CN106821865A - A kind of anti-apolexis composition and its application - Google Patents
A kind of anti-apolexis composition and its application Download PDFInfo
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- CN106821865A CN106821865A CN201710187739.1A CN201710187739A CN106821865A CN 106821865 A CN106821865 A CN 106821865A CN 201710187739 A CN201710187739 A CN 201710187739A CN 106821865 A CN106821865 A CN 106821865A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/906—Zingiberaceae (Ginger family)
- A61K36/9062—Alpinia, e.g. red ginger or galangal
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/522—Antioxidants; Radical scavengers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/77—Perfumes having both deodorant and antibacterial properties
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/78—Enzyme modulators, e.g. Enzyme agonists
- A61K2800/782—Enzyme inhibitors; Enzyme antagonists
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Abstract
The present invention discloses a kind of anti-apolexis composition and its application, and anti-apolexis composition includes following components by weight：0.02~1.0 part of Alpinia galanga extract, 0.03~1.5 part of safflower extract, 0.05~2.0 part of dateplum persimmon extract；Alpinia galanga extract, safflower extract, the weight part ratio of dateplum persimmon extract is (3~8):(4.5~12):(9~16).Anti-apolexis composition of the present invention is naturally safe and non-stimulating, and obtained cosmetics have significant removing power to DPPH and refresh oneself and dispel cold to significantly inhibiting property of tyrosinase.
Description
Technical field
The present invention relates to cosmetic field, and in particular to a kind of anti-apolexis composition and its application.
Background technology
Aging is inevitable law of nature in life process, and skin is used as first barrier of human body, during skin
Moment is carved all in aging, aging, and its elasticity is slowly reduced, and thin down, it is more and more fragile and lax, what is given people is directly perceived
Impression is exactly wrinkle long.Skin aging typically has natural aging and light aging.The former refers mainly to age, by body
It is aging that such as heredity, gravity, endocrine and the immunologic function for existing can not resist that factor causes；The latter is mainly due to ultraviolet
Effect, accelerate the process of naturally-aged, and a series of environmental exposures such as climate change and environmental pollution are to the light of skin
It is aging also to have directly influence.The approach of anti-aging, mainly includes：Protect the skin from external environment stimulation；Scavenger-cell
Interior unnecessary free radical；Skin Cell is repaired and is supplemented the nutrients.Skin anti-aging is to prevent skin because the time elapses
There is the gradually function of property and organic moving back to sexually revise, show as preventing wrinkle, drying, play bits, lax and color spot.It is anti-ageing
Aging cosmetic is exactly to realize the cosmetics of senile-resistant efficacy, is one of important effect type cosmetics.
What present anti-aging cosmetics had has used the strong industry of inoxidizability to reach good anti-aging effects
Composition, instant effect in short-term, but for a long time using very big to harm；Some anti-aging cosmetics add vitamins antioxygen
Agent, but this kind of antioxidant less stable.The natural plant extracts that will have senile-resistant efficacy are made the group of good stability
Compound is added in cosmetics, assigns product good senile-resistant efficacy, is a trend of anti-aging product.
With the development and the raising of standard of living of society, requirement of the people to cosmetics also more and more higher is particularly produced
The security of product, it is desirable to which anti-aging is made up has good anti-aging effects, while being natural safe and non-stimulating.
The content of the invention
Based on this, it is an object of the invention to provide a kind of anti-apolexis composition, and face cream is applied it to, make face cream
Safety, effectively antagonizes free radical, delay skin aging.
The present invention is realized by following scheme：
A kind of anti-apolexis composition includes following components by weight：0.02~1.0 part of Alpinia galanga extract, safflower are carried
Take 0.03~1.5 part of thing, 0.05~2.0 part of dateplum persimmon extract, Alpinia galanga extract, safflower extract, dateplum persimmon extract
Weight part ratio is (3~8):(4.5~12):(9~16).The preparation method of the Alpinia galanga extract is comprised the following steps：
(1) Alpinia galanga is dried, crushed 40~60 mesh sieves, use petroleum ether degreasing 24h, volatilize petroleum ether；
(2) with ethanol as Extraction solvent, by solid-liquid ratio 1：(65~85), 70~90 DEG C of Extracting temperature extracts 5h, extract solution
20min is centrifuged in 3000r/min；
(3) to take and be concentrated under reduced pressure into paste through the supernatant after centrifugation in step (2).
