CN105532919B - A kind of full nutrition children prescription emulsifiable powder and preparation method thereof - Google Patents

A kind of full nutrition children prescription emulsifiable powder and preparation method thereof Download PDF

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CN105532919B
CN105532919B CN201510990246.2A CN201510990246A CN105532919B CN 105532919 B CN105532919 B CN 105532919B CN 201510990246 A CN201510990246 A CN 201510990246A CN 105532919 B CN105532919 B CN 105532919B
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content
feed liquid
preparation
powder
mixed
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CN105532919A (en
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陈文亮
苏米亚
刘振民
刘翠平
齐晓彦
贾宏信
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Shanghai Bright Dairy and Food Co Ltd
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C21/00Whey; Whey preparations
    • A23C21/06Mixtures of whey with milk products or milk components
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C21/00Whey; Whey preparations
    • A23C21/04Whey; Whey preparations containing non-milk components as source of fats or proteins
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C21/00Whey; Whey preparations
    • A23C21/08Whey; Whey preparations containing other organic additives, e.g. vegetable or animal products
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C21/00Whey; Whey preparations
    • A23C21/10Whey; Whey preparations containing inorganic additives

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  • Chemical & Material Sciences (AREA)
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  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
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  • Inorganic Chemistry (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)
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  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)

Abstract

The invention discloses a kind of full nutrition children prescription emulsifiable powders and preparation method thereof.Its component includes: 20~30% whole-fat milk powders, 12~19% skimmed milk powders, 18~21% desalted whey powders, 12~18% carbohydrate, 6~12% vegetable fat, 5~10% concentrated whey protein powders, 2~6% prebiotic compositions, 1.5~4.5% lipid compositions, 0.15~0.25% multi-vitamins and 0.45~0.55% composite mineral matter;Full nutrition children prescription emulsifiable powder of the invention contains whole minerals, vitamins and other nutritious components necessary to good lactalbumin and children's torso, can be used as the single source of nutrition of the crowd including malnourished children;Preparation method of the invention adds lipid composition using wet processing, reduces the loss of DHA and ARA in wet process adding procedure.

Description

A kind of full nutrition children prescription emulsifiable powder and preparation method thereof
Technical field
The present invention relates to a kind of full nutrition children prescription emulsifiable powders and preparation method thereof.
Background technique
Although modern life level is continuously improved, the Dietary Quality of China school children and nutrition, health status It has clear improvement, but has children and malnutritive phenomenon occur.One for 6-17 year old " school children's nutrition and Health status " report display, China school children malnutrition rate are 9.2%.
Malnutrition is also referred to as chronic nutritional disorders, common to have protein-energy nutrition not caused by being chronic subalimentation Inorganic salts deficiency disease such as good disease, vitamin-deficiency, zinc etc..Malnutritive reason may be various, such as inappropriate Feeding patterns, food intake is insufficient, physical fitness is bad etc., and reasons cause that nutrition cannot effectively absorb by body or excessively Edible fast food etc..The phenomenon that subalimentation, overnutrition belong to unbalanced nutrition also belongs to underfed model It encloses.Long-term severe malnutrition can cause pubertal growth hypoevolutism, intellection and the decline of study tolerance and human body It immunity degradation and goes to bits, even results in certain diseases and occur.
Children are after there is underfed symptom, if taking effective nutritional intervention not in time, by serious shadow The body development of noise child.According to the suggestion of committee on Nutrition,American Academy of Pediatrics, the ideal diet of children should be able to make its growth Speed and will not cause to bear close to the speed of growth of normal child to developmental metabolism and excretory system, and nutrition is special Point should include the protein and fat, vitamin and mineral combined equalization with absorption easy to digest.Therefore, for malnutrition The physiology and nutritional characteristic of pediatric population, providing the formula food that a kind of nutrition is comprehensive and Nutrient Availability is high is always ability The hot spot of field technique personnel research.
Summary of the invention
Technical problem to be solved by the present invention lies in for malnourished children crowd Nutrition intake it is unbalanced, disappear Change the problems such as absorption rate is low, and provide a kind of full nutrition children prescription emulsifiable powder and preparation method thereof.Full battalion of the invention Each nutrient compositions content for supporting children's prescription emulsifiable powder is designed according to the physilogical characteristics of malnourished children and nutritional need, can Meet the nutritional need of malnourished children crowd as single source of nutrition, and various nutrient detected values are in safe model It encloses.
The present invention solves above-mentioned technical problem by the following technical programs.
