。
实施例2
抗紫外线防泼水环保伞布的制作方法，包括如下步骤：
步骤一，基布处理：取涤纶基布，除去基布表面的灰尘杂质，水洗后烘干定型；
步骤二，柔软整理：缸内入水，按照水量计，将12.5g/L十六烷基磺基甜菜碱、30g/L乙醇加入水中，以2℃/min的速率升温至50℃，于200r/min下搅拌均匀后，再加入4g/L柠檬酸，于200r/min下恒温搅拌均匀，冷却，将步骤一所得涤纶基布浸入其中，一浸一轧，轧余率80％；
步骤三，一次烘干定型：将步骤二经过柔软整理的涤纶基布于温度120℃，车速30m/min下烘干定型1min；
步骤四，防泼水整理：缸内入水，按照水量计，依次加入50g/L iHeir-666水性全氟防泼水剂、5g/L乙酸和15g/L脂肪醇聚氧乙烯醚，于200r/min下混合搅拌均匀，将步骤三经过烘干定型的涤纶基布以20m/min的车速入缸，二浸二轧，轧余率75％；
步骤五，二次烘干定型：将步骤四经过防泼水整理的涤纶基布于温度160℃，车速10m/min下时间烘干定型60s；
步骤六，防水抗紫外线处理：按照质量份数计，将60份水性聚氨酯乳液、5份水性有机硅树脂乳液加入100份水中，于100r/min下搅拌均匀，再依次加入10份十六烷基三乙氧基硅烷、12份聚乙烯吡咯烷酮，于100r/min下搅拌均匀，得混合液Ⅰ，将4份紫外线吸收剂HTUV160加入10份丁酮中，于100r/mi n下搅拌均匀，得混合液Ⅱ，将混合液Ⅱ加入混合液Ⅰ中，升温至40℃，加入5份纳米二氧化钛，于100r/min下搅拌均匀，自然冷却，得防水抗紫外线胶，将防水抗紫外线胶刮涂于经过二次烘干定型的涤纶基布的表面，湿涂量20g/m2，干燥后即得所述抗紫外线防泼水环保伞布。
实施例3
抗紫外线防泼水环保伞布的制作方法，包括如下步骤：
步骤一，基布处理：取涤纶基布，除去基布表面的灰尘杂质，水洗后烘干定型；
步骤二，柔软整理：缸内入水，按照水量计，将14.8g/L十六烷基磺基甜菜碱、35g/L乙醇加入水中，以2℃/min的速率升温至60℃，于300r/min下搅拌均匀后，再加入6g/L柠檬酸，于300r/min下恒温搅拌均匀，冷却，将步骤一所得涤纶基布浸入其中，一浸一轧，轧余率80％；
步骤三，一次烘干定型：将步骤二经过柔软整理的涤纶基布于温度135℃，车速40m/min下烘干定型3min；
步骤四，防泼水整理：缸内入水，按照水量计，依次加入70g/L iHeir-666水性全氟防泼水剂、9g/L乙酸和20g/L脂肪醇聚氧乙烯醚，于300r/min下混合搅拌均匀，将步骤三经过烘干定型的涤纶基布以30m/min的车速入缸，二浸二轧，轧余率75％；
步骤五，二次烘干定型：将步骤四经过防泼水整理的涤纶基布于温度170℃，车速20m/min下时间烘干定型70s；
步骤六，防水抗紫外线处理：按照质量份数计，将80份水性聚氨酯乳液、9份水性有机硅树脂乳液加入150份水中，于200r/min下搅拌均匀，再依次加入15份十六烷基三乙氧基硅烷、14份聚乙烯吡咯烷酮，于200r/min下搅拌均匀，得混合液Ⅰ，将8份紫外线吸收剂HTUV160加入15份丁酮中，于200r/mi n下搅拌均匀，得混合液Ⅱ，将混合液Ⅱ加入混合液Ⅰ中，升温至50℃，加入8份纳米二氧化钛，于200r/min下搅拌均匀，自然冷却，得防水抗紫外线胶，将防水抗紫外线胶刮涂于经过二次烘干定型的涤纶基布的表面，湿涂量30g/m2，干燥后即得所述抗紫外线防泼水环保伞布。
对照例1
该对照例与实施例1的区别为：涤纶基布未经过柔软整理，其余步骤相同。
对照例2
该对照例与实施例1的区别为：涤纶基布未经过防泼水整理，其余步骤相同。
对照例3
该对照例与实施例1的区别为：涤纶基布既未经过柔软整理，也未经过防泼水整理，其余步骤相同。
对照例4
以市售某品牌晴雨两用伞的伞布作为对照。
将本发明实施例1至3制得的伞布进行性能测试，同时测试对照例1至4的伞布的性能，并对胶层附着力进行测试，结果如下表1所示：
表1实施例1至3所得伞布及对照例1至4的伞布的性能测试结果
本行业的技术人员应该了解，本发明不受上述实施例的限制，上述实施例和说明书中描述的只是说明本发明的原理，在不脱离本发明精神和范围的前提下，本发明还会有各种变化和改进，这些变化和改进都落入要求保护的本发明范围内。本发明要求保护范围由所附的权利要求书及其等效物界定。

