CN105768101A - 一种红豆加工预煮液的利用方法 - Google Patents
一种红豆加工预煮液的利用方法 Download PDFInfo
- Publication number
- CN105768101A CN105768101A CN201610185443.1A CN201610185443A CN105768101A CN 105768101 A CN105768101 A CN 105768101A CN 201610185443 A CN201610185443 A CN 201610185443A CN 105768101 A CN105768101 A CN 105768101A
- Authority
- CN
- China
- Prior art keywords
- semen phaseoli
- red bean
- liquid
- enzymolysis
- essence
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000007788 liquid Substances 0.000 title claims abstract description 40
- 238000000034 method Methods 0.000 title claims abstract description 35
- 240000001417 Vigna umbellata Species 0.000 title abstract description 18
- 235000011453 Vigna umbellata Nutrition 0.000 title abstract description 18
- 230000008569 process Effects 0.000 claims abstract description 17
- 238000001694 spray drying Methods 0.000 claims abstract description 17
- 102000004190 Enzymes Human genes 0.000 claims abstract description 16
- 108090000790 Enzymes Proteins 0.000 claims abstract description 16
- 239000000463 material Substances 0.000 claims abstract description 15
- 150000008442 polyphenolic compounds Chemical class 0.000 claims abstract description 15
- 235000013824 polyphenols Nutrition 0.000 claims abstract description 15
- 229930182490 saponin Natural products 0.000 claims abstract description 14
- 235000017709 saponins Nutrition 0.000 claims abstract description 14
- 150000007949 saponins Chemical class 0.000 claims abstract description 14
- 229930003935 flavonoid Natural products 0.000 claims abstract description 13
- 235000017173 flavonoids Nutrition 0.000 claims abstract description 13
- 150000002215 flavonoids Chemical class 0.000 claims abstract description 13
- 102000004169 proteins and genes Human genes 0.000 claims abstract description 13
- 108090000623 proteins and genes Proteins 0.000 claims abstract description 13
- 239000000706 filtrate Substances 0.000 claims abstract description 12
- 235000013305 food Nutrition 0.000 claims abstract description 12
- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract description 11
- 239000011707 mineral Substances 0.000 claims abstract description 11
- 238000001914 filtration Methods 0.000 claims abstract description 9
- 230000036541 health Effects 0.000 claims abstract description 8
- 239000012535 impurity Substances 0.000 claims abstract description 8
- 239000000047 product Substances 0.000 claims abstract description 8
- 239000002537 cosmetic Substances 0.000 claims abstract description 7
- 210000000582 semen Anatomy 0.000 claims description 81