One of technical solution of the present invention has been to provide a kind of preparation method of full nutrition children prescription emulsifiable powder, described complete Nutrition children's prescription emulsifiable powder includes following components: 20%~30% whole-fat milk powder or lactogenesis, 12%~19% skimmed milk powder or de- It is rouge cream, 18%~21% desalted whey powder, 12%~18% carbohydrate, 6%~12% vegetable fat, 5%~10% dense Contracting PURE WHEY, 2%~6% prebiotic compositions, 1.5%~4.5% lipid composition, 0.15%~0.25% compound dimension Raw element and 0.45%~0.55% composite mineral matter, the percentage are that each component quality accounts for the full nutrition children prescription emulsifiable powder The percentage of gross mass;The lipid composition is by medium chain triglycerides (MCT), docosahexaenoic acid (DHA), peanut four Olefin(e) acid (ARA) and phosphatidylserine (PS) composition;The prebiotic compositions are made of polyfructosan and oligofructose, institute Stating mass percent of the polyfructosan in the combination of prebiotics is 40%~60%;The preparation method includes following steps It is rapid:
(1) it is matched by said components, respectively preparation liquid A, feed liquid B, feed liquid D and feed liquid F;Wherein, by whole-fat milk powder or Lactogenesis, skimmed milk powder or skimmed milk, desalted whey powder, carbohydrate, concentrated whey protein powder, prebiotic compositions and water are mixed It closes, obtains feed liquid A, feed sequence in no particular order when material mixes;Lipid composition and vegetable fat are mixed, feed liquid B is obtained;It will answer Vitamin and water mixing are closed, feed liquid D is obtained;Composite mineral matter and water are mixed, feed liquid F is obtained;
(2) the feed liquid A and feed liquid B is mixed, homogeneous obtains feed liquid C;
(3) the feed liquid C and feed liquid D is mixed, obtains feed liquid E;
(4) the feed liquid E and feed liquid F is mixed, obtains feed liquid G;
(5) the feed liquid G is sterilized, concentration, it is dry to get.
In the present invention, the whole-fat milk powder and the skimmed milk powder can for whole-fat milk powder commonly used in the art and Skimmed milk powder.
In the present invention, the lactogenesis and skimmed milk can be lactogenesis and skimmed milk commonly used in the art;The life The dosage of cream is with the meter of lactogenesis dry matter;The dosage of the skimmed milk is with the meter of degreasing milk dry matter.
In the present invention, the desalted whey powder can be desalted whey powder commonly used in the art, protein content General to be not less than 12%, ash content is not higher than 3%.
In the present invention, the carbohydrate can be carbohydrate commonly used in the art, preferably lactose, One of maltodextrin and glucose are a variety of.
In the present invention, the vegetable fat can be vegetable fat commonly used in the art, preferably soybean oil and/ Or corn oil.
In the present invention, the concentrated whey protein powder is concentrated whey protein powder commonly used in the art, albumen Matter content is generally 34%~82%.
In the present invention, in the lipid composition, medium chain triglycerides (MCT), docosahexaenoic acid (DHA), flower Raw tetraenoic acid (ARA) and phosphatidylserine (PS) mass ratio are preferably (8.0~9.0): (0.3~0.6): (0.3~ 0.6): (1.0~1.5).
In the present invention, the multi-vitamins can for it is commonly used in the art be capable of providing vitamin A, vitamin D, Vitamin E, vitamin K1, vitamin B1, vitamin B2, vitamin B6, vitamin B12, niacin, folic acid, pantothenic acid, vitamin C and The multi-vitamins of biotin;The multi-vitamins can be the multivitamin monomer compounding of semi-finished product after evenly mixing Raw material;The dosage form of the multi-vitamins is generally respectively retinol acetate, Vitamin D3, dl- α-D-α-tocopherol acetate, plant Menadione, thiamine hydrochloride, riboflavin, puridoxine hydrochloride, cyanocobalamin, niacinamide, D-VB5 calcium, L-AA and D- biology Element;The multi-vitamins are preferably the model Li get Wei A- that the offer of food science and technology limited liability company is encouraged into Shanghai The multi-vitamins of vit.
In the present invention, the composition and dosage of the multi-vitamins can the full nutrition children laboratory milks according to the present invention The vitamin content of powder finished product is adjusted, and need to only make various vitamins in full nutrition children prescription emulsifiable powder of the present invention Content reaches the content's index of each vitamin in the full nutrition formula food of this field;Preferably, full battalion described in every 100g Support the type and content of vitamin described in children's prescription emulsifiable powder are as follows: the content of vitamin A is the 380 μ g μ g of RE~1080 RE; The content of vitamin D is 5.2 μ of μ g~12.9 g;The content of vitamin E is 5.2mg α-TE~14.5mg α-TE;Vitamin K1's Content is 30 μ of μ g~98 g;Vitamin B1Content be 300 μ of μ g~985 g;Vitamin B2Content be 250 μ of μ g~1250 g;Dimension Raw element B6Content be 280 μ of μ g~1090 g;Vitamin B12Content be 0.75 μ of μ g~7.65 g;The content of niacinamide is 2100 The μ of μ g~6250 g;The content of folic acid is 20 μ of μ g~239 g;The content of pantothenic acid is 650 μ of μ g~3980 g;Ascorbic content is 39mg~285mg;The content of biotin is 10 μ of μ g~86 g.
In the present invention, the composite mineral matter can for it is commonly used in the art be capable of providing magnesium, copper, iron, zinc, manganese, The composite mineral matter of calcium, iodine and selenium element;The composite mineral matter can be several mineral materials monomer after evenly mixing half Finished product compounds raw material;The composite mineral matter is generally magnesium sulfate, copper gluconate, ferrous gluconate, zinc sulfate, sulfuric acid Manganese, calcium carbonate, potassium iodide and sodium selenite, preferably Shanghai encourage into the model power of food science and technology limited liability company offer The composite mineral matter of A-min must be tieed up.
