CN111118934B - 抗紫外线涤纶面料的制作方法 - Google Patents

抗紫外线涤纶面料的制作方法 Download PDF

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CN111118934B
CN111118934B CN201911413889.5A CN201911413889A CN111118934B CN 111118934 B CN111118934 B CN 111118934B CN 201911413889 A CN201911413889 A CN 201911413889A CN 111118934 B CN111118934 B CN 111118934B
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CN111118934A (zh
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邱煌艺
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Fujian Shishi Jinxiang Dyeing Co ltd
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Abstract

本发明公开了一种抗紫外线涤纶面料的制作方法，属于面料技术领域。本发明的抗紫外线涤纶面料的制作方法包括如下步骤：退浆、水洗、染色、后处理，其中，后处理包括柔软处理、固色、烘干定型和包装。制得的抗紫外线涤纶面料具有优异的抗紫外线性能。

Description

抗紫外线涤纶面料的制作方法
技术领域
本发明属于面料技术领域，具体涉及一种抗紫外线涤纶面料的制作方法。
背景技术
随着工业的高度发展，越来越多的高新科技产品问世，然而，工业发展过程中，产生了大量不可避免的废气，且随着人们生活水平的提高，汽车数量越来越多，尾气排放量越来越大，以上种种原因，导致全球气候的恶性变化，其中，臭氧空洞的出现，臭氧层稀薄，紫外线照射强度越来越大，其所带来的危害可想而知。
在户外活动的人越来越注意防晒，各种防晒品齐上阵，而服装是保护皮肤面积最大的防晒品，而抗紫外线面料也就应运而生，而如何提高面料的抗紫外线性能是亟需解决的问题。
发明内容
本发明的目的在于克服现有技术的不足，提供一种具有抗紫外线性能，柔软度高的抗紫外线涤纶面料。
本发明采用如下技术方案：
抗紫外线涤纶面料的制作方法包括如下步骤：退浆、水洗、染色、后处理，其中，后处理包括柔软处理、固色、烘干定型和包装。
抗紫外线涤纶面料的制作方法，具体步骤如下：
步骤一、退浆：
将涤纶面料进行退浆处理，得退浆面料，退浆过程中加入了退浆助剂，退浆温度为80～95℃；
步骤二、水洗：
将步骤一所得退浆面料进行水洗，得水洗面料，水洗温度为60～70℃，水洗时间为40～50min；
步骤三、染色：
将步骤二所得水洗面料进行染色，得染色面料，所述染色过程时添加了染色助剂，所述染色时先升温至60～70℃，然后以1～1.2℃/min升温速率，升温至110～125℃，保温30～60min，然后1～1.2℃/min降温至60～70℃；
步骤四、柔软处理：
采用柔软剂对步骤三所得染料面料进行柔软处理，得柔软面料；
步骤五、烘干定型：
采用定型剂对步骤四所得柔软面料进行定型处理，并进行烘干，经包装后得抗紫外线面料。
进一步的，步骤一所述退浆助剂包括按照水量计的如下组分：亚溴酸钠8～11g/L，脂肪醇聚氧乙烯醚13～15g/L。
进一步的，步骤二所述水洗过程中加入按照水量计的如下组分：果胶酶1～3g/L和异构醇聚氧乙烯醚2～3g/L。
进一步的，步骤三所述染色助剂包括按照水量计的如下组分：冰醋酸2～3g/，元明粉4～6g/，碳酸二甲酯8～11g/，二丁基二硫代氨基甲酸镍4～7g/L。
进一步的，步骤五所述定型过程中，加入了按照水量计的如下定型助剂：邻苯二甲酸二丁酯11～16g/L，聚乙烯吡咯烷酮4～8g/L，硫代乙酰胺11～13g/L，脂肪酰二乙醇胺7～8g/L，7～21g/L抗紫外线整理剂DM-30911。
本发明与现有技术相比，具有以下有益效果：
第一、本发明的在退浆过程中，采用具有退浆性能的亚溴酸钠，采用脂肪醇聚氧乙烯醚作为表面活性剂，提高退浆效果，从而提高染色效率，提高色牢度；
第二、在进行染色前，先通过果胶酶对面料进行清洗，通过异构醇聚氧乙烯醚作为渗透剂，促进果胶酶对面料的酶解效果，进一步去除面料杂质，而下一步的染色做好充分准备；
第三、有了前面几个对面料的处理，在染色过程中采用碳酸二甲酯作为表面活性剂，二丁基二硫代氨基甲酸镍作为光稳定剂，同时加入冰醋酸和元明粉，进一步提高染色效果，制得的面料色牢度高，且添加了二丁基二硫代氨基甲酸镍，有助于提高光照色牢度；
第四、定型过程中，采用聚乙烯吡咯烷酮作为表面活性剂，以脂肪酰二乙醇胺作为润滑剂，配合具有柔软效果的邻苯二甲酸二丁酯和抗紫外线整理剂DM-30911，提高面料的抗紫外线性能，并通过添加硫代乙酰胺，进一步提高面料的色牢度，起到固色效果。
具体实施方式
本发明所使用的的原料均为市售品。
实施例1
抗紫外线涤纶面料的制作方法，包括如下步骤：退浆、水洗、染色、后处理，其中，后处理包括柔软处理、固色、烘干定型和包装。
抗紫外线涤纶面料的制作方法的具体步骤如下：
步骤一、退浆：
将涤纶面料进行退浆处理，得退浆面料，退浆过程中加入了退浆助剂，所述退浆助剂包括按照水量计的如下组分：亚溴酸钠8g/L，脂肪醇聚氧乙烯醚13g/L，退浆温度为80℃；
步骤二、水洗：
将步骤一所得退浆面料进行水洗，得水洗面料，所述水洗过程中加入按照水量计的如下组分：果胶酶1g/L和异构醇聚氧乙烯醚2g/L，水洗温度为60℃，水洗时间为40min；
