CN105746728A - Infant formula milk powder simulating breast milk and preparation method of infant formula milk powder - Google Patents

Infant formula milk powder simulating breast milk and preparation method of infant formula milk powder Download PDF

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Publication number
CN105746728A
CN105746728A CN201610143847.4A CN201610143847A CN105746728A CN 105746728 A CN105746728 A CN 105746728A CN 201610143847 A CN201610143847 A CN 201610143847A CN 105746728 A CN105746728 A CN 105746728A
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vitamin
powder
milk powder
acid
premix
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涂醉桃
张艳杰
马粉娟
江雨婷
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Shanghai Cheng Guan Dairy Co Ltd
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Shanghai Cheng Guan Dairy Co Ltd
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C21/00Whey; Whey preparations
    • A23C21/06Mixtures of whey with milk products or milk components
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C21/00Whey; Whey preparations
    • A23C21/02Whey; Whey preparations containing, or treated with, microorganisms or enzymes
    • A23C21/026Whey; Whey preparations containing, or treated with, microorganisms or enzymes containing, or treated only with, lactic acid producing bacteria, bifidobacteria or propionic acid bacteria
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C21/00Whey; Whey preparations
    • A23C21/04Whey; Whey preparations containing non-milk components as source of fats or proteins
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C21/00Whey; Whey preparations
    • A23C21/08Whey; Whey preparations containing other organic additives, e.g. vegetable or animal products
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C21/00Whey; Whey preparations
    • A23C21/10Whey; Whey preparations containing inorganic additives

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Microbiology (AREA)
  • Inorganic Chemistry (AREA)
  • Zoology (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)

Abstract

The invention discloses infant formula milk powder simulating breast milk and a preparation method of the infant formula milk powder.The infant formula milk powder is prepared from, by weight percentage, base powder, galactooligosaccharide, fructo-oligosaccharide, L-carnitine, inositol, probiotic, docosahexaenoic acid, eicostatetraenoic acid, nucleotide, lutein, taurine and choline.Fatty acid in the infant formula milk powder is formed by mixing and proportioning five plant oils, and 1, 3 dioleic acid 2-palmitic acid triglyceride (OPO structure lipid) is added.The infant formula milk powder is conducive to absorption of fatty acid and calcium, can promote infant skeleton health, can effectively reduce calcium soap constipation caused by palmitic acidin conventional formula milk powder, can soften excrement of infants and is easier for the infants to digest and absorb.

Description

A kind of baby formula milk powder simulating breast milk and preparation method thereof
Technical field
The present invention relates to food compositions processing technique field, particularly relate to a kind of infant formula milk simulating breast milk Powder and preparation method thereof.
Background technology
Breast milk is infant optimal natural nutrition source, can not carry out breast feeding yet with individual's reason , baby formula milk powder is then preferable breast milk succedaneum.Therefore breast milk is also baby formula milk powder research and development Golden standard, breast milk nutrition is also constantly studied by scientist, promote baby formula milk powder development. The nutrient categories the most contained by adding breast milk at present simulates breast milk nutrition, as protein, fat, As far as possible close to breast milk in the nutrient categories such as carbohydrate, mineral, vitamin and quantity.
Along with the development of science and technology, research is constantly found that other nutrient of breast milk, as probiotic bacteria, 1,3 Two oleic acid 2-palmitic acid three esters etc., Structure grease spy contain 1,3-bis-oleic acid ,-2-palmitic acid three Ester be in breast milk Palmic acid be primarily present form.Research shows, the satisfied fatty acid that in breast milk, content is the highest is Palmic acid, accounts for the 17-25% of ripe breast milk fatty acids, wherein has the Palmic acid of about 70% to be distributed in Sn-2 position On, in breast milk, a kind of main triglyceride is 1,3-bis-oleic acid ,-2-palmitic acid three ester.Structure grease from Fatty acid structure simulates Palmic acid structure composition in breast milk in form.Be conducive to fatty acid and calcareous absorption, and Promote infant bone health, the calcium soap constipation problem that in conventional formulation milk powder, Palmic acid causes can be eliminated.Research Show that breast milk nutrient is a complicated trophosome, in macroscopic view nutrient categories and quantity, only simulate breast milk Not enough, Nutrients Absorption and the functional development of baby be there is also important by ratio and the microstructure of its nutrient Relation.
Summary of the invention
The present invention solves the problems referred to above of the prior art, it is provided that a kind of infant formula milk simulating breast milk Powder, inventive formulation Fatty Acids In Milk Powder forms through 5 vegetable oil mixing match, its fatty acid composition after proportioning Form closer to breast milk fatty acids, add OPO structured lipid (OPO) fat Fat acid structural simulation breast milk fatty acids structure, carbohydrate is full milk sugar, and 2 kinds can effectively facilitate intestinal The propagation of the multiple bacillus bifidus in road, and suppress harmful bacteria and the prebiotic, fructooligosaccharide, oligomeric of amphimicrobe propagation Galactose, simultaneously regulation lactalbumin and casein ratio, for all ages and classes 0-6 month baby milk albumin: Casein >=6:4, more than 6 months bigger infants and young's lactalbumins: casein >=1:1, make protein ratio and Aminoacid forms closer to breast milk.Can effectively reduce infant to get angry and constipation, support infant intestinal Group's stability, it is easier to digest and assimilate, reduces metabolism burden.