In the present invention, the composition and dosage of the composite mineral matter can the full nutrition children laboratory milks according to the present invention The content of mineral substances of powder finished product is adjusted, and need to only make various minerals in full nutrition children prescription emulsifiable powder of the present invention Content reaches the content's index of each minerals in the full nutrition formula food of this field;Preferably, full battalion described in every 100g Support the type and content of children's prescription emulsifiable powder Mineral Elements in Jadeite Shellfish are as follows: the content of sodium is 60mg~395mg;The content of potassium is 390mg~1280mg;The content of copper is 140 μ of μ g~690 g;The content of magnesium is 28mg~128mg;The content of iron be 5.1mg~ 9.8mg;The content of zinc is 2.0mg~6.2mg;The content of manganese is 20 μ of μ g~480 g;The content of calcium is 350mg~880mg;Phosphorus Content be 190mg~860mg;The content of iodine is 30 μ of μ g~280 g;The content of chlorine is 210mg~920mg;The content of selenium is 10 μ of μ g~45 g.
In step (1) of the invention, when preparation liquid A, the mixed method and condition can refer to this field routine Mixed method and condition is generally mixed with to the whole-fat milk powder etc. and is completely dissolved;The preferred following methods of the present invention and condition: The mixing preferably uses Vacuum mixer to carry out circulation mixing;The mixed temperature is preferably 45 DEG C~50 DEG C, the mixed time is preferably 10min~15min;The dosage of the water can be conventional amount used, as long as making material It can disperse in water and be uniformly mixed.
In step (1) of the invention, when preparation liquid B, the mixed method and condition can refer to this field routine Mixed method and condition, the preferred following methods of the present invention and condition: the mixed temperature is preferably 40 DEG C~45 DEG C, The mixed time is preferably 10min~15min.
In step (1) of the invention, when preparation liquid D, the mixed method and condition can refer to this field routine Mixed method and condition, the preferred following methods of the present invention and condition: the mixed temperature is preferably 25 DEG C~35 DEG C; Multi-vitamins concentration in the feed liquid D is preferably 2.5wt%~4.5wt%.
In step (1) of the invention, when preparation liquid F, the mixed method and condition can refer to this field routine Mixed method and condition, the preferred following methods of the present invention and condition: the mixed temperature is preferably 25 DEG C~35 DEG C; Composite mineral matter concentration in the feed liquid F is preferably 2.5wt%~4.5wt%.
In step (2) of the invention, the mixed method and condition can refer to method that this field routinely mixes and Condition, the preferred following methods of the present invention and condition: the mixed temperature is preferably 35 DEG C~40 DEG C, the mixing Time is preferably 10min~15min.
In step (2) of the invention, it includes level-one homogeneous and double-stage homogenization that the homogeneous, which is preferably, wherein level-one The pressure of homogeneous is preferably 16MPa~18MPa, and the pressure of double-stage homogenization is preferably 2MPa~4MPa, the temperature of the homogeneous Preferably 52 DEG C~54 DEG C of degree.
In step (3) of the invention, the mixed method and condition can refer to method that this field routinely mixes and Condition, the preferred the following conditions of the present invention: the mixed temperature is preferably 30 DEG C~38 DEG C.
In step (4) of the invention, the mixed method and condition can refer to method that this field routinely mixes and Condition, the preferred the following conditions of the present invention: the mixed temperature is preferably 30 DEG C~38 DEG C, the solid of the feed liquid G Object concentration is preferably 12.0wt%~14.0wt%.
In step (5) of the invention, the sterilization is preferably pasteurize, and the temperature of the pasteurize is preferably It is 86 DEG C~88 DEG C, the time of the sterilization is preferably 20s~30s;The concentration is preferably triple effect or quadruple effect vacuum Concentration, the concentration are preferably 48wt%~50wt% to solid concentration;The drying is preferably spray-dried, more It goodly is pressure spray dryer;The parameter of the pressure spray dryer can refer to the ginseng of the pressure spray dryer of this field routine Number, the preferably following parameter of the present invention: feeding temperature is preferably 72 DEG C~74 DEG C, and inlet air temperature is preferably 180 DEG C~182 DEG C, temperature of outgoing air is preferably 80 DEG C~82 DEG C, and atomisation pressure is preferably 200bar~230bar.
There is provided the full nutrition children as made from any of the above-described preparation method to be formulated by the two of technical solution of the present invention Milk powder.
The technical indicator of full nutrition children prescription emulsifiable powder of the present invention is as shown in table 1 below.
The technical indicator of the full nutrition children prescription emulsifiable powder of the invention of table 1
The technical indicator is that the conventional index of reference this field full nutrition formula food is set, on this basis, then root The nutritive element contents such as various vitamins, minerals in every 100kJ are had adjusted according to children feature, are that one kind contains The full nutrition formula food of higher level Density of nutrient.Lipid composition (the medium chain triglyceride three of specific composition is increased simultaneously Rouge, docosahexaenoic acid, arachidonic acid and phosphatidylserine composition), medium chain triglyceride therein is than common rouge Fat is easier to absorb and improve metabolic efficiency by children, and phosphatidylserine is the main component of brain cell and facilitates The brain development of children.Formula also added the combination of prebiotics (polyfructosan and oligofructose) of specific composition, promote children Intestines peristalsis.It is different from the conventional dry mixing process of DHA and ARA, in the process of the invention, the DHA in lipid composition Adding technology with ARA, by adjusting order of addition of ingredients, can effectively reduce DHA and ARA by the way of the addition of finish wet process Loss in process.
