CN105555710A - 用于制备气凝胶材料的方法 - Google Patents

用于制备气凝胶材料的方法 Download PDF

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Publication number
CN105555710A
CN105555710A CN201480050734.9A CN201480050734A CN105555710A CN 105555710 A CN105555710 A CN 105555710A CN 201480050734 A CN201480050734 A CN 201480050734A CN 105555710 A CN105555710 A CN 105555710A
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China
Prior art keywords
gel
suo shu
hydrophobization
sol
hydrophobizing
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Pending
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CN201480050734.9A
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English (en)
Chinese (zh)
Inventor
M.凯贝尔
赵善宇
S.布伦纳
C.西门
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Eidgenoessische Materialpruefungs und Forschungsanstalt
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Eidgenoessische Materialpruefungs und Forschungsanstalt
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Priority to CN202111139256.7A priority Critical patent/CN114408931A/zh
Publication of CN105555710A publication Critical patent/CN105555710A/zh
Pending legal-status Critical Current

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    • E—FIXED CONSTRUCTIONS
    • E04—BUILDING
    • E04B—GENERAL BUILDING CONSTRUCTIONS; WALLS, e.g. PARTITIONS; ROOFS; FLOORS; CEILINGS; INSULATION OR OTHER PROTECTION OF BUILDINGS
    • E04B1/00—Constructions in general; Structures which are not restricted either to walls, e.g. partitions, or floors or ceilings or roofs
    • E04B1/62—Insulation or other protection; Elements or use of specified material therefor
    • E04B1/74—Heat, sound or noise insulation, absorption, or reflection; Other building methods affording favourable thermal or acoustical conditions, e.g. accumulating of heat within walls
    • E04B1/76—Heat, sound or noise insulation, absorption, or reflection; Other building methods affording favourable thermal or acoustical conditions, e.g. accumulating of heat within walls specifically with respect to heat only
    • E04B1/78—Heat insulating elements
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/145—Preparation of hydroorganosols, organosols or dispersions in an organic medium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/155—Preparation of hydroorganogels or organogels
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/157—After-treatment of gels
    • C01B33/158—Purification; Drying; Dehydrating
    • C01B33/1585—Dehydration into aerogels

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Architecture (AREA)
  • Acoustics & Sound (AREA)
  • Electromagnetism (AREA)
  • Civil Engineering (AREA)
  • Structural Engineering (AREA)
  • Silicon Compounds (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Thermal Insulation (AREA)
CN201480050734.9A 2013-08-02 2014-07-28 用于制备气凝胶材料的方法 Pending CN105555710A (zh)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202111139256.7A CN114408931A (zh) 2013-08-02 2014-07-28 用于制备气凝胶材料的方法

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP13179185.7A EP2832690A1 (de) 2013-08-02 2013-08-02 Verfahren zur Herstellung eines Aerogelmaterials
EP13179185.7 2013-08-02
PCT/EP2014/066213 WO2015014813A1 (de) 2013-08-02 2014-07-28 Verfahren zur herstellung eines aerogelmaterials

Related Child Applications (1)

Application Number Title Priority Date Filing Date
CN202111139256.7A Division CN114408931A (zh) 2013-08-02 2014-07-28 用于制备气凝胶材料的方法

Publications (1)

Publication Number Publication Date
CN105555710A true CN105555710A (zh) 2016-05-04

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CN201480050734.9A Pending CN105555710A (zh) 2013-08-02 2014-07-28 用于制备气凝胶材料的方法
CN202111139256.7A Pending CN114408931A (zh) 2013-08-02 2014-07-28 用于制备气凝胶材料的方法

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CN202111139256.7A Pending CN114408931A (zh) 2013-08-02 2014-07-28 用于制备气凝胶材料的方法

Country Status (8)

Country Link
US (1) US20160258153A1 (enExample)
EP (2) EP2832690A1 (enExample)
JP (1) JP6449279B2 (enExample)
KR (1) KR101813898B1 (enExample)
CN (2) CN105555710A (enExample)
AU (1) AU2014298538B2 (enExample)
BR (1) BR112016002360A2 (enExample)
WO (1) WO2015014813A1 (enExample)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106955650A (zh) * 2017-04-01 2017-07-18 东华大学 一种三维多孔框架增强纤维气凝胶材料及其制备方法
CN109475833A (zh) * 2016-05-20 2019-03-15 罗克伍尔国际公司 用于制备气凝胶复合材料的设备和方法以及气凝胶复合材料
CN111818994A (zh) * 2018-03-05 2020-10-23 赢创运营有限公司 生产气凝胶材料的方法
CN115485239A (zh) * 2020-04-30 2022-12-16 赢创运营有限公司 具有增大的碱性稳定性的二氧化硅气凝胶