- 229940088598 enzyme Drugs 0.000 claims description 15
- 239000000126 substance Substances 0.000 claims description 15
- 108091005804 Peptidases Proteins 0.000 claims description 7
- 239000004365 Protease Substances 0.000 claims description 7
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 claims description 7
- 102000004139 alpha-Amylases Human genes 0.000 claims description 7
- 108090000637 alpha-Amylases Proteins 0.000 claims description 7
- 229940024171 alpha-amylase Drugs 0.000 claims description 7
- 238000001728 nano-filtration Methods 0.000 claims description 7
- 239000007787 solid Substances 0.000 claims description 7
- 238000007738 vacuum evaporation Methods 0.000 claims description 6
- 239000002351 wastewater Substances 0.000 abstract description 6
- 239000004615 ingredient Substances 0.000 abstract description 5
- 238000005516 engineering process Methods 0.000 abstract description 3
- 239000000843 powder Substances 0.000 abstract description 3
- 230000000415 inactivating effect Effects 0.000 abstract 1
- 230000001766 physiological effect Effects 0.000 abstract 1
- 235000018102 proteins Nutrition 0.000 description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- 235000013361 beverage Nutrition 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 6
- 239000008280 blood Substances 0.000 description 4
- 210000004369 blood Anatomy 0.000 description 4
- 235000015097 nutrients Nutrition 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 235000016709 nutrition Nutrition 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 2
- PVNIIMVLHYAWGP-UHFFFAOYSA-N Niacin Chemical compound OC(=O)C1=CC=CN=C1 PVNIIMVLHYAWGP-UHFFFAOYSA-N 0.000 description 2
- 244000046052 Phaseolus vulgaris Species 0.000 description 2
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 2
- 208000004880 Polyuria Diseases 0.000 description 2
- AUNGANRZJHBGPY-SCRDCRAPSA-N Riboflavin Chemical compound OC[C@@H](O)[C@@H](O)[C@@H](O)CN1C=2C=C(C)C(C)=CC=2N=C2C1=NC(=O)NC2=O AUNGANRZJHBGPY-SCRDCRAPSA-N 0.000 description 2
- 230000000975 bioactive effect Effects 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 235000009508 confectionery Nutrition 0.000 description 2
- 230000035619 diuresis Effects 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 235000020124 milk-based beverage Nutrition 0.000 description 2
- 230000035764 nutrition Effects 0.000 description 2
- 239000000049 pigment Substances 0.000 description 2
- 230000001737 promoting effect Effects 0.000 description 2