In the present invention, the children that the full nutrition children prescription emulsifiable powder is preferably suitable for 3~10 years old are edible.
Without prejudice to the field on the basis of common sense, above-mentioned each optimum condition, can any combination to get the present invention it is each preferably Example.
The reagents and materials used in the present invention are commercially available.
The positive effect of the present invention is that:
(1) full nutrition children prescription emulsifiable powder of the invention is a kind of novel infant formula, various nutrient compositions Content designed according to the physilogical characteristics of children and nutritional need.
(2) full nutrition children prescription emulsifiable powder of the invention contains necessary to good lactalbumin and children's torso all Minerals, vitamins and other nutritious components can be used as the single source of nutrition of the crowd including malnourished children.
(3) preparation method of the invention is changed using wet processing addition lipid composition (containing DHA grease and ARA grease) It has been apt to DHA and ARA in the uniformity of finished product and has reduced the loss of DHA and ARA in wet process adding procedure.
Specific embodiment
The present invention is further illustrated below by the mode of embodiment, but does not therefore limit the present invention to the reality It applies among a range.In the following examples, the experimental methods for specific conditions are not specified, according to conventional methods and conditions, or according to quotient The selection of product specification.
Each raw material sources in following embodiments:
Desalted whey powder and concentrated whey protein powder: Wei Liao (Shanghai) food trade Co., Ltd, GB11674-2010; Desalted whey powder model D70 or D90, raw material sources are whey;Concentrated whey protein powder model WPC34, protein content It is >=34%, raw material sources are whey.
Lactose: Wei Liao (Shanghai) food trade Co., Ltd, GB 25595-2010, raw material sources are whey.
Maltodextrin: DE value 16~20, the universal De Nong limited liability company in Heilungkiang, raw material sources are starch.
Glucose: Shandong continent biotechnology (Shandong) Co., Ltd meets GB/T20880-2007, source is starch.
Soybean oil: grain and oil (Yingkou) Co., Ltd in good, GB 1535-2003, raw material sources are soybean.
Corn oil: grain and oil (Yingkou) Co., Ltd in good, GB 19111-2003, raw material sources are soybean.
Docosahexaenoic acid grease (DHA grease): Shantou Run Ke bioengineering Co., Ltd, GB26400-2011 are former Material source is to split pot algae biofermentation.
Arachidonic acid oil (ARA grease): Shantou Run Ke bioengineering Co., Ltd, GB26401-2011, raw material come Source is Mortierella alpina biofermentation.
Medium chain triglyceride: food-grade, GB2716, Kening Co., Ltd, raw material sources are coconut oil or palm oil.
Polyfructosan, oligofructose: Belgian ORAFTI company, raw material sources are witloof.
Multi-vitamins: food science and technology limited liability company, model Li get Wei A-vit, the compound dimension life are encouraged into Shanghai The concrete composition of element see the table below 2.
Composite mineral matter: food science and technology limited liability company, model Li get Wei A-min, the complex mineral are encouraged into Shanghai The concrete composition of matter see the table below 3.
2 multi-vitamins of table composition
3 composite mineral matter of table composition
Mineral element title Content
Calcium 318~515mg/g
Iron 11.5~16.5mg/g
Manganese 53~108 μ g/g
Copper 525~760 μ g/g
Zinc 5.3~7.3mg/g
Selenium 47~66 μ g/g
Iodine 89~133 μ g/g
Embodiment 1
The composition of raw materials of 4 embodiment 1 of table
It is specific the preparation method is as follows:
(1) by Vacuum mixer by whole-fat milk powder, skimmed milk powder, desalted whey powder, lactose, concentrated whey protein powder, Prebiotic compositions mix at 45 DEG C with water, to obtain feed liquid A to uniformly mixed within circulation mixing 10 minutes;By lipid composition ingredient It is added separately in vegetable fat mix 10 minutes to obtain feed liquid B to uniformly mixed at 40 DEG C;By multi-vitamins at 25 DEG C It is scattered in deionized water and forms vitamin solution, the vitamine concentration in vitamin solution is 2.5wt%, and it is molten to obtain vitamin Liquid, i.e. feed liquid D;It disperses composite mineral matter in deionized water at 25 DEG C and forms mineral solution, in mineral solution Mineral concentration is 2.5wt%, obtains mineral solution, i.e. feed liquid F;
(2) feed liquid B and feed liquid A are mixed to 10 minutes at 35 DEG C to being uniformly mixed, feed liquid C is obtained after homogeneous.Wherein, Matter is double-stage homogenization, and the pressure of level-one homogeneous is 16MPa, and the pressure of double-stage homogenization is 2MPa, and the temperature of the homogeneous is 52 DEG C;
(3) feed liquid D is uniformly mixed at 30 DEG C with feed liquid C, obtains feed liquid E;
(4) feed liquid F is uniformly mixed at 30 DEG C with feed liquid E, obtains feed liquid G, solid concentration 12.0wt%;
(5) feed liquid G is subjected to pasteurize, be concentrated, is dried.Sterilization temperature is 86 DEG C, sterilizing time 20s;Concentration Stage uses quadruple effect vacuum concentration process, and the solid concentration of gained concentrated milk is 48wt%;Drying stage uses pressure-type spray Mist drying process, feeding temperature are 72 DEG C, and inlet air temperature is 180 DEG C, and temperature of outgoing air is 80 DEG C, pressure 200bar;To obtain the final product.
