CN106176468A - A kind of antipollution cosmetic composition and preparation method thereof - Google Patents

A kind of antipollution cosmetic composition and preparation method thereof Download PDF

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Publication number
CN106176468A
CN106176468A CN201610772356.6A CN201610772356A CN106176468A CN 106176468 A CN106176468 A CN 106176468A CN 201610772356 A CN201610772356 A CN 201610772356A CN 106176468 A CN106176468 A CN 106176468A
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China
Prior art keywords
extract
cortex eucommiae
black pepper
cosmetic composition
temperature
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CN201610772356.6A
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Chinese (zh)
Inventor
金基洙
李俊宏
金荣熙
卢勇
金庚泰
朴智浩
李昭宪
陈秀玉
胡宾
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100 Landes Biochemistry (haimen) Co Ltd
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100 Landes Biochemistry (haimen) Co Ltd
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Priority to CN201610772356.6A priority Critical patent/CN106176468A/en
Publication of CN106176468A publication Critical patent/CN106176468A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/65Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Dermatology (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Mycology (AREA)
  • Microbiology (AREA)
  • Botany (AREA)
  • Biotechnology (AREA)
  • Engineering & Computer Science (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Cosmetics (AREA)

Abstract

The invention provides a kind of antipollution cosmetic composition, count by weight percentage, formula comprises following components: burdock extract 5 20%;Cortex Eucommiae extract 5 20%;Black pepper extracting solution 0 2%;Bathypelagic fish collagen protein 0 0.1%;Surplus is cosmetic base.The present invention uses the pure natural plants such as Fructus Arctii, the Cortex Eucommiae, black pepper to be raw material; burdock extract can effectively reduce the AhR increased because of benzopyrene; CYP1A1 gene; calmness also protects the skin becoming sensitive owing to environmental factors stimulates; and maintain pure and fresh and clean skin; coordinate the defying age of Cortex Eucommiae extract, white-skinned face function, superpower infiltration effect of black pepper extracting solution and moisturizing moisturizing effect of bathypelagic fish collagen protein simultaneously; quality is gentle; easily absorb; non-stimulated, meet people's requirement to cosmetics safety effectiveness.

