CN105733776A - 一种利用石油脂制备的齿轮润滑脂 - Google Patents

一种利用石油脂制备的齿轮润滑脂 Download PDF

Info

Publication number
CN105733776A
CN105733776A CN201610153441.4A CN201610153441A CN105733776A CN 105733776 A CN105733776 A CN 105733776A CN 201610153441 A CN201610153441 A CN 201610153441A CN 105733776 A CN105733776 A CN 105733776A
Authority
CN
China
Prior art keywords
parts
petrolatum
gear
add
heated
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610153441.4A
Other languages
English (en)
Inventor
黄帮义
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Anhui Haydite Oil Chemical Co Ltd
Original Assignee
Anhui Haydite Oil Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Anhui Haydite Oil Chemical Co Ltd filed Critical Anhui Haydite Oil Chemical Co Ltd
Priority to CN201610153441.4A priority Critical patent/CN105733776A/zh
Publication of CN105733776A publication Critical patent/CN105733776A/zh
Pending legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04—Mixtures of base-materials and additives
    • C10M169/048—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution, non-macromolecular and macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/10—Compounds containing silicon
    • C10M2201/102—Silicates
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
    • C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/04—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing aromatic monomers, e.g. styrene
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/06—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing conjugated dienes
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/18—Natural waxes, e.g. ceresin, ozocerite, bees wax, carnauba; Degras
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/02—Hydroxy compounds
    • C10M2207/021—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/04—Ethers; Acetals; Ortho-esters; Ortho-carbonates
    • C10M2207/046—Hydroxy ethers
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/14—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to carbon atoms of six-membered aromatic rings
    • C10M2207/141—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to carbon atoms of six-membered aromatic rings monocarboxylic
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/20—Rosin acids
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/28—Esters
    • C10M2207/281—Esters of (cyclo)aliphatic monocarboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/40—Fatty vegetable or animal oils
    • C10M2207/401—Fatty vegetable or animal oils used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/02—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/08—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds containing monomers having an unsaturated radical bound to a carboxyl radical, e.g. acrylate type
    • C10M2209/084—Acrylate; Methacrylate
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/12—Polysaccharides, e.g. cellulose, biopolymers
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/10—Amides of carbonic or haloformic acids
    • C10M2215/102—Ureas; Semicarbazides; Allophanates
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2217/00—Organic macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2217/04—Macromolecular compounds from nitrogen-containing monomers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2217/044—Polyamides
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives

Abstract

本发明公开了一种利用石油脂制备的齿轮润滑脂，涉及石油化工技术领域，由如下重量份数的原料制成：石油脂4050份、亚麻籽油1015份、羟乙基纤维素1015份、卡波树脂813份、凹凸棒土610份、月桂醇聚氧乙烯醚610份、鲸蜡醇58份、丁苯橡胶58份、明胶46份、纳米陶瓷粉35份、防锈助剂35份、氧化胺12份、丙二醇丁醚1015份、渣油2025份。本发明润滑脂粘度适中，涂覆于齿轮后能快速在齿轮表面形成一层保护膜，并起到润滑作用，降低传动阻力，提高传动效率，并且粘度稳定、耐腐蚀性强，同时也不会对齿轮产生腐蚀作用，从而有利于延长齿轮的使用寿命。