Product index testing result such as the following table 5 of the full nutrition children prescription emulsifiable powder.
The product index testing result of 5 embodiment 1 of table
Embodiment 2
The composition of raw materials of 6 embodiment 2 of table
It is specific the preparation method is as follows:
(1) pass through Vacuum mixer for whole-fat milk powder, skimmed milk powder, desalted whey powder, maltodextrin, whey protein concentrate Powder, prebiotic compositions mix at 50 DEG C with water, to obtain feed liquid A to uniformly mixed within circulation mixing 15 minutes;By lipid composition Ingredient is added separately in vegetable fat mix 15 minutes to obtain feed liquid B to uniformly mixed at 45 DEG C;By multi-vitamins in 35 It is scattered in deionized water at DEG C and forms vitamin solution, the vitamine concentration in vitamin solution is 4.5wt%, obtains vitamin Solution, i.e. feed liquid D;It disperses composite mineral matter in deionized water at 35 DEG C and forms mineral solution, in mineral solution Mineral concentration be 4.5wt%, obtain mineral solution, i.e. feed liquid F;
(2) feed liquid B and feed liquid A are mixed to 15 minutes at 40 DEG C to being uniformly mixed, feed liquid C is obtained after homogeneous.Wherein, Matter is double-stage homogenization, and the pressure of level-one homogeneous is 17MPa, and the pressure of double-stage homogenization is 3MPa, and the temperature of the homogeneous is 53 DEG C;
(3) feed liquid D is uniformly mixed at 38 DEG C with feed liquid C, obtains feed liquid E;
(4) feed liquid F is uniformly mixed at 38 DEG C with feed liquid E, obtains feed liquid G, solid concentration 14.0wt%;
(5) feed liquid G is sterilized respectively, is concentrated, is dried.Sterilization temperature is 88 DEG C, sterilizing time 30s;Concentration Stage uses triple effect vacuum concentration process, and the solid concentration of gained concentrated milk is 50wt%;Drying stage uses pressure-type spray Mist drying process, feeding temperature are 74 DEG C, and inlet air temperature is 182 DEG C, and temperature of outgoing air is 82 DEG C, pressure 230bar;To obtain the final product.
Product index testing result such as the following table 7 of the full nutrition children prescription emulsifiable powder.
The product index testing result of 7 embodiment 2 of table
Embodiment 3
The composition of raw materials of 8 embodiment 3 of table
It is specific the preparation method is as follows:
(1) by Vacuum mixer by whole-fat milk powder, skimmed milk powder, desalted whey powder, lactose, maltodextrin, glucose, Concentrated whey protein powder, prebiotic compositions mix at 48 DEG C with water, to obtain feed liquid A to uniformly mixed within circulation mixing 12 minutes; Lipid composition ingredient is added separately in vegetable fat mix 12 minutes to obtain feed liquid B to uniformly mixed at 43 DEG C;It will answer Conjunction vitamin is scattered in deionized water at 30 DEG C forms vitamin solution, and the vitamine concentration in vitamin solution is 3.5wt% obtains vitamin solution, i.e. feed liquid D;It is molten to disperse composite mineral matter at 30 DEG C formation minerals in deionized water Liquid, the mineral concentration in mineral solution is 3.0wt%, obtains mineral solution, i.e. feed liquid F;
(2) feed liquid B and feed liquid A are mixed to 13 minutes at 38 DEG C to being uniformly mixed, feed liquid C is obtained after homogeneous.Wherein, Matter is double-stage homogenization, and the pressure of level-one homogeneous is 18MPa, and the pressure of double-stage homogenization is 4MPa, and the temperature of the homogeneous is 54 DEG C;
(3) feed liquid D is uniformly mixed at 35 DEG C with feed liquid C, obtains feed liquid E;
(4) feed liquid F is uniformly mixed at 36 DEG C with feed liquid E, obtains feed liquid G, solid concentration 13.0wt%;
(5) feed liquid G is sterilized respectively, is concentrated, is dried.Sterilization temperature is 87 DEG C, sterilizing time 25s;Concentration Stage uses quadruple effect vacuum concentration process, and the solid concentration of gained concentrated milk is 49wt%;Drying stage uses pressure-type spray Mist drying process, feeding temperature are 73 DEG C, and inlet air temperature is 181 DEG C, and temperature of outgoing air is 81 DEG C, pressure 210bar;To obtain the final product.
Product index testing result such as the following table 9 of the full nutrition children prescription emulsifiable powder.