Description

A kind of antipollution cosmetic composition and preparation method thereof
Technical field
The invention belongs to cosmetic field, be specifically related to a kind of antipollution cosmetic composition and preparation method thereof.
Background technology
Owing to producing and economic fast development, pollute to living environment, and climate change, working environment paces Hurry up, cause the factors such as overstrain, pressure, thus cause skin aging speed to be accelerated.The most topmost polluter benzene And pyrene (representational ambient pressure mutagenic agent) can destroy DNA, inflammation, there is ROS, the activity of MMP-1 is impacted.
Therefore, the harmful city environmental pollution source (thin dirt, flue gas, waste gas, ambient pressure mutagenic agent etc.) of human body antagonism is improved Ability, the root problem of skin could be solved.
Summary of the invention
The technical problem to be solved is to provide a kind of antipollution cosmetic composition and preparation method thereof.
For solving above-mentioned technical problem, the technical solution used in the present invention is:
A kind of antipollution cosmetic composition, count by weight percentage, formula comprises following components:
Burdock extract 5-20%;
Cortex Eucommiae extract 5-20%;
Black pepper extracting solution 0-2%;
Bathypelagic fish collagen protein 0-0.1%;
Surplus is cosmetic base.
The preparation method of this antipollution cosmetic composition, comprises the following steps:
(1) add solvent after Fructus Arctii is peeled and chopped up, at a temperature of 80-95 DEG C, extract 3-5h, then by lixiviating solution at 70-80 DEG C At a temperature of decompression distillation, dried burdock extract, Fructus Arctii is 1:10-15 with the weight ratio of solvent;
(2) add solvent after the Cortex Eucommiae is pulverized, at a temperature of 80-95 DEG C, extract 3-5h, then by lixiviating solution the temperature of 70-80 DEG C Reducing pressure under degree distillation, dried Cortex Eucommiae extract, the Cortex Eucommiae is 1:8-10 with the weight ratio of solvent;
(3) black pepper dries 45-80h at a temperature of 50-60 DEG C, adds enzyme and sodium dihydrogen phosphate-citric acid buffering after pulverizing Liquid, is then placed in the thermostat water bath of 30-40 DEG C soaking ultrasonic, filters, and filtering residue is dried and added 6-8 times of dehydrated alcohol dark place and surpass Sound, filters, collects twice filtrate, obtains black pepper extracting solution, and black pepper is 1:10-12 with the weight ratio of buffer;
(4) burdock extract, Cortex Eucommiae extract, black pepper extracting solution and bathypelagic fish collagen protein and cosmetics are measured by formula Substrate, loads in the bottle sterilized after dissolving mixing.
Described solvent is the one in water or associating 1,3 butanediols, propylene glycol, dipropylene glycol.
Described be dried for lyophilization, be vacuum dried, be spray-dried in one or more.
The dosage form of this antipollution cosmetic composition is essence, elite breast, cream or gelatinous product.
The invention has the beneficial effects as follows: the present invention uses the pure natural plants such as Fructus Arctii, the Cortex Eucommiae, black pepper to be raw material, Fructus Arctii Extract can effectively reduce the AhR increased because of benzopyrene, CYP1A1 gene, calm and protect and become owing to environmental factors stimulates Sensitive skin, and maintain pure and fresh and clean skin, coordinate the defying age of Cortex Eucommiae extract, white-skinned face function, black Hu simultaneously Superpower infiltration effect of green pepper extracting solution and moisturizing moisturizing effect of bathypelagic fish collagen protein, quality is gentle, easily absorbs, stingless Swash, meet people's requirement to cosmetics safety effectiveness.
Detailed description of the invention:
The present invention is a kind of antipollution cosmetic composition, and count by weight percentage, formula comprises following components:
Burdock extract 5-20%;
Cortex Eucommiae extract 5-20%;
Black pepper extracting solution 0-2%;
Bathypelagic fish collagen protein 0-0.1%;
Surplus is cosmetic base.
The dosage form of this antipollution cosmetic composition is essence, elite breast, cream or gelatinous product.
Below in conjunction with embodiment, the present invention is described in further details, but these embodiments are not the limit to the present invention Fixed.
Embodiment 1
A kind of antipollution cosmetic composition, its dosage form is essence, and count by weight percentage, formula comprises following group Point:
Burdock extract 15%;Cortex Eucommiae extract 15%;Black pepper extracting solution 1%;Bathypelagic fish collagen protein 0.02%;1,3 fourths Glycol 2%;Preservative 1%;Xanthan gum 0.5%;Essence 0.1%;Surplus is deionized water.
The preparation method of this antipollution cosmetic composition, comprises the following steps:
(1) add solvent after Fructus Arctii is peeled and chopped up, at a temperature of 80 DEG C, extract 4h, then by lixiviating solution at a temperature of 80 DEG C Decompression distillation, obtains burdock extract after lyophilization, Fructus Arctii is 1:10 with the weight ratio of solvent, and solvent is water;