Present invention also offers the preparation method of a kind of baby formula milk powder simulating breast milk, by controlling product The technology such as middle water activity and packaging remaining oxygen, at utmost preserve the baby formula milk powder of probiotic active, Avoid probiotic bacteria and producing the activity decay in a large number of storage process, extend the shelf life of product;Probiotic bacteria warp After crossing special embedding treatment, can still retain higher survival rate after by gastric juice and bile and intestinal mucosa adheres to Ability;Probiotic bacteria adds employing two-stage mixing, dry process, it is ensured that mixing homogeneity.
For achieving the above object, the present invention is by the following technical solutions:
The first aspect of the invention is to provide a kind of baby formula milk powder simulating breast milk, by weight percentage Meter, formulated by following raw material components: skimmed milk powder 10~40%, desalted whey powder 25~45%, to concentrate Lactalbumin powder 1.0~8.0%, 1,3-bis-oleic acid 2-palmitic acid three ester (OPO structured lipid) 5~20%, Vegetable oil 5~20%, lactose 5~20%, phosphatidase 0~0.5%, calcium carbonate 0.01~0.5%, compounding mineral Premix material 0.05~0.95%, compounding vitamin premix 0.01~0.12%, oligomeric galactose 0.1~5.0%, Oligofructose 0.1~5.0%, animal bifidobacteria (Bb-12) 0~0.1%, Bifidobacterium lactis (Bi-07) 0~ 0.1%, docosahexenoic acid 0~0.14%, eicosatetraenoic acid 0~0.18%, choline 0~0.05%, core Thuja acid 0~0.06%, phylloxanthin 0~0.0004%, L-carnitine 0.01~0.1%, taurine 0~0.07%, Inositol 0.01~0.2%, L-AA sodium 0.03~0.12%;
Described compounding mineral substance premix by mass percentage, including following raw material components: potassium chloride 5~ 33%, sodium chloride 6~18%, copper sulfate 0.01~0.50%, magnesium sulfate 5~15%, ferrous sulfate 10~45%, Zinc sulfate 0.5~8.0%, manganese sulfate 0.1~1.0%, sodium selenite 0.1~5.0%, sodium citrate 10~21%, Lactose 10~25%;
Described compounding vitamin premix by mass percentage, including following raw material components: retinol acetate (dimension Raw element A) 5~18%, cholecalciferol (vitamin D3) 3~12%, dl-α-tocopheryl acetate (vitamin E) 27~40%, phytonadione (vitamin K) 0.5~5.0%, thiamine nitrate (vitamin B1) 0.5~ 4.0%, riboflavin (vitamin B2) 0.05~3.00%, pyridoxine hydrochloride (vitamin B6) 0.5~3.0%, Cobalamin (vitamin B12) 0.5~5.0%, nicotiamide 4~12%, folic acid 0.5~5.0%, D-VB5 calcium 0.5~5.0%, biotin 0.5~5.0%, potassium iodide 0.5~5.0%, lactose 15~30%;
Described animal bifidobacteria (Bb-12) specification is 30IF (30 × 108Cfu/g), Bifidobacterium lactis (Bi-07) Specification is 300B (300 × 108Cfu/g), described animal bifidobacteria (Bb-12) and Bifidobacterium lactis (Bi-07) Interpolation total amount be 0.5 × 107~3 × 107cfu/g。
Further, by weight percentage, the raw material components of inventive formulation milk powder also includes lactoferrin 0.001~0.05%, sialic acid 0.002~0.007%.
Further, described compounding mineral substance premix also includes calcium hydrogen phosphate 0.1~1.0%, calcium pyrophosphate 0.5~2.0%.
Further, by weight percentage, the raw material components of inventive formulation milk powder also includes medium chain triglyceride The use of three esters, described medium chain triglyceride and OPO (OPO structured lipid) Amount ratio is 1:4~1:6.
Further, by weight percentage, formulated by following raw material components: skimmed milk powder 15~35%, Desalted whey powder 30~45%, concentrated whey protein powder 1.0~5.0%, 1,3-bis-oleic acid 2-palmitic acid three Ester (OPO structured lipid) 7~13%, vegetable oil 8~15%, lactose 8~15%, phosphatidase 0 .2~0.4%, Calcium carbonate 0.1~0.35%, compounding mineral substance premix 0.1~0.8%, compounding vitamin premix 0.05~ 0.10%, oligomeric galactose 0.5~2%, oligofructose 0.2~2%, animal bifidobacteria (Bb-12) 0.001~ 0.05%, Bifidobacterium lactis (Bi-07) 0.001~0.05%, docosahexenoic acid 0.01~0.1%, 20 Carbon tetraenoic acid 0.05~0.1%, choline 0.02~0.04%, nucleotide 0~0.03%, phylloxanthin 0.0001~ 0.0003%, L-carnitine 0~0.02%, taurine 0.01~0.04%, inositol 0~0.1%, L-Vitamin C Acid sodium 0.04~0.11%.