The preparation method of the safflower extract is：By safflower drying, 40~60 mesh sieves were crushed, it is standby；Take safflower powder
End, adds ethanol, solid-liquid ratio 1：(10~30), fully soak 20~30min, are placed in 50 DEG C of water bath chaders, mechanical shaking extraction
2h, filtering, centrifuging and taking supernatant is concentrated into paste with rotavapor under vacuum.
The preparation method of the dateplum persimmon extract is：Dateplum persimmon is dried, powder is ground into, 60~90% ethanol are added, in
At 45 DEG C after 2~3h of ultrasonic extraction, supernatant is collected by centrifugation, residue is repeated to extract 1 time, supernatant is merged after centrifugation, with rotation
Turn evaporimeter concentration and remove ethanol.
The present invention also provides application of the plant composition with anti-senescence function in cosmetics are prepared, the cosmetics
It is whitening anti-aging face cream.
Whitening anti-aging face cream is made up of the raw material of following weight part ratio：Anti-apolexis composition of the present invention 1.0~4.5%；
Stearine/PEG-100 stearates 1.2-1.8%；Cetostearyl alcohol 1.8-2.2%；Saualane 2.5-3.5%；It is poly-
Dimethyl siloxane 1-3%；Caprylic/capric triglyceride 2-4%；Avocado oil 1-3%；Hydrogenated jojoba oil 1-3%；Oxybenzene first
Ester 0.1-0.2%；Nipasol 0.1-0.2%；Sodium Hyaluronate 0.01-0.04%；Glycerine 1-4%；Polyacrylamide 0.8-
1.5%；Polydimethyl siloxanes/polydimethy siloxanes alcohol 1.5-2%；Deionized water surplus.
The preparation method of the face cream is comprised the following steps：
(1) by stearine/PEG-100 stearates, cetostearyl alcohol, saualane, dimethyl silicone polymer, pungent
Acid/Triglyceride DDD, avocado oil, hydrogenated jojoba oil, polyacrylamide, polydimethyl siloxanes/polydimethy siloxanes
Alcohol, methyl hydroxybenzoate, Nipasol mixing put into oil phase pot heating stirring to 85 degree as A phases, and stirring and dissolving completely treat afterwards by insulation
With；
(2) Sodium Hyaluronate, glycerine, deionized water mixing are added to heating stirring in water phase pot and, to 85 degree, are stirred as B
Mix heat preservation for standby use after dissolving completely；
(3) emulsification pot is preheated to 60-65 degree, first be pumped into for B phases by 50 revs/min of mixing speed, then A phases are pumped into, and is stirred
Mix 30 minutes, temperature is maintained at 85 degree；
(4) 45 degree of plant compositions of addition anti-senescence function are cooled to, insulated and stirred 10 minutes is cooled to 40 degree and goes out
Material.
Part material to anti-apolexis composition of the present invention makees following introduction：
Dateplum persimmon extract：Contain the phenolic materials such as gallic acid, P- coumaric acids, syringic acid, myricetin, Quercetin and tannin
Matter, can effectively remove free radical, prevention lipid peroxidation and anti-malignant cell proliferation.
Alpinia galanga extract：Rich in big sorghum ginger essential oil, with broad-spectrum antimicrobial effect, can effectively suppress Gram-positive
Bacterium and the activity of Gram-negative bacteria.
Safflower extract：Rich in flavone compound, Flos Carthami volatile oil；Safflower total flavone is significantly inhibited to tyrosinase
Property, when safflower flavone concentration is 3mg/m L, inhibiting rate reaches 63.5%, has significant removing power to DPPH, and presents
A certain amount imitates relation, and optimal proportion is 400~500 μ g/mL.