- 239000001397 quillaja saponaria molina bark Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 210000000952 spleen Anatomy 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- 238000004065 wastewater treatment Methods 0.000 description 2
- 235000017060 Arachis glabrata Nutrition 0.000 description 1
- 244000105624 Arachis hypogaea Species 0.000 description 1
- 235000010777 Arachis hypogaea Nutrition 0.000 description 1
- 235000018262 Arachis monticola Nutrition 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 206010007247 Carbuncle Diseases 0.000 description 1
- 206010010774 Constipation Diseases 0.000 description 1
- AUNGANRZJHBGPY-UHFFFAOYSA-N D-Lyxoflavin Natural products OCC(O)C(O)C(O)CN1C=2C=C(C)C(C)=CC=2N=C2C1=NC(=O)NC2=O AUNGANRZJHBGPY-UHFFFAOYSA-N 0.000 description 1
- 206010012735 Diarrhoea Diseases 0.000 description 1
- 208000015220 Febrile disease Diseases 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- IMQLKJBTEOYOSI-GPIVLXJGSA-N Inositol-hexakisphosphate Chemical compound OP(O)(=O)O[C@H]1[C@H](OP(O)(O)=O)[C@@H](OP(O)(O)=O)[C@H](OP(O)(O)=O)[C@H](OP(O)(O)=O)[C@@H]1OP(O)(O)=O IMQLKJBTEOYOSI-GPIVLXJGSA-N 0.000 description 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 1
- 206010030113 Oedema Diseases 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- IMQLKJBTEOYOSI-UHFFFAOYSA-N Phytic acid Natural products OP(O)(=O)OC1C(OP(O)(O)=O)C(OP(O)(O)=O)C(OP(O)(O)=O)C(OP(O)(O)=O)C1OP(O)(O)=O IMQLKJBTEOYOSI-UHFFFAOYSA-N 0.000 description 1
- 108010073771 Soybean Proteins Proteins 0.000 description 1
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 description 1
- JZRWCGZRTZMZEH-UHFFFAOYSA-N Thiamine Natural products CC1=C(CCO)SC=[N+]1CC1=CN=C(C)N=C1N JZRWCGZRTZMZEH-UHFFFAOYSA-N 0.000 description 1
- 241000219977 Vigna Species 0.000 description 1
- 235000010716 Vigna mungo Nutrition 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000036772 blood pressure Effects 0.000 description 1
- 210000001124 body fluid Anatomy 0.000 description 1
- 239000010839 body fluid Substances 0.000 description 1
- 235000012970 cakes Nutrition 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 235000014510 cooky Nutrition 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 235000013325 dietary fiber Nutrition 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- 150000002212 flavone derivatives Chemical class 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- 235000015203 fruit juice Nutrition 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 238000002372 labelling Methods 0.000 description 1
- 235000004213 low-fat Nutrition 0.000 description 1