Further, by weight percentage, formulated by following raw material components: skimmed milk powder 18%, de- Salt whey powder 40%, concentrated whey protein powder 1.5%, vegetable oil 14%, 1,3-bis-oleic acid 2-palmitic acid three Ester (OPO structured lipid) 12%, lactose 11.7568%, phosphatidase 0 .15%, calcium carbonate 0.3%, compounding mineral Premix material 0.7%, compounding vitamin premix 0.07%, oligomeric galactose 0.8%, oligofructose 0.4%, dynamic Thing bacillus bifidus (Bb-12) 0.003%, Bifidobacterium lactis (Bi-07) 0.005%, docosahexenoic acid 0.03%, eicosatetraenoic acid 0.06%, choline 0.06%, inositol 0.03%, nucleotide 0.03%, phylloxanthin 0.0002%, L-carnitine 0.01%, taurine 0.035%, L-AA sodium 0.06%.
Further, by mass percentage, described compounding mineral substance premix includes following raw material components: chlorine Change potassium 26%, sodium chloride 12.5%, copper sulfate 0.12%, magnesium sulfate 10.5%, ferrous sulfate 13.5%, sulfur Acid zinc 1.78%, manganese sulfate 0.15%, sodium selenite 0.55%, sodium citrate 14.4%, lactose 19.5%.
Further, by mass percentage, described compounding vitamin premix includes following raw material components: vinegar Acid retinyl ester (vitamin A) 9.8%, cholecalciferol (vitamin D3) 6.5%, dl-α-tocopheryl acetate (dimension Raw element E) 34.5%, phytonadione (vitamin K) 2.2%, thiamine nitrate (vitamin B1) 0.95%, Riboflavin (vitamin B2) 0.23%, pyridoxine hydrochloride (vitamin B6) 0.91%, cobalamin (vitamin B12) 2.91%, nicotiamide 8.0%, folic acid 2.2%, D-VB5 calcium 2.7%, biotin 2.8%, potassium iodide 2.0%, lactose 24.3%.
Described vegetable oil is mixed vegetable oil and OPO Structure grease mixes according to 1.2:1 ratio.
Wherein, described mixed vegetable oil is soybean oil, high oleic sunflower oil, Semen Maydis oil, Petiolus Trachycarpi oil and Cortex cocois radicis Oil is by weight 1:(0.5-1.2): (1-1.6): (0.3-0.8): (1.5-2.3) mixes.
Further, described vegetable oil is soybean oil, high oleic sunflower oil, Semen Maydis oil, Petiolus Trachycarpi oil and Cortex cocois radicis Oil is by weight 1:(0.6-1.2): (1-1.5): (0.4-0.7): (1.6-2.2) mixes.
Further, mixed vegetable oil is by soybean oil, high oleic sunflower oil, Semen Maydis oil, Petiolus Trachycarpi oil and Cortex cocois radicis Oil is by weight 1:(0.7-0.9): (1-1.1): (0.5-0.6): (1.7-2) mixes.
Preferably, described vegetable oil is soybean oil, high oleic sunflower oil, Semen Maydis oil, Petiolus Trachycarpi oil and Oleum Cocois Compound lard, by mass percentage, described soybean oil, high oleic sunflower oil, Semen Maydis oil, Petiolus Trachycarpi oil and Oleum Cocois amount ratio is 1:0.8:1.1:0.6:1.8.
Further, described animal bifidobacteria (Bb-12) and Bifidobacterium lactis (Bi-07) interpolation total amount are 1×107cfu/g。
The second aspect of the invention, method provides the preparation side of a kind of baby formula milk powder simulating breast milk Method, specifically includes following steps:
Step 1, one-level batch mixing: by skimmed milk powder, desalted whey powder, concentrated whey protein powder, vegetable oil, Lactose, phospholipid and calcium carbonate use the pure water mixed dissolution of 50~70 DEG C, are sufficiently stirred for;
Step 2, two grades of batch mixings: by compounding mineral substance premix, compounding vitamin premix respectively each special By 20 times amount 30~the dissolved in purified water of 40 DEG C in container, substep add step 1 to) batch mixing in fill Divide mixing, compounding mineral and compounding vitamin to add incorporation time and answer >=10min;
Step 3, homogenizing: by step 2) dissolve the material mixed and carry out homogenizing, homogenization pressure be 20~ 22Mpa;
Step 4, pre-sterilizing: by step 3) material after homogenizing carries out pre-sterilizing, sterilization temperature 80~90 DEG C, Sterilizing time 16s, cools down, keeps in, temporary temperature 8~15 DEG C, temporary storage time≤4h;
Step 5, sterilization concentrates: by step 4) temporary material sends into vaporization chamber and carries out sterilization and concentrate, sterilization Temperature 87~90 DEG C, sterilizing time 24s, an effect evaporating temperature 62~72 DEG C, two effect evaporating temperatures 46~56 DEG C, Evaporating pressure-0.086~-0.095Mpa, sterilization pressure 0.05~0.02Mpa;Discharge concentration 16.0~21.0 ° of Be;
Step 6, be dried: by step 5) concentrate after material send into drying tower through high-pressure pump, process conditions are: Inlet temperature 145~175 DEG C, temperature of outgoing air 65~92 DEG C, negative pressure (-0.5~-4.0) × 100pa in tower, fluidisation Bed negative pressure: (-0.5~-3.5) × 100pa, one section of temperature 30~85 DEG C, two-stage nitration temperature 5~55 DEG C, three sections of temperature 5~35 DEG C, four sections of temperature 5~30 DEG C, high-pressure pump pressure 15~30Mpa is spray-dried;And by stream Change bed and carry out redrying powder delivery, powder delivery temperature≤38 DEG C, moisture≤4.0%, obtain original washing powder;
Step 7, premix: by animal bifidobacteria (Bb-12), Bifidobacterium lactis (Bi-07), oligomeric half Lactose, oligofructose, docosahexenoic acid, eicosatetraenoic acid, choline, nucleotide, phylloxanthin, a left side Rotation carnitine, taurine, inositol, L-AA sodium premix respectively according to addition;
Step 8, mixing: by original washing powder and step 7) premix material mixes according to formula proportion, obtains finished powder.
