CN106038330A - Facial cleanser and preparation method thereof - Google Patents

Facial cleanser and preparation method thereof Download PDF

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Publication number
CN106038330A
CN106038330A CN201610494944.8A CN201610494944A CN106038330A CN 106038330 A CN106038330 A CN 106038330A CN 201610494944 A CN201610494944 A CN 201610494944A CN 106038330 A CN106038330 A CN 106038330A
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parts
skin
facial milk
sodium
milk cleanser
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CN106038330B (en
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束毅峰
李旭东
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Zhejiang Gaoyan Technology Co.,Ltd.
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Hangzhou Daisy Cosmetics Co Ltd
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
    • A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/20—Halogens; Compounds thereof
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    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
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    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
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    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60—Sugars; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
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    • A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86—Polyethers
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    • A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • A61K8/988—Honey; Royal jelly, Propolis
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    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
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    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/48—Thickener, Thickening system
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    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59—Mixtures
    • A61K2800/596—Mixtures of surface active compounds
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    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/70—Biological properties of the composition as a whole
    • A61K2800/72—Hypo-allergenic

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Abstract

The invention discloses a facial cleanser and a preparation method thereof. The problem of skin tension caused by using the present facial cleanser for cleaning skin is solved. According to the technical scheme, the facial cleanser comprises the following components in parts by weight: 8-22 parts of sodium methyl cocoyl taurate, 3-12 parts of sodium cocoyl isethionate, 2-5 parts of lauryl sulfo succinate disodium, 2-10 parts of cocamidopropyl betaine, 1-5 parts of lauryl alcohol polyether ammonium sulfate, 3-10 parts of a thickening agent, 0.1-0.5 part of a preservative, 0.05-0.2 part of EDTA disodium, 0.2-0.6 part of propylene glycol, 2-12 parts of glycerinum, 0.1-0.5 part of essence and 10-18 parts of water. The prepared facial cleanser belongs to an amino acid facial cleanser, has the characteristics of safety, no stimulation, skin-relieving effect and deep skin-cleaning effect, and can be used by a user for a long term.

Description

A kind of facial milk cleanser and preparation method thereof
Technical field
The present invention relates to technical field of skin care, particularly to a kind of facial milk cleanser and preparation method thereof.
Background technology
Skin is one of vitals of human body, is the important symbol of health beauty, and human skin is by sebum The sebum of glandular secretion is covered, and forms natural protecting film, makes skin surface soft smooth.But due to human body face every day antiperspirant The pollution of stain, dust and other filths, brings various skin condition shape, and such as PM2.5 enters skin less than pore and causes pore thick Greatly, second hand smoking is attached to skin surface and causes it obscure, and in long-time labour work causes skin, fat secretion is unbalance, is dried pine Relaxing, tarnish, colour of skin wan shape, all factors accelerate skin aging.Protection skin is very urgent, and every day uses face cleaning The skin care item cleanings such as breast are very important.
Facial milk cleanser be cleansing milk be a kind of, by composition structures such as oil phase thing, aqueous-phase material, surfactant, wetting agent, nutrients The liquiform product become, thus there is the effects such as cleaning, nutrition and protection skin.In facial milk cleanser, surfactant has moistening, divides Dissipate, foaming, decontamination, emulsifying five acts on greatly, is the chief active thing of facial milk cleanser.According to the similar principle that mixes, washed one's face in skin protection Cheng Zhong, dissolves, by means of oil phase thing, the oils and fats that facial oil-soluble fat is dirty and unnecessary；Water miscible antiperspirant on face is dissolved by means of its aqueous-phase material Stain dirt.
Chinese patent application CN105560146A discloses a kind of whitening cleansing facial milk containing, by the raw material group of following parts by weight Become: lauric acid 3～5 parts, potassium hydroxide 0.01～0.05 part, glycerol 15～20 parts, hydroxyethyl cellulose 15～20 parts, stearic acid 2～5 parts, propylene glycol 6～10 parts, ethylenediaminetetraacetic acid 0.5～1 part, Margarita powder 5～8 parts, the Rhizoma Atractylodis Macrocephalae 0.5～1 part, Poria 0.5 ～1 part, the Radix Paeoniae Alba 0.3～0.5 part, the Pseudobulbus Bletillae (Rhizoma Bletillae) 0.1～0.3 part, Radix Rhodiolae 1～2 parts, glycyrrhizic acid dipotassium 1～3 parts, coconut oleoyl amine third Base glycine betaine 1～3 parts, deionized water 10～15 parts.It contains potassium hydroxide, uses rear skin to be easily generated tight sense and hydropenia is existing As, unsuitable life-time service.