- 239000008204 material by function Substances 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 239000002366 mineral element Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 235000001968 nicotinic acid Nutrition 0.000 description 1
- 229960003512 nicotinic acid Drugs 0.000 description 1
- 239000011664 nicotinic acid Substances 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 235000020232 peanut Nutrition 0.000 description 1
- 230000000144 pharmacologic effect Effects 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 235000002949 phytic acid Nutrition 0.000 description 1
- 229940068041 phytic acid Drugs 0.000 description 1
- 239000000467 phytic acid Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 235000021251 pulses Nutrition 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 230000003014 reinforcing effect Effects 0.000 description 1
- 235000019192 riboflavin Nutrition 0.000 description 1
- 229960002477 riboflavin Drugs 0.000 description 1
- 239000002151 riboflavin Substances 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 235000019991 rice wine Nutrition 0.000 description 1
- 230000002000 scavenging effect Effects 0.000 description 1
- 238000005201 scrubbing Methods 0.000 description 1
- 239000010865 sewage Substances 0.000 description 1
- 235000013555 soy sauce Nutrition 0.000 description 1
- 235000019710 soybean protein Nutrition 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 235000018553 tannin Nutrition 0.000 description 1
- 239000001648 tannin Substances 0.000 description 1
- 229920001864 tannin Polymers 0.000 description 1
- 238000002560 therapeutic procedure Methods 0.000 description 1
- 235000019157 thiamine Nutrition 0.000 description 1
- KYMBYSLLVAOCFI-UHFFFAOYSA-N thiamine Chemical compound CC1=C(CCO)SCN1CC1=CN=C(C)N=C1N KYMBYSLLVAOCFI-UHFFFAOYSA-N 0.000 description 1
- 229960003495 thiamine Drugs 0.000 description 1
- 239000011721 thiamine Substances 0.000 description 1
- 239000003440 toxic substance Substances 0.000 description 1
- 235000021419 vinegar Nutrition 0.000 description 1
- 239000000052 vinegar Substances 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 1
- 235000014101 wine Nutrition 0.000 description 1
- 235000013618 yogurt Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/19—Preparation or pretreatment of starting material involving fermentation using yeast, bacteria or both; enzymatic treatment
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- General Health & Medical Sciences (AREA)
- Epidemiology (AREA)