The product index testing result of 9 embodiment 3 of table
Comparative example 1
The composition of raw materials of 10 comparative example 1 of table (formula is with embodiment 3)
It is specific the preparation method is as follows:
(1) whole-fat milk powder, skimmed milk powder, desalted whey powder, vegetable fat, lactose, malt are pasted by Vacuum mixer Essence, glucose, concentrated whey protein powder, prebiotic compositions, lipid composition ingredient mix at 48 DEG C with water, circulation mixing Feed liquid A is obtained to uniformly mixed within 12 minutes;It disperses multi-vitamins in deionized water at 30 DEG C and forms vitamin solution, tie up Vitamine concentration in raw element solution is 3.5wt%, obtains vitamin solution, i.e. feed liquid C;Composite mineral matter is dispersed at 30 DEG C Mineral solution is formed in deionized water, the mineral concentration in mineral solution is 3.0wt%, obtains mineral solution, i.e., Feed liquid E;
(2) feed liquid A is mixed to 13 minutes at 38 DEG C to being uniformly mixed, feed liquid B is obtained after homogeneous.Wherein, homogeneous two Grade homogeneous, the pressure of level-one homogeneous are 18MPa, and the pressure of double-stage homogenization is 4MPa, and the temperature of the homogeneous is 54 DEG C;
(3) feed liquid C is uniformly mixed at 35 DEG C with feed liquid B, obtains feed liquid D;
(4) feed liquid E is uniformly mixed at 36 DEG C with feed liquid D, obtains feed liquid G, solid concentration 13.0wt%;
(5) feed liquid F is sterilized respectively, is concentrated, is dried.Sterilization temperature is 87 DEG C, sterilizing time 25s;Concentration Stage uses quadruple effect vacuum concentration process, and the solid concentration of gained concentrated milk is 49wt%;Drying stage uses pressure-type spray Mist drying process, feeding temperature are 73 DEG C, and inlet air temperature is 181 DEG C, and temperature of outgoing air is 81 DEG C, pressure 210bar;To obtain the final product.
Product index testing result such as the following table 11 of the full nutrition children prescription emulsifiable powder.
The product index testing result of 11 comparative example 1 of table
Comparative example 2
The composition of raw materials of 12 comparative example 2 of table
(vegetable fat being replaced with into whole-fat milk powder, remaining is with formula with embodiment 3)
It is specific the preparation method is as follows:
(1) by Vacuum mixer by whole-fat milk powder, skimmed milk powder, desalted whey powder, lactose, maltodextrin, glucose, Concentrated whey protein powder, prebiotic compositions, lipid composition ingredient mix at 48 DEG C with water, and circulation mixing 12 minutes is to mixed Close uniform feed liquid A;It disperses multi-vitamins in deionized water at 30 DEG C and forms vitamin solution, in vitamin solution Vitamine concentration be 3.5wt%, obtain vitamin solution, i.e. feed liquid C;Deionized water is dispersed at 30 DEG C by composite mineral matter Middle formation mineral solution, the mineral concentration in mineral solution is 3.0wt%, obtains mineral solution, i.e. feed liquid E;
(2) feed liquid A is mixed to 13 minutes at 38 DEG C to being uniformly mixed, feed liquid B is obtained after homogeneous.Wherein, homogeneous two Grade homogeneous, the pressure of level-one homogeneous are 18MPa, and the pressure of double-stage homogenization is 4MPa, and the temperature of the homogeneous is 54 DEG C;
(3) feed liquid C is uniformly mixed at 35 DEG C with feed liquid B, obtains feed liquid D;
(4) feed liquid E is uniformly mixed at 36 DEG C with feed liquid D, obtains feed liquid G, solid concentration 13.0wt%;
(5) feed liquid F is sterilized respectively, is concentrated, is dried.Sterilization temperature is 87 DEG C, sterilizing time 25s;Concentration Stage uses quadruple effect vacuum concentration process, and the solid concentration of gained concentrated milk is 49wt%;Drying stage uses pressure-type spray Mist drying process, feeding temperature are 73 DEG C, and inlet air temperature is 181 DEG C, and temperature of outgoing air is 81 DEG C, pressure 210bar;To obtain the final product.
Product index testing result such as the following table 13 of the full nutrition children prescription emulsifiable powder.
The product index testing result of 13 comparative example 2 of table
Comparative example 3
The composition of raw materials of 14 comparative example 3 of table
(phosphatidylserine being replaced with into whole-fat milk powder, remaining is with formula with embodiment 3)
It is specific the preparation method is as follows:
(1) by Vacuum mixer by whole-fat milk powder, skimmed milk powder, desalted whey powder, lactose, maltodextrin, glucose, Concentrated whey protein powder, prebiotic compositions mix at 48 DEG C with water, to obtain feed liquid A to uniformly mixed within circulation mixing 12 minutes; Lipid composition ingredient is added separately in vegetable fat mix 12 minutes to obtain feed liquid B to uniformly mixed at 43 DEG C;It will answer Conjunction vitamin is scattered in deionized water at 30 DEG C forms vitamin solution, and the vitamine concentration in vitamin solution is 3.5wt% obtains vitamin solution, i.e. feed liquid D;It is molten to disperse composite mineral matter at 30 DEG C formation minerals in deionized water Liquid, the mineral concentration in mineral solution is 3.0wt%, obtains mineral solution, i.e. feed liquid F;
(2) feed liquid B and feed liquid A are mixed to 13 minutes at 38 DEG C to being uniformly mixed, feed liquid C is obtained after homogeneous.Wherein, Matter is double-stage homogenization, and the pressure of level-one homogeneous is 18MPa, and the pressure of double-stage homogenization is 4MPa, and the temperature of the homogeneous is 54 DEG C;
(3) feed liquid D is uniformly mixed at 35 DEG C with feed liquid C, obtains feed liquid E;
(4) feed liquid F is uniformly mixed at 36 DEG C with feed liquid E, obtains feed liquid G, solid concentration 13.0wt%;
(5) feed liquid G is sterilized respectively, is concentrated, is dried.Sterilization temperature is 87 DEG C, sterilizing time 25s;Concentration Stage uses quadruple effect vacuum concentration process, and the solid concentration of gained concentrated milk is 49wt%;Drying stage uses pressure-type spray Mist drying process, feeding temperature are 73 DEG C, and inlet air temperature is 181 DEG C, and temperature of outgoing air is 81 DEG C, pressure 210bar;To obtain the final product.