Step 9, packaging, detection, warehouse-in.
Further, described step 2) in, when dissolving compounding mineral substance premix and compounding vitamin premix, First dissolving compounding mineral substance premix, after 10min, re-dissolved compounds vitamin premix.
Further, described step 7) in, described animal bifidobacteria (Bb-12), Bifidobacterium lactis (Bi-07), Oligomeric galactose, oligofructose, docosahexenoic acid, eicosatetraenoic acid, choline, nucleotide, leaf are yellow Element, L-carnitine, taurine, inositol, L-AA sodium need, through expanding dilution, to expand dilute before premix material Releasing use HS-10 three-dimensional motion mixer, motion frequency is 35HZ, and incorporation time is 30s.
The present invention uses technique scheme, compared with prior art, has the following technical effect that
In inventive formulation milk powder, oligofructose and oligomeric galactose are as the food of beneficial bacteria of intestinal tract, can promote intestinal benefit The increment of raw bacterium, after with the addition of prebiotics, adds probiotic bacteria simultaneously, and infant can be helped to quickly form with benefit Raw bacterium is the intestinal microbial population of dominant microflora, and maintains stablizing of intestinal dominant microflora, thus suppresses harmful bacteria, limit Pathogenic microorganism processed and intestinal mucosa adhere to, field planting;Inventive formulation milk powder scalable intestinal microbial population, optimizes intestinal Environment, forms stable intestinal dominant microflora, promotes Nutrients Absorption, promotes defecation speed, softens stool, Constipation, prevents healthy babies from suffering from acute diarrhea.
Accompanying drawing explanation
Fig. 1 is the probiotic bacteria Bb-12 fading curve that the present invention simulates in the baby formula milk powder of breast milk.
Detailed description of the invention
The invention provides the preparation method of a kind of baby formula milk powder simulating breast milk.
Below by specific embodiment, the present invention is carried out detailed and concrete introduction, so that being better understood from this Bright, but following embodiment is not limiting as the scope of the invention.
The baby formula milk powder of embodiment 1 preparation simulation breast milk
Including following raw material components: skimmed milk powder 18%, desalted whey powder 40%, concentrated whey protein powder 1.5%, Vegetable oil 14%, 1,3-bis-oleic acid 2-palmitic acid three ester (OPO structured lipid) 12%, lactose 11.7568%, Phosphatidase 0 .15%, calcium carbonate 0.3%, compounding mineral substance premix 0.7%, compounding vitamin premix 0.07%, Oligomeric galactose 0.8%, oligofructose 0.4%, animal bifidobacteria (Bb-12) 0.003%, Bifidobacterium lactis (Bi-07) 0.005%, docosahexenoic acid 0.03%, eicosatetraenoic acid 0.06%, choline 0.06%, Inositol 0.03%, nucleotide 0.03%, phylloxanthin 0.0002%, L-carnitine 0.01%, taurine 0.035%, L-AA sodium 0.06%.
Wherein, compounding mineral substance premix by mass percentage, including following raw material components: potassium chloride 26%, Sodium chloride 12.5%, copper sulfate 0.12%, magnesium sulfate 10.5%, ferrous sulfate 13.5%, zinc sulfate 1.78%, Manganese sulfate 0.15%, sodium selenite 0.55%, sodium citrate 14.4%, lactose 19.5%.
Compounding vitamin premix by mass percentage, including following raw material components: (dimension is raw for retinol acetate Element A) 9.8%, cholecalciferol (vitamin D3) 6.5%, dl-α-tocopheryl acetate (vitamin E) 34.5%, Phytonadione (vitamin K) 2.2%, thiamine nitrate (vitamin B1) 0.95%, (dimension is raw for riboflavin Element B2) 0.23%, pyridoxine hydrochloride (vitamin B6) 0.91%, cobalamin (vitamin B12) 2.91%, Nicotiamide 8.0%, folic acid 2.2%, D-VB5 calcium 2.7%, biotin 2.8%, potassium iodide 2.0%, lactose 24.3%.
