CN105475385A - Method for preparing Chinese-chive-maggot-preventing pesticide through biogas slurry - Google Patents

Method for preparing Chinese-chive-maggot-preventing pesticide through biogas slurry Download PDF

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CN105475385A
CN105475385A CN201610057665.5A CN201610057665A CN105475385A CN 105475385 A CN105475385 A CN 105475385A CN 201610057665 A CN201610057665 A CN 201610057665A CN 105475385 A CN105475385 A CN 105475385A
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parts
liquid
herb
natural pond
leaf
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CN105475385B (en
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甘海南
段明秀
梁立宽
张广兰
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Wuhu Spaceflight Special Cable Factory Co Ltd
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Jinan Situo Xinyuan Pharmaceutical Technology Co Ltd
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Priority to CN201810084867.8A priority patent/CN108283191B/en
Priority to CN201810084268.6A priority patent/CN108283190B/en
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/12Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/20Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/22Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F9/00Fertilisers from household or town refuse
    • C05F9/04Biological compost
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/60Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants

Abstract

The invention discloses a method for preparing Chinese-chive-maggot-preventing pesticide through biogas slurry. A flocculating agent is added into the biogas slurry passing a 200-mesh sieve, standing is performed for 5-8 h after uniform stirring, then liquid supernatant is taken, traditional Chinese medicine liquid is added into the liquid supernatant and uniformly mixed so that the pesticide can be obtained, and the volume ratio of the liquid supernatant to the traditional Chinese medicine liquid is 3:1 to 4:3. The method has the advantages that the preventing and treating method is low in cost, the biogas slurry produced from kitchen waste is utilized for solving the product disposal problem after refuse disposal, cost is low, and waste is turned into wealth; the biogas slurry serves as a source of an organic fertilizer effective for planting, nutrients needed for growth of Chinese chives are provided, the yield of Chinese chives is effectively increased, and the quality of Chinese chives is effectively improved. The pesticide is free of poison and harm to people and livestock, environmentally friendly and free of pollution, the environment is not damaged or polluted, and pesticide which is used currently and chemically synthesized in chemical engineering can be replaced. According to large-area experiment, the preventing and treating method is good in chive maggot preventing and treating effect, visual chive maggot harm is not seen, and meanwhile the yield of Chinese chives can be increased.

Description

A kind of method utilizing the agricultural chemicals of natural pond liquid preparation control fragrant-flowered garlic maggot
Technical field
The present invention relates to technical field of pesticide, particularly a kind of method utilizing the agricultural chemicals of natural pond liquid preparation control fragrant-flowered garlic maggot.
Background technology
Fragrant-flowered garlic maggot is the larva that diptera belongs to Bradysia odoriphaga.Fragrant-flowered garlic maggot foraging territories is comparatively wide, and can endanger 30 various vegetables such as Liliaceae, Chenopodiaceae, composite family, Curcurbitaceae, Cruciferae, Umbelliferae, wherein leek is injured the most serious.In the main producing region of China's leek plantation, this worm occurs comparatively general, and occurring area reaches 90%.Between Chinese chive field, attacked trees rate is generally more than 20%, causes leek production loss between 30% ~ 80%.Statistics shows, grow the leek after 2 years and reached about 80% by the probability of fragrant-flowered garlic infestation by maggots, particularly along with the increase that anti-season leek and hotbed chives produce, leek is increased year by year by the probability of fragrant-flowered garlic infestation by maggots, and some area almost reaches 100%.Fragrant-flowered garlic maggot is a kind of soil insect of stubbornness, is the crushing insect of harm leek growth.Fragrant-flowered garlic maggot larva is mainly clustered in underground, on the bulb of leek underground part, and moth food bulb and tender shoots.After leek is injured, gently then affect commodity value, heavy then cause leek bulb local or overall to rot, make the ground blade of leek thin and weak withered and yellow, wilt that it is dead even in flakes to rot, greatly compromise the interests of fragrant-flowered garlic agriculture.