Product index testing result such as the following table 15 of the full nutrition children prescription emulsifiable powder.
The product index testing result of 15 comparative example 3 of table
Effect example 1
For full nutrition children's prescription emulsifiable powder made from the embodiment of the present invention 1 and embodiment 3, with " food safety country Standard special medicine purposes formula food general rule " 1~10 years old crowd in GB 29922-2013 be reference, to embodiment 1 and real It applies full nutrition children's prescription emulsifiable powder nutritive index made from example 3 and compares evaluation, comparing result is as shown in table 16.
The evaluation of 16 nutritive index of table
As can be seen from Table 16, the full nutrition children prescription emulsifiable powder of embodiment 1 and embodiment 3 all meets " food safety state Family's standard special medicine purposes formula food general rule " the defined requirement of GB29922-2013, it is suitble to children to come as single nutrition Source is edible.The effect of embodiment 3 is suitable with embodiment 1.
Effect example 2
For full nutrition children's prescription emulsifiable powder made from the embodiment of the present invention 3 and comparative example 1, comparative example 2, it incite somebody to action this respectively DHA, ARA content of full nutrition children's prescription emulsifiable powder made from inventive embodiments 3 and comparative example 1, comparative example 2 compare, right It is more as shown in table 17 than result.
Table 17DHA and ARA comparision contents
The formula composition of the embodiment of the present invention 3 and comparative example 1 is consistent, only the preparation method of comparative example 1 and this hair Bright embodiment 3 is slightly different, and wherein comparative example 1 is by lipid composite (containing DHA grease and ARA grease) and whole-fat milk powder, takes off The raw materials such as fat milk powder, lactose, maltodextrin, vegetable fat dissolve ingredient simultaneously together, and embodiment 3 is first by lipid composite (containing DHA grease and ARA grease) is mixed with other ingredients solutions again after mixing with vegetable fat.The formula of comparative example 2, will Vegetable fat replaces all with whole-fat milk powder, remaining is completely the same with the embodiment of the present invention 3, so in the formula of comparative example 2 not Containing vegetable fat, with this influence of observation of plant grease to DHA and ARA.The formula of comparative example 3, by phosphatidylserine whole Whole-fat milk powder is replaced with, remaining is completely the same with the embodiment of the present invention 3, so being free of phosphatidyl silk ammonia in the formula of comparative example 3 Acid observes influence of the phosphatidylserine to DHA and ARA with this.As can be seen from Table 17, comparative example 1, comparative example 2 and comparison Content of the content of the DHA and ARA of example 3 obviously than the embodiment of the present invention 3 is low, illustrates in comparative example 1, comparative example 2 and comparative example 3 Preparation process in DHA and ARA loss it is all larger.Therefore, preparation method of the invention adds lipid group using wet processing Object (containing DHA grease and ARA grease) is closed, not only improve DHA and ARA in the uniformity of finished product and reduces DHA and ARA exists Loss in wet process adding procedure.

Claims (11)

1. a kind of preparation method of full nutrition children prescription emulsifiable powder, which is characterized in that the full nutrition children prescription emulsifiable powder includes Following components: 20%~30% whole-fat milk powder or lactogenesis, 12%~19% skimmed milk powder or skimmed milk, 18%~21% desalination cream Clear powder, 12%~18% carbohydrate, 6%~12% vegetable fat, 5%~10% concentrated whey protein powder, 2%~6% Prebiotic compositions, 1.5%~4.5% lipid composition, 0.15%~0.25% multi-vitamins and 0.45%~0.55% Composite mineral matter, the percentage are the percentage that each component quality accounts for the full nutrition children prescription emulsifiable powder gross mass;It is described Lipid composition be made of medium chain triglycerides, docosahexaenoic acid, arachidonic acid and phosphatidylserine;Described Prebiotic compositions are made of polyfructosan and oligofructose, quality percentage of the polyfructosan in the combination of prebiotics Than being 40%~60%;
The preparation method includes the following steps:
(1) it is matched by said components, respectively preparation liquid A, feed liquid B, feed liquid D and feed liquid F;Wherein, by whole-fat milk powder or lactogenesis, Skimmed milk powder or skimmed milk, desalted whey powder, carbohydrate, concentrated whey protein powder, prebiotic compositions and water mixing, obtain Feed liquid A, feed sequence in no particular order when material mixes;Lipid composition and vegetable fat are mixed, feed liquid B is obtained;By compound dimension Raw element and water mixing, obtain feed liquid D;Composite mineral matter and water are mixed, feed liquid F is obtained;
(2) the feed liquid A and feed liquid B is mixed, homogeneous obtains feed liquid C;
(3) the feed liquid C and feed liquid D is mixed, obtains feed liquid E;
(4) the feed liquid E and feed liquid F is mixed, obtains feed liquid G;
(5) the feed liquid G is sterilized, concentration, it is dry to get.