Compared with prior art, the device have the advantages that as follows：
(1) anti-apolexis composition dateplum persimmon extract of the present invention, Alpinia galanga extract and safflower extract, according to specific ratio
Example is arranged in pairs or groups, and the phenols such as gallic acid, P- coumaric acids, syringic acid, myricetin, Quercetin and tannin are contained in dateplum persimmon extract
Material, can effectively remove free radical；Alpinia galanga extract is always rich in big sorghum ginger essential oil, with broad-spectrum antimicrobial effect, energy
Effectively suppress the activity of gram-positive bacteria and Gram-negative bacteria；Safflower extract volatilizees rich in flavone compound, safflower
Oily total safflower total flavone has significant removing power to DPPH to significantly inhibiting property of tyrosinase；Three passes through Reasonable
Than Synergistic so that the whitening anti-aging face cream containing anti-apolexis composition of the present invention to significantly inhibiting property of tyrosinase,
There is significant removing power to DPPH, so as to play good anti-aging effects.
(2) due to the unique perfume that Alpinia galanga is carried, its essential oil may act as flavouring agent, and Alpinia galanga composition has outstanding
Antibacterial ability may act as artificial preservative's usage amount that natural preservative reduces product, and with distinctive pungent sense and temperature
Thermal sensation so that the present invention has effect of dispeling cold of refreshing oneself to a certain extent.
Specific embodiment
Below in conjunction with specific embodiment, the present invention is further elaborated.
The following component title occurred in text is INCI (International Nomenclature Cosmetic
Ingredient, i.e. international cosmetic raw material name institute to regulation title, including:Stearine/PEG-100 is hard
Resin acid ester, caprylic/capric triglyceride, polydimethyl siloxanes/polydimethy siloxanes alcohol.
The whitening anti-aging face cream formula of the present invention of embodiment 1~5 is shown in Table one
Table one
The preparation method of the Alpinia galanga extract is comprised the following steps：
(4) Alpinia galanga is dried, crushed 60 mesh sieves, use petroleum ether degreasing 24h, volatilize petroleum ether；
(5) with ethanol as Extraction solvent, by solid-liquid ratio 1：70,70 DEG C of Extracting temperature extracts 5h, and extract solution is in 3000r/
Min is centrifuged 20min；
(6) to take and be concentrated under reduced pressure into paste through the supernatant after centrifugation in step (2).
The preparation method of the safflower extract is：By safflower drying, 60 mesh sieves were crushed, it is standby.Saffron powder is taken, plus
Enter ethanol, solid-liquid ratio 1：30,30min is fully soaked, it is placed in 50 DEG C of water bath chaders, mechanical shaking extraction 2h, filter, in centrifuging and taking
Clear liquid, paste is concentrated into rotavapor under vacuum.
The preparation method of the dateplum persimmon extract is：Dateplum persimmon is dried, powder is ground into, 90% ethanol is added, in 45 DEG C
After lower ultrasonic extraction 3h, supernatant is collected by centrifugation, residue is repeated to extract 1 time, supernatant is merged after centrifugation, use Rotary Evaporators
Concentration removes ethanol.
Whitening anti-aging face cream preparation method described in embodiment 1~5 is comprised the following steps：
(1) by stearine/PEG-100 stearates, cetostearyl alcohol, saualane, dimethyl silicone polymer, pungent
Acid/Triglyceride DDD, avocado oil, hydrogenated jojoba oil, polyacrylamide, polydimethyl siloxanes/polydimethy siloxanes
Alcohol, methyl hydroxybenzoate, Nipasol mixing put into oil phase pot heating stirring to 85 degree as A phases, and stirring and dissolving completely treat afterwards by insulation
With；
(2) Sodium Hyaluronate, glycerine, deionized water mixing are added to heating stirring in water phase pot and, to 85 degree, are stirred as B
Mix heat preservation for standby use after dissolving completely；
(3) emulsification pot is preheated to 60 degree, first be pumped into for B phases by 50 revs/min of mixing speed, then A phases are pumped into, stirring
30 minutes, temperature was maintained at 85 degree；
(5) 45 degree of plant compositions of addition anti-senescence function are cooled to, insulated and stirred 10 minutes is cooled to 40 degree of dischargings
Obtain whitening anti-aging face cream.
