CN1068600C - 由膦酰基甲基亚氨基二乙酸合成膦酰基甲基甘氨酸的简易方法 - Google Patents

由膦酰基甲基亚氨基二乙酸合成膦酰基甲基甘氨酸的简易方法 Download PDF

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Publication number
CN1068600C
CN1068600C CN96195765A CN96195765A CN1068600C CN 1068600 C CN1068600 C CN 1068600C CN 96195765 A CN96195765 A CN 96195765A CN 96195765 A CN96195765 A CN 96195765A CN 1068600 C CN1068600 C CN 1068600C
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CN
China
Prior art keywords
oxygen concentration
oxygen
activated carbon
phosphonomethyliminodiacetic acid
salt
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
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CN96195765A
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English (en)
Chinese (zh)
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CN1191539A (zh
Inventor
B·A·库伦
B·A·帕克尔
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Hampshire Chemical Corp
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Hampshire Chemical Corp
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Publication of CN1191539A publication Critical patent/CN1191539A/zh
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
    • C07F9/3804—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)] not used, see subgroups
    • C07F9/3808—Acyclic saturated acids which can have further substituents on alkyl
    • C07F9/3813—N-Phosphonomethylglycine; Salts or complexes thereof

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CN96195765A 1995-05-30 1996-04-17 由膦酰基甲基亚氨基二乙酸合成膦酰基甲基甘氨酸的简易方法 Expired - Fee Related CN1068600C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US08/453,003 1995-05-30
US08/453,003 US6365772B1 (en) 1995-05-30 1995-05-30 Facile synthesis of phosphonomethylglycine from phosphonomethyliminodiacetic acid

Publications (2)

Publication Number Publication Date
CN1191539A CN1191539A (zh) 1998-08-26
CN1068600C true CN1068600C (zh) 2001-07-18

Family

ID=23798842

Family Applications (1)

Application Number Title Priority Date Filing Date
CN96195765A Expired - Fee Related CN1068600C (zh) 1995-05-30 1996-04-17 由膦酰基甲基亚氨基二乙酸合成膦酰基甲基甘氨酸的简易方法

Country Status (12)

Country Link
US (1) US6365772B1 (enExample)
CN (1) CN1068600C (enExample)
AP (1) AP9701127A0 (enExample)
AR (1) AR002119A1 (enExample)
AU (1) AU698565B2 (enExample)
HU (1) HU218307B (enExample)
IN (1) IN185297B (enExample)
IS (1) IS4614A (enExample)
NZ (1) NZ306837A (enExample)
TW (1) TW323281B (enExample)
WO (1) WO1996038455A1 (enExample)
ZA (1) ZA963362B (enExample)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BR9907000A (pt) * 1998-09-08 2000-09-26 Hampshire Chemical Corp Sìntese de ácido fosfonometiliminodiacético com efluente reduzido
SK1042002A3 (en) 1999-07-23 2002-07-02 Basf Ag Method of producing glyphosate or a salt thereof
DE19938622C2 (de) * 1999-08-14 2002-10-02 Sueddeutsche Kalkstickstoff Verfahren zur Herstellung von N-(Phosphonomethyl)glycin
DE10007702A1 (de) * 2000-02-19 2001-08-23 Sueddeutsche Kalkstickstoff Verfahren zur Herstellung von N-(Phosphonomethyl)glycin
CN102250141B (zh) * 2000-05-22 2014-10-01 孟山都技术有限责任公司 制备n－(膦酰基甲基)甘氨酸化合物的反应系统
US6921834B2 (en) * 2002-05-22 2005-07-26 Dow Agrosciences Llc Continuous process for preparing N-phosphonomethyl glycine
WO2006096617A2 (en) 2005-03-04 2006-09-14 Monsanto Technology Llc Mitigating necrosis in transgenic glyphosate-tolerant cotton plants treated with herbicidal glyphosate formulations
BRPI0607713A2 (pt) * 2005-04-01 2009-09-22 Monsanto Technology Llc métodos para monitorar ou detectar a conversão do ácido n-(fosfonometil) iminodiacético para n-(fosfonometil)glicina ou outro intermediário para n-(fosfonometil)glicina no curso da oxidação catalìtica de ácido n-(fosfonometil)iminodiacético em um meio aquoso
CN101337977B (zh) * 2008-05-13 2011-09-14 浙江新安化工集团股份有限公司 一种含分子氧气体催化氧化合成草甘膦的终点控制方法
CN101481387B (zh) * 2008-11-27 2012-02-01 浙江新安化工集团股份有限公司 一种催化氧化合成草甘膦的制备方法

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3950402A (en) * 1972-05-31 1976-04-13 Monsanto Company Process for producing N-phosphonomethyl glycine
US3969398A (en) * 1974-05-01 1976-07-13 Monsanto Company Process for producing N-phosphonomethyl glycine

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4002672A (en) 1972-03-22 1977-01-11 Monsanto Company Process for producing N-phosphonomethyl glycine
US3954848A (en) 1972-05-31 1976-05-04 Monsanto Company Process for producing N-phosphonomethyl glycine
ES465139A1 (es) 1976-12-20 1978-10-01 Monsanto Co Un procedimiento para preparar una mono-o disal de n-fosfo- nometilglicina.
US4724103A (en) 1984-02-27 1988-02-09 Monsanto Company Process for preparing N,N-diacetic acid aminomethylenephosphonic acid
US4775498A (en) 1984-12-05 1988-10-04 Monsanto Company Process for preparing N,N-diacetic acid aminomethylenephosphonic acid
US4579689A (en) 1985-02-11 1986-04-01 Monsanto Company Oxidation with coated catalyst
US4582650A (en) 1985-02-11 1986-04-15 Monsanto Company Oxidation with encapsulated co-catalyst
US4696772A (en) 1985-02-28 1987-09-29 Monsanto Company Amine oxidation using carbon catalyst having oxides removed from surface
US4898972A (en) 1988-09-26 1990-02-06 Monsanto Company Process for producing N-phosphonomethylglycine

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3950402A (en) * 1972-05-31 1976-04-13 Monsanto Company Process for producing N-phosphonomethyl glycine
US3969398A (en) * 1974-05-01 1976-07-13 Monsanto Company Process for producing N-phosphonomethyl glycine

Also Published As

Publication number Publication date
US6365772B1 (en) 2002-04-02
HUP9802219A3 (en) 1999-03-01
WO1996038455A1 (en) 1996-12-05
AR002119A1 (es) 1998-01-07
AP9701127A0 (en) 1997-10-31
IN185297B (enExample) 2000-12-23
AU5551096A (en) 1996-12-18
TW323281B (enExample) 1997-12-21
HUP9802219A2 (hu) 1999-01-28
HU218307B (en) 2000-07-28
IS4614A (is) 1997-11-14
AU698565B2 (en) 1998-11-05
CN1191539A (zh) 1998-08-26
NZ306837A (en) 1998-11-25
ZA963362B (en) 1996-11-08

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