Chinese patent application CN105287302A discloses a kind of anti-acne facial cleanser, is made up of following raw material: hard Fat acid 15～20 parts, lauric acid 5～10 parts, myristic acid 4～8 parts, Palmic acid 3～6 parts, glycol distearate 1～2 Part, tocopherol acetas 0.1～0.5 part, ceteareth-60 myristyl glycol 0.1～0.5 part, butylated hydroxytoluene 0.1 ～0.2 part, methyl hydroxybenzoate 0.1～0.2 part, propyl hydroxybenzoate 0.05～0.15 part, glycerol 15～25 parts, propylene glycol 0.1～0.5 Part, modified corn starch 2～5 parts, lauric acid sodium taurocholate 2～4 parts, sodium cocoyl glycinate 2～4 parts, dodecanamide propyl Glycine betaine 2～4 parts, microcrystalline Cellulose 0.1～0.5 part, hydroxypropyl methyl cellulose 0.1～0.5 part, EDETATE SODIUM 0.05～ 0.2 part, allantoin 0.05～0.2 part, polyquaternary ammonium salt-70.5～1 part, mannitol 0.5～1 part, potassium hydroxide 4.5～6.5 Part, CI778910.1～0.5 part, CI774910.1～0.5 part, leaf of Mentha piperita extract nano-liposome 0.5～5 parts, double (methylol) imidazolidinyl urea 0.1～0.5 part, iodine propilolic alcohol butyl mephenesin Carbamate 0.002～0.0075 part, essence 0.1～0.5 Part, 100 parts of water.This various complexity of facial milk cleanser composition, composition is high, is also containing potassium hydroxide simultaneously, easily causes skin tight Hydropenia, unsuitable life-time service.
It is, therefore, desirable to provide a kind of new scheme solves the problems referred to above.
Summary of the invention
The first object of the present invention is to provide a kind of facial milk cleanser, belongs to amino acid cleansing breast, has safe and non-stimulating, flesh of releiving Skin, the feature of deep layer cleaning skin, it has certain pharmacological action simultaneously, it is possible to improves skin surface swelling situation, can grow Phase uses.
The above-mentioned technical purpose of the present invention has the technical scheme that a kind of facial milk cleanser, including following The component of weight portion: sodium methyl cocoyl taurate 8～22 parts, cocos nucifera oil acyl isethionic acid ester sodium 3～12 parts, lauryl alcohol sulfo group Succinate disodium 2～5 parts, cocamido propyl betaine 2～10 parts, laureth sulfuric ester ammonium 1～5 parts, thickening agent 3 ～10 parts, preservative 0.1～0.5 part, EDETATE SODIUM 0.05～0.2 part, propylene glycol 0.2～0.6 part, glycerol 2～12 parts, essence 0.1～0.5 part, water 10～18 parts.
By technique scheme, sodium methyl cocoyl taurate, cocos nucifera oil acyl isethionic acid ester sodium, lauryl alcohol sulfo group amber Amber acid esters disodium is anion surfactant, has the effects such as emulsifying, de-sludging, dispersion, moistening, bubble, its stronger moistening Performance makes facial milk cleanser be easily dispersed thus is uniformly attached to skin surface, has the advantages that to tend to smear out.And to skin Zest aspect, owing to three kinds of anion surfactants in the middle of facial milk cleanser are faintly acid, meets skin acidity at pH5～7 In the range of, therefore skin will not be caused excitement in acid-base value, simultaneously three to have character gentle, spread upon on skin not Can cause stimulating skin to produce untoward reaction with other component phase separations in formula, its feature with emulsifying can on the contrary Skin plays soft effect, and the epidermis of diastole skin makes skin have comfort.Furthermore its intramolecular contains substantial amounts of parent Water base group and two kinds of groups of lipophilic group, and when spreading upon skin surface, quickly skin can will be adsorbed by two kinds of groups The small particulate solid such as the PM2.5 on surface or dissolving have organic nuisance drop of harm to skin, when when cleaning Due to internal hydrophilic group, therefore facial milk cleanser quickly can be eluted in clear water, reach to remove skin surface dirt Purpose, a large amount of foam can be produced during wiping.Cocamido propyl betaine is a kind of amphoteric surfactant, nothing Opinion is that the skin in acid skin or alkalescence can be shown good stability, therefore spreads upon on skin not Can arrive skin all without stimulating, thus skin will not produce tight sense, skin also will not produce untoward reaction.Laureth sulfur Acid esters ammonium as main active agent, plays foaming and cleaning action equally, but the content added is certain in facial milk cleanser, and it is right to reduce The zest of skin.Above-mentioned surfactant synergism promotes the nursing efficacy that facial milk cleanser is good so that human body skin Obtain good improvement.