Description

一种利用石油脂制备的齿轮润滑脂
技术领域：
本发明涉及石油化工技术领域，具体涉及一种利用石油脂制备的齿轮润滑脂。
背景技术：
石油脂又名蜡膏，是微结晶地蜡与石油的混合物。一般石油脂中含有70％-80％地蜡，以及20％-30％重质润滑油馏份。常用于某些机械的润滑脂配料，也可作为防锈油料、油膏，或作为生产凡士林和地蜡的材料。
齿轮在工作中容易损坏，原因如下：一是润滑油因粘度小，速度太低，负荷太大，不能建立油膜；二是圆周速度过大，负荷过重，产生滑动滚动、润滑油的质量等级差，粘度不合适、缺油等造成的不同程度黏着磨损；三是润滑系统内混进外部的尘埃等微粒以及内部磨屑、胶质等杂质造成微粒磨损；四是在周期循环接触应力的反复作用下，使表面材料产生点蚀、剥落以及断裂；五是润滑系统内混进水、金属微粒、化学污染物、以及润滑油的化学作用和氧的参与下等造成腐蚀磨损等。而目前市售齿轮润滑脂的润滑性能虽然能满足使用要求，但使用一段时间后粘度增大，从而增加齿轮的传动阻力，磨损齿轮，缩短齿轮的使用寿命；或在使用过程中被氧化，产生的氧化产物对齿轮有腐蚀作用，从而导致齿轮失效。
发明内容：
本发明所要解决的技术问题在于提供一种粘度适宜、性能稳定和利于延长齿轮使用寿命的利用石油脂制备的齿轮润滑脂。
本发明所要解决的技术问题采用以下的技术方案来实现：
一种利用石油脂制备的齿轮润滑脂，由如下重量份数的原料制成：
石油脂40-50份、亚麻籽油10-15份、羟乙基纤维素10-15份、卡波树脂8-13份、凹凸棒土6-10份、月桂醇聚氧乙烯醚6-10份、鲸蜡醇5-8份、丁苯橡胶5-8份、明胶4-6份、纳米陶瓷粉3-5份、防锈助剂3-5份、氧化胺1-2份、丙二醇丁醚10-15份、渣油20-25份；
其制备方法如下：
(1)向石油脂中加入卡波树脂和明胶，混合均匀后于微波频率2450MHz、功率800W下微波处理10min，待自然冷却至室温后再加入羟乙基纤维素和氧化胺，研磨30min，即得物料I；
(2)向渣油中加入丁苯橡胶，先加热至60-70℃保温混合10min，再加入凹凸棒土和纳米陶瓷粉，继续加热至120-130℃保温混合10min，即得物料II；
(3)向物料I中加入物料II、亚麻籽油、月桂醇聚氧乙烯醚、鲸蜡醇、防锈助剂和丙二醇丁醚，充分混合均匀。
所述防锈助剂由如下重量份数的原料制成：油茶叶12-16份、芦荟叶7-11份、仙人掌5-8份、蓖麻油10-15份、巴西棕榈蜡8-12份、单硬脂酸甘油酯6-10份、丙烯酸树脂4-7份、聚丙烯酰胺3-6份、氢化松香3-6份、硫化猪油2-4份、油酸2-4份、尿素1-2份、水50-60份，其制备方法为：(1)将油茶叶加入水中浸泡12h，然后加入芦荟叶和仙人掌，混合物送入磨浆机充分磨浆，再经过滤后向滤液中加入单硬脂酸甘油酯和聚丙烯酰胺，充分混合后送入冷冻干燥机，所得固体经粉碎机制成粉末，即得混合粉料；(2)将氢化松香溶于蓖麻油中，再加入巴西棕榈蜡和丙烯酸树脂，充分混合后先加热至85-90℃保温混合10min，然后加热至115-120℃保温混合10min，待自然冷却至室温后加入混合粉料、硫化猪油、油酸和尿素，充分混合均匀。
本发明的有益效果是：本发明以石油脂为主要原料，辅以渣油和亚麻籽油等多种助剂制得齿轮润滑脂，该润滑脂粘度适中，涂覆于齿轮后能快速在齿轮表面形成一层保护膜，并起到润滑作用，降低传动阻力，提高传动效率，并且粘度稳定、耐腐蚀性强，同时也不会对齿轮产生腐蚀作用，从而有利于延长齿轮的使用寿命。
具体实施方式：
为了使本发明实现的技术手段、创作特征、达成目的与功效易于明白了解，下面结合具体实施例，进一步阐述本发明。
实施例1
(1)向40份石油脂中加入8份卡波树脂和4份明胶，混合均匀后于微波频率2450MHz、功率800W下微波处理10min，待自然冷却至室温后再加入12份羟乙基纤维素和1份氧化胺，研磨30min，即得物料I；
(2)向20份渣油中加入5份丁苯橡胶，先加热至60-70℃保温混合10min，再加入6份凹凸棒土和4份纳米陶瓷粉，继续加热至120-130℃保温混合10min，即得物料II；
(3)向物料I中加入物料II、10份亚麻籽油、6份月桂醇聚氧乙烯醚、5份鲸蜡醇、3份防锈助剂和10份丙二醇丁醚，充分混合均匀。
防锈助剂的制备：(1)将12份油茶叶加入50份水中浸泡12h，然后加入7份芦荟叶和6份仙人掌，混合物送入磨浆机充分磨浆，再经过滤后向滤液中加入8份单硬脂酸甘油酯和3份聚丙烯酰胺，充分混合后送入冷冻干燥机，所得固体经粉碎机制成粉末，即得混合粉料；(2)将5份氢化松香溶于10份蓖麻油中，再加入8份巴西棕榈蜡和4份丙烯酸树脂，充分混合后先加热至85-90℃保温混合10min，然后加热至115-120℃保温混合10min，待自然冷却至室温后加入混合粉料、4份硫化猪油、2份油酸和2份尿素，充分混合均匀。
实施例2
(1)向50份石油脂中加入12份卡波树脂和5份明胶，混合均匀后于微波频率2450MHz、功率800W下微波处理10min，待自然冷却至室温后再加入10份羟乙基纤维素和1份氧化胺，研磨30min，即得物料I；
(2)向25份渣油中加入8份丁苯橡胶，先加热至60-70℃保温混合10min，再加入8份凹凸棒土和3份纳米陶瓷粉，继续加热至120-130℃保温混合10min，即得物料II；
(3)向物料I中加入物料II、15份亚麻籽油、8份月桂醇聚氧乙烯醚、6份鲸蜡醇、3份防锈助剂和15份丙二醇丁醚，充分混合均匀。
防锈助剂的制备：(1)将16份油茶叶加入60份水中浸泡12h，然后加入8份芦荟叶和5份仙人掌，混合物送入磨浆机充分磨浆，再经过滤后向滤液中加入10份单硬脂酸甘油酯和4份聚丙烯酰胺，充分混合后送入冷冻干燥机，所得固体经粉碎机制成粉末，即得混合粉料；(2)将4份氢化松香溶于15份蓖麻油中，再加入10份巴西棕榈蜡和6份丙烯酸树脂，充分混合后先加热至85-90℃保温混合10min，然后加热至115-120℃保温混合10min，待自然冷却至室温后加入混合粉料、3份硫化猪油、2份油酸和2份尿素，充分混合均匀。
以上显示和描述了本发明的基本原理和主要特征和本发明的优点。本行业的技术人员应该了解，本发明不受上述实施例的限制，上述实施例和说明书中描述的只是说明本发明的原理，在不脱离本发明精神和范围的前提下，本发明还会有各种变化和改进，这些变化和改进都落入要求保护的本发明范围内。本发明要求保护范围由所附的权利要求书及其等效物界定。