Claims (9)

1.抗紫外线防泼水环保伞布的制作方法，其特征在于：包括如下步骤：
步骤一，基布处理：取涤纶基布，除去基布表面的灰尘杂质，水洗后烘干定型；
步骤二，柔软整理：缸内入水，按照水量计，将12.5-14.8g/L柔软剂、30-35g/L乙醇加入水中，以2℃/min的速率升温至50-60℃，搅拌均匀后，再加入4-6g/L柠檬酸，恒温搅拌均匀，冷却，将步骤一所得涤纶基布浸入其中，一浸一轧，轧余率80%；
步骤三，一次烘干定型：将步骤二经过柔软整理的涤纶基布烘干定型；
步骤四，防泼水整理：缸内入水，按照水量计，依次加入50-70g/L全氟防泼水剂、5-9g/L乙酸和15-20g/L脂肪醇聚氧乙烯醚，混合搅拌均匀，将步骤三经过烘干定型的涤纶基布以20-30m/min的车速入缸，二浸二轧，轧余率75%；
步骤五，二次烘干定型：将步骤四经过防泼水整理的涤纶基布烘干定型；
步骤六，防水抗紫外线处理：按照质量份数计，将60-80份水性聚氨酯乳液、5-9份水性有机硅树脂乳液加入100-150份水中，搅拌均匀，再依次加入10-15份防水剂、12-14份聚乙烯吡咯烷酮，搅拌均匀，得混合液Ⅰ，将4-8份紫外线吸收剂加入10-15份丁酮中，搅拌均匀，得混合液Ⅱ，将混合液Ⅱ加入混合液Ⅰ中，升温至40-50℃，加入5-8份纳米二氧化钛，搅拌均匀，自然冷却，得防水抗紫外线胶，将防水抗紫外线胶刮涂于经过二次烘干定型的涤纶基布的表面，湿涂量20-30g/m2，干燥后即得所述抗紫外线防泼水环保伞布。
2.根据权利要求1所述的抗紫外线防泼水环保伞布的制作方法，其特征在于：步骤二中所述柔软剂为十六烷基磺基甜菜碱。
3.根据权利要求1所述的抗紫外线防泼水环保伞布的制作方法，其特征在于：步骤三中所述一次烘干定型时的温度为120-135℃，车速为30-40m/min，时间1-3min。
4.根据权利要求1所述的抗紫外线防泼水环保伞布的制作方法，其特征在于：步骤四中所述全氟防泼水剂为 iHeir-666水性全氟防泼水剂。
5.根据权利要求1所述的抗紫外线防泼水环保伞布的制作方法，其特征在于：步骤五中所述二次烘干定型时的温度为160-170℃，车速为10-20m/min，时间为60-70s。
6.根据权利要求1所述的抗紫外线防泼水环保伞布的制作方法，其特征在于：步骤六中所述紫外线吸收剂为苯并三唑类紫外线吸收剂。
7.根据权利要求6所述的抗紫外线防泼水环保伞布的制作方法，其特征在于：步骤六中所述紫外线吸收剂为紫外线吸收剂HTUV160。
8.根据权利要求1所述的抗紫外线防泼水环保伞布的制作方法，其特征在于：步骤六中所述防水剂为十六烷基三乙氧基硅烷。
9.根据权利要求1至8任一项所述的抗紫外线防泼水环保伞布的制作方法，其特征在于：步骤二中所述搅拌的速度为200-300r/min，步骤四中所述搅拌的速度为200-300r/min，步骤五中所述搅拌的速度为100-200r/min。
CN201710098332.1A 2017-02-22 2017-02-22 抗紫外线防泼水环保伞布的制作方法 Pending CN106868876A (zh)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710098332.1A CN106868876A (zh) 2017-02-22 2017-02-22 抗紫外线防泼水环保伞布的制作方法