Families Citing this family (37)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102291408B1 (ko) * 2014-02-26 2021-08-18 쇼와덴코머티리얼즈가부시끼가이샤 에어로겔
CH710694B1 (de) * 2015-02-04 2019-05-15 Rockwool Int Verfahren zur Herstellung eines Aerogels resp. eines Aerogel-Verbundwerkstoffs, sowie Aerogel resp. Aerogel-Verbundwerkstoff erhältlich nach dem Verfahren.
KR101789371B1 (ko) 2015-02-13 2017-10-23 주식회사 엘지화학 실리카 에어로겔 함유 블랑켓의 제조방법 및 이에 따라 제조된 실리카 에어로겔 함유 블랑켓
GB201502613D0 (en) * 2015-02-17 2015-04-01 Univ Newcastle Aerogels
DE102015211812A1 (de) 2015-06-25 2016-12-29 Wacker Chemie Ag Wirtschaftliches Verfahren zur Herstellung von organisch modifizierten Lyo- oder Aerogelen
EP3124443A1 (de) * 2015-07-28 2017-02-01 D. Swarovski KG Kontinuierliches sol-gel verfahren zur herstellung von quarzglas
KR101931569B1 (ko) 2015-11-03 2018-12-21 주식회사 엘지화학 소수성의 산화금속-실리카 복합 에어로겔의 제조방법 및 이로부터 제조된 소수성의 산화금속-실리카 복합 에어로겔
KR101774140B1 (ko) * 2016-01-19 2017-09-01 주식회사 엘지화학 에어로겔 시트의 제조방법 및 장치
KR101953371B1 (ko) 2016-01-19 2019-02-28 주식회사 엘지화학 에어로겔 시트의 제조방법 및 장치
KR101962207B1 (ko) 2016-02-17 2019-03-27 주식회사 엘지화학 에어로겔 시트를 포함하는 복합시트 제조방법 및 제조장치
KR101962206B1 (ko) * 2016-02-19 2019-03-27 주식회사 엘지화학 에어로겔 시트를 포함하는 복합시트 제조방법 및 제조장치
KR101968648B1 (ko) * 2016-02-19 2019-04-12 주식회사 엘지화학 에어로겔 시트의 제조방법 및 장치
KR20170110993A (ko) 2016-03-24 2017-10-12 주식회사 엘지화학 실리카 에어로겔 제조시스템
FR3050013B1 (fr) * 2016-04-11 2019-08-02 Saint-Gobain Isover Fours et produits d'isolation pour fours
FR3053263B1 (fr) * 2016-07-04 2018-08-31 Keey Aerogrl Procede continu de fabrication d'un aerogel
WO2018019599A1 (de) 2016-07-29 2018-02-01 Evonik Degussa Gmbh Verfahren zur herstellung eines hydrophoben, wärmedämmenden materiales
EP3281920A1 (de) * 2016-08-12 2018-02-14 D. Swarovski KG Kontinuierliches sol-gel-verfahren zur herstellung von silicathaltigen gläsern oder glaskeramiken
US11279622B2 (en) 2016-09-12 2022-03-22 Lg Chem, Ltd. Method for producing silica aerogel and silica aerogel produced thereby
KR101942474B1 (ko) * 2016-11-18 2019-01-25 주식회사 엘지화학 전가수분해된 알킬 폴리실리케이트의 합성방법