步骤三、染色：
将步骤二所得水洗面料进行染色，得染色面料，所述染色过程时添加了染色助剂，所述染色时先升温至60℃，然后以1℃/min升温速率，升温至110℃，保温30min，然后1℃/min降温至60℃；
所述染色助剂包括按照水量计的如下组分：冰醋酸2g/，元明粉4g/，碳酸二甲酯8g/，二丁基二硫代氨基甲酸镍4g/L；
步骤四、柔软处理：
采用柔软剂对步骤三所得染料面料进行柔软处理，得柔软面料；
步骤五、烘干定型：
采用定型剂对步骤四所得柔软面料进行定型处理，所述定型过程中，加入了按照水量计的如下定型助剂：邻苯二甲酸二丁酯11g/L，聚乙烯吡咯烷酮4g/L，硫代乙酰胺11g/L，脂肪酰二乙醇胺7g/L，7g/L抗紫外线整理剂DM-30911；之后进行烘干，经包装后得抗紫外线面料。
实施例2
抗紫外线涤纶面料的制作方法，包括如下步骤：退浆、水洗、染色、后处理，其中，后处理包括柔软处理、固色、烘干定型和包装。
抗紫外线涤纶面料的制作方法的具体步骤如下：
步骤一、退浆：
将涤纶面料进行退浆处理，得退浆面料，退浆过程中加入了退浆助剂，所述退浆助剂包括按照水量计的如下组分：亚溴酸钠9g/L，脂肪醇聚氧乙烯醚14g/L，退浆温度为85℃；
步骤二、水洗：
将步骤一所得退浆面料进行水洗，得水洗面料，所述水洗过程中加入按照水量计的如下组分：果胶酶2g/L和异构醇聚氧乙烯醚3g/L，水洗温度为65℃，水洗时间为45min；
步骤三、染色：
将步骤二所得水洗面料进行染色，得染色面料，所述染色过程时添加了染色助剂，所述染色时先升温至65℃，然后以1.1℃/min升温速率，升温至115℃，保温40min，然后1.1℃/min降温至65℃；
所述染色助剂包括按照水量计的如下组分：冰醋酸3g/，元明粉5g/，碳酸二甲酯9g/，二丁基二硫代氨基甲酸镍5g/L；
步骤四、柔软处理：
采用柔软剂对步骤三所得染料面料进行柔软处理，得柔软面料；
步骤五、烘干定型：
采用定型剂对步骤四所得柔软面料进行定型处理，所述定型过程中，加入了按照水量计的如下定型助剂：邻苯二甲酸二丁酯12g/L，聚乙烯吡咯烷酮5g/L，硫代乙酰胺12g/L，脂肪酰二乙醇胺8g/L，15g/L抗紫外线整理剂DM-30911，之后进行烘干，经包装后得抗紫外线面料。
实施例3
抗紫外线涤纶面料的制作方法，包括如下步骤：退浆、水洗、染色、后处理，其中，后处理包括柔软处理、固色、烘干定型和包装。
抗紫外线涤纶面料的制作方法的具体步骤如下：
步骤一、退浆：
将涤纶面料进行退浆处理，得退浆面料，退浆过程中加入了退浆助剂，所述退浆助剂包括按照水量计的如下组分：亚溴酸钠10g/L，脂肪醇聚氧乙烯醚15g/L，退浆温度为90℃；
步骤二、水洗：
将步骤一所得退浆面料进行水洗，得水洗面料，所述水洗过程中加入按照水量计的如下组分：果胶酶2g/L和异构醇聚氧乙烯醚3g/L，水洗温度为65℃，水洗时间为45min；
步骤三、染色：
将步骤二所得水洗面料进行染色，得染色面料，所述染色过程时添加了染色助剂，所述染色时先升温至65℃，然后以1.2℃/min升温速率，升温至120℃，保温50min，然后1.2℃/min降温至65℃；
所述染色助剂包括按照水量计的如下组分：冰醋酸3g/，元明粉4g/，碳酸二甲酯8g/，二丁基二硫代氨基甲酸镍6g/L；
步骤四、柔软处理：
采用柔软剂对步骤三所得染料面料进行柔软处理，得柔软面料；
步骤五、烘干定型：
采用定型剂对步骤四所得柔软面料进行定型处理，所述定型过程中，加入了按照水量计的如下定型助剂：邻苯二甲酸二丁酯14g/L，聚乙烯吡咯烷酮6g/L，硫代乙酰胺13g/L，脂肪酰二乙醇胺7g/L，17g/L抗紫外线整理剂DM-30911，之后进行烘干，经包装后得抗紫外线面料。
实施例4
抗紫外线涤纶面料的制作方法，包括如下步骤：退浆、水洗、染色、后处理，其中，后处理包括柔软处理、固色、烘干定型和包装。
抗紫外线涤纶面料的制作方法的具体步骤如下：
步骤一、退浆：
将涤纶面料进行退浆处理，得退浆面料，退浆过程中加入了退浆助剂，所述退浆助剂包括按照水量计的如下组分：亚溴酸钠11g/L，脂肪醇聚氧乙烯醚15g/L，退浆温度为95℃；
步骤二、水洗：
将步骤一所得退浆面料进行水洗，得水洗面料，所述水洗过程中加入按照水量计的如下组分：果胶酶3g/L和异构醇聚氧乙烯醚3g/L，水洗温度为70℃，水洗时间为50min；
步骤三、染色：
将步骤二所得水洗面料进行染色，得染色面料，所述染色过程时添加了染色助剂，所述染色时先升温至70℃，然后以1.2℃/min升温速率，升温至125℃，保温60min，然后1.2℃/min降温至70℃；
所述染色助剂包括按照水量计的如下组分：冰醋酸3g/，元明粉6g/，碳酸二甲酯11g/，二丁基二硫代氨基甲酸镍7g/L；
步骤四、柔软处理：
采用柔软剂对步骤三所得染料面料进行柔软处理，得柔软面料；
步骤五、烘干定型：
采用定型剂对步骤四所得柔软面料进行定型处理，所述定型过程中，加入了按照水量计的如下定型助剂：邻苯二甲酸二丁酯16g/L，聚乙烯吡咯烷酮8g/L，硫代乙酰胺13g/L，脂肪酰二乙醇胺8g/L，21g/L抗紫外线整理剂DM-30911；之后进行烘干，经包装后得抗紫外线面料。
表1：实施例1～4及所得的抗紫外线面料的检测结果
Figure BDA0002350686900000071
从表1中可知，实施例1～4制得的抗紫外线面料具有较高的UPF值，UVA透过率小，具有优异的抗紫外线性能，其光照色牢度达到4级，具有优异的色牢度。
本行业的技术人员应该了解，本发明不受上述实施例的限制，上述实施例和说明书中描述的只是说明本发明的原理，在不脱离本发明精神和范围的前提下，本发明还会有各种变化和改进，这些变化和改进都落入要求保护的本发明范围内。本发明要求保护范围由所附的权利要求书及其等效物界定。