The present invention is further: described thickening agent is sodium chloride, acrylic copolymer and methyl glucose dioleate One or more.
By technique scheme, use a certain amount of sodium chloride as the thickening agent of facial milk cleanser so that in facial milk cleanser Surfactant forms micelle in emulsion, and sodium chloride has the effect of salt bridge and the association number of micelle is increased, and carries out spherical Micelle to rod-shaped micelle convert so that the resistance of motion increase so that system viscosity increase, then product is increased Thick.And acrylic copolymer is the most under mildly acidic conditions, its molecule generation ionizing the main chain along polymer produce Raw negative charge, and repelling each other between the same sex promotes uncoiling of molecule to open formation network structure thus reaches the effect of thickening；For Methyl glucose dioleate has the feature with skin-compatible, is added in facial milk cleanser and has excellent emulsifying, disperse and increase Thick effect so that be mutually dissolved between each component more fully and thorough.When three kinds of thickening agents are added into simultaneously as raw material When other components being carried out thickening in the middle of facial milk cleanser, the facial milk cleanser prepared is more stable.
The present invention is further: described preservative be hydantoin, methylchloroisothiazandnone, Methylisothiazolinone, One or more of magnesium nitrate and magnesium chloride.
By technique scheme, the antibacterial ability of hydantoin not by surfactant in such scheme or component other The impact of reagent, can keep stable antibacterial ability in oil hydrosol；Methylchloroisothiazandnone, Methylisothiazolinone Belonging to efficient germicide, microbial bacterial is bred by the substructure of thalline inner cell, such as cell wall, cell membrane and metabolism Relevant enzyme, protein synthesis system and hereditary material, methylchloroisothiazandnone, Methylisothiazolinone only need to act on wherein One substructure just can reach antibacterial purpose, this is because each substructure is necessary for antibacterial；Magnesium nitrate and Magnesium chloride makes an addition to improve in facial milk cleanser antiseptic property.
The present invention is further: also include propolis extract, in parts by weight, described propolis extract 0.2～0.5 Part.
By technique scheme, containing antibacterial flavone compound in propolis extract, it also has antibacterial and anti- The effect of allergy, it is possible to prevent facial milk cleanser from stimulating skin, thus cause skin generation pain, and flavone compound and glycerol Synergism be coated in skin surface and can form the oil film of closure, long-time use after promote the hydration of skin, Epidermis is thickened, keratinization and softening protective effect of having chapped.Flavone compound and other medicines in propolis extract simultaneously The compound confrontation skin of rationality is respectively provided with effect of heat-clearing and toxic substances removing, reducing swelling and alleviating pain, not only in the situation that user face is red and swollen Under can use, even remove red and swollen effect, diastole skin of face to having.
The present invention is further: also include Aloe vulgaris leaf extract, in parts by weight, described Aloe Barbadensis Miller Extract 0.05～0.35 part.
By technique scheme, the anthraquinones of Aloe vulgaris leaf extract has biocidal property, and it mainly can Suppression bacillus subtilis, escherichia coli and the growth of staphylococcus aureus and breeding, when Aloe vulgaris leaf extract adds The effect making the facial milk cleanser of the present invention when adding in the middle of facial milk cleanser reaches optimal, amino in Aloe vulgaris leaf extract simultaneously Acid and complex polysaccharide material constitute natural moisture preserving factor, and it can supplement the moisture of loss in skin, recovers collagen protein Function, prevents face skin wrinkle, unfolds skin and makes skin without tight sense；Aloe vulgaris leaf extract and propolis simultaneously Extract has the effect in terms of identical pharmacology, and the face spreading upon swelling can enhance metabolism, skin care, and energy The convergence open sore part, promotes cell regeneration, eases the pain and pruritus；Work in coordination with propolis extract and promote red and swollen the going down of face so that Tight face is releived.