2. preparation method as described in claim 1, which is characterized in that the protein content of the desalted whey powder is not less than 12%, ash content is not higher than 3%;
And/or the carbohydrate is one of lactose, maltodextrin and glucose or a variety of;
And/or the vegetable fat is soybean oil and/or corn oil;
And/or the protein content of the concentrated whey protein powder is 34%~82%.
3. preparation method as described in claim 1, which is characterized in that in the lipid composition, medium chain triglycerides, two The mass ratio of dodecahexaene acid, arachidonic acid and phosphatidylserine is (8.0~9.0): (0.3~0.6): (0.3~ 0.6): (1.0~1.5).
4. preparation method as described in claim 1, which is characterized in that institute in full nutrition children prescription emulsifiable powder described in every 100g State the type and content of vitamin are as follows: the content of vitamin A is the 380 μ g μ g of RE~1080 RE;The content of vitamin D is 5.2 μ The μ of g~12.9 g;The content of vitamin E is 5.2mg α-TE~14.5mg α-TE;Vitamin K1Content be 30 μ of μ g~98 g;Dimension Raw element B1Content be 300 μ of μ g~985 g;Vitamin B2Content be 250 μ of μ g~1250 g;Vitamin B6Content be 280 μ g ~1090 μ g;Vitamin B12Content be 0.75 μ of μ g~7.65 g;The content of niacinamide is 2100 μ of μ g~6250 g;Folic acid contains Amount is 20 μ of μ g~239 g;The content of pantothenic acid is 650 μ of μ g~3980 g;Ascorbic content is 39mg~285mg;Biotin Content is 10 μ of μ g~86 g;
And/or the type and content of full nutrition children prescription emulsifiable powder Mineral Elements in Jadeite Shellfish described in every 100g are as follows: the content of sodium is 60mg~395mg;The content of potassium is 390mg~1280mg;The content of copper is 140 μ of μ g~690 g;The content of magnesium be 28mg~ 128mg;The content of iron is 5.1mg~9.8mg;The content of zinc is 2.0mg~6.2mg;The content of manganese is 20 μ of μ g~480 g;Calcium Content be 350mg~880mg;The content of phosphorus is 190mg~860mg;The content of iodine is 30 μ of μ g~280 g;The content of chlorine is 210mg~920mg;The content of selenium is 10 μ of μ g~45 g.
5. preparation method as described in claim 1, which is characterized in that in step (1), when preparation liquid A, described is mixed into The circulation mixing carried out using Vacuum mixer;The mixed temperature is 45 DEG C~50 DEG C, and the mixed time is 10min~15min;
And/or when preparation liquid B, the mixed temperature be 40 DEG C~45 DEG C, the mixed time be 10min~ 15min;
And/or when preparation liquid D, the mixed temperature is 25 DEG C~35 DEG C, and the multi-vitamins in the feed liquid D are dense Degree is 2.5wt%~4.5wt%;
And/or when preparation liquid F, the mixed temperature is 25 DEG C~35 DEG C, and the composite mineral matter in the feed liquid F is dense Degree is 2.5wt%~4.5wt%.
6. preparation method as described in claim 1, which is characterized in that in step (2), the mixed temperature be 35 DEG C~ 40 DEG C, the mixed time is 10min~15min;
And/or the homogeneous includes level-one homogeneous and double-stage homogenization;The pressure of the level-one homogeneous be 16MPa~ 18MPa, the pressure of the double-stage homogenization are 2MPa~4MPa, and the temperature of the homogeneous is 52 DEG C~54 DEG C.
7. preparation method as described in claim 1, which is characterized in that in step (3), the mixed temperature be 30 DEG C~ 38℃。
8. preparation method as described in claim 1, which is characterized in that in step (4), the mixed temperature be 30 DEG C~ 38 DEG C, the solid concentration of the feed liquid G is 12.0wt%~14.0wt%.
9. preparation method as described in claim 1, which is characterized in that in step (5), the sterilization is pasteurize;Institute The temperature for stating pasteurize is 86 DEG C~88 DEG C, and the time of the sterilization is 20s~30s;The concentration is that triple effect vacuum is dense Contracting or quadruple effect vacuum concentration, the concentration are 48wt%~50wt% to be concentrated into solid concentration;
And/or the drying is spray drying.
10. preparation method as claimed in claim 9, which is characterized in that the spray drying is pressure spray dryer, described Pressure spray dryer parameter it is as described below: feeding temperature be 72 DEG C~74 DEG C, inlet air temperature be 180 DEG C~182 DEG C, air draft Temperature is 80 DEG C~82 DEG C, and atomisation pressure is 200bar~230bar.
11. a kind of full nutrition children prescription emulsifiable powder, which is characterized in that it is by as described in any one of claim 1~10 Made from preparation method.
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