RU2759942C2 (ru) 2017-01-18 2021-11-18 Эвоник Оперейшенс ГмбХ Гранулированный теплоизоляционный материал и способ его получения
DE102017209782A1 (de) 2017-06-09 2018-12-13 Evonik Degussa Gmbh Verfahren zur Wärmedämmung eines evakuierbaren Behälters
EP3498671A1 (en) * 2017-12-15 2019-06-19 EMPA Eidgenössische Materialprüfungs- und Forschungsanstalt Superinsulating silica aerogel with high stiffness and density
EP3597615A1 (en) 2018-07-17 2020-01-22 Evonik Operations GmbH Granular mixed oxide material and thermal insulating composition on its basis
CN112424139B (zh) 2018-07-17 2022-04-26 赢创运营有限公司 基于二氧化硅颗粒的隔热组合物
MX2021000626A (es) 2018-07-18 2021-03-25 Evonik Operations Gmbh Procedimiento de hidrofobizacion de cuerpos de material de aislamiento conformados a base de silice a presion ambiental.
CN111039583B (zh) * 2018-10-11 2022-10-11 卢孟磊 一种低成本快速制备微纳结构气凝胶膨胀珍珠岩的方法
DE102018128410A1 (de) * 2018-11-13 2020-05-14 Fraunhofer Gesellschaft zur Förderung der angewandten Forschung e.V. Verfahren zur Herstellung von Aerogelen und mit diesem erhältliche Aerogele
WO2020125956A1 (de) 2018-12-18 2020-06-25 Wacker Chemie Ag Verfahren zur herstellung abgerundeter gelpartikel
FR3094975B1 (fr) * 2019-04-10 2022-11-18 Keey Aerogel Procédé de synthèse d’un aérogel de silice hydrophobique de type « one pot » à partir d’un précurseur de silice
WO2021204815A1 (en) * 2020-04-06 2021-10-14 Empa Eidgenössische Materialprüfungs- Und Forschungsanstalt Silica aerogels
EP3896035A1 (en) * 2020-04-15 2021-10-20 EMPA Eidgenössische Materialprüfungs- und Forschungsanstalt Silica aerogels and silica aerogel blankets
CN113563012B (zh) * 2020-04-29 2022-11-04 台湾气凝胶科技材料开发股份有限公司 御寒、隔热的疏水性气凝胶复合胶状物的制备方法及其相关产物
CH717558A1 (de) 2020-06-22 2021-12-30 Rockwool Int Aerogel-Verbundwerkstoffen, sowie Wärmedämmelement.
EP4177231A1 (de) 2021-11-03 2023-05-10 Evonik Operations GmbH Wärmedämmsysteme mit verbesserter kosteneffizienz
CN117510181B (zh) * 2023-11-07 2024-04-16 武汉中科先进材料科技有限公司 一种超疏水、增强型二氧化硅气凝胶毡及其制备方法
CN117658589A (zh) * 2023-12-07 2024-03-08 翌江新材(江苏)有限公司 一种制备气凝胶材料的新型方法
CN118561286A (zh) * 2024-04-15 2024-08-30 湖南尚成新材料科技有限责任公司 采用醇混合溶液的亚临界态流体制备疏水气凝胶的方法