Animal bifidobacteria (Bb-12) specification is 30IF, and Bifidobacterium lactis (Bi-07) specification is 300B, It is 1 × 10 that probiotic bacteria animal bifidobacteria (Bb-12) and Bifidobacterium lactis (Bi-07) add total amount7cfu/g。
The preparation method of the present embodiment 1, specifically includes following steps:
Step 1, one-level batch mixing: by skimmed milk powder, desalted whey powder, concentrated whey protein powder, vegetable oil, Lactose, phospholipid and calcium carbonate use the pure water mixed dissolution of 50~70 DEG C, are sufficiently stirred for;
Step 2, two grades of batch mixings: by compounding mineral substance premix, compounding vitamin premix respectively each special By 20 times amount 30~the dissolved in purified water of 40 DEG C in container, substep add step 1 to) batch mixing in fill Divide mixing, compounding mineral and compounding vitamin to add incorporation time and answer >=10min;
Step 3, homogenizing: by step 2) dissolve the material mixed and carry out homogenizing, homogenization pressure be 20~ 22Mpa;
Step 4, pre-sterilizing: by step 3) material after homogenizing carries out pre-sterilizing, sterilization temperature 80~90 DEG C, Sterilizing time 16s, cools down, keeps in, temporary temperature 8~15 DEG C, temporary storage time≤4h;
Step 5, sterilization concentrates: by step 4) temporary material sends into vaporization chamber and carries out sterilization and concentrate, sterilization Temperature 87~90 DEG C, sterilizing time 24s, an effect evaporating temperature 62~72 DEG C, two effect evaporating temperatures 46~56 DEG C, Evaporating pressure-0.086~-0.095Mpa, sterilization pressure 0.05~0.02Mpa;Discharge concentration 16.0~21.0 ° of Be;
Step 6, be dried: by step 5) concentrate after material send into drying tower through high-pressure pump, process conditions are: Inlet temperature 145~175 DEG C, temperature of outgoing air 65~92 DEG C, negative pressure (-0.5~-4.0) × 100pa in tower, fluidisation Bed negative pressure: (-0.5~-3.5) × 100pa, one section of temperature 30~85 DEG C, two-stage nitration temperature 5~55 DEG C, three sections of temperature 5~35 DEG C, four sections of temperature 5~30 DEG C, high-pressure pump pressure 15~30Mpa is spray-dried;And by stream Change bed and carry out redrying powder delivery, powder delivery temperature≤38 DEG C, moisture≤4.0%, obtain original washing powder;
Step 7, premix: by animal bifidobacteria (Bb-12), Bifidobacterium lactis (Bi-07), oligomeric half Lactose, oligofructose, docosahexenoic acid, eicosatetraenoic acid, choline, nucleotide, phylloxanthin, a left side Rotation carnitine, taurine, inositol, L-AA sodium premix respectively according to addition;
Step 8, mixing: by original washing powder and step 7) premix material mixes according to formula proportion, obtains finished powder.
Step 9, packaging, detection, warehouse-in, testing result such as table 1 below.
The baby formula milk powder of embodiment 2 preparation simulation breast milk
Including following raw material components: skimmed milk powder 29%, desalted whey powder 31%, concentrated whey protein powder 3.4%, Vegetable oil 11%, 1,3-bis-oleic acid 2-palmitic acid three ester (OPO structured lipid) 9%, lactose 14.6276%, Phosphatidase 0 .3%, calcium carbonate 0.3%, compounding mineral substance premix 0.25%, compounding vitamin premix 0.06%, Oligomeric galactose 0.8%, oligofructose 0.4%, animal bifidobacteria (Bb-12) 0.003%, breast bifid bar Bacterium (Bi-07) 0.005%, docosahexenoic acid 0.03%, eicosatetraenoic acid 0.05%, choline 0.03%, Inositol 0.03%, nucleotide 0.03%, phylloxanthin 0.0004%, L-carnitine 0.012%, taurine 0.032%, L-AA sodium 0.04%.
Wherein, compounding mineral substance premix by mass percentage, including following raw material components: potassium chloride 7.5%, Sodium chloride 10.5%, copper sulfate 0.33%, magnesium sulfate 6.5%, ferrous sulfate 41.3%, zinc sulfate 4.4%, Manganese sulfate 0.32%, sodium selenite 1.6%, sodium citrate 17.3%, lactose 10.25%.
Compounding vitamin premix by mass percentage, including following raw material components: (dimension is raw for retinol acetate Element A) 11.8%, cholecalciferol (vitamin D3) 8.4%, dl-α-tocopheryl acetate (vitamin E) 31.5%, Phytonadione (vitamin K) 2.7%, thiamine nitrate (vitamin B1) 1.4%, (dimension is raw for riboflavin Element B2) 0.15%, pyridoxine hydrochloride (vitamin B6) 1.2%, cobalamin (vitamin B12) 3.2%, cigarette Amide 8.4%, folic acid 2.2%, D-VB5 calcium 2.8%, biotin 3.3%, potassium iodide 1.5%, lactose 21.45%.
Animal bifidobacteria (Bb-12) specification is 30IF, and Bifidobacterium lactis (Bi-07) specification is 300B, It is 1 × 10 that probiotic bacteria animal bifidobacteria (Bb-12) and Bifidobacterium lactis (Bi-07) add total amount7cfu/g。
The preparation method of the present embodiment is same as in Example 1, prepares formula milk, testing result such as table 1 below institute Show.
