CN105705035A - 包囊 - Google Patents

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CN105705035A
CN105705035A CN201480059592.2A CN201480059592A CN105705035A CN 105705035 A CN105705035 A CN 105705035A CN 201480059592 A CN201480059592 A CN 201480059592A CN 105705035 A CN105705035 A CN 105705035A
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F·惠特文
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    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
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    • A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
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    • A23L29/206—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents of vegetable origin
    • A23L29/212—Starch; Modified starch; Starch derivatives, e.g. esters or ethers
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    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
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Abstract

包囊的香料，包含芯材料、香料物质和包衣材料，所述芯材料包含细碎的天然淀粉、黄原胶和魔芋。包囊的香料可以是完全不含明胶的，同时保留期望的明胶品质。

Description

包囊
本公开涉及香料包囊。
香料的包囊是一种极为重要的技术，因为使用它使得能够保护香料，直到其期望的释放时间为止。已经发现了这项技术进入各种消费组合物的方式，即口服摄取用于摄入(例如食品、糖食、烘烤食品和饮料)或用于吐出(例如牙膏和漱口液)的组合物。
用于这一应用的最常用的材料之一是明胶。明胶具有许多优点；它低廉且易于得到，在胶凝和溶胀行为、口感和在消费时在口腔中的特定熔化行为方面还具有独特的特性。这些组合使得其广泛应用。
与这些优点相反，存在增加的众多优点。明胶是动物产物，由此意味着它不能用于素食产品。此外，根据其来源的不同，它可能牵涉宗教禁令。使用明胶产品难以克服犹太教戒律和伊斯兰法律的禁令。然而，已经证实难以找到可以得到其所有的优点、而不会有任何其缺点的明胶的替代品。
目前已经发现，能够提供无缺点的明胶益处。因此，提供包囊的香料，其包含芯材料、香料物质和包衣材料，所述芯材料包含细碎的天然淀粉、黄原胶和魔芋。
还提供制备包囊的香料的方法，所述方法包括混合天然淀粉、黄原胶和魔芋的混合物与香料乳液，得到颗粒。
天然淀粉即非化学改性的淀粉是众所周知的和易于得到的商品。典型的实例包括稻米淀粉和木薯淀粉。
黄原胶是众所周知的由细菌野油菜黄单胞菌(Xanthomonascampestris)分泌的多糖且广泛用作食品和化妆品中的流变调节剂、增稠剂和稳定剂。
魔芋是亚洲植物魔芋(Amorphophalluskonjac)的根。目前因其营养含量及其高含量的葡甘露聚糖纤维而广泛地用于保健和膳食食品，这是注意到了其溶胀能力。可以以粉末(磨粉)和凝胶形式得到它。粉末形式优选用于本方法。
尽管所有材料均为本领域众所周知的，但是令人惊奇地发现，组合可以用于替代明胶并且赋予组合物期望的明胶品质。
香料可以是任意适合的期望的香料。其以水性乳液形式使用。在一些情况中，香料可以被乳化，无需任何乳化剂，但通常存在至少一些食品级乳化剂是有益的。典型实例包括阿拉伯树胶、改性的食物淀粉和OSA淀粉。
在一个具体的实施方案中，乳化剂得自脱水山梨糖醇。一个具体的实施方案是商购的聚氧乙烯山梨糖醇酐单油酸酯，例如，商品名TweenTM、PolysorbateTM和AdmulTM。已经令人惊奇地发现，这些乳化剂的应用产生非常小尺寸(小至1微米)的乳化剂香料液滴，这与使用其它乳化剂可能的3-4微米尺寸相反。液滴越大，则香料在流化床工艺中的损耗越大，由此较小的尺寸带来显著的优势。
在一种典型的方法中，通过将成分混入加热的流化床制备芯材料。然后将香料的乳液喷在芯材料上。喷雾持续至得到期望的香料含量。典型的流化床设备包括Wurster、转子造粒机和塔顶喷雾系统。
