CN105862106A - 一种钛及钛合金表面双色膜层的制备方法 - Google Patents
一种钛及钛合金表面双色膜层的制备方法 Download PDFInfo
- Publication number
- CN105862106A CN105862106A CN201610354758.4A CN201610354758A CN105862106A CN 105862106 A CN105862106 A CN 105862106A CN 201610354758 A CN201610354758 A CN 201610354758A CN 105862106 A CN105862106 A CN 105862106A
- Authority
- CN
- China
- Prior art keywords
- titanium
- titanium alloy
- alloy surface
- acid
- film layer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229910001069 Ti alloy Inorganic materials 0.000 title claims abstract description 111
- 239000010936 titanium Substances 0.000 title claims abstract description 107
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 title claims abstract description 106
- 229910052719 titanium Inorganic materials 0.000 title claims abstract description 106
- 238000000034 method Methods 0.000 title claims abstract description 71
- 238000005530 etching Methods 0.000 claims abstract description 36
- 238000005554 pickling Methods 0.000 claims abstract description 34
- 239000003960 organic solvent Substances 0.000 claims abstract description 24
- 238000004040 coloring Methods 0.000 claims abstract description 15
- 238000004140 cleaning Methods 0.000 claims abstract description 8
- 239000002253 acid Substances 0.000 claims description 61
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 42
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 24
- 229910017604 nitric acid Inorganic materials 0.000 claims description 24
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 23
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 23
- 238000002360 preparation method Methods 0.000 claims description 21
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 18
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 16
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 16
- 239000003292 glue Substances 0.000 claims description 14
- 229920002521 macromolecule Polymers 0.000 claims description 14
- 230000003746 surface roughness Effects 0.000 claims description 14
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 12
- 239000001117 sulphuric acid Substances 0.000 claims description 12
- 235000011149 sulphuric acid Nutrition 0.000 claims description 12
- 238000004090 dissolution Methods 0.000 claims description 10
- 239000003795 chemical substances by application Substances 0.000 claims description 7
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 claims description 2
- 238000001035 drying Methods 0.000 claims description 2
- 238000007654 immersion Methods 0.000 claims description 2
- 239000002904 solvent Substances 0.000 claims description 2
- 230000007547 defect Effects 0.000 abstract description 4
- 230000000873 masking effect Effects 0.000 abstract 2
- 238000000861 blow drying Methods 0.000 abstract 1
- 230000003647 oxidation Effects 0.000 abstract 1
- 238000007254 oxidation reaction Methods 0.000 abstract 1
- 239000010408 film Substances 0.000 description 35
- 239000000243 solution Substances 0.000 description 33
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 24
- 239000008213 purified water Substances 0.000 description 10
- 239000012459 cleaning agent Substances 0.000 description 5
- 239000011259 mixed solution Substances 0.000 description 5
- 238000002156 mixing Methods 0.000 description 5
- 239000003086 colorant Substances 0.000 description 3
- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 description 2
- 239000004925 Acrylic resin Substances 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- 238000010923 batch production Methods 0.000 description 2
- 238000002513 implantation Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 229920001568 phenolic resin Polymers 0.000 description 2
- 239000005011 phenolic resin Substances 0.000 description 2
- FFRBMBIXVSCUFS-UHFFFAOYSA-N 2,4-dinitro-1-naphthol Chemical compound C1=CC=C2C(O)=C([N+]([O-])=O)C=C([N+]([O-])=O)C2=C1 FFRBMBIXVSCUFS-UHFFFAOYSA-N 0.000 description 1
- 101001018064 Homo sapiens Lysosomal-trafficking regulator Proteins 0.000 description 1
- 241000222065 Lycoperdon Species 0.000 description 1
- 102100033472 Lysosomal-trafficking regulator Human genes 0.000 description 1
- 244000038561 Modiola caroliniana Species 0.000 description 1
- 235000010703 Modiola caroliniana Nutrition 0.000 description 1
- 241000768494 Polymorphum Species 0.000 description 1
- 244000061458 Solanum melongena Species 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000003822 epoxy resin Substances 0.000 description 1
- 230000001795 light effect Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229920000647 polyepoxide Polymers 0.000 description 1