Table 1: testing result, product nutrient composition content:
Test basis is GB10765-2010 " food security standard infant formula ", and with reference to this standard, The formula milk nutrient composition content result prepared from above-mentioned table one illustrated embodiment 1, embodiment 2, this The formula milk that inventive embodiments 1, embodiment 2 prepare all complies with the national standard requirements.
Water activity and bifidobacteria viable bacteria fungal counting:
Detection sample: embodiment 1, embodiment 2, comparative example (commercial prebiotics probiotic bacteria milk powder)
Detection method: GB/T 4789.35-2010
Testing result: such as table 2 below
Table 2 water activity and bifidobacteria viable bacteria fungal counting result
Color Bacillus bifidus number cfu/g Water activity
Embodiment 1 Milk yellow 2.30E+7 0.127Aw
Embodiment 2 Milk yellow 2.19E+7 0.108Aw
Comparative example Milk yellow 1.14E+7 0.206Aw
Research shows, compared with existing milk powder, the simulation breast milk baby formula milk powder of the present invention has higher Active bacteria number and lower low moisture activity, can better ensure that probiotic stability.
Sensory evaluation: Example 1 and Example 2 of the present invention carries out sense organ experiment, evaluation criterion is according to " China Dairy processing industry industry standard RHB 204-2004 " infant formula sense organ criticism detailed rules and regulations.
15.1 grams of milk powder of formula milk that Example 1,2 prepares respectively, add 90 milliliters of water, are configured to The milk of about 100 milliliters, energy contained under instant state is about 290kJ/100mL.It is observed that and understand this The formula milk color and luster that bright embodiment 1,2 prepares is homogeneous, in milk yellow, milk yellow light yellow, shallow, deep yellow The colors such as color, glossy;Granule is uniform, moderate, loose, good fluidity, and when being dissolved in water, sinking time is little In 10s, brew is good;Producing without agglomerate, milk has the distinctive fragrance of breast milk, and abnormal smells from the patient is natural.
Tracking of products is evaluated:
One, testing program
According to " baby formula milk powder nutrition, safe tracking evaluation scheme ", to embodiment of the present invention 1-2 system The baby formula milk powder milk powder commercialized product of the simulation breast milk obtained is paid a return visit, its trophism of tracking evaluation, peace Full property and product sensory characteristic, wherein babies ' formula milk powder, bigger babies ' formula milk powder, baby formulas milk powder return Visit number is respectively no less than 5 people.
Two, result and conclusion are paid a return visit
It is as follows that result paid a return visit by inventive formulation milk powder:
Table 3 is simulated the baby formula milk powder of breast milk and is paid a return visit result
From statistical result in table 3: during the baby formula milk powder of edible simulation breast milk, baby's height Grow normal with body weight, there is good resistance;All do not occur getting angry, constipation, allergy/eczema etc. bad Reaction, only 1 mild diarrhea paying a return visit object appearance the most once, and 1,2 days just get well, Getting rid of the impact of milk powder, therefore milk powder has good trophism and safety;The structural state of milk powder is normal, Growing abnormal smells from the patient is normal Olibanum, but has 1 return visit object the most improper, so that there is brew because reconstituting method The phenomenon of difference, therefore brew is normal, acceptance level is normal or fine, has good product sensory characteristic.
Table 4 is simulated the baby formula milk powder of breast milk and is paid a return visit result
From statistical result in table 4: during the baby formula milk powder of edible simulation breast milk, bigger baby Height and body weight are grown normal, have good resistance;All do not occur getting angry, the untoward reaction such as constipation, have Pay a return visit object mild diarrhea once in a while, pay a return visit object slight allergy once in a while, but the most quickly get well for 1 for 1, Therefore get rid of the impact of milk powder, therefore milk powder has good trophism and safety;Milk powder structural state is normal, Growing the normal Olibanum of abnormal smells from the patient, brew is normal or very well, acceptance level is fine, has good product sensory characteristic.
From statistical result in table 5: during the baby formula milk powder of edible simulation breast milk, child's height Grow normal with body weight, there is good resistance;The untoward reaction such as allergy, eczema does not all occur, has 1 Pay a return visit object and mild diarrhea occurs when turning milk, pay a return visit object for 1 and slight constipation occurs once in a while, therefore get rid of milk powder Impact, therefore milk powder has good trophism and safety;The structural state of milk powder is normal, is just growing abnormal smells from the patient Often Olibanum, brew is normal or very well, acceptance level is normal or fine, has good product sensory characteristic.
Table 5 is simulated the baby formula milk powder of breast milk and is paid a return visit result
Conclusion: in sum, the present invention simulate breast milk baby formula milk powder milk powder listing after eating condition good Good, there is good trophism, safety and product sensory characteristic.
Being described in detail the specific embodiment of the present invention above, but it is intended only as example, the present invention is also It is not restricted to particular embodiments described above.To those skilled in the art, any the present invention is carried out Equivalent modifications and substitute the most all among scope of the invention.Therefore, without departing from the spirit of the present invention and model Enclose lower made impartial conversion and amendment, all should contain within the scope of the invention.