The a large amount of of fragrant-flowered garlic maggot add its breeding rapidly, have had a strong impact on the economic benefit of leek.Propose root dial native Disinsection method to effect a radical cure fragrant-flowered garlic maggot, fly net and sugar-vinegar liquid trapping method, crop rotation, foundation earthing, fertilizer become thoroughly decomposed deep placement, pick the cool soil of root, ash pulls out dry, bioanalysis, but, it is large all to there is workload in these methods, efficiency is low, input cost is high, goes out except the deficiency such as less effective of fragrant-flowered garlic maggot.Kill at present fragrant-flowered garlic maggot fast and effectively method be still chemical method.The medicine of the specialty control fragrant-flowered garlic maggot of country's approved applications is main mainly with the strong phoxim (organophosphorus insecticide) of interior absorption and chlopyrifos, but the harvest time of leek is short, do not reach safety interval of pesticide pollution during leek harvesting, and fragrant-flowered garlic agriculture uses the quantity of this type of medicine and frequency also cannot be effectively controlled; While killing fragrant-flowered garlic maggot, soil is to the strong adsorptivity of agricultural chemicals, and cause its degradation speed slow, on the leek of some areas, residue of pesticide exceed standard, and are also often absorbed in body by leek.Along with using of this type of agricultural chemicals, fragrant-flowered garlic maggot is also more and more stronger to the resistance of agricultural chemicals, forces fragrant-flowered garlic agriculture go to use higher poison in violation of rules and regulations, and the agricultural chemicals such as more effective 3911,1605, form vicious circle, cause leek residue of pesticide to exceed standard.The leek after fragrant-flowered garlic maggot is killed owing to using highly toxic pesticide, its growth and development is unaffected, meanwhile, also cannot differentiate in appearance in leek, therefore, in daily life often edible this " malicious leek ", malicious leek event takes place frequently in recent years, and continuous print poison leek exposure event, causes injury severe patient even threat to life greatly to human body, make consumer " talk fragrant-flowered garlic look to become ", have a strong impact on the economic interests of vegetable grower and the food security of consumer.
The applications of pesticide have been arrived in the middle of natural environment in addition, although reach the object wanted, also bring pollution problem simultaneously.If environment and Pesticide Residues amount exceed standard, then can cause harmful effect to the mankind, other biological body and even the whole ecosystem.After agricultural chemicals enters natural ecological environment, human body can be entered by approach such as respiratory tract, digestive tract, skins.If reagent toxicity is comparatively large, just likely causes acute poisoning or subacute poisoning, even cause life danger.Although some medicament acute toxicities are little, if stable in properties, not easily decompose after using, disappear, will remain in water, air, crops, agricultural product or aquatic products, animal product, finally enter human body, cause chronic poisoning.Meanwhile, it is poisoning even dead that pesticide pollution also can cause other biological, to such an extent as to destroy the ecological balance, therefore must control the residual of agricultural chemicals and pollute, to reduce impact on human society and harm.
In addition, the output of China's changing food waste is increasing in recent years, estimates to account for more than 50% of domestic waste total amount; Its harm directly affects the appearance of the city health in city, causes insect pest, the plague of rats, even transmission; More seriously, part changing food waste is unprocessed and be processed into " waste oil " and come into the market or flow to underground plant to become feed, and the life and health of the people in serious threat.The main processing ways of changing food waste comprises both at home and abroad at present: burning, compost, landfill, Fodder making and anaerobic fermentation.People have also been invented multiple different treatment process method and apparatus.Such as application number: 201010224280.6, patent name is the integrated conduct method utilizing changing food waste gas composting.Application number: 201110339482.X, a kind of municipal organic waste combined anaerobic treatment process of patent name and equipment.Application number 201210532285.4, patent name changing food waste recycle method etc. be all disclose rubbish is carried out anaerobic fermentation after be divided into biogas, natural pond liquid and natural pond slag process application respectively.
Natural pond liquid is otherwise known as anaerobic fermented liquid, is people, animal ight soil and the liquid residue of the various organic matter such as agricultural crop straw, weeds after anaerobic fermentation.The conventional nutrients that in the liquid of natural pond, crops need has nitrogen, phosphorus, potassium, magnesium, the multiple elements such as calcium are micro-on a small quantity, active organic component has humic acid, heteroauxin, lactic acid bacteria, gibberellin, the plant hormones such as the basic element of cell division, B family vitamin has B1, B2, B5, B6, B11, B12, also containing several amino acids, protein, hydrolase and the organic molecule such as multiple inorganic acid and some antibiotic, between these compositions, mutual coordinative role is present in the liquid of natural pond with the form of available nutrient and biopesticide, can directly be absorbed and be killed harmful levels of pathogens and worm's ovum rapidly and be promoted the growth of the plant such as crops and flowers, therefore natural pond liquid is alternatively that a kind of medicine is fertile.