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710098332.1A CN106868876A (zh) 2017-02-22 2017-02-22 抗紫外线防泼水环保伞布的制作方法

Publications (1)

Publication Number Publication Date
CN106868876A true CN106868876A (zh) 2017-06-20

Family

ID=59168635

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710098332.1A Pending CN106868876A (zh) 2017-02-22 2017-02-22 抗紫外线防泼水环保伞布的制作方法

Country Status (1)

Country Link
CN (1) CN106868876A (zh)

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107217495A (zh) * 2017-07-24 2017-09-29 安徽柏拉图涂层织物有限公司 一种中空尼龙涤纶混纺轻量化推拉篷涂层布的制备方法
CN107336482A (zh) * 2017-06-24 2017-11-10 嘉兴欣业纺织科技有限公司 一种复合牛皮布的生产工艺
CN107354763A (zh) * 2017-07-24 2017-11-17 吴江园达特种纺织整理技术有限公司 一种遮阳布涂料涂覆织物的方法
CN107558231A (zh) * 2017-10-17 2018-01-09 苏州雨维斯纺织纤维有限公司 一种伞布及其制造方法
CN107904961A (zh) * 2017-11-01 2018-04-13 浙江圣山科纺有限公司 一种涤塔夫耐撕伞面布
CN109537283A (zh) * 2018-11-08 2019-03-29 湖州织里瑞茜服饰有限公司 一种抗菌、防过敏纺织面料及其制备工艺
CN111005208A (zh) * 2019-12-30 2020-04-14 无锡太平针织有限公司 高阻隔性纤维制品制作方法
CN111118934A (zh) * 2019-12-31 2020-05-08 石狮市锦祥漂染有限公司 抗紫外线涤纶面料的制作方法
CN113152110A (zh) * 2021-05-18 2021-07-23 广东欧美斯家具有限公司 一种绿色环保沙发家具用聚氨酯合成革及其制备方法
CN113914106A (zh) * 2021-10-19 2022-01-11 浙江亦阳新材料有限公司 一种抗紫外线防水抗静电的帐篷材料及制备方法
CN114193866A (zh) * 2021-12-07 2022-03-18 常州雅美特窗饰股份有限公司 一种提高抗菌防紫外线型复合窗帘面料耐黄变性能的方法

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1940174A (zh) * 2005-09-28 2007-04-04 东丽纤维研究所（中国）有限公司 高透湿高防水涂层织物的制造方法
CN104727151A (zh) * 2015-04-01 2015-06-24 丹东优耐特纺织品有限公司 纺织品用防水、透气、抗菌、抗紫外线、补强涂层胶及制备方法
CN105401443A (zh) * 2015-12-16 2016-03-16 晋江市龙兴隆染织实业有限公司 耐寒抗紫外线面料及其制作工艺
CN105401445A (zh) * 2015-10-31 2016-03-16 泉州迈特富纺织科技有限公司 防水防油阻燃透气芳纶面料及其制作方法
CN105442326A (zh) * 2015-12-29 2016-03-30 陕西科技大学 一种纳米复合抗紫外有机涂层整理剂及其制备方法

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1940174A (zh) * 2005-09-28 2007-04-04 东丽纤维研究所（中国）有限公司 高透湿高防水涂层织物的制造方法
CN104727151A (zh) * 2015-04-01 2015-06-24 丹东优耐特纺织品有限公司 纺织品用防水、透气、抗菌、抗紫外线、补强涂层胶及制备方法
CN105401445A (zh) * 2015-10-31 2016-03-16 泉州迈特富纺织科技有限公司 防水防油阻燃透气芳纶面料及其制作方法
CN105401443A (zh) * 2015-12-16 2016-03-16 晋江市龙兴隆染织实业有限公司 耐寒抗紫外线面料及其制作工艺
CN105442326A (zh) * 2015-12-29 2016-03-30 陕西科技大学 一种纳米复合抗紫外有机涂层整理剂及其制备方法

Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107336482A (zh) * 2017-06-24 2017-11-10 嘉兴欣业纺织科技有限公司 一种复合牛皮布的生产工艺
CN107217495A (zh) * 2017-07-24 2017-09-29 安徽柏拉图涂层织物有限公司 一种中空尼龙涤纶混纺轻量化推拉篷涂层布的制备方法
CN107354763A (zh) * 2017-07-24 2017-11-17 吴江园达特种纺织整理技术有限公司 一种遮阳布涂料涂覆织物的方法
CN107558231A (zh) * 2017-10-17 2018-01-09 苏州雨维斯纺织纤维有限公司 一种伞布及其制造方法
CN107904961A (zh) * 2017-11-01 2018-04-13 浙江圣山科纺有限公司 一种涤塔夫耐撕伞面布
CN109537283A (zh) * 2018-11-08 2019-03-29 湖州织里瑞茜服饰有限公司 一种抗菌、防过敏纺织面料及其制备工艺
CN111005208A (zh) * 2019-12-30 2020-04-14 无锡太平针织有限公司 高阻隔性纤维制品制作方法
CN111118934A (zh) * 2019-12-31 2020-05-08 石狮市锦祥漂染有限公司 抗紫外线涤纶面料的制作方法
CN111118934B (zh) * 2019-12-31 2022-09-20 石狮市锦祥漂染有限公司 抗紫外线涤纶面料的制作方法
CN113152110A (zh) * 2021-05-18 2021-07-23 广东欧美斯家具有限公司 一种绿色环保沙发家具用聚氨酯合成革及其制备方法
CN113914106A (zh) * 2021-10-19 2022-01-11 浙江亦阳新材料有限公司 一种抗紫外线防水抗静电的帐篷材料及制备方法
CN114193866A (zh) * 2021-12-07 2022-03-18 常州雅美特窗饰股份有限公司 一种提高抗菌防紫外线型复合窗帘面料耐黄变性能的方法

Similar Documents

Publication Publication Date Title
CN106868876A (zh) 抗紫外线防泼水环保伞布的制作方法
CN102628211B (zh) 超细涤纶织物染整加工工艺
CN106521986B (zh) 一种水性双面绒面超纤pu合成革及其制备方法
CN105155297B (zh) 一种水性聚氨酯含浸超细纤维合成革贝斯的制备方法
CN107236833B (zh) 二层双色蜡感裂纹皮的制作方法
CN106756967A (zh) 一种无铬钝化剂及对铝或铝合金表面进行钝化的方法
CN107489046B (zh) 一种涤纶织物的染整工艺
CN109137550A (zh) 一种高耐水压高撕裂的pu涂层面料制作工艺
CN105671988B (zh) 一种仿干羊皮聚氨酯沙发革的制备方法
CN109112846B (zh) 一种高强度耐磨性镀膜pvc人造革
CN105133368A (zh) 一种水性聚氨酯超细纤维合成革沙发革直涂工艺
CN100547154C (zh) 涤纶纤维毛绒布的印花拔染工艺
CN108411651A (zh) 一种烫金用浆料及其制备方法和用途
CN110485166B (zh) 一种有机硅乳液增深手感整理剂及制备方法、应用
CN106752831A (zh) 一种用于电力金具防腐的复合有机硅改性聚氨酯水性涂料及其制备方法
CN113402960A (zh) 氧化石墨烯改性木器水性抗菌型聚氨酯涂料及制备工艺
CN101581056B (zh) 金属充皮纸的生产方法
CN107841733A (zh) 一种拉链齿牙的发灰色料、灰色链牙的制作方法及灰色链牙拉链
CN110952337A (zh) 一种抗老化耐水解pu合成革面料及其制备方法
CN110670355A (zh) 一种婚纱晚礼服免烫防皱整理工艺
CN106884346B (zh) 涂料仿活性印花布料的制作工艺
KR20010046156A (ko) 버니시드피혁 가공방법
CN111893771B (zh) 一种羊毛织物的防毡缩整理方法
CN107723393A (zh) 一种用于皮具生产的皮革原料用的高品质雾面处理剂
CN108624723A (zh) 一种汽车皮革生产工艺

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20170620

WD01 Invention patent application deemed withdrawn after publication