Claims (10)

1. the baby formula milk powder simulating breast milk, it is characterised in that by weight percentage, by following former Material component is formulated: skimmed milk powder 10~40%, desalted whey powder 25~45%, concentrated whey protein powder 1.0~ 8.0%, 1,3-bis-oleic acid 2-palmitic acid three ester (OPO structured lipid) 5~20%, vegetable oil 5~20%, Lactose 5~20%, phosphatidase 0~0.5%, calcium carbonate 0.01~0.5%, compounding mineral substance premix 0.05~0.95%, Compounding vitamin premix 0.01~0.12%, oligomeric galactose 0.1~5.0%, oligofructose 0.1~5.0%, Animal bifidobacteria (Bb-12) 0~0.1%, Bifidobacterium lactis (Bi-07) 0~0.1%, two dodecahexaenes Acid 0~0.14%, eicosatetraenoic acid 0~0.18%, choline 0~0.05%, nucleotide 0~0.06%, leaf are yellow Element 0~0.0004%, L-carnitine 0.01~0.1%, taurine 0~0.07%, inositol 0.01~0.2%, L- Sodium ascorbate 0.03~0.12%;
Described compounding mineral substance premix by mass percentage, including following raw material components: potassium chloride 5~ 33%, sodium chloride 6~18%, copper sulfate 0.01~0.50%, magnesium sulfate 5~15%, ferrous sulfate 10~45%, Zinc sulfate 0.5~8.0%, manganese sulfate 0.1~1.0%, sodium selenite 0.1~5.0%, sodium citrate 10~21%, Lactose 10~25%;
Described compounding vitamin premix by mass percentage, including following raw material components: retinol acetate (dimension Raw element A) 5~18%, cholecalciferol (vitamin D3) 3~12%, dl-α-tocopheryl acetate (vitamin E) 27~40%, phytonadione (vitamin K) 0.5~5.0%, thiamine nitrate (vitamin B1) 0.5~ 4.0%, riboflavin (vitamin B2) 0.05~3.00%, pyridoxine hydrochloride (vitamin B6) 0.5~3.0%, Cobalamin (vitamin B12) 0.5~5.0%, nicotiamide 4~12%, folic acid 0.5~5.0%, D-VB5 calcium 0.5~5.0%, biotin 0.5~5.0%, potassium iodide 0.5~5.0%, lactose 15~30%;
Described animal bifidobacteria (Bb-12) specification is 30IF (30 × 108Cfu/g), Bifidobacterium lactis (Bi-07) Specification is 300B (300 × 108Cfu/g), described animal bifidobacteria (Bb-12) and Bifidobacterium lactis (Bi-07) Interpolation total amount be 0.5 × 107~3 × 107cfu/g。
The baby formula milk powder of simulation breast milk the most according to claim 1, it is characterised in that by weight hundred Proportion by subtraction meter, formulated by following raw material components: skimmed milk powder 15~35%, desalted whey powder 30~45%, Concentrated whey protein powder 1.0~5.0%, 1,3-bis-oleic acid 2-palmitic acid three ester (OPO structured lipid) 7~ 13%, vegetable oil 8~15%, lactose 8~15%, phosphatidase 0 .2~0.4%, calcium carbonate 0.1~0.35%, compounding Mineral substance premix 0.1~0.8%, compounding vitamin premix 0.05~0.10%, oligomeric galactose 0.5~ 2%, oligofructose 0.2~2%, animal bifidobacteria (Bb-12) 0.001~0.05%, Bifidobacterium lactis (Bi-07) 0.001~0.05%, docosahexenoic acid 0.01~0.1%, eicosatetraenoic acid 0.05~0.1%, choline 0.02~0.04%, nucleotide 0~0.03%, phylloxanthin 0.0001~0.0003%, L-carnitine 0~0.02%, Taurine 0.01~0.04%, inositol 0~0.1%, L-AA sodium 0.04~0.11%.
The baby formula milk powder of simulation breast milk the most according to claim 1, it is characterised in that by weight hundred Proportion by subtraction meter, formulated by following raw material components: skimmed milk powder 18%, desalted whey powder 40%, condensed whey Egg albumen powder 1.5%, vegetable oil 14%, 1,3-bis-oleic acid 2-palmitic acid three ester (OPO structured lipid) 12%, Lactose 11.7568%, phosphatidase 0 .15%, calcium carbonate 0.3%, compounding mineral substance premix 0.7%, compounding dimension are raw Element premix material 0.07%, oligomeric galactose 0.8%, oligofructose 0.4%, animal bifidobacteria (Bb-12) 0.003%, Bifidobacterium lactis (Bi-07) 0.005%, docosahexenoic acid 0.03%, eicosatetraenoic acid 0.06%, gallbladder Alkali 0.06%, inositol 0.03%, nucleotide 0.03%, phylloxanthin 0.0002%, L-carnitine 0.01%, cattle sulphur Acid 0.035%, L-AA sodium 0.06%.
The baby formula milk powder of simulation breast milk the most according to claim 1, it is characterised in that by quality hundred Proportion by subtraction meter, described compounding mineral substance premix includes following raw material components: potassium chloride 26%, sodium chloride 12.5%, Copper sulfate 0.12%, magnesium sulfate 10.5%, ferrous sulfate 13.5%, zinc sulfate 1.78%, manganese sulfate 0.15%, Sodium selenite 0.55%, sodium citrate 14.4%, lactose 19.5%.