But these effective component contents are lower in the liquid of natural pond, concentration is generally about 10%, all the other are all water and vegetable fiber, silt, bacterium, clay, colloid, pesticide residue, suspension and the organic matter containing fishy odor of free state, as during Crop fertilizer, often consumption is large, weak effect, thus peasant is unwilling to utilize natural pond liquid to make fertilizer more.If natural pond liquid discharges, not only waste resource everywhere, and contaminated environment, if processed by sewage, cost is high, and is difficult to process.The plant such as crops and flowers directly uses this natural pond liquid, do not meet agricultural health accurate, the secondary pollution in farmland can be caused, also can cause adverse effect to growth conditions and growing environment, moreover the amount directly using this natural pond liquid is also larger, this certainly will increase cost of transportation and the labour intensity of natural pond liquid, still more in non-fertile season, natural pond liquid can not be fully used, the unnecessary unordered discharge of natural pond liquid causes pollution and the waste of environment, in order to avoid transmission and soil pollution, can use after needing to do further processing process as fertilizer.
The great attention of the leek safety in production of people is aroused in the poisoning that a large amount of excessive problem of residue of pesticide causes.Numerous agriculture practitioners also recognizes the seriousness of this type of event, also strong-willedly find environmentally friendly method, also work out the biologic product of some control fragrant-flowered garlic maggots, but due to cost higher, effect, not as reasons such as chemical pesticides, does not obtain effective propagation and employment on a large scale.
Therefore, how cheaply effectively kill fragrant-flowered garlic maggot, improve the safety of food, make the relieved edible leek of people be one of important topic of studying of those skilled in the art.And the generation of changing food waste, seriously test current environment ability to bear, Appropriate application of classifying after being processed in time by rubbish, turn waste into wealth extremely urgent.
Summary of the invention
In order to satisfied improvement fragrant-flowered garlic maggot and the demand making full use of natural pond liquid, embodiments provide a kind of method utilizing the agricultural chemicals of natural pond liquid preparation control fragrant-flowered garlic maggot.
In order to realize foregoing invention object, the invention provides a kind of method utilizing the agricultural chemicals of natural pond liquid preparation control fragrant-flowered garlic maggot, to in the natural pond liquid crossed after 200 mesh sieves, add after flocculant stirs and leave standstill 5-8h, then supernatant is got, in supernatant, add herb liquid mix and obtain agricultural chemicals, the volume ratio of described supernatant and herb liquid is 3:1-4:3.
Utilize changing food waste to carry out processing the natural pond liquid produced in prior art all can use, but the changing food waste that utilizes that natural pond liquid must take from normal gas producing more than 3 months carries out the marsh gas fermentation pool fermented.
Chinese medicine in described herb liquid comprises following raw medicinal material: humulus grass, rhizoma atractylodis, honeysuckle, kitchen garden, juglandis folia, sword brake herb, swallow tail, cannalike dona rhizome and pinkflower ecdysanthera root and leaf.
In described herb liquid, the mass parts of each raw medicinal material is: humulus grass 15-20 part, rhizoma atractylodis 5-10 part, honeysuckle 20-26 part, kitchen garden 13-18 part, juglandis folia 5-12 part, sword brake herb 3-8 part, swallow tail 12-21 part, cannalike dona rhizome 7-14 part and pinkflower ecdysanthera root and leaf 12-16 part.
In described herb liquid, the mass parts of each raw medicinal material is: humulus grass 15 parts, rhizoma atractylodis 8 parts, honeysuckle 26 parts, kitchen garden 18 parts, juglandis folia 11 parts, sword brake herb 3 parts, 16 parts, swallow tail, cannalike dona rhizome 14 parts and pinkflower ecdysanthera root and leaf 12 parts.
In described herb liquid, the mass parts of each raw medicinal material is: humulus grass 18 parts, rhizoma atractylodis 10 parts, honeysuckle 23 parts, kitchen garden 15 parts, juglandis folia 5 parts, sword brake herb 6 parts, 21 parts, swallow tail, cannalike dona rhizome 7 parts and pinkflower ecdysanthera root and leaf 14 parts.
In described herb liquid, the mass parts of each raw medicinal material is: humulus grass 20 parts, rhizoma atractylodis 5 parts, honeysuckle 20 parts, kitchen garden 13 parts, juglandis folia 12 parts, sword brake herb 8 parts, 12 parts, swallow tail, cannalike dona rhizome 10 parts and pinkflower ecdysanthera root and leaf 16 parts.