Comparative example 1
It is not add Alpinia galanga extract with the difference of embodiment 1, other preparation conditions and method and the phase of embodiment 1
Together.
Comparative example 2
It is not add safflower extract with the difference of embodiment 1, other preparation conditions and method are same as Example 1.
Comparative example 3
It is not add dateplum persimmon extract with the difference of embodiment 1, other preparation conditions and method are same as Example 1.
Comparative example 4
It is to add 0.9 part of plant composition with the difference of embodiment 1, other preparation conditions and method are same as Example 1.
Comparative example 5
It is to add 4.6 parts of plant composition with the difference of embodiment 1, other preparation conditions and method are same as Example 1.
Comparative example 6
It is not add plant composition with the difference of embodiment 1, other preparation conditions and method are same as Example 1.
Whitening anti-aging efficacy validation：
Detection results on probation are carried out to product prepared by embodiment 1-5 and comparative example 1-6, while being declared with a commercially available
Face cream with good whitening anti-aging effect is control group.Test object：Each experimental group is 20 women (35-50 Sui)；
Test zone：Face and crows feet area；Use：Twice daily, persistently use 6 weeks；Test event：Humidity of skin, skin are tender
Slippery, skin elasticity, skin-whitening, wrinkle desalination.Result on trial refers to table two.
Table two
Changed by the desalination of the visible humidity of skin of embodiment 1~5 of table two, the soft degree of skin, skin elasticity, skin-whitening and wrinkle
It is apt to obvious number and is significantly more than comparative example 1~6 and control group, illustrates that whitening anti-aging face cream of the present invention is significantly improved skin
Skin effect, the humidity of skin of comparative example 4 and 5, the soft degree of skin, skin elasticity, skin-whitening and wrinkle desalination improvement number is obvious
Less than embodiment, plant extracts component span is better than other spans in illustrating whitening anti-aging face cream of the present invention；
The humidity of skin of comparative example 6 is obviously improved 4 people, and the soft degree of skin is obviously improved 6 people, and skin elasticity is obviously improved 7 people, skin-whitening
7 people are obviously improved, wrinkle desalination is obviously improved 10 people, hence it is evident that less than other embodiment and comparative example, illustrates that whitening of the present invention resists
Principle active component is plant composition in aging face cream；The whitening anti-aging face cream of comparative example 1 does not add Alpinia galanga to extract
Thing, the soft degree of its humidity of skin, skin, skin elasticity, skin-whitening and wrinkle desalination improves obvious number and is respectively 9 people, 7
People, 8 people, 10 people and 10 people, hence it is evident that less than the number of embodiment 1；Comparative example 2 and 3 is respectively and is not added with safflower extract and black
Jujube extract, it is bright that the desalination of the soft degree of its humidity of skin, skin, skin elasticity, skin-whitening and wrinkle improves obvious number
Aobvious to be less than embodiment 1, comparative example 1~3 contrasts visible in whitening anti-aging face cream of the present invention with embodiment 1, and Alpinia galanga is carried
Take thing, safflower extract and dateplum persimmon extract extract Synergistic.
Above example only illustrates embodiment of the present invention, does not there is any formal limitation to the present invention；Appoint
What is engaged in professional and technical personnel, all has the ability to make some changes using the technology contents for disclosing or modifies, as equivalent
The Equivalent embodiments of change, according to the technology of the present invention essence, simply modification, equivalent variations and modification are carried out to the present invention, are belonged to
In the range of technical solution of the present invention.
Claims (9)
1. a kind of plant composition with anti-senescence function, it is characterised in that the plant composition include by weight with
Lower component：0.02~1.0 part of Alpinia galanga extract, 0.03~1.5 part of safflower extract, 0.05~2.0 part of dateplum persimmon extract.
