CN106266252A - A kind of lycopene Oleum Camelliae soft capsule and preparation method thereof - Google Patents
A kind of lycopene Oleum Camelliae soft capsule and preparation method thereof Download PDFInfo
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- CN106266252A CN106266252A CN201610717170.0A CN201610717170A CN106266252A CN 106266252 A CN106266252 A CN 106266252A CN 201610717170 A CN201610717170 A CN 201610717170A CN 106266252 A CN106266252 A CN 106266252A
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- lycopene
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- oleum camelliae
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/82—Theaceae (Tea family), e.g. camellia
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/01—Hydrocarbons
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/48—Preparations in capsules, e.g. of gelatin, of chocolate
- A61K9/4841—Filling excipients; Inactive ingredients
- A61K9/4858—Organic compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/48—Preparations in capsules, e.g. of gelatin, of chocolate
- A61K9/4841—Filling excipients; Inactive ingredients
- A61K9/4866—Organic macromolecular compounds
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Abstract
The invention belongs to field of medicine preparing technology, it particularly relates to a kind of lycopene Oleum Camelliae soft capsule and preparation method thereof.The content of described soft capsule in parts by mass, including the Oleum Camelliae of 100 parts, the lycopene of 4 15 parts and the suspending agent of 0.2 4 parts;The capsule material of described soft capsule in parts by mass, including the gelatin of 100 parts, the plasticizer of 30 60 parts, the disintegrating agent of 5 10 parts, the coloring agent of 0.1 0.5 parts and the opacifier of 0.1 1 parts.Compared with prior art, lycopene Oleum Camelliae soft capsule of the present invention have the advantage that by by miscible for lycopene in a large amount of Oleum Camelliae, make oxygen only contact with Oleum Camelliae, thus with lycopene completely cut off;Oleum Camelliae is mainly composed of unsaturated fatty acid, can be used as antioxidant, and the product after aoxidizing is the satisfied fatty acid still can taken.
Description
Technical field
The invention belongs to field of medicine preparing technology, it particularly relates to a kind of lycopene Oleum Camelliae soft capsule and
Preparation method.
Background technology
Oleum Camelliae is the edible oil that wild camellia seed refines, and has another name called camellia seed oil, Camellia oil.The unsaturated fatty acid of Oleum Camelliae
Amount is more than 85%, and vitamin A and E content are high, and storage tolerance, easily it is absorbed by the body.Oleum Camelliae is without harmful mustard
Acid, moreover it is possible to prevent and treat hypertension, cardiovascular disease, be the outstanding person in edible vegetable oil.Industrially, Oleum Camelliae can be produced
Oleic acid and esters, production soap and vaseline etc., it is possible to make stearic acid and glycerol.Pharmaceutically, Oleum Camelliae can be used for making
Injection and modulation various ointment, pill etc., among the people also with Oleum Camelliae treatment scald and burn and the skin such as tinea corporis, chronic eczema
Sick.
Lycopene (Lycopene) is a kind of natural pigment contained in plant, is primarily present in plant of Solanaceae Fructus Lycopersici esculenti
Mature fruit in, it also has in red fruit such as Citrullus vulgaris and Citrua paradiai, is the most common and the strongest Carotenoids Isolated of human body
One of oxygen agent.The research of decades confirms: lycopene is 5~10mg/ days for the health care amount of normal population, sick for some
Suffer from crowd's such as prostate, enhancing fertility, blood fat reducing, radioprotective etc. and then need 20-30mg/ days;Some consumers take after also
Not feeling the value place of lycopene, main cause is exactly that the lycopene effective dose taken is the lowest.
In the formulation, lycopene does not only have the requirement of certain content.And, lycopene is unsaturated compound, pole
The most oxidized, quality is unstable, it is difficult to effect of bringing into normal play.Just because of this, the soft capsule of lycopene that prior art is made is normal
There is insoluble matter, it is impossible to meet formulation requirements.Lycopene and Oleum Camelliae are as health product, though gaining great popularity, but both of which is independent
Use.At present, we attempt, by lycopene and Oleum Camelliae use in conjunction, to strengthen drug effect, reducing or remitting defect, but by facing upward with Jiangxi
The cooperation of Shan Yuan oil tea development corporation, Ltd. finds, lycopene dissolubility in Oleum Camelliae is extremely low.
Summary of the invention
For solving above-mentioned technical problem, the invention provides a kind of dissolubility lycopene Oleum Camelliae good, stay-in-grade soft
Capsule and preparation method thereof.
A kind of lycopene Oleum Camelliae soft capsule of the present invention, the content of described soft capsule in parts by mass, including
Oleum Camelliae, the lycopene of 4-15 part and the suspending agent of 0.2-4 part of 100 parts;The capsule material of described soft capsule in parts by mass, including
Gelatin, the plasticizer of 30-60 part, the disintegrating agent of 5-10 part, the coloring agent of 0.1-0.5 part and the shading of 0.1-1 part of 100 parts
Agent.