The present invention is further: also include Mentholum, and the weight portion of described Mentholum with the weight part ratio of propylene glycol is (0.5～0.15): 1.
By technique scheme, the propylene glycol containing 5%～15% Mentholum makes skin to propolis extract and Ku La The absorption of rope Folium Aloe extract has facilitation effect, changes the physicochemical property of skin, promote skin after being predominantly applied to skin Skin diastole, pore is opened so that have pharmacological action component can rapid osmotic enter in skin epidermal tissue in so that The skin at red and swollen place recovers at short notice, and Mentholum to be solid, shaped will not enter in skin.
The second object of the present invention is to provide the preparation method of a kind of facial milk cleanser, and the aminoacid prepared by the method is clean Face breast, has safe and non-stimulating, skin of releiving, and the feature of deep layer cleaning skin can life-time service.
The above-mentioned technical purpose of the present invention has the technical scheme that a kind of prepares above-mentioned facial milk cleanser Method, comprises the steps: step S1, takes formula ratio sodium methyl cocoyl taurate 8～22 parts, cocos nucifera oil acyl isethionic acid ester Sodium 3～12 parts, lauryl alcohol sulfosuccinate disodium 2～5 parts, cocamido propyl betaine 2～10 parts, laureth sulfur Acid esters ammonium 1～5 parts, EDETATE SODIUM 0.05～0.2 part, propylene glycol 0.2～0.6 part, glycerol 2～12 parts and water 10～18 parts of additions To reactor, it is warming up to 75～80 DEG C, stirs 30～35 minutes mixed dissolutions and uniformly obtain mixture S1；Step S2, in step The mixture S1 of the reactor of S1 adds the thickening agent 3 of formula ratio～10 parts, stirs 15～20 minutes mix homogeneously and is mixed Thing S2；Step S3, is incubated at a temperature of environment 75～80 DEG C in reactor the mixture S2 in step S2, and period enters Row low rate mixing 20～do defoaming treatment after 30 minutes；Step S4, cools to 30～55 DEG C by the reactor of step S3, and addition is joined Side amount preservative 0.1～0.5 part, stir 15～20 minutes mix homogeneously and prepare product.
Pass through technique scheme, it is possible to prepare one facial milk cleanser of the present invention.
The present invention is further: add propylene glycol 0.4 part in described step S1；In described step 4, by Mentholum with The remaining propylene glycol of formula ratio first mixes and is then added to afterwards in reactor.
By technique scheme, the propylene glycol containing 5%～15% Mentholum makes skin to propolis extract and Ku La The absorption of rope Folium Aloe extract has facilitation effect and reaches optimal.
Detailed description of the invention
Hereinafter the present invention is described in further detail.
Test by formulating 7 embodiments and 2 comparative examples, wherein embodiment 1～6 and comparative example 1 in facial milk cleanser Each component and parts by weight the most different, embodiment 1～6 and comparative example 1 all use the preparation method of the present invention to test, Embodiment 7 is that from the difference of embodiment 6 mode adding propylene glycol is different.Operation specific as follows: step S1, takes formula Amount sodium methyl cocoyl taurate, cocos nucifera oil acyl isethionic acid ester sodium, lauryl alcohol sulfosuccinate disodium, cocamidopropyl propyl amide Glycine betaine, laureth sulfuric ester ammonium, EDETATE SODIUM, propylene glycol, G & W add to reactor, are warming up to 75～80 DEG C, stir 30～35 minutes mixed dissolutions and uniformly obtain mixture S1；Step S2, adds in the mixture S1 of the reactor of step S1 Enter the thickening agent of formula ratio, stir 15～20 minutes mix homogeneously and obtain mixture S2；Step S3, to the mixture in step S2 S2 is incubated at a temperature of environment 75～80 DEG C in reactor, and period carries out low rate mixing 20～does at froth breaking after 30 minutes Reason；Step S4, cools to 30～55 DEG C by the reactor of step S3, adds the preservative of formula ratio, propolis extract, Mentholum With Aloe vulgaris leaf extract, stir 15～20 minutes mix homogeneously and prepare product.Wherein embodiment 1～6 facial milk cleanser is each Component and parts by weight thereof are as shown in table 1～6.