- Veterinary Medicine (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Engineering & Computer Science (AREA)
- Public Health (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Animal Behavior & Ethology (AREA)
- Medical Informatics (AREA)
- Pharmacology & Pharmacy (AREA)
- Chemical & Material Sciences (AREA)
- Medicinal Chemistry (AREA)
- Alternative & Traditional Medicine (AREA)
- Birds (AREA)
- Cosmetics (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
本发明公开了一种红豆加工预煮液的利用方法,本发明涉及废水利用和食品加工技术领域,本发明方法中,红豆加工预煮液经酶解后,灭酶,然后过滤除去固体杂质,滤液浓缩后喷雾干燥得富含多酚类物质、黄酮类物质、皂苷类物质、可溶性蛋白和矿物质的红豆精华素。通过本发明方法,对红豆加工过程中产生的大量废水(红豆加工预煮液)加以高值利用,工艺简单,得到的红豆精华素富含多酚类物质、黄酮类物质、皂苷类物质、可溶性蛋白质和矿物质;红豆精华素具有很好的生理活性,且得到的红豆精华素为粉末物质,可作为食品、保健品和化妆品的配料。
Description
技术领域
本发明涉及废水利用和食品加工技术领域,特别涉及一种红豆加工预煮液的利用方法。
背景技术
红豆,又名红小豆、赤小豆、赤豆,属豆科豇豆属,一年生直立或缠绕草本植物,为豆科植物赤豆的成熟种子。红豆是一种低蛋白、低脂肪、高碳水化合物的食物,常与大米一起煮饭熬粥,故此被人们称为“饭豆”,是餐桌上老少皆食的豆类食品。据有关测定,每100g红豆中含蛋白质20.0g、脂肪0.5g、糖类58.5g、粗纤维4.9g、总膳食纤维23.5g,微量维生素B10.3mg、B20.11mg等。还含有钙67.00mg、磷305.00mg、铁5.20mg、硫胺素0.31mg、核黄素0.11mg、尼克酸2.70mg。可见,红豆中含有丰富的营养物质。
在中医药学发展史上,赤小豆很早就作为药物应用,《神农本草经》中记载:“赤小豆,主下水,排痈肿脓血。”《伤寒论》和《金匮要略》中的多个方剂中都用到了红小豆。李时珍将之称为“心之谷”,认为其味甘酸、性平,无毒,有健脾止泻、利水消肿、解毒排脓、清热去湿、补脾补血、生津益气等功效,现代研究还发现红豆种皮中含有多种生物活性成分,如多酚、单宁、植酸、皂甙和色素等,具有抗氧化、增强免疫、抗菌等药理作用。红豆中所含的丰富的功能性物质,使红豆的开发利用在医药和保健品行业占有重要地位。在我国红豆已是食品和饮料加工业的重要原料之一。在饮料行业中,可以做成红豆饮料,如红豆番茄乳饮料、红豆花生饮料、红豆果汁乳饮料、红豆纤维饮料,也可做成红豆酸奶、红豆果醋、红豆米酒,红豆糕点和红豆沙等。国外因为红豆资源较少,研究利用不是很多,但在日本和国内,红豆主要用来制作甜豆和红豆沙。
红豆加工预煮液的产生来源于红豆沙的生产。在工厂化生产过程中,大量红豆经清洗后和水以1:3-1:4的质量体积比混合,高温煮制3个小时,直至红豆松软,过滤后红豆预煮液被作为废水,经处理后直接排放。基于红豆所含的丰富营养物质和功能性成分,在其长时间高温煮制过程中大量营养物质释放并溶于水中,而将红豆水当做废水处理排放是目前红豆沙生产企业的普遍处理办法。
红豆沙的加工过程中产生了大量的加工废弃液,但其中含有大量的蛋白质、矿物元素、黄酮,多酚等营养及生物活性成分。目前,红豆沙生产企业对预煮液的处理方式普遍为当做废水处理,这一方法不仅使处理过程中产生大量污水,污染环境,增加除污资金,而且其营养物质未能得到充分利用,使红豆利用价值大打折扣。如若将预煮液再利用,不仅可以节约大量水资源,而且保留了红豆中大量的色素,酚类化合物等营养物质,这些对人类身体都大有益处。
申请人前期已经利用红豆预煮液开发了饮料、酒等产品,并申请了国家发明专利并获得授权。随着研究的深入,申请人发现红豆加工预煮液中实际上存在的是红豆的可溶性精华成分,开发一种提取红豆预煮液中精华成分并适于工业应用的工艺意义重大。
发明内容
为了弥补以上不足,利用大豆分离蛋白废水发酵生产酱油的方法,该方法生产原料易得,生产周期短,原料利用率高。
本发明的技术方案为:
一种红豆加工预煮液的利用方法,红豆加工预煮液经酶解后,灭酶,然后过滤除去固体杂质,滤液浓缩后喷雾干燥得富含多酚类物质、黄酮类物质、皂苷类物质、可溶性蛋白和矿物质的红豆精华素。
作为优选方案,所述酶解的过程为:加入30-100U/mL的α-淀粉酶,于60-90℃酶解5-30min;再加入100-300U/mL的糖化酶和50-100U/mL蛋白酶,于50-70℃酶解10-20min。基于对红豆加工预煮液成分的分析与研究,为降低料液粘性,且能得到富含多酚类物质、黄酮类物质和皂苷类物质的红豆精华素,采用以上酶解方法。
作为优选方案,所述浓缩采用纳滤浓缩或真空蒸发浓缩。这些浓缩方法简单可行,适于工业应用;且浓缩过程中产生的水可回收利用。
作为优选方案,将滤液浓缩至波美度为1.15-1.25。将滤液浓缩至该浓度范围时,便于后续喷雾干燥制成粉状产品。
作为优选方案,所述喷雾干燥时,进风温度为160-190℃,出风温度为70-90℃。喷雾干燥得参数是从保持红豆精华素营养成分不受破坏以及提高工作效率两方面考虑设置,经过大量研究确定,喷雾干燥时的进风温度和出风温度范围。
采用所述方法得到的红豆精华素在食品、保健品和化妆品中的应用。富含多酚类物质、黄酮类物质、皂苷类物质、可溶性蛋白质和矿物质的红豆精华素作为一种具有生理活性的物质,可用作食品、保健品和化妆品的配料,也可直接食用;应用非常方便且应用范围非常广阔。
当然,绿豆加工预煮液和黑豆加工预煮液也可以采用本发明的方法分别得到绿豆精华素和黑豆精华素。