The baby formula milk powder of simulation breast milk the most according to claim 1, it is characterised in that by quality hundred Proportion by subtraction meter, described compounding vitamin premix includes following raw material components: retinol acetate (vitamin A) 9.8%, Cholecalciferol (vitamin D3) 6.5%, dl-α-tocopheryl acetate (vitamin E) 34.5%, phytonadione (vitamin K) 2.2%, thiamine nitrate (vitamin B1) 0.95%, riboflavin (vitamin B2) 0.23%, Pyridoxine hydrochloride (vitamin B6) 0.91%, cobalamin (vitamin B12) 2.91%, nicotiamide 8.0%, Folic acid 2.2%, D-VB5 calcium 2.7%, biotin 2.8%, potassium iodide 2.0%, lactose 24.3%.
The baby formula milk powder of simulation breast milk the most according to claim 1, it is characterised in that described plant Oil mixes according to 1.2:1 ratio for mixed vegetable oil and OPO Structure grease, and wherein mixed vegetable oil is by greatly Oleum Glycines, high oleic sunflower oil, Semen Maydis oil, Petiolus Trachycarpi oil and Oleum Cocois are by weight 1:(0.5-1.2): (1-1.6): (0.3-0.8): (1.5-2.3) mixes.
The baby formula milk powder of simulation breast milk the most according to claim 1, it is characterised in that described animal It is 1 × 10 that bacillus bifidus (Bb-12) and Bifidobacterium lactis (Bi-07) add total amount7cfu/g。
8. a preparation method for the baby formula milk powder of the simulation breast milk as described in claim 1-7, its feature It is, comprises the following steps:
Step 1, one-level batch mixing: by skimmed milk powder, desalted whey powder, concentrated whey protein powder, vegetable oil, Lactose, phospholipid and calcium carbonate use the pure water mixed dissolution of 50~70 DEG C, are sufficiently stirred for;
Step 2, two grades of batch mixings: by compounding mineral substance premix, compounding vitamin premix respectively each special By 20 times amount 30~the dissolved in purified water of 40 DEG C in container, substep add step 1 to) batch mixing in fill Divide mixing, compounding mineral and compounding vitamin to add incorporation time and answer >=10min;
Step 3, homogenizing: by step 2) dissolve the material mixed and carry out homogenizing, homogenization pressure be 20~ 22Mpa;
Step 4, pre-sterilizing: by step 3) material after homogenizing carries out pre-sterilizing, sterilization temperature 80~90 DEG C, Sterilizing time 16s, cools down, keeps in, temporary temperature 8~15 DEG C, temporary storage time≤4h;
Step 5, sterilization concentrates: by step 4) temporary material sends into vaporization chamber and carries out sterilization and concentrate, sterilization Temperature 87~90 DEG C, sterilizing time 24s, an effect evaporating temperature 62~72 DEG C, two effect evaporating temperatures 46~56 DEG C, Evaporating pressure-0.086~-0.095Mpa, sterilization pressure 0.05~0.02Mpa;Discharge concentration 16.0~21.0 ° of Be;
Step 6, be dried: by step 5) concentrate after material send into drying tower through high-pressure pump, process conditions are: Inlet temperature 145~175 DEG C, temperature of outgoing air 65~92 DEG C, negative pressure (-0.5~-4.0) × 100pa in tower, fluidisation Bed negative pressure: (-0.5~-3.5) × 100pa, one section of temperature 30~85 DEG C, two-stage nitration temperature 5~55 DEG C, three sections of temperature 5~35 DEG C, four sections of temperature 5~30 DEG C, high-pressure pump pressure 15~30Mpa is spray-dried;And by stream Change bed and carry out redrying powder delivery, powder delivery temperature≤38 DEG C, moisture≤4.0%, obtain original washing powder;
Step 7, premix: by animal bifidobacteria (Bb-12), Bifidobacterium lactis (Bi-07), oligomeric half Lactose, oligofructose, docosahexenoic acid, eicosatetraenoic acid, choline, nucleotide, phylloxanthin, a left side Rotation carnitine, taurine, inositol, L-AA sodium premix respectively according to addition;
Step 8, mixing: by original washing powder and step 7) premix material mixes according to formula proportion, obtains finished powder;
Step 9, packaging, detection, warehouse-in.
The preparation method of the baby formula milk powder of simulation breast milk the most according to claim 8, it is characterised in that Described step 2) in, when dissolving compounding mineral substance premix and compounding vitamin premix, first dissolve compounding ore deposit Material premix material, after 10min, re-dissolved compounds vitamin premix.
The preparation method of the baby formula milk powder of simulation breast milk the most according to claim 8, it is characterised in that Step 7) in, described animal bifidobacteria (Bb-12), Bifidobacterium lactis (Bi-07), oligomeric galactose, Oligofructose, docosahexenoic acid, eicosatetraenoic acid, choline, nucleotide, phylloxanthin, L-carnitine, Taurine, inositol, L-AA sodium need, through expanding dilution, to expand dilution and use HS-10 tri-before premix material Dimension movement mixer, motion frequency is 35HZ, and incorporation time is 30s.
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