Claims (2)

1.一种利用石油脂制备的齿轮润滑脂，其特征在于，由如下重量份数的原料制成：
石油脂40-50份、亚麻籽油10-15份、羟乙基纤维素10-15份、卡波树脂8-13份、凹凸棒土6-10份、月桂醇聚氧乙烯醚6-10份、鲸蜡醇5-8份、丁苯橡胶5-8份、明胶4-6份、纳米陶瓷粉3-5份、防锈助剂3-5份、氧化胺1-2份、丙二醇丁醚10-15份、渣油20-25份；
其制备方法如下：
(1)向石油脂中加入卡波树脂和明胶，混合均匀后于微波频率2450MHz、功率800W下微波处理10min，待自然冷却至室温后再加入羟乙基纤维素和氧化胺，研磨30min，即得物料I；
(2)向渣油中加入丁苯橡胶，先加热至60-70℃保温混合10min，再加入凹凸棒土和纳米陶瓷粉，继续加热至120-130℃保温混合10min，即得物料II；
(3)向物料I中加入物料II、亚麻籽油、月桂醇聚氧乙烯醚、鲸蜡醇、防锈助剂和丙二醇丁醚，充分混合均匀。
2.根据权利要求1所述的利用石油脂制备的齿轮润滑脂，其特征在于，所述防锈助剂由如下重量份数的原料制成：油茶叶12-16份、芦荟叶7-11份、仙人掌5-8份、蓖麻油10-15份、巴西棕榈蜡8-12份、单硬脂酸甘油酯6-10份、丙烯酸树脂4-7份、聚丙烯酰胺3-6份、氢化松香3-6份、硫化猪油2-4份、油酸2-4份、尿素1-2份、水50-60份，其制备方法为：(1)将油茶叶加入水中浸泡12h，然后加入芦荟叶和仙人掌，混合物送入磨浆机充分磨浆，再经过滤后向滤液中加入单硬脂酸甘油酯和聚丙烯酰胺，充分混合后送入冷冻干燥机，所得固体经粉碎机制成粉末，即得混合粉料；(2)将氢化松香溶于蓖麻油中，再加入巴西棕榈蜡和丙烯酸树脂，充分混合后先加热至85-90℃保温混合10min，然后加热至115-120℃保温混合10min，待自然冷却至室温后加入混合粉料、硫化猪油、油酸和尿素，充分混合均匀。
CN201610153441.4A 2016-03-16 2016-03-16 一种利用石油脂制备的齿轮润滑脂 Pending CN105733776A (zh)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610153441.4A CN105733776A (zh) 2016-03-16 2016-03-16 一种利用石油脂制备的齿轮润滑脂

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610153441.4A CN105733776A (zh) 2016-03-16 2016-03-16 一种利用石油脂制备的齿轮润滑脂

Publications (1)

Publication Number Publication Date
CN105733776A true CN105733776A (zh) 2016-07-06

Family

ID=56251756

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610153441.4A Pending CN105733776A (zh) 2016-03-16 2016-03-16 一种利用石油脂制备的齿轮润滑脂

Country Status (1)