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101014535A (zh) * 2004-01-06 2007-08-08 白杨气凝胶股份有限公司 含有键合硅的聚甲基丙烯酸酯的有机改性的二氧化硅气凝胶
CN101372337A (zh) * 2008-09-28 2009-02-25 厦门大学 共前驱体法常压干燥制备透明二氧化硅气凝胶的方法
CN101646622A (zh) * 2007-03-27 2010-02-10 Neb株式会社 制备疏水气凝胶的方法以及由其制备的疏水气凝胶
CN101691227A (zh) * 2009-10-13 2010-04-07 厦门大学 二氧化硅气凝胶材料的制备方法
CN102951650A (zh) * 2012-08-31 2013-03-06 卢斌 一种快速制备SiO2气凝胶的常压干燥方法
WO2013053951A1 (en) * 2011-10-14 2013-04-18 Enersens Process for manufacturing xerogels

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2659155B2 (ja) * 1992-02-03 1997-09-30 松下電工株式会社 疎水性エアロゲルの製造方法
EP0585456B1 (en) * 1992-02-18 1997-05-07 Matsushita Electric Works Ltd Process for producing hydrophobic aerogel
US5565142A (en) 1992-04-01 1996-10-15 Deshpande; Ravindra Preparation of high porosity xerogels by chemical surface modification.
US5738801A (en) 1993-08-31 1998-04-14 Basf Aktiengesellschaft Hydrophobic silica aerogels
DE19631267C1 (de) 1996-08-02 1998-04-30 Hoechst Ag Verfahren zur Herstellung von organisch modifizierten Aerogelen
DE19648798C2 (de) * 1996-11-26 1998-11-19 Hoechst Ag Verfahren zur Herstellung von organisch modifizierten Aerogelen durch Oberflächenmodifikation des wäßrigen Gels (ohne vorherigen Lösungsmitteltausch) und anschließender Trocknung
JP3954842B2 (ja) * 2001-08-02 2007-08-08 株式会社アルバック 疎水性多孔質材料の製造方法
FR2849444B1 (fr) * 2002-12-30 2006-07-28 Rhodia Chimie Sa Procede de preparation d'un suspension de silice dans une matiere silicone eventuellement reticulable
FR2873677B1 (fr) * 2004-07-29 2007-08-17 Armines Ass Pour La Rech Et Le Procede d'elaboration de serogels de silice hydrophobes
JP2007134420A (ja) * 2005-11-09 2007-05-31 Ulvac Japan Ltd 疎水性多孔質シリカ材料による構造物内部の埋め込み方法
KR101429318B1 (ko) * 2007-02-02 2014-08-11 닛산 가가쿠 고교 가부시키 가이샤 반응성 모노머 분산 실리카 졸, 이의 제조방법, 경화용 조성물 및 이의 경화체
KR100924781B1 (ko) * 2007-09-19 2009-11-03 주식회사 넵 영구적인 소수성을 갖는 고투광성 입상형 에어로겔제조방법 및 이로부터 제조된 입상형 에어로겔
KR101187568B1 (ko) 2010-09-29 2012-10-04 한국에너지기술연구원 실리카 에어로겔 과립의 제조방법
JP5669617B2 (ja) * 2011-02-21 2015-02-12 株式会社トクヤマ エアロゲル及び該エアロゲルを用いた断熱材
KR102172825B1 (ko) * 2013-06-10 2020-11-02 닛산 가가쿠 가부시키가이샤 실리카 함유 수지 조성물 및 그 제조 방법 그리고 실리카 함유 수지 조성물의 성형품

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101014535A (zh) * 2004-01-06 2007-08-08 白杨气凝胶股份有限公司 含有键合硅的聚甲基丙烯酸酯的有机改性的二氧化硅气凝胶
CN101646622A (zh) * 2007-03-27 2010-02-10 Neb株式会社 制备疏水气凝胶的方法以及由其制备的疏水气凝胶
CN101372337A (zh) * 2008-09-28 2009-02-25 厦门大学 共前驱体法常压干燥制备透明二氧化硅气凝胶的方法
CN101691227A (zh) * 2009-10-13 2010-04-07 厦门大学 二氧化硅气凝胶材料的制备方法
WO2013053951A1 (en) * 2011-10-14 2013-04-18 Enersens Process for manufacturing xerogels
CN102951650A (zh) * 2012-08-31 2013-03-06 卢斌 一种快速制备SiO2气凝胶的常压干燥方法

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
MICHEL A. AEGERTER ET AL.: "《Aerogels Handbook》", 31 December 2011, SPRINGER *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109475833A (zh) * 2016-05-20 2019-03-15 罗克伍尔国际公司 用于制备气凝胶复合材料的设备和方法以及气凝胶复合材料
CN106955650A (zh) * 2017-04-01 2017-07-18 东华大学 一种三维多孔框架增强纤维气凝胶材料及其制备方法
CN111818994A (zh) * 2018-03-05 2020-10-23 赢创运营有限公司 生产气凝胶材料的方法
CN115485239A (zh) * 2020-04-30 2022-12-16 赢创运营有限公司 具有增大的碱性稳定性的二氧化硅气凝胶

Also Published As

Publication number Publication date
WO2015014813A1 (de) 2015-02-05
KR101813898B1 (ko) 2018-01-02
CN114408931A (zh) 2022-04-29
JP2016530199A (ja) 2016-09-29
AU2014298538A1 (en) 2016-02-25
EP2832690A1 (de) 2015-02-04
KR20160054462A (ko) 2016-05-16
EP3027558A1 (de) 2016-06-08
AU2014298538B2 (en) 2018-02-22
JP6449279B2 (ja) 2019-01-09
BR112016002360A2 (pt) 2017-08-01
US20160258153A1 (en) 2016-09-08

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