Embodiment 1
The each component of facial milk cleanser of form 1 embodiment 1 and parts by weight thereof
Component Number (part) Component Number (part)
Sodium methyl cocoyl taurate 12 Cocos nucifera oil acyl isethionic acid ester sodium 6.0
Lauryl alcohol sulfosuccinate disodium 3.0 Acrylic copolymer 4.0
Methylchloroisothiazandnone 0.3 Magnesium nitrate 0.3
Magnesium chloride 0.1 EDETATE SODIUM 0.2
Propylene glycol 0.3 Glycerol 6.0
Water 13 Essence 0.4
Embodiment 2
The each component of facial milk cleanser of form 2 embodiment 2 and parts by weight thereof
Component Number (part) Component Number (part)
Sodium methyl cocoyl taurate 13 Cocos nucifera oil acyl isethionic acid ester sodium 7.0
Cocamido propyl betaine 4.0 Laureth sulfuric ester ammonium 3.0
Lauryl alcohol sulfosuccinate disodium 5.0 Methyl glucose dioleate 6.0
Methylchloroisothiazandnone 0.2 Magnesium nitrate 0.1
Magnesium chloride 0.2 EDETATE SODIUM 0.1
Propylene glycol 0.2 Glycerol 8.0
Water 15 Essence 0.3
Embodiment 3
The each component of facial milk cleanser of form 3 embodiment 3 and parts by weight thereof
Component Number (part) Component Number (part)
Sodium methyl cocoyl taurate 22 Cocos nucifera oil acyl isethionic acid ester sodium 12
Cocamido propyl betaine 10 Laureth sulfuric ester ammonium 5.0
Lauryl alcohol sulfosuccinate disodium 5.0 Acrylic copolymer 6.0
Methylchloroisothiazandnone 0.2 Magnesium nitrate 0.1
Sodium chloride 2.0 Hydantoin 0.2
Magnesium chloride 0.1 EDETATE SODIUM 0.1
Propylene glycol 0.4 Glycerol 12
Water 18 Propolis extract 0.4
Essence 0.1 / /
Embodiment 4
The each component of facial milk cleanser of form 4 embodiment 4 and parts by weight thereof
Component Number (part) Component Number (part)
Sodium methyl cocoyl taurate 8.0 Cocos nucifera oil acyl isethionic acid ester sodium 3.0
Cocamido propyl betaine 4.0 Laureth sulfuric ester ammonium 5.0
Lauryl alcohol sulfosuccinate disodium 3.0 Acrylic copolymer 4.0
Methylchloroisothiazandnone 0.05 Magnesium nitrate 0.15
Methyl glucose dioleate 2.5 Hydantoin 0.05
Magnesium chloride 0.15 EDETATE SODIUM 0.1
Propylene glycol 0.3 Glycerol 12
Water 14 Propolis extract 0.2
Aloe vulgaris leaf extract 0.35 Essence 0.4
Embodiment 5
The each component of facial milk cleanser of form 5 embodiment 5 and parts by weight thereof
Embodiment 6
The each component of facial milk cleanser of form 6 embodiment 6 and parts by weight thereof
Component Number (part) Component Number (part)
Sodium methyl cocoyl taurate 12 Cocos nucifera oil acyl isethionic acid ester sodium 10
Cocamido propyl betaine 5.0 Laureth sulfuric ester ammonium 3.0
Lauryl alcohol sulfosuccinate disodium 3.5 Acrylic copolymer 4.5
Sodium chloride 2.5 Magnesium nitrate 0.25
Methyl glucose dioleate 1.4 Hydantoin 0.05
Magnesium chloride 0.1 Methylchloroisothiazandnone 0.15
Methylisothiazolinone 0.05 Mentholum 0.02
EDETATE SODIUM 0.15 Propylene glycol urea 0.2
Glycerol 3.0 Propolis extract 0.4
Essence 0.2 Aloe vulgaris leaf extract 0.05
Water 14 / /
Embodiment 7, is with the difference of embodiment 6, adds propylene glycol weight portion different with mode.Operation specific as follows: Step S1, takes formula ratio sodium methyl cocoyl taurate, cocos nucifera oil acyl isethionic acid ester sodium, lauryl alcohol sulfosuccinate two Sodium, cocamido propyl betaine, laureth sulfuric ester ammonium, EDETATE SODIUM, propylene glycol 0.2 part (0.6 part altogether), glycerol Add to reactor with water, be warming up to 75～80 DEG C, stir 30～35 minutes mixed dissolutions and uniformly obtain mixture S1；Step S2, in the thickening agent that the mixture S1 of the reactor of step S1 adds formula ratio, stirs 15～20 minutes mix homogeneously and is mixed Compound S2；Step S3, is incubated at a temperature of environment 75～80 DEG C in reactor the mixture S2 in step S2, period Carry out low rate mixing 20～do defoaming treatment after 30 minutes；Step S4, cools to 30～55 DEG C by the reactor of step S3, adds The preservative of formula ratio, propolis extract, Mentholum 0.04 part, residue propylene glycol 0.4 part and Aloe vulgaris leaf extract, stir Mix 15～20 minutes mix homogeneously and prepare product.