本发明的有益效果为:
通过本发明方法,对红豆加工过程中产生的大量废水(红豆加工预煮液)加以高值利用,工艺简单,得到的红豆精华素富含多酚类物质、黄酮类物质、皂苷类物质、可溶性蛋白质和矿物质;红豆精华素具有很好的生理活性,且得到的红豆精华素为粉末物质,其所含的多酚类物质、黄酮类物质和皂苷等活性物质具有增强机体免疫力、清除自由基、抗氧化的作用,并能起到利尿、除湿、消肿、润肠通便、调节血糖、调节血压、调节血脂、预防结石、减肥等效果。可作为食品、保健品和化妆品的配料。
本发明不仅解决了废水排放问题,同时提供了一种新的保健物质,且工艺简单,成本低廉,适于产业化应用,意义重大。
具体实施方式
为了使本发明实现的技术手段、创作特征、达成目的与功效易于明白了解,下面结合具体实施例,进一步阐述本发明。
实施例1:
一种红豆加工预煮液的利用方法,包括步骤:
1)向红豆加工预煮液中加入65U/mL的α-淀粉酶,于75℃酶解15min;再加入200U/mL的糖化酶和75U/mL蛋白酶,于60℃酶解15min;
2)灭酶;
3)过滤除去固体杂质;
4)滤液采用纳滤浓缩,浓缩至波美度为1.2;
5)对浓缩液进行喷雾干燥,得富含多酚类物质、黄酮类物质、皂苷类物质、可溶性蛋白和矿物质的红豆精华素;其中喷雾干燥时,进风温度为180℃,出风温度为80℃。
实施例2
一种红豆加工预煮液的利用方法,包括步骤:
1)向红豆加工预煮液中加入90U/mL的α-淀粉酶,于85℃酶解30min;再加入120U/mL的糖化酶和90U/mL蛋白酶,于70℃酶解10min;
2)灭酶;
3)过滤除去固体杂质;
4)滤液采用纳滤浓缩或真空蒸发浓缩,浓缩至波美度为1.15;
5)对浓缩液进行喷雾干燥,得富含多酚类物质、黄酮类物质、皂苷类物质、可溶性蛋白和矿物质的红豆精华素;其中喷雾干燥时,进风温度为170℃,出风温度为70℃。
实施例3
一种红豆加工预煮液的利用方法,包括步骤:
1)向红豆加工预煮液中加入40U/mL的α-淀粉酶,于60℃酶解25min;再加入280U/mL的糖化酶和60U/mL蛋白酶,于50℃酶解20min;
2)灭酶;
3)过滤除去固体杂质;
4)滤液采用纳滤浓缩或真空蒸发浓缩,浓缩至波美度为1.25;
5)对浓缩液进行喷雾干燥,得富含多酚类物质、黄酮类物质、皂苷类物质、可溶性蛋白和矿物质的红豆精华素;其中喷雾干燥时,进风温度为165℃,出风温度为75℃。
实施例4
一种红豆加工预煮液的利用方法,包括步骤:
1)向红豆加工预煮液中加入70U/mL的α-淀粉酶,于70℃酶解20min;再加入180U/mL的糖化酶和70U/mL蛋白酶,于65℃酶解12min;
2)灭酶;
3)过滤除去固体杂质;
4)滤液采用纳滤浓缩或真空蒸发浓缩,浓缩至波美度为1.2;
5)对浓缩液进行喷雾干燥,得富含多酚类物质、黄酮类物质、皂苷类物质、可溶性蛋白和矿物质的红豆精华素;其中喷雾干燥时,进风温度为170℃,出风温度为85℃。
实施例5
一种红豆加工预煮液的利用方法,包括步骤:
1)向红豆加工预煮液中加入50U/mL的α-淀粉酶,于75℃酶解18min;再加入220U/mL的糖化酶和55U/mL蛋白酶,于55℃酶解16min;
2)灭酶;
3)过滤除去固体杂质;
4)滤液采用纳滤浓缩或真空蒸发浓缩,浓缩至波美度为1.25;
5)对浓缩液进行喷雾干燥,得富含多酚类物质、黄酮类物质、皂苷类物质、可溶性蛋白和矿物质的红豆精华素;其中喷雾干燥时,进风温度为170℃,出风温度为80℃。
实施例1-5所制备的红豆精华素可作为饼干、蛋糕、奶粉等食品的配料;也可作为各种饮料的配料添加;还可以作为化妆品的添加组分。赋予食品、饮料和化妆品保健功能。本发明实现了变废为宝。
Claims (6)
1.一种红豆加工预煮液的利用方法,其特征在于:红豆加工预煮液经酶解后,灭酶,然后过滤除去固体杂质,滤液浓缩后喷雾干燥得富含多酚类物质、黄酮类物质、皂苷类物质、可溶性蛋白和矿物质的红豆精华素。
2.如权利要求1所述红豆加工预煮液的利用方法,其特征在于,所述酶解的过程为:加入30-100U/mL的α-淀粉酶,于60-90℃酶解5-30min;再加入100-300U/mL的糖化酶和50-100U/mL蛋白酶,于50-70℃酶解10-20min。
3.如权利要求1所述红豆加工预煮液的利用方法,其特征在于:所述浓缩采用纳滤浓缩或真空蒸发浓缩。
4.如权利要求1或3所述红豆加工预煮液的利用方法,其特征在于:将滤液浓缩至波美度为1.15-1.25。
5.如权利要求1所述红豆加工预煮液的利用方法,其特征在于:所述喷雾干燥时,进风温度为160-190℃,出风温度为70-90℃。
6.采用如权利要求1所述方法得到的红豆精华素在食品、保健品和化妆品中的应用。
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610185443.1A CN105768101A (zh) | 2016-03-29 | 2016-03-29 | 一种红豆加工预煮液的利用方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610185443.1A CN105768101A (zh) | 2016-03-29 | 2016-03-29 | 一种红豆加工预煮液的利用方法 |
Publications (1)
Publication Number | Publication Date |
---|---|
CN105768101A true CN105768101A (zh) | 2016-07-20 |
Family
ID=56391115