Country Link
CN (1) CN105733776A (zh)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106190491A (zh) * 2016-07-15 2016-12-07 东至绿洲环保化工有限公司 一种混凝土浇筑用建筑模板脱模剂
CN106190521A (zh) * 2016-07-15 2016-12-07 东至绿洲环保化工有限公司 一种建筑模板用水性有机硅脱模剂
CN106497634A (zh) * 2016-09-29 2017-03-15 东至绿洲环保化工有限公司 一种利用油粕制备的建筑金属模板脱模剂用成膜助剂
CN106701280A (zh) * 2016-12-16 2017-05-24 池州恒和精密机械有限公司 一种齿轮传动用润滑油
CN106833837A (zh) * 2016-12-23 2017-06-13 安徽国威电动车制造有限公司 一种电动车链条链轮保养用润滑脂
CN109054935B (zh) * 2018-09-21 2021-04-16 安徽意博润滑科技有限公司 一种润滑脂组合物及其制备方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103710118A (zh) * 2013-11-28 2014-04-09 安徽速克达车业有限公司 一种水基切削冷却防锈液及其制备方法
CN104250575A (zh) * 2013-06-25 2014-12-31 中国石油天然气股份有限公司 一种性能优异的钢丝绳脂组合物及其制备方法
CN104893808A (zh) * 2015-06-09 2015-09-09 广东富行洗涤剂科技有限公司 一种高转速全合成水溶性切削液

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104250575A (zh) * 2013-06-25 2014-12-31 中国石油天然气股份有限公司 一种性能优异的钢丝绳脂组合物及其制备方法
CN103710118A (zh) * 2013-11-28 2014-04-09 安徽速克达车业有限公司 一种水基切削冷却防锈液及其制备方法
CN104893808A (zh) * 2015-06-09 2015-09-09 广东富行洗涤剂科技有限公司 一种高转速全合成水溶性切削液

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
唐晓东: "《石油加工助剂作用原理与应用》", 30 November 2004, 石油工业出版社 *
张英主编: "《精细化学品配方大全》", 31 May 2001, 化学工业出版社与精细化工出版中心出版 *
陈文刚主编: "《汽车运行材料》", 31 August 2013, 中国林业出版社 *

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106190491A (zh) * 2016-07-15 2016-12-07 东至绿洲环保化工有限公司 一种混凝土浇筑用建筑模板脱模剂
CN106190521A (zh) * 2016-07-15 2016-12-07 东至绿洲环保化工有限公司 一种建筑模板用水性有机硅脱模剂
CN106497634A (zh) * 2016-09-29 2017-03-15 东至绿洲环保化工有限公司 一种利用油粕制备的建筑金属模板脱模剂用成膜助剂
CN106701280A (zh) * 2016-12-16 2017-05-24 池州恒和精密机械有限公司 一种齿轮传动用润滑油
CN106833837A (zh) * 2016-12-23 2017-06-13 安徽国威电动车制造有限公司 一种电动车链条链轮保养用润滑脂
CN109054935B (zh) * 2018-09-21 2021-04-16 安徽意博润滑科技有限公司 一种润滑脂组合物及其制备方法

Similar Documents

Publication Publication Date Title
CN105733776A (zh) 一种利用石油脂制备的齿轮润滑脂
CN102533422B (zh) 一种利用硫化地沟油制备的微乳液型金属切削液及其制备方法
CN103614221A (zh) 一种铜拉丝润滑液及其制备方法
CN102925274A (zh) 一种光学玻璃磨削液及其制备方法
CN105345919A (zh) 一种纳米二氧化钛增强型混凝土脱模剂
CN103305325A (zh) 一种脱模剂及其制备方法
CN102604723B (zh) 一种润滑脂组合物及制备方法
CN105623813A (zh) 一种泵联轴器专用润滑脂
CN102443463A (zh) 一种涡轮机油抗氧添加剂
CN109810771A (zh) 一种离子液体与微纳固体协同强化磨削液及制备方法
CN103992853A (zh) 一种不锈钢拉丝用拉丝油
CN105316096A (zh) 一种离心泵滑动轴承用润滑脂
CN103966005A (zh) 一种铜线快速拉拔用拉丝液
CN103614214A (zh) 一种合金拉丝润滑剂及其制备方法
CN103992838A (zh) 一种含纳米银的拉丝油
CN104611110A (zh) 一种机床用切削液
CN102360672A (zh) 一种新型复合软磁材料及其制备方法
CN107142134A (zh) 一种具有优异极压性能的金属切削液
CN105060866B (zh) 一种高机械强度的陶瓷刀具材料
CN102703140B (zh) 一种具有良好配伍性燃油贮存稳定剂及制备方法
CN110229712A (zh) 高润滑性切削液及其制备方法
CN108559576A (zh) 一种石墨烯包覆纳米铜润滑油添加剂及其制备方法
CN103614222A (zh) 一种铜拉丝油及其制备方法
CN105733775A (zh) 一种利用渣油制备的传动轴润滑油
CN104450128A (zh) 一种沉降性水基切削液及其制备方法

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20160706