Comparative example 1
Form 7 comparative example 1: each component of facial milk cleanser and parts by weight thereof
Component Number (part) Component Number (part)
Lauric acid sodium taurocholate 12 Sodium lauroyl glutamate 10
Glycol distearate 5.0 Laureth sulfuric ester ammonium 3.0
Sorbitol 3.5 Acrylic copolymer 4.5
Sodium chloride 2.5 Magnesium nitrate 0.25
Comparative example 2
Form 8 comparative example 2: each component of facial milk cleanser and parts by weight thereof
Product property characterizes one, pain symptom test when using facial milk cleanser: respectively by embodiment 1～7, comparative example 1 and comparative example 2 Prepared facial milk cleanser cleaning face, observes and experiences using effect.Using method: randomly select 100 experimenters, be divided into 5 Group, often organizes 20 people, directly uses tested products, face is drenched with clear water before using, and extrudes appropriate facial milk cleanser in the centre of the palm, adds A small amount of clear water has rubbed abundant foam, rinses well with clear water in a moment at face message.Observe and inquire with or without local bad Reaction, and itemized record result, result is presented as pain weight symptom, has drafted twinge, slight twinge, skin tight, without pain Pain is without tight, comfortable, 5 indexs as snug as a bug in a rug, and record result is as shown in table 9；
Product property characterizes two, skin repair aptitude tests: respectively with prepared by embodiment 1～7, comparative example 1 and comparative example 2 Facial milk cleanser cleaning face, observes and experiences using effect.Using method: the experimenter that 40 skin of face of certain selected are red and swollen, It is divided into 8 groups, often organizes 5 people, directly use tested products, before using, face is drenched with clear water, extrude appropriate facial milk cleanser in the centre of the palm, Add a small amount of clear water and rubbed abundant foam, rinse well with clear water in a moment at face message.See after adhering to using one month Examining the red and swollen degree of skin of face, and itemized record result, red and swollen degree is presented as 0～100 grade, and wherein 0 grade is red and swollen elimination, 100 grades for red and swollen degree for weakening, record result as shown in table 11.
Form 9: pain symptom and the performance parameter of skin repair ability when using facial milk cleanser
This specific embodiment is only explanation of the invention, and it is not limitation of the present invention, and those skilled in the art exist As required the present embodiment can be made after reading this specification and there is no the amendment of creative contribution, but as long as in the present invention Right in all protected by Patent Law.

Claims (8)

1. a facial milk cleanser, it is characterised in that include the component of following weight portion: sodium methyl cocoyl taurate 8 ~ 22 parts, 3 ~ 12 parts of cocos nucifera oil acyl isethionic acid ester sodium, lauryl alcohol sulfosuccinate disodium 2 ~ 5 parts, cocamido propyl betaine 2 ~ 10 Part, laureth sulfuric ester ammonium 1 ~ 5 part, thickening agent 3 ~ 10 parts, preservative 0.1 ~ 0.5 part, EDETATE SODIUM 0.05 ~ 0.2 part, third Glycol 0.2 ~ 0.6 part, glycerol 2 ~ 12 parts, 0.1 ~ 0.5 part of essence, 10 ~ 18 parts of water.
A kind of facial milk cleanser the most according to claim 1, it is characterised in that described thickening agent is that sodium chloride, acrylic compounds are common One or more of polymers and methyl glucose dioleate.
A kind of facial milk cleanser the most according to claim 1, it is characterised in that described preservative is that hydantoin, methyl chloride are different One or more of thiazolinone, Methylisothiazolinone, magnesium nitrate and magnesium chloride.