The changing food waste that utilizes that described natural pond liquid takes from normal gas producing more than 3 months carries out the fermentation vat fermented.
Described flocculant is aluminium polychloride and polyacrylamide, and aluminium polychloride addition in the liquid of natural pond is 3.2-3.3g/L, and polyacrylamide addition in the liquid of natural pond is 0.01-0.015g/L.
The preparation method of described herb liquid comprises the following steps: the first step, humulus grass, swallow tail, rhizoma atractylodis and honeysuckle are mixed to get mixture one in proportion, be that the ethanol of 70% ~ 80% is as solvent with determining alcohol, adopt percolation with the speed of 0.3-0.8ml per minute slowly diacolation, collect percolate, reduced pressure concentration is also dry, obtains and gets dry extract, be ground into powder one, the quality of the ethanol added is 3 ~ 5 times of mixture one quality;
Second step, mixes in proportion by kitchen garden, juglandis folia, sword brake herb, cannalike dona rhizome and pinkflower ecdysanthera root and leaf, obtains mixture two, adds the distilled water relative to mixture two quality 9 ~ 10 times, decocts 2 ~ 4 hours, filters, obtains the first filtered fluid; Filter residue is added the distilled water relative to filter residue quality 3 ~ 5 times, decoct 1 ~ 2 hour, filter, obtain the second filtered fluid; Merge the first filtered fluid and the second filtered fluid, reduced pressure concentration, dry, obtain and get dry extract, be ground into powder two;
3rd step, powder two mixing that the powder one first step obtained and second step obtain, add the honey of the distilled water relative to mixed-powder quality 3 ~ 5 times amount, 0.5 ~ 0.8 times amount, stir acquisition herb liquid.
The preparation method of described herb liquid comprises the following steps:
Step one: by described raw medicinal material, mixes in described ratio, adds appropriate water, and water consumption is 6-10 times of raw material gross weight, soaks 1-2 hour;
Step 2: first for soaked raw medicinal material intense fire is fried open, fire of larding speech with literary allusions is continuous to be decocted, decoct after 1-2 hour, filter to get filtrate one and filter residue, described filter residue weight 3-4 water is doubly added in filter residue, decoct after 0.5-1 hour, cross leaching filtrate and obtain filtrate two, filtrate one and filtrate two are mixed and is herb liquid of the present invention.
The beneficial effect that the technical scheme that the embodiment of the present invention provides is brought is:
The prevention and controls natural pond liquid utilizing changing food waste to produce with low cost solves the process problem of product after garbage disposal, with low cost, turn waste into wealth.Natural pond liquid plants effective organic manure source as leek, and the nutrient needed for the growth of supply leek, effectively raises leek yield and quality.Nontoxic to people and animals, environmental protection is pollution-free, to the broken ring of the Nature, free from environmental pollution, can replace the chemistry of domestic current use, chemical industry synthetic pesticide.Raw material sources of the present invention are extensive, and manufacture craft is simple, and energy consumption is little, and preparation cost is cheap.Leek without any residue of pesticide, the edible safety Resolving probiems of leek.
Control efficiency is stablized, and this prevention and controls is tested through large area, after using the method, prove that the control efficiency of fragrant-flowered garlic maggot is better, existing not visible fragrant-flowered garlic maggot harm, can increase the output of leek simultaneously, all can use in each period of farming growth, meet application by peasants custom, without the need to safety interval.
Embodiment
Bad for current agricultural chemicals improvement fragrant-flowered garlic maggot effect, residue of pesticide are high, the problem that cost is high, the invention provides a kind of method utilizing the agricultural chemicals of natural pond liquid preparation control fragrant-flowered garlic maggot.
In agricultural chemicals, the pharmacology of each Chinese medicine material medicinal material is as follows:
Humulus grass: another name is uprooted plants after their edible portions have been harvested, draws rattan, cairo morningglory root or leaf, le grass, great Ye cairo morningglory root or leaf, draws dog egg, cut people rattan.The herb of source Moraceae humulus plants humulus grass.Nature and flavor are sweet, bitter, cold.Clearing heat and detoxicating, inducing diuresis to reduce edema.For pulmonary tuberculosis hectic fever, enterogastritis, dysentery, cold, fever, difficult urination, pyelonephritis, acute nephritis, cystitis, stone in urinary system; Carbuncle furuncle poison is controlled in external application, eczema, venomous snake bite.