(2) add solvent after the Cortex Eucommiae is pulverized, at a temperature of 80 DEG C, extract 4h, then lixiviating solution is reduced pressure at a temperature of 80 DEG C Distillation, obtains Cortex Eucommiae extract after lyophilization, the Cortex Eucommiae is 1:8 with the weight ratio of solvent, and solvent is water;
(3) black pepper dries 45h at a temperature of 50 DEG C, adds enzyme and sodium dihydrogen phosphate-citrate buffer solution, then after pulverizing Put into the thermostat water bath of 30 DEG C soaks ultrasonic, filter, filtering residue dry add 6 times of dehydrated alcohol dark places ultrasonic, filter, collect Twice filtrate, obtains black pepper extracting solution, and black pepper is 1:12 with the weight ratio of buffer;
(4) burdock extract, Cortex Eucommiae extract, black pepper extracting solution and bathypelagic fish collagen protein and cosmetics are measured by formula Substrate, loads in the bottle sterilized after dissolving mixing under room temperature.
Embodiment 2
A kind of antipollution cosmetic composition, its dosage form is elite breast, and count by weight percentage, formula comprises following group Point:
A phase: cetearyl alcohol 2%;Tristerin 1%;Sorbitan stearate 1%;Polyethylene Glycol 40 stearate 0.6%;D-panthenol 0.5%;Polyethylene Glycol-100 stearate 1%;
B phase: burdock extract 5%;Cortex Eucommiae extract 8%;Black pepper extracting solution 1%;Preservative 1%;1,3 butanediols 5%;Yellow Virgin rubber 3%;Card ripple 5%;Surplus is deionized water.
The preparation method of this antipollution cosmetic composition, comprises the following steps:
(1) add solvent after Fructus Arctii is peeled and chopped up, at a temperature of 90 DEG C, extract 3h, then by lixiviating solution at a temperature of 70 DEG C Decompression distillation, obtains burdock extract after vacuum drying, Fructus Arctii is 1:12 with the weight ratio of solvent, and solvent is that water combines 1,3 fourths two Alcohol;
(2) add solvent after the Cortex Eucommiae is pulverized, at a temperature of 90 DEG C, extract 3h, then lixiviating solution is reduced pressure at a temperature of 70 DEG C Distillation, obtains Cortex Eucommiae extract after vacuum drying, the described Cortex Eucommiae is 1:9 with the weight ratio of solvent, and solvent is that water combines 1,3 fourths two Alcohol;
(3) black pepper dries 60h at a temperature of 50 DEG C, adds enzyme and sodium dihydrogen phosphate-citrate buffer solution, then after pulverizing Put into the thermostat water bath of 35 DEG C soaks ultrasonic, filter, filtering residue dry add 6 times of dehydrated alcohol dark places ultrasonic, filter, collect Twice filtrate, obtains black pepper extracting solution, and black pepper is 1:10 with the weight ratio of buffer;
(4) take A phase and B phase by formula, dissolve at a temperature of 80 DEG C respectively, then mix, load in the bottle sterilized.
Embodiment 3
A kind of antipollution cosmetic composition, its dosage form is gel, and count by weight percentage, formula comprises following group Point:
Burdock extract 10%;Cortex Eucommiae extract 5%;Black pepper extracting solution 1%;Bathypelagic fish collagen protein 0.05%;1,3 fourths two Alcohol 2%;Preservative 1%;Xanthan gum 2%;Essence 0.1%;Card ripple 2%;Surplus is deionized water.
The preparation method of this antipollution cosmetic composition, comprises the following steps:
(1) add solvent after Fructus Arctii is peeled and chopped up, at a temperature of 85 DEG C, extract 5h, then by lixiviating solution at a temperature of 75 DEG C Decompression distillation, obtains burdock extract after lyophilization, Fructus Arctii is 1:15 with the weight ratio of solvent, and solvent is that water combines propylene glycol;
(2) add solvent after the Cortex Eucommiae is pulverized, at a temperature of 85 DEG C, extract 5h, then lixiviating solution is reduced pressure at a temperature of 75 DEG C Distillation, obtains Cortex Eucommiae extract after lyophilization, the Cortex Eucommiae is 1:10 with the weight ratio of solvent, and solvent is that water combines propylene glycol;
(3) black pepper dries 80h at a temperature of 60 DEG C, adds enzyme and sodium dihydrogen phosphate-citrate buffer solution, then after pulverizing Put into the thermostat water bath of 40 DEG C soaks ultrasonic, filter, filtering residue dry add 6 times of dehydrated alcohol dark places ultrasonic, filter, collect Twice filtrate, obtains black pepper extracting solution, and black pepper is 1:10 with the weight ratio of buffer;
(4) burdock extract, Cortex Eucommiae extract, black pepper extracting solution and bathypelagic fish collagen protein and cosmetics are measured by formula After substrate dissolves mixing at a temperature of 70 DEG C, load in the bottle sterilized.
Detect the cosmetic composition that above-mentioned 3 embodiments prepare respectively free radical and TYR enzymatic activity are pressed down Situation processed:
Take 1.5ml centrifuge tube, add TYR (0.3mg/ml) 500 μ L, buffer 500 μ L, water 450 μ L, enzyme 50 μ L and change Cosmetic compositions 20 μ L, at spectrophotometer wavelength 480nm, absorbance is as shown in the table, wherein: comparative example is corresponding embodiment The formula of cosmetic base.
As can be known from the above table, the cosmetic composition of the present invention has potent stable pressing down to free radical and TYR enzymatic activity Making use, and the increase of the extract concentrations along with Fructus Arctii, its inhibition becomes apparent from.