A kind of facial milk cleanser the most according to claim 1, it is characterised in that also include propolis extract, in parts by weight, Described propolis extract 0.2 ~ 0.5 part.
A kind of facial milk cleanser the most according to claim 4, it is characterised in that also include Aloe vulgaris leaf extract, with Weight portion meter, described Aloe vulgaris leaf extract 0.05 ~ 0.35 part.
A kind of facial milk cleanser the most according to claim 4, it is characterised in that also include Mentholum, the weight of described Mentholum Amount part is (0.5 ~ 0.15) with the weight part ratio of propylene glycol: 1.
7. the method preparing a kind of facial milk cleanser as claimed in claim 6, comprises the steps: step S1, takes formula ratio Sodium methyl cocoyl taurate 8 ~ 22 parts, 3 ~ 12 parts of cocos nucifera oil acyl isethionic acid ester sodium, lauryl alcohol sulfosuccinate disodium 2 ~ 5 Part, cocamido propyl betaine 2 ~ 10 parts, laureth sulfuric ester ammonium 1 ~ 5 part, EDETATE SODIUM 0.05 ~ 0.2 part, propylene glycol 0.2 ~ 0.6 part, glycerol 2 ~ 12 parts and 10 ~ 18 parts of water add to reactor, are warming up to 75 ~ 80 DEG C, stir mixing in 30 ~ 35 minutes molten Solution uniformly obtains mixture S1；Step S2, adds the thickening agent 3 ~ 10 parts of formula ratio in the mixture S1 of the reactor of step S1, Stir 15 ~ 20 minutes mix homogeneously and obtain mixture S2；Step S3, to mixture S2 environment 75 in reactor in step S2 Be incubated at a temperature of ~ 80 DEG C, period carry out low rate mixing 20 ~ 30 minutes after do defoaming treatment；Step S4, by step S3 Reactor cools to 30 ~ 55 DEG C, adds the preservative 0.1 ~ 0.5 part of formula ratio, stirs 15 ~ 20 minutes mix homogeneously and prepares product Thing.
A kind of facial milk cleanser the most according to claim 7, it is characterised in that in parts by weight, add in described step S1 Propylene glycol 0.4 part；In described step 4, remaining to Mentholum and formula ratio propylene glycol is first mixed and is then added to reactor afterwards In.
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CN106491387A (en) * 2016-12-06 2017-03-15 广州聚禅现代农业研究院有限公司 A kind of skin Caring facial milk cleanser containing chive polysaccharide
CN107049816A (en) * 2017-04-25 2017-08-18 佛山市富馨科技实业有限公司 One kind hair washing, face cleaning and take a shower three-in-one purification breast and preparation method
CN107184460A (en) * 2017-05-22 2017-09-22 邵洁明 A kind of cucumber mildy wash
CN107184419A (en) * 2017-05-22 2017-09-22 邵洁明 A kind of gel-type mildy wash and preparation method
CN107693403A (en) * 2017-11-02 2018-02-16 青海喜玛拉雅健康产业发展有限公司 A kind of face cleaning emulsion and preparation method thereof
CN107714553A (en) * 2017-11-23 2018-02-23 丹东欣时代生物医药科技有限公司 A kind of anti-oxidant mildy wash and preparation method thereof
CN108096048A (en) * 2018-01-20 2018-06-01 广州康芙莱生物科技有限公司 A kind of pure amino acid mildy wash with reproducibility and preparation method thereof and application method
CN110035738A (en) * 2016-12-09 2019-07-19 莱雅公司 Flexible solid cosmetic composition and cosmetic treatment method comprising sulfonic acid analog anion surfactants, fatty ester and fatty alcohol
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CN110711154A (en) * 2019-11-15 2020-01-21 广州市攸澜化妆品有限公司 Sea salt particle frosted facial cleanser and preparation method thereof
CN111000768A (en) * 2019-12-19 2020-04-14 天津达仁堂京万红药业有限公司 Plant extract soothing amino acid facial cleanser and preparation method thereof
CN111743790A (en) * 2020-07-21 2020-10-09 广东盐业健康产业发展有限公司 Low-viscosity sea salt oral care mouth wash