2. a kind of plant composition with anti-senescence function according to claim 1, it is characterised in that the big Gao Liang
Ginger extract, safflower extract, the weight part ratio of dateplum persimmon extract is (3~8):(4.5~12):(9~16).
3. a kind of plant composition with anti-senescence function according to claim 1 and 2, it is characterised in that described big
The preparation method of galangal rhizome extract is comprised the following steps：
(1) Alpinia galanga is dried, crushed 40~60 mesh sieves, use petroleum ether degreasing 24h, volatilize petroleum ether；
(2) with ethanol as Extraction solvent, by solid-liquid ratio 1：(65~85), 70~90 DEG C of Extracting temperature, extract 5h, extract solution in
3000r/min is centrifuged 20min；
(3) to take and be concentrated under reduced pressure into paste through the supernatant after centrifugation in step (2).
4. a kind of plant composition with anti-senescence function according to claim 1 and 2, it is characterised in that described red
The preparation method of flower extract is：By safflower drying, 40~60 mesh sieves were crushed, it is standby；Saffron powder is taken, ethanol, material is added
Liquor ratio 1：(10~30), fully soak 20~30min, are placed in 50 DEG C of water bath chaders, mechanical shaking extraction 2h, filter, centrifuging and taking
Supernatant, paste is concentrated into rotavapor under vacuum.
5. a kind of plant composition with anti-senescence function according to claim 1 and 2, it is characterised in that described black
The preparation method of jujube extract is：Dateplum persimmon is dried, powder is ground into, 60~90% ethanol is added, in ultrasonic extraction 2 at 45 DEG C
After~3h, supernatant is collected by centrifugation, residue is repeated to extract 1 time, supernatant is merged after centrifugation, concentrated with Rotary Evaporators and removed
Ethanol.
6. a kind of plant composition with anti-senescence function according to claim any one of 1-5 is in cosmetics are prepared
Application.
7. application according to claim 6, it is characterised in that the cosmetics are whitening anti-aging face cream.
8. a kind of whitening anti-aging face cream, it is characterised in that the face cream is made up of the raw material of following weight part ratio：As right will
Seek the plant composition 1.0~4.5% described in 1 or 2；Stearine/PEG-100 stearates 1.2-1.8%；Spermaceti is hard
Lipidol 1.8-2.2%；Saualane 2.5-3.5%；Dimethyl silicone polymer 1-3%；Caprylic/capric triglyceride 2-4%；Avocado
Oily 1-3%；Hydrogenated jojoba oil 1-3%；Methyl hydroxybenzoate 0.1-0.2%；Nipasol 0.1-0.2%；Sodium Hyaluronate 0.01-
0.04%；Glycerine 1-4%；Polyacrylamide 0.8-1.5%；Polydimethyl siloxanes/polydimethy siloxanes alcohol 1.5-2%；
Deionized water surplus.
9. a kind of preparation method of whitening anti-aging face cream as claimed in claim 8, it is characterised in that the preparation method bag
Include following steps：
(1) by stearine/PEG-100 stearates, cetostearyl alcohol, saualane, dimethyl silicone polymer, octanoic acid/
Triglyceride DDD, avocado oil, hydrogenated jojoba oil, polyacrylamide, polydimethyl siloxanes/polydimethy siloxanes alcohol,
Methyl hydroxybenzoate, Nipasol mixing put into oil phase pot heating stirring to 85 degree, the completely rear heat preservation for standby use of stirring and dissolving as A phases；
(2) Sodium Hyaluronate, glycerine, deionized water mixing are added to heating stirring in water phase pot and, to 85 degree, are stirred molten as B
The completely rear heat preservation for standby use of solution；
(3) emulsification pot is preheated to 60-65 degree, first be pumped into for B phases by 50 revs/min of mixing speed, then A phases are pumped into, stirring 30
Minute, temperature is maintained at 85 degree；
(4) 45 degree are cooled to and add plant composition as claimed in claim 1, insulated and stirred 10 minutes is cooled to 40 degree and goes out
Material.
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