Claims (5)

1. an antipollution cosmetic composition, it is characterised in that count by weight percentage, formula comprises following components:
Burdock extract 5-20%;
Cortex Eucommiae extract 5-20%;
Black pepper extracting solution 0-2%;
Bathypelagic fish collagen protein 0-0.1%;
Surplus is cosmetic base.
The preparation method of antipollution cosmetic composition the most according to claim 1, it is characterised in that include following step Rapid:
(1) add solvent after Fructus Arctii is peeled and chopped up, at a temperature of 80-95 DEG C, extract 3-5h, then by lixiviating solution at 70-80 DEG C At a temperature of decompression distillation, dried burdock extract, described Fructus Arctii is 1:10-15 with the weight ratio of solvent;
(2) add solvent after the Cortex Eucommiae is pulverized, at a temperature of 80-95 DEG C, extract 3-5h, then by lixiviating solution the temperature of 70-80 DEG C Reducing pressure under degree distillation, dried Cortex Eucommiae extract, the described Cortex Eucommiae is 1:8-10 with the weight ratio of solvent;
(3) black pepper dries 45-80h at a temperature of 50-60 DEG C, adds enzyme and sodium dihydrogen phosphate-citric acid buffering after pulverizing Liquid, is then placed in the thermostat water bath of 30-40 DEG C soaking ultrasonic, filters, and filtering residue is dried and added 6-8 times of dehydrated alcohol dark place and surpass Sound, filters, collects twice filtrate, obtains black pepper extracting solution, and described black pepper is 1:10-12 with the weight ratio of buffer;
(4) burdock extract, Cortex Eucommiae extract, black pepper extracting solution and bathypelagic fish collagen protein and cosmetics are measured by formula Substrate, loads in the bottle sterilized after dissolving mixing.
The preparation method of antipollution cosmetic composition the most according to claim 2, it is characterised in that described solvent is water Or the one in associating 1,3 butanediols, propylene glycol, dipropylene glycol.
The preparation method of antipollution cosmetic composition the most according to claim 2, it is characterised in that described be dried as cold Lyophilizing is dry, be vacuum dried, be spray-dried in one or more.
Antipollution cosmetic composition the most according to claim 1, it is characterised in that this antipollution cosmetic composition Dosage form is essence, elite breast, cream or gelatinous product.
CN201610772356.6A 2016-08-31 2016-08-31 A kind of antipollution cosmetic composition and preparation method thereof Pending CN106176468A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106983703A (en) * 2017-05-24 2017-07-28 广州珈源日化用品有限公司 A kind of cosmetic composition for repairing hormone injured skin and its preparation method and application
CN111658581A (en) * 2019-03-06 2020-09-15 惠州绵俪生物科技有限公司 Cosmetic composition for improving skin comprising mixed fermented extract of root system plant
CN111803420A (en) * 2020-08-11 2020-10-23 爱思开百朗德生物科技(海门)有限公司 A cosmetic complex with anti-pollution and anti-heavy metals

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20000045575A (en) * 1998-12-30 2000-07-25 유상옥 Antioxidant cosmetic composition containing the seed extract of arctium lappa
JP2005194290A (en) * 2005-03-30 2005-07-21 Pola Chem Ind Inc Cleansing cosmetic
CN101129433A (en) * 2007-09-12 2008-02-27 青岛宝德生物科技开发有限公司 Method for extracting active component of edible burdock
CN103251539A (en) * 2013-05-24 2013-08-21 上海韩束化妆品有限公司 Nanostructured lipid carrier for composite skin lightener and preparation method of composite skin lightener
JP2014019695A (en) * 2012-07-12 2014-02-03 Shonan Institute For Medical & Preventive Science Tyrosinase inhibitor containing burdock fine powder as an active ingredient
CN105232438A (en) * 2015-10-10 2016-01-13 严建明 Moisturizing and repairing facial mask and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20000045575A (en) * 1998-12-30 2000-07-25 유상옥 Antioxidant cosmetic composition containing the seed extract of arctium lappa
JP2005194290A (en) * 2005-03-30 2005-07-21 Pola Chem Ind Inc Cleansing cosmetic
CN101129433A (en) * 2007-09-12 2008-02-27 青岛宝德生物科技开发有限公司 Method for extracting active component of edible burdock
JP2014019695A (en) * 2012-07-12 2014-02-03 Shonan Institute For Medical & Preventive Science Tyrosinase inhibitor containing burdock fine powder as an active ingredient
CN103251539A (en) * 2013-05-24 2013-08-21 上海韩束化妆品有限公司 Nanostructured lipid carrier for composite skin lightener and preparation method of composite skin lightener
CN105232438A (en) * 2015-10-10 2016-01-13 严建明 Moisturizing and repairing facial mask and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
冯居秦等: "《美容中药学》", 28 February 2015, 中国中医药出版社 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106983703A (en) * 2017-05-24 2017-07-28 广州珈源日化用品有限公司 A kind of cosmetic composition for repairing hormone injured skin and its preparation method and application
CN111658581A (en) * 2019-03-06 2020-09-15 惠州绵俪生物科技有限公司 Cosmetic composition for improving skin comprising mixed fermented extract of root system plant
CN111803420A (en) * 2020-08-11 2020-10-23 爱思开百朗德生物科技(海门)有限公司 A cosmetic complex with anti-pollution and anti-heavy metals
CN111803420B (en) * 2020-08-11 2023-01-31 现代百朗德生物科技(江苏)有限公司 A cosmetic complex with anti-pollution and anti-heavy metals

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