Rhizoma atractylodis: call red art (Tao Hongjing), horse Ji (" saying that literary composition system passes "), blue or green art (ceremonial dress for royalty " water south writing brush note "), magic arts (" detailed outline ").For the rhizome of feverfew RHIZOMA ATRACTYLODIS IANCEAE or Atractylis chinensis etc.Return spleen, stomach warp.Function cures mainly invigorating the spleen, eliminating dampness, Xie Yu, wards off dirty.Controlling and wet containing tired spleen, burnout addicted to sleeping, gastral cavity ruffian abdominal distension, poor appetite, vomiting, has loose bowels, dysentery, malaria, phlegm and retained fluid, oedema, time gas flu, wind-cold-dampness arthralgia, sufficient impotence, yctalopia.
Honeysuckle: sweet, cold.Return lung, the heart, stomach warp.Clearing heat and detoxicating, wind-heat dissipating.To swell furunculosis for carbuncle, larynx numbness, erysipelas, toxic-heat and blood stasis, anemopyretic cold, warm disease is generated heat.
Kitchen garden: acid, cold.Clearing heat and promoting diuresis, removing pattogenic heat from the blood and toxic material from the body.For bacillary dysentery, acute gastroenteritis, acute appendicitis, mastitis, hemorrhoid hemorrhage, leukorrhea; Furuncle swelling toxin is controlled in external application, eczema, herpes zoster.
Juglandis folia: medicinal material Ji Yuan: be the leaf of juglandaceae plant English walnut.Bitter; Puckery; Property is put down.Convergence is band only; Desinsection is subsided a swelling.Housewife female leukorrhea; Mange; Elephantiasis crus.
Sword brake herb: another name FENGHUACAO (" the sward property of medicine standby want "), phoenix-tail fern (" south of the Five Ridges gather medicinal herbs record "), trident grass (" Guangzhou flora "), little Feng Wei, Uncinata Spikemoss Herb (" south of the Five Ridges herbal "), Shan Fengwei, well limit madder (" Guangdong Chinese medicine ").For the herb of Pteridaceae plant Pteris ensiformis.Lightly seasoned micro-hardship, cold in nature.Heat-clearing, dampness removing, cool blood, removing toxic substances.Control dysentery, malaria, jaundice, gonorrhoea, lower blood, metrorrhagia, traumatic injury, tonsillitis, parotitis, sore, eczema.
Swallow tail: another name slice leaf, mouse bell.Passifloraceae swallow tail, with all herbal medicine.Bitter, micro-sweet, temperature.Invigorating the lung and benefiting vital QI, anti-inflammatory, sterilization.Cure mainly dysentery, pulmonary tuberculosis, bronchitis.Drop into manure pit sump and kill maggot, wriggler.
Cannalike dona rhizome: another name dagger-axe swallow [Dai Nationality's name].Marantaceae cannalike dona rhizome ,be used as medicine with block root or stem.Light, cool.Clearing heat and detoxicating, relieving cough and relieving asthma, anti-inflammation and sterilization.Cure mainly pulmonary tuberculosis, tracheitis, bronchitis, asthma, high heat, children's measles, merges pneumonia, flu, heating, various skin disease.
Pinkflower ecdysanthera root and leaf: another name head woods oozes (" Guangzhou flora "), common embelia root branchlet and leaf (" Luchuan book on Chinese herbal medicine "), Caulis Fissistigmae, the wind certain kind of berries, sour rattan (" Guangxi Chinese medicinal herbal ").For root and the leaf of apocynaceae plant acid leaf glue rattan.Acid; Property is put down.Return Liver Channel.Clearing heat and detoxicating; Dampness removingization is stagnant; Activating blood circulation and reducing swelling.Main abscess of throat; Stomatitis; Enteritis; Chronic nephritis; Food stagflation is full; Carbuncle sore tumefacting virus; Arthralgia due to wind-dampness; Treating swelling and pain by traumatic injury.
PB1 gene: purchased from Zhen Yu water-purifying material factory of Gongyi City, yellow powdery solid, Al2O3 mass fraction is about 30%.
Polyacrylamide PAM: purchased from traditional Chinese medicines group, relative molecular mass >300 ten thousand, active ingredient >85%.
Below adopt embodiment to describe embodiments of the present invention in detail, to the present invention, how application technology means solve technical problem whereby, and the implementation procedure reaching technique effect can fully understand and implement according to this.