A kind of lycopene Oleum Camelliae soft capsule of the present invention, described suspending agent is Cera Flava, double protocatechuic acid glycosides, ethyl
Cellulose or aluminum monostearate.
A kind of lycopene Oleum Camelliae soft capsule of the present invention, described plasticizer is glycerol;Described opacifier is oxidation
Ferrum or titanium white.
A kind of lycopene Oleum Camelliae soft capsule of the present invention, described disintegrating agent is cyclodextrin, sorbitol or poly-second two
Alcohol.
A kind of lycopene Oleum Camelliae soft capsule of the present invention, described coloring agent is that curcumin, amaranth or red rice are red.
The preparation method of a kind of lycopene Oleum Camelliae soft capsule of the present invention, described preparation method specifically includes as follows
Step:
1) taking Oleum Camelliae, lycopene and suspending agent, stirring makes its mix homogeneously, and evacuation takes off bubble, makes the material of content
Liquid;
2) take plasticizer, add the purified water of 1-1.5 times of gelatin amount, 70-80 degree heating for dissolving, add disintegrating agent, coloring agent
And opacifier, after stirring, it being subsequently adding gelatin heating 1h, 100 mesh screen, evacuation takes off bubble, makes softgel shell
Glue, 60 degree of insulations, stand-by;
3) being placed in soft capsule pellet press by the glue of the feed liquid of content Yu softgel shell respectively, be pressed into soft capsule, content is every
Grain dress 0.5g.
Compared with prior art, lycopene Oleum Camelliae soft capsule of the present invention has the advantage that by by Fructus Lycopersici esculenti
Red pigment is miscible in a large amount of Oleum Camelliae, makes oxygen only contact with Oleum Camelliae, thus completely cuts off with lycopene;Oleum Camelliae is mainly composed of insatiable hunger
And fatty acid, can be used as antioxidant, and the product after aoxidizing is the satisfied fatty acid still can taken.
Detailed description of the invention
Below in conjunction with specific embodiment lycopene Oleum Camelliae soft capsule of the present invention and preparation method thereof done into
One step explanation, but protection scope of the present invention is not limited to this.
Embodiment 1
A kind of lycopene Oleum Camelliae soft capsule, the content of described soft capsule in parts by mass, including the Oleum Camelliae of 100 parts, 4 parts
Lycopene and the suspending agent of 0.2 part;The capsule material of described soft capsule in parts by mass, including the gelatin of 100 parts, the plasticising of 30 parts
Agent, the disintegrating agent of 5 parts, the coloring agent of 0.1 part and the opacifier of 0.1 part.Described suspending agent is Cera Flava.Described plasticizer is sweet
Oil;Described opacifier is ferrum oxide.Described disintegrating agent is cyclodextrin.Described coloring agent is curcumin.
The preparation method of lycopene Oleum Camelliae soft capsule, described preparation method specifically includes following steps: 1) take Oleum Camelliae, kind
Lycopene and suspending agent, stirring makes its mix homogeneously, and evacuation takes off bubble, makes the feed liquid of content;2) take plasticizer, add
Enter the purified water of 1 times of gelatin amount, 70 degree of heating for dissolving, add disintegrating agent, coloring agent and opacifier, after stirring, then
Adding gelatin heating 1h, 100 mesh screen, evacuation takes off bubble, makes the glue of softgel shell, and 60 degree of insulations are stand-by;3) respectively
The glue of the feed liquid of content Yu softgel shell is placed in soft capsule pellet press, is pressed into soft capsule, content every dress 0.5g.
Embodiment 2
A kind of lycopene Oleum Camelliae soft capsule, the content of described soft capsule in parts by mass, including the Oleum Camelliae of 100 parts, 15 parts
Lycopene and the suspending agent of 4 parts;The capsule material of described soft capsule in parts by mass, including the gelatin of 100 parts, the plasticising of 60 parts
Agent, the disintegrating agent of 10 parts, the coloring agent of 0.5 part and the opacifier of 1 part.Described suspending agent is aluminum monostearate.Described plasticizer
For glycerol;Described opacifier is titanium white.Described disintegrating agent is sorbitol.Described coloring agent is amaranth.
The preparation method of lycopene Oleum Camelliae soft capsule, described preparation method specifically includes following steps: 1) take Oleum Camelliae, kind
Lycopene and suspending agent, stirring makes its mix homogeneously, and evacuation takes off bubble, makes the feed liquid of content;2) take plasticizer, add
Enter the purified water of 1.5 times of gelatin amounts, 80 degree of heating for dissolving, add disintegrating agent, coloring agent and opacifier, after stirring, so
Rear addition gelatin heating 1h, 100 mesh screen, evacuation takes off bubble, makes the glue of softgel shell, and 60 degree of insulations are stand-by;3) divide
The glue of the feed liquid of content Yu softgel shell is not placed in soft capsule pellet press, is pressed into soft capsule, content every dress 0.5g.