流化床设备工具正常操作和本领域公认的参数范围内运行。典型操作条件如下：
入口温度60-110℃，特别是约95℃
产品温度35-90℃，特别是约65℃
空气流量20-140M3/h，特别是约60M3/h
喷嘴气压0.5-6巴，特别是约4巴
在另一个实施方案中，可以将至少一层保护层涂布于颗粒上。保护层可以是能够形成包衣薄膜的任意食品级材料，典型实例是纤维素材料、例如甲基和乙基纤维素和基于淀粉的材料。将其作为水溶液喷在流化的香料颗粒上。
上文所述的香料颗粒可以以所有种类的固体可食用产品的形式使用，即通过口腔摄取摄入或吐出的产品。因此，还提供包含可食用产品基料和如上文所定义的包囊的香料的固体可食用组合物。
所谓“固体”是指非流体即不是液体或可涂抹的糊状物的产品。所谓“可食用产品基料”是指所有本领域公认的与包囊的香料合并以制成可食用产品的成分。它们取决于特定产品的性质，但它们包括例如其它香料、粘合剂和成膜材料、增稠剂、流变调节剂、增充剂和研磨剂、溶剂和稀释剂、色素、染料和着色物质、防腐剂、香味增强剂和调节剂、甜味剂、口感添加剂、抗菌剂和药物化合物和组合物等这样的材料。
可食用产品的非限制性实例包括食品、口腔护理产品和用于与这类产品混合的组合物，特别是香料组合物。可以将香料组合物在加工过程中添加到加工的食品中，或它们实际上可以以其自身作为消费品，例如作料，例如调味料等。
可食用产品的另外的非限制性实例包括糖食，例如巧克力和糖果产品、谷类制品、烘烤产品、面包产品、树胶类产品、口香糖、酵母产品、咸味产品和调料产品、芥末产品、醋产品、酱油(作料)、汤、加工食品、熟化水果和蔬菜产品、肉类和肉制品、蛋制品、食用油和脂肪产品、药剂、食物提取物、植物提取物、肉类提取物、作料、甜味剂、营养制品、药物和非药物树胶、片剂、锭剂和滴剂。
上文所述的颗粒的应用提供了获得不含明胶(由此满足明胶存在导致的所有宗教和膳食问题)但是具有明胶存在所带来的所有期望的品质的可能性。因此，还提供不含明胶的固体可食用组合物，其包含可食用产品基料和如上文所定义的包囊的香料。
本公开参照下列非限制性实施例进一步描述。
实施例1
颗粒的制备
成分如下所示：
1.麦芽糖糊精(葡萄糖当量为12)
2.糖醇
3.商购的薄荷香料
4.聚氧乙烯(20)山梨糖醇酐单油酸酯
该方法在如下条件下操作的转子造粒机中进行(具有通常的适度实际改变)：
制备两批材料，第一批仅使用阶段A和B(“未包衣的颗粒”)，第二批还使用C，其中将甲基纤维素的溶液喷在流化床中的颗粒上(“包衣颗粒”)。对于阶段B和C维持相同的加工条件。
然后采集两组颗粒并且过筛，得到最大500μM的颗粒。
实施例2
颗粒的测试
以2％重量将两组颗粒掺入如下口香糖制品：
山梨糖醇 56.3
Solsona-T1 30.0
甘露糖醇 5.0
麦芽糖醇(Malitol)糖浆剂2 8.0
卵磷脂 0.4
阿司帕坦2 0.2
乙酰舒泛-K2 0.1
1.商购的口香糖胶基
2.甜味剂
在室温通过使用Z-桨叶混合器并且捏合上述成分的混合物将颗粒掺入，直到形成均匀的粘性混合物(糊状物)。将粘性糊状物分成各自1.2克的口香糖片。
为了进行比较，向同一口香糖基质中添加相同比例的传统的喷雾干燥的淀粉香料颗粒，它们携带与实施例1中所制备的那些相同比例的相同香料。使用最大尺寸为150和75μm的两批不同尺寸的喷雾干燥的颗粒。
由15个成员的专家小组进行评价并且通过ANOVA对数据进行统计学分析。结果如图1中所示。
从附图中可以明显地看出：
1.如上所述制备的未包衣的颗粒具有快速和极为有效的“直接(upfront)”释放，相当于开始咀嚼后立刻有香味冲击；
2.包衣的颗粒具有相同的冲击，但因额外的包衣而延迟。
3.两批基本上均优于已知的喷雾干燥的香料颗粒。

Claims (6)

1.包囊的香料，包含芯材料、香料物质和包衣材料，所述芯材料包含细碎的天然淀粉、黄原胶和魔芋。
2.制备包囊的香料的方法，所述方法包括混合天然淀粉、黄原胶和魔芋的混合物与香料乳液，得到颗粒。
3.权利要求2的方法，其中所述香料乳液在乳化剂的存在下制备。
4.权利要求3的方法，其中所述乳化剂是聚氧乙烯山梨糖醇酐单油酸酯。
5.固体可食用组合物，包含可食用产品基料和权利要求1的包囊的香料。
6.权利要求5的固体可食用组合物，其完全不含明胶。
CN201480059592.2A 2013-10-30 2014-10-29 包囊 Active CN105705035B (zh)

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PCT/EP2014/073186 WO2015063130A1 (en) 2013-10-30 2014-10-29 Encapsulation

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US11234451B2 (en) 2022-02-01
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US11871764B2 (en) 2024-01-16
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