Embodiment 1
A kind of method utilizing the agricultural chemicals of natural pond liquid preparation control fragrant-flowered garlic maggot, to in the natural pond liquid crossed after 200 mesh sieves, add after flocculant stirs and leave standstill 5h, then get supernatant, in supernatant, add herb liquid mix and obtain agricultural chemicals, the volume ratio of described supernatant and herb liquid is 2:1.
In herb liquid, the quality of each raw medicinal material is: humulus grass 15kg, rhizoma atractylodis 8kg, honeysuckle 26kg, kitchen garden 18kg, juglandis folia 11kg, sword brake herb 3kg, swallow tail 16kg, cannalike dona rhizome 14kg and pinkflower ecdysanthera root and leaf 12kg.
The changing food waste that utilizes that natural pond liquid takes from Chongqing City's black stone changing food waste treatment plant normal gas producing more than 3 months carries out the fermentation vat fermented.
Flocculant is aluminium polychloride and polyacrylamide, and aluminium polychloride addition in the liquid of natural pond is 3.2g/L, and polyacrylamide addition in the liquid of natural pond is 0.012g/L.
The preparation method of herb liquid comprises the following steps: the first step, humulus grass, swallow tail, rhizoma atractylodis and honeysuckle are mixed to get mixture one in proportion, be that the ethanol of 70% is as solvent with determining alcohol, adopt percolation with the speed of 0.8ml per minute slowly diacolation, collect percolate, reduced pressure concentration is also dry, obtains and gets dry extract, be ground into powder one, the quality of the ethanol added is 5 times of mixture one quality;
Second step, mixes in proportion by kitchen garden, juglandis folia, sword brake herb, cannalike dona rhizome and pinkflower ecdysanthera root and leaf, obtains mixture two, adds the distilled water relative to mixture two quality 10 times, decocts 2 hours, filters, obtains the first filtered fluid; Filter residue is added the distilled water relative to filter residue quality 5 times, decoct 2 hours, filter, obtain the second filtered fluid; Merge the first filtered fluid and the second filtered fluid, reduced pressure concentration, dry, obtain and get dry extract, be ground into powder two;
3rd step, powder two mixing that the powder one first step obtained and second step obtain, add the honey of the distilled water relative to mixed-powder quality 3 times amount, 0.5 times amount, stir acquisition herb liquid.
Embodiment 2
A kind of method utilizing the agricultural chemicals of natural pond liquid preparation control fragrant-flowered garlic maggot, to in the natural pond liquid crossed after 200 mesh sieves, add after flocculant stirs and leave standstill 6h, then get supernatant, in supernatant, add herb liquid mix and obtain agricultural chemicals, the volume ratio of described supernatant and herb liquid is 4:3.
In herb liquid, the quality of each raw medicinal material is: humulus grass 18kg, rhizoma atractylodis 10kg, honeysuckle 23kg, kitchen garden 15kg, juglandis folia 5kg, sword brake herb 6kg, swallow tail 21kg, cannalike dona rhizome 7kg and pinkflower ecdysanthera root and leaf 14kg.
The changing food waste that utilizes that natural pond liquid takes from Chongqing City's black stone changing food waste treatment plant normal gas producing more than 3 months carries out the fermentation vat fermented.
Flocculant is aluminium polychloride and polyacrylamide, and aluminium polychloride addition in the liquid of natural pond is 3.3g/L, and polyacrylamide addition in the liquid of natural pond is 0.015g/L.
The preparation method of described herb liquid comprises the following steps: the first step, humulus grass, swallow tail, rhizoma atractylodis and honeysuckle are mixed to get mixture one in proportion, be that the ethanol of 80% is as solvent with determining alcohol, adopt percolation with the speed of 0.3ml per minute slowly diacolation, collect percolate, reduced pressure concentration is also dry, obtains and gets dry extract, be ground into powder one, the quality of the ethanol added is 3 times of mixture one quality;
Second step, mixes in proportion by kitchen garden, juglandis folia, sword brake herb, cannalike dona rhizome and pinkflower ecdysanthera root and leaf, obtains mixture two, adds the distilled water relative to mixture two quality 9 times, decocts 4 hours, filters, obtains the first filtered fluid; Filter residue is added the distilled water relative to filter residue quality 3 times, decoct 1 hour, filter, obtain the second filtered fluid; Merge the first filtered fluid and the second filtered fluid, reduced pressure concentration, dry, obtain and get dry extract, be ground into powder