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201610185443.1A Pending CN105768101A (zh) | 2016-03-29 | 2016-03-29 | 一种红豆加工预煮液的利用方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN105768101A (zh) |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2003070263A1 (fr) * | 2002-02-20 | 2003-08-28 | Kaneka Corporation | Procede de production d'un extrait hydrophobe de glycyrrhiza de haute qualite |
CN101731581A (zh) * | 2008-11-24 | 2010-06-16 | 陈振贵 | 一种细胞营养素及其制备方法 |
CN103948130A (zh) * | 2014-05-05 | 2014-07-30 | 齐鲁工业大学 | 一种新型红豆饮料的制备方法 |
CN103952259A (zh) * | 2014-05-05 | 2014-07-30 | 齐鲁工业大学 | 一种红豆红枣蜂蜜保健酒的制备方法 |
CN103952258A (zh) * | 2014-05-05 | 2014-07-30 | 齐鲁工业大学 | 一种红豆保健酒的制备方法 |
CN103966049A (zh) * | 2014-05-05 | 2014-08-06 | 齐鲁工业大学 | 一种红豆蜂蜜保健酒的制备方法 |
-
2016
- 2016-03-29 CN CN201610185443.1A patent/CN105768101A/zh active Pending
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2003070263A1 (fr) * | 2002-02-20 | 2003-08-28 | Kaneka Corporation | Procede de production d'un extrait hydrophobe de glycyrrhiza de haute qualite |
CN101731581A (zh) * | 2008-11-24 | 2010-06-16 | 陈振贵 | 一种细胞营养素及其制备方法 |
CN103948130A (zh) * | 2014-05-05 | 2014-07-30 | 齐鲁工业大学 | 一种新型红豆饮料的制备方法 |
CN103952259A (zh) * | 2014-05-05 | 2014-07-30 | 齐鲁工业大学 | 一种红豆红枣蜂蜜保健酒的制备方法 |
CN103952258A (zh) * | 2014-05-05 | 2014-07-30 | 齐鲁工业大学 | 一种红豆保健酒的制备方法 |
CN103966049A (zh) * | 2014-05-05 | 2014-08-06 | 齐鲁工业大学 | 一种红豆蜂蜜保健酒的制备方法 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN103540493B (zh) | 一种灵芝茶酒的配制方法 | |
CN100340651C (zh) | 一种大鲵保健酒及制备方法 | |
CN101558872B (zh) | 一种健脑饮料及大豆蛋白粉的制备方法 | |
CN105475787A (zh) | 一种石斛麦冬乳饮料及其制备方法 | |
CN104255927A (zh) | 一种营养骆驼奶片及其制备方法 | |
CN103948000B (zh) | 一种滁菊酱油的生产方法 | |
CN106666396A (zh) | 一种盐地碱蓬复合营养面条及其制备方法 | |
KR100994196B1 (ko) | 마늘 청국장 발효액의 제조방법 | |
KR20160006427A (ko) | 포제법으로 처리된 한방성분들을 포함하는 어린이용 건강식품 | |
CN100387152C (zh) | 一种以蘑菇和肉类为主的罐头及制作方法 | |
CN1062089A (zh) | 一种食用真菌制备天然饮料的工艺 | |
CN105768101A (zh) | 一种红豆加工预煮液的利用方法 | |
CN106617104A (zh) | 一种清热润肺核桃多肽咀嚼片及其制备方法 | |
CN106579223A (zh) | 一种海芦笋营养面条汤料及其制备方法 | |
KR20060111989A (ko) | 손바닥선인장을 이용한 두부 응고용 조성물 및 그 제조방법 | |
CN106509661A (zh) | 一种驴皮糕及其制备方法 | |
CN106434173A (zh) | 一种红茶味补气强身紫薯糯米酒及其制备方法 | |
CN106262388A (zh) | 一种佛手柑人参果蜂蜜膏及其制作方法 | |
CN105901657A (zh) | 香圆薤白茶酱油的制作工艺 | |
CN1374036A (zh) | 食药用真菌与水果混合酿制保健品和医药及新方法 | |
CN104560573A (zh) | 一种香菇米酒保健饮料 | |
CN104799297B (zh) | 一种山菇健胃颗粒及其制作方法 | |
CN108902351A (zh) | 一种牛奶豆腐乳 | |
CN105995992A (zh) | 一种牛樟芝银耳保健口服液的制备方法 | |
KR102585344B1 (ko) | 낙지볶음 소스 조성물 및 이의 제조 방법 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
RJ01 | Rejection of invention patent application after publication |
Application publication date: 20160720 |
|
RJ01 | Rejection of invention patent application after publication |