Claims (1)

1.抗紫外线涤纶面料的制作方法，其特征在于，包括如下步骤：退浆、水洗、染色、后处理，其中，后处理包括柔软处理、固色、烘干定型和包装；
具体步骤如下：
步骤一、退浆：
将涤纶面料进行退浆处理，得退浆面料，退浆过程中加入了退浆助剂，退浆温度为80~95℃；
所述退浆助剂包括按照水量计的如下组分：亚溴酸钠8~11g/L，脂肪醇聚氧乙烯醚13~15g/L；
步骤二、水洗：
将步骤一所得退浆面料进行水洗，得水洗面料，水洗温度为60~70℃，水洗时间为40~50min；
所述水洗过程中加入按照水量计的如下组分：果胶酶1~3g/L和异构醇聚氧乙烯醚2~3g/L；
步骤三、染色：
将步骤二所得水洗面料进行染色，得染色面料，所述染色过程时添加了染色助剂，所述染色时先升温至60~70℃，然后以1~1.2℃/min升温速率，升温至110~125℃，保温30~60min，然后1~1.2℃/min降温至60~70℃；
所述染色助剂包括按照水量计的如下组分：冰醋酸2~3 g/，元明粉4~6 g/，碳酸二甲酯8~11 g/，二丁基二硫代氨基甲酸镍4~7g/L；
步骤四、柔软处理：
采用柔软剂对步骤三所得染料面料进行柔软处理，得柔软面料；
步骤五、烘干定型：
采用定型剂对步骤四所得柔软面料进行定型处理，并进行烘干，经包装后得抗紫外线面料；
所述定型过程中，加入了按照水量计的如下定型助剂：邻苯二甲酸二丁酯11~16 g/L，聚乙烯吡咯烷酮4~8 g/L，硫代乙酰胺11~13 g/L，脂肪酰二乙醇胺7~8 g/L，7~21g/L抗紫外线整理剂DM-30911。
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