Embodiment 3
A kind of lycopene Oleum Camelliae soft capsule, the content of described soft capsule in parts by mass, including the Oleum Camelliae of 100 parts, 8 parts
Lycopene and the suspending agent of 1 part;The capsule material of described soft capsule in parts by mass, including the gelatin of 100 parts, the plasticising of 45 parts
Agent, the disintegrating agent of 8 parts, the coloring agent of 0.3 part and the opacifier of 0.5 part.Described suspending agent is ethyl cellulose.Described plasticizer
For glycerol;Described opacifier is titanium white.Described disintegrating agent is cyclodextrin.Described coloring agent is that red rice is red.
The preparation method of lycopene Oleum Camelliae soft capsule, described preparation method specifically includes following steps: 1) take Oleum Camelliae, kind
Lycopene and suspending agent, stirring makes its mix homogeneously, and evacuation takes off bubble, makes the feed liquid of content;2) take plasticizer, add
Enter the purified water of 1.2 times of gelatin amounts, 75 degree of heating for dissolving, add disintegrating agent, coloring agent and opacifier, after stirring, so
Rear addition gelatin heating 1h, 100 mesh screen, evacuation takes off bubble, makes the glue of softgel shell, and 60 degree of insulations are stand-by;3) divide
The glue of the feed liquid of content Yu softgel shell is not placed in soft capsule pellet press, is pressed into soft capsule, content every dress 0.5g.
Embodiment 4
A kind of lycopene Oleum Camelliae soft capsule, the content of described soft capsule in parts by mass, including the Oleum Camelliae of 100 parts, 8 parts
Lycopene and the suspending agent of 1 part;The capsule material of described soft capsule in parts by mass, including the gelatin of 100 parts, the plasticising of 45 parts
Agent, the disintegrating agent of 8 parts, the coloring agent of 0.3 part and the opacifier of 0.5 part.Described suspending agent is double protocatechuic acid glycosides.Described plasticising
Agent is glycerol;Described opacifier is titanium white.Described disintegrating agent is cyclodextrin.Described coloring agent is that red rice is red.
The preparation method of lycopene Oleum Camelliae soft capsule, described preparation method specifically includes following steps: 1) take Oleum Camelliae, kind
Lycopene and suspending agent, stirring makes its mix homogeneously, and evacuation takes off bubble, makes the feed liquid of content;2) take plasticizer, add
Enter the purified water of 1.2 times of gelatin amounts, 75 degree of heating for dissolving, add disintegrating agent, coloring agent and opacifier, after stirring, so
Rear addition gelatin heating 1h, 100 mesh screen, evacuation takes off bubble, makes the glue of softgel shell, and 60 degree of insulations are stand-by;3) divide
The glue of the feed liquid of content Yu softgel shell is not placed in soft capsule pellet press, is pressed into soft capsule, content every dress 0.5g.
Embodiment 5
A kind of lycopene Oleum Camelliae soft capsule, the content of described soft capsule in parts by mass, including the Oleum Camelliae of 100 parts, 15 parts
Lycopene and the suspending agent of 4 parts;The capsule material of described soft capsule in parts by mass, including the gelatin of 100 parts, the plasticising of 60 parts
Agent, the disintegrating agent of 10 parts, the coloring agent of 0.5 part and the opacifier of 1 part.Described suspending agent is double protocatechuic acid glycosides.Described plasticising
Agent is glycerol;Described opacifier is titanium white.Described disintegrating agent is sorbitol.Described coloring agent is amaranth.
The preparation method of lycopene Oleum Camelliae soft capsule, described preparation method specifically includes following steps: 1) take Oleum Camelliae, kind
Lycopene and suspending agent, stirring makes its mix homogeneously, and evacuation takes off bubble, makes the feed liquid of content;2) take plasticizer, add
Enter the purified water of 1.5 times of gelatin amounts, 80 degree of heating for dissolving, add disintegrating agent, coloring agent and opacifier, after stirring, so
Rear addition gelatin heating 1h, 100 mesh screen, evacuation takes off bubble, makes the glue of softgel shell, and 60 degree of insulations are stand-by;3) divide
The glue of the feed liquid of content Yu softgel shell is not placed in soft capsule pellet press, is pressed into soft capsule, content every dress 0.5g.