CN111840185A (en) * 2020-08-27 2020-10-30 刘克武 Chinese medicinal wormwood face wash
CN112076144A (en) * 2020-10-19 2020-12-15 湖南金昌生物技术有限公司 Soft skin and face cleaning powder and preparation method thereof
CN112438923A (en) * 2020-11-27 2021-03-05 山东花物堂生物科技有限公司 Ice cream appearance texture scrub cream and manufacturing process
CN112842925A (en) * 2021-01-20 2021-05-28 广州杨森药业有限公司 Mild amino acid facial cleanser and preparation method thereof
CN113509410A (en) * 2021-08-12 2021-10-19 青海湖宝生物科技有限公司 Cleansing cream containing black mud of Qinghai salt lake and preparation method thereof
CN114522114A (en) * 2022-01-25 2022-05-24 广州暨大美塑生物科技有限公司 Skin cleaning product and preparation method and application thereof
CN116459196A (en) * 2023-05-06 2023-07-21 广州芙莉莱化妆品有限公司 Soft, moist and mild facial cleanser with high starch content and preparation method thereof

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CN106491387A (en) * 2016-12-06 2017-03-15 广州聚禅现代农业研究院有限公司 A kind of skin Caring facial milk cleanser containing chive polysaccharide
CN110035738B (en) * 2016-12-09 2022-06-28 莱雅公司 Flexible solid cosmetic composition and cosmetic treatment method
CN110035738A (en) * 2016-12-09 2019-07-19 莱雅公司 Flexible solid cosmetic composition and cosmetic treatment method comprising sulfonic acid analog anion surfactants, fatty ester and fatty alcohol
CN107049816A (en) * 2017-04-25 2017-08-18 佛山市富馨科技实业有限公司 One kind hair washing, face cleaning and take a shower three-in-one purification breast and preparation method
CN107184460A (en) * 2017-05-22 2017-09-22 邵洁明 A kind of cucumber mildy wash
CN107184419A (en) * 2017-05-22 2017-09-22 邵洁明 A kind of gel-type mildy wash and preparation method
CN107693403A (en) * 2017-11-02 2018-02-16 青海喜玛拉雅健康产业发展有限公司 A kind of face cleaning emulsion and preparation method thereof
CN107714553A (en) * 2017-11-23 2018-02-23 丹东欣时代生物医药科技有限公司 A kind of anti-oxidant mildy wash and preparation method thereof
CN108096048A (en) * 2018-01-20 2018-06-01 广州康芙莱生物科技有限公司 A kind of pure amino acid mildy wash with reproducibility and preparation method thereof and application method
CN110074991A (en) * 2019-05-28 2019-08-02 南靖珠曼生物科技有限公司 A kind of amino acid facial cleanser and processing technology
CN110711154A (en) * 2019-11-15 2020-01-21 广州市攸澜化妆品有限公司 Sea salt particle frosted facial cleanser and preparation method thereof
CN111000768A (en) * 2019-12-19 2020-04-14 天津达仁堂京万红药业有限公司 Plant extract soothing amino acid facial cleanser and preparation method thereof
CN111743790A (en) * 2020-07-21 2020-10-09 广东盐业健康产业发展有限公司 Low-viscosity sea salt oral care mouth wash
CN111840185A (en) * 2020-08-27 2020-10-30 刘克武 Chinese medicinal wormwood face wash
CN112076144A (en) * 2020-10-19 2020-12-15 湖南金昌生物技术有限公司 Soft skin and face cleaning powder and preparation method thereof
CN112438923A (en) * 2020-11-27 2021-03-05 山东花物堂生物科技有限公司 Ice cream appearance texture scrub cream and manufacturing process
CN112842925A (en) * 2021-01-20 2021-05-28 广州杨森药业有限公司 Mild amino acid facial cleanser and preparation method thereof
CN113509410A (en) * 2021-08-12 2021-10-19 青海湖宝生物科技有限公司 Cleansing cream containing black mud of Qinghai salt lake and preparation method thereof
CN114522114A (en) * 2022-01-25 2022-05-24 广州暨大美塑生物科技有限公司 Skin cleaning product and preparation method and application thereof
CN114522114B (en) * 2022-01-25 2024-02-23 广州暨大美塑生物科技有限公司 Skin cleaning product and preparation method and application thereof
CN116459196A (en) * 2023-05-06 2023-07-21 广州芙莉莱化妆品有限公司 Soft, moist and mild facial cleanser with high starch content and preparation method thereof

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