- 229910001753 sapphirine Inorganic materials 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000004381 surface treatment Methods 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D11/00—Electrolytic coating by surface reaction, i.e. forming conversion layers
- C25D11/02—Anodisation
- C25D11/26—Anodisation of refractory metals or alloys based thereon
Abstract
Description
Claims (10)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201610354758.4A CN105862106B (zh) | 2016-05-26 | 2016-05-26 | 一种钛及钛合金表面双色膜层的制备方法 |
Applications Claiming Priority (1)
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CN201610354758.4A CN105862106B (zh) | 2016-05-26 | 2016-05-26 | 一种钛及钛合金表面双色膜层的制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN105862106A true CN105862106A (zh) | 2016-08-17 |
CN105862106B CN105862106B (zh) | 2018-05-18 |
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Family Applications (1)
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CN201610354758.4A Active CN105862106B (zh) | 2016-05-26 | 2016-05-26 | 一种钛及钛合金表面双色膜层的制备方法 |
Country Status (1)
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106801244A (zh) * | 2016-12-19 | 2017-06-06 | 佛山市安齿生物科技有限公司 | 一种牙种植体基台的着色方法 |
CN109750338A (zh) * | 2017-11-08 | 2019-05-14 | 天津正天医疗器械有限公司 | 钛及钛合金高光亮着色工艺 |
CN110965098A (zh) * | 2019-11-30 | 2020-04-07 | 华南理工大学 | 一种多孔多级结构阳极氧化铝模板及其制备方法 |
CN112779583A (zh) * | 2020-12-26 | 2021-05-11 | 常州市钛宇新材料科技有限公司 | 一种彩色和厚膜结合的钛合金表面处理方法 |
CN113684517A (zh) * | 2021-09-10 | 2021-11-23 | 西安赛特思捷金属制品有限公司 | 一种基于阳极氧化的钛板画制备方法 |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS6270599A (ja) * | 1985-09-24 | 1987-04-01 | Kowa Eng Kk | 装飾品における多色被膜形成方法 |
CN1421548A (zh) * | 2001-11-22 | 2003-06-04 | 鸿富锦精密工业(深圳)有限公司 | 金属基体表面阳极处理方法 |
CN101096772A (zh) * | 2006-06-30 | 2008-01-02 | 佛山市顺德区汉达精密电子科技有限公司 | 钛合金阳极氧化多彩图案的制备方法 |
CN101457380A (zh) * | 2007-12-14 | 2009-06-17 | 深圳富泰宏精密工业有限公司 | 金属表面阳极处理方法 |
CN102864480A (zh) * | 2012-08-31 | 2013-01-09 | 北京工业大学 | 一种三维网络结构二氧化钛纳米管阵列的制备方法 |
CN102953109A (zh) * | 2011-08-26 | 2013-03-06 | 可成科技股份有限公司 | 双色阳极钛膜形成方法及其制品 |
-
2016
- 2016-05-26 CN CN201610354758.4A patent/CN105862106B/zh active Active
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS6270599A (ja) * | 1985-09-24 | 1987-04-01 | Kowa Eng Kk | 装飾品における多色被膜形成方法 |
CN1421548A (zh) * | 2001-11-22 | 2003-06-04 | 鸿富锦精密工业(深圳)有限公司 | 金属基体表面阳极处理方法 |
CN101096772A (zh) * | 2006-06-30 | 2008-01-02 | 佛山市顺德区汉达精密电子科技有限公司 | 钛合金阳极氧化多彩图案的制备方法 |
CN101457380A (zh) * | 2007-12-14 | 2009-06-17 | 深圳富泰宏精密工业有限公司 | 金属表面阳极处理方法 |
CN102953109A (zh) * | 2011-08-26 | 2013-03-06 | 可成科技股份有限公司 | 双色阳极钛膜形成方法及其制品 |
CN102864480A (zh) * | 2012-08-31 | 2013-01-09 | 北京工业大学 | 一种三维网络结构二氧化钛纳米管阵列的制备方法 |
Non-Patent Citations (2)
Title |
---|
徐浩等: ""不同酸处理对钛基体性能的影响"", 《稀有金属材料与工程》 * |
石瑶: ""微纳米图案化处理对钛表面性能的影响"", 《中国优秀硕士学位论文全文数据库(电子期刊)》 * |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106801244A (zh) * | 2016-12-19 | 2017-06-06 | 佛山市安齿生物科技有限公司 | 一种牙种植体基台的着色方法 |
CN109750338A (zh) * | 2017-11-08 | 2019-05-14 | 天津正天医疗器械有限公司 | 钛及钛合金高光亮着色工艺 |
CN110965098A (zh) * | 2019-11-30 | 2020-04-07 | 华南理工大学 | 一种多孔多级结构阳极氧化铝模板及其制备方法 |
CN112779583A (zh) * | 2020-12-26 | 2021-05-11 | 常州市钛宇新材料科技有限公司 | 一种彩色和厚膜结合的钛合金表面处理方法 |
CN113684517A (zh) * | 2021-09-10 | 2021-11-23 | 西安赛特思捷金属制品有限公司 | 一种基于阳极氧化的钛板画制备方法 |
Also Published As
Publication number | Publication date |
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CN105862106B (zh) | 2018-05-18 |
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Effective date of registration: 20190430 Address after: 361027 No. 18 Shanbian Hongdong Road, Haicang District, Xiamen City, Fujian Province Co-patentee after: BOYINING (XIAMEN) MEDICAL APPARATUS AND INSTRUMENTS CO.,LTD. Patentee after: DOUBLE MEDICAL TECHNOLOGY Inc. Address before: 361027 No. 18 Shanbian Hongdong Road, Haicang District, Xiamen City, Fujian Province Patentee before: DOUBLE MEDICAL TECHNOLOGY Inc. |
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Effective date of registration: 20231207 Address after: No. 18 Shanbian Hongdong Road, Haicang District, Xiamen City, Fujian Province, 361000 Patentee after: DOUBLE MEDICAL TECHNOLOGY Inc. Patentee after: BOYINING (XIAMEN) MEDICAL APPARATUS AND INSTRUMENTS CO.,LTD. Patentee after: SHENZHEN WORLD SURGERY MEDICAL DEVICE TECHNOLOGY Co.,Ltd. Address before: 361027 No. 18 Shanbian Hongdong Road, Haicang District, Xiamen City, Fujian Province Patentee before: DOUBLE MEDICAL TECHNOLOGY Inc. Patentee before: BOYINING (XIAMEN) MEDICAL APPARATUS AND INSTRUMENTS CO.,LTD. |
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TR01 | Transfer of patent right |