Effect experiment
Aged (more than 12 monthly ages) Kunming mouse 90, body weight 30-50g, male and female half and half, it is randomly divided into 9 groups, often group 10.9
Group correspond to respectively: normal group, model group, matched group 1(lack the embodiment 4 after lycopene), matched group 2(soybean oil replace
Embodiment 4 after Oleum Camelliae), embodiment 1, embodiment 2, embodiment 3, embodiment 4 and embodiment 5.In addition to normal group, other 8 groups
It is AlCl3Model of Dementia.Each administration group respectively by body weight converting doses gavage, every day gavage 1 time, and successive administration 30 days,
Heart extracting blood after last administration 4h.Utilize various antioxidation test kit, detect in each group of sample serum classical anti-respectively
Aging index composition, including malonaldehyde (MDA), glutathion peroxidase (GSH-Px) and superoxide dismutase (SOD).
Testing result is shown in Table 1.
The impact on mice defying age index components of the table 1:7 group soft capsule
Claims (6)
1. a lycopene Oleum Camelliae soft capsule, it is characterised in that the content of described soft capsule in parts by mass, including 100
Oleum Camelliae, the lycopene of 4-15 part and the suspending agent of 0.2-4 part of part;The capsule material of described soft capsule in parts by mass, including 100
Gelatin, the plasticizer of 30-60 part, the disintegrating agent of 5-10 part, the coloring agent of 0.1-0.5 part and the opacifier of 0.1-1 part of part.
Lycopene Oleum Camelliae soft capsule the most according to claim 1, it is characterised in that described suspending agent is Cera Flava, double former
Catechuic acid glycosides, ethyl cellulose or aluminum monostearate.
Lycopene Oleum Camelliae soft capsule the most according to claim 1, it is characterised in that described plasticizer is glycerol;Described
Opacifier is ferrum oxide or titanium white.
Lycopene Oleum Camelliae soft capsule the most according to claim 1, it is characterised in that described disintegrating agent is cyclodextrin, mountain
Pears alcohol or Polyethylene Glycol.
Lycopene Oleum Camelliae soft capsule the most according to claim 1, it is characterised in that described coloring agent is curcumin, Herba Amaranthi tricoloris
Dish is red or red rice is red.
The preparation method of lycopene Oleum Camelliae soft capsule the most according to claim 1, it is characterised in that described preparation method
Specifically include following steps:
1) taking Oleum Camelliae, lycopene and suspending agent, stirring makes its mix homogeneously, and evacuation takes off bubble, makes the material of content
Liquid;
2) take plasticizer, add the purified water of 1-1.5 times of gelatin amount, 70-80 degree heating for dissolving, add disintegrating agent, coloring agent
And opacifier, after stirring, it being subsequently adding gelatin heating 1h, 100 mesh screen, evacuation takes off bubble, makes softgel shell
Glue, 60 degree of insulations, stand-by;
3) being placed in soft capsule pellet press by the glue of the feed liquid of content Yu softgel shell respectively, be pressed into soft capsule, content is every
Grain dress 0.5g.
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107348304A (en) * | 2017-07-21 | 2017-11-17 | 郑州博凯医药保健品有限公司 | Effervescent tablet containing Tea Polyphenols and curcumin and preparation method thereof |
CN109430847A (en) * | 2018-12-04 | 2019-03-08 | 安徽省金天柱农业科技有限公司 | A kind of tea oil soft capsule and preparation method thereof |
CN111991365A (en) * | 2020-08-15 | 2020-11-27 | 盈姿生物科技(上海)有限公司 | Lycopene soft capsule and preparation method thereof |
CN113575948A (en) * | 2021-08-04 | 2021-11-02 | 上海健康医学院 | Lycopene soft capsule and preparation method and application thereof |
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CN101496796A (en) * | 2008-01-29 | 2009-08-05 | 北京康必得药业有限公司 | Composite soft capsule of lycopene |
CN105660885A (en) * | 2016-01-07 | 2016-06-15 | 伊国群 | Natural nutriment with function of regulating blood lipid |
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107348304A (en) * | 2017-07-21 | 2017-11-17 | 郑州博凯医药保健品有限公司 | Effervescent tablet containing Tea Polyphenols and curcumin and preparation method thereof |
CN107348304B (en) * | 2017-07-21 | 2024-02-09 | 博凯药业有限公司 | Effervescent tablet containing tea polyphenols and curcumin and its preparation method |
CN109430847A (en) * | 2018-12-04 | 2019-03-08 | 安徽省金天柱农业科技有限公司 | A kind of tea oil soft capsule and preparation method thereof |
CN111991365A (en) * | 2020-08-15 | 2020-11-27 | 盈姿生物科技(上海)有限公司 | Lycopene soft capsule and preparation method thereof |
CN113575948A (en) * | 2021-08-04 | 2021-11-02 | 上海健康医学院 | Lycopene soft capsule and preparation method and application thereof |
CN113575948B (en) * | 2021-08-04 | 2024-01-26 | 上海健康医学院 | Lycopene soft capsule and preparation method and application thereof |
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