CN106146363A - The synthetic method of medical material 3-methyl sulfinic acid amine salt - Google Patents
The synthetic method of medical material 3-methyl sulfinic acid amine salt Download PDFInfo
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- CN106146363A CN106146363A CN201510749084.3A CN201510749084A CN106146363A CN 106146363 A CN106146363 A CN 106146363A CN 201510749084 A CN201510749084 A CN 201510749084A CN 106146363 A CN106146363 A CN 106146363A
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- amine salt
- sulfinic acid
- acid amine
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- medical material
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Abstract
The present invention relates to the synthetic method of a kind of medical material 3-methyl sulfinic acid amine salt, be under 2-3 atmospheric pressure at temperature 180-220 DEG C, pressure, by raw material sulfinic acid amine salt by the generation 3-methyl sulfinic acid amine salt that methylates.The synthetic method of medical material 3-methyl sulfinic acid amine salt of the present invention is simple, efficient, and operates safety, very useful in concrete production.
Description
Technical field
The present invention relates to the synthetic method of a kind of medical material 3-methyl sulfinic acid amine salt.
Background technology
3-methyl sulfinic acid amine salt is the initiation material of many pharmaceutical synthesis, the initiation material of particularly a lot of sulfinic acid amines, the domestic at present synthetic method having no this compound of report.
Content of the invention
It is an object of the invention to overcome above-mentioned deficiency, provide a kind of simple, efficiently, the synthetic method of the medical material 3-methyl sulfinic acid amine salt of safety operation.
The object of the present invention is achieved like this:
The synthetic method of a kind of medical material 3-methyl sulfinic acid amine salt, is under 2-3 atmospheric pressure at temperature 180-220 DEG C, pressure, by raw material sulfinic acid amine salt by the generation 3-methyl sulfinic acid amine salt that methylates.
Compared with prior art, the invention has the beneficial effects as follows:
The synthetic method of medical material 3-methyl sulfinic acid amine salt of the present invention is simple, efficient, and operates safety, very useful in concrete production.
Detailed description of the invention
The synthetic method of medical material 3-methyl sulfinic acid amine salt of the present invention is specific as follows:
It is under 2-3 atmospheric pressure at temperature 180-220 DEG C, pressure, by raw material sulfinic acid amine salt by the generation 3-methyl sulfinic acid amine salt that methylates.The purity of this crude product can meet general reaction requirement, can direct plunge in reaction.
Claims (1)
1. the synthetic method of a medical material 3-methyl sulfinic acid amine salt, it is characterised in that be under 2-3 atmospheric pressure at temperature 180-220 DEG C, pressure, by raw material sulfinic acid amine salt by the generation 3-methyl sulfinic acid amine salt that methylates.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510749084.3A CN106146363A (en) | 2015-11-08 | 2015-11-08 | The synthetic method of medical material 3-methyl sulfinic acid amine salt |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510749084.3A CN106146363A (en) | 2015-11-08 | 2015-11-08 | The synthetic method of medical material 3-methyl sulfinic acid amine salt |
Publications (1)
| Publication Number | Publication Date |
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| CN106146363A true CN106146363A (en) | 2016-11-23 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201510749084.3A Pending CN106146363A (en) | 2015-11-08 | 2015-11-08 | The synthetic method of medical material 3-methyl sulfinic acid amine salt |
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| CN (1) | CN106146363A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109422748A (en) * | 2017-08-21 | 2019-03-05 | 南京理工大学 | The method for synthesizing TNNI3K inhibitor |
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2015
- 2015-11-08 CN CN201510749084.3A patent/CN106146363A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109422748A (en) * | 2017-08-21 | 2019-03-05 | 南京理工大学 | The method for synthesizing TNNI3K inhibitor |
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Legal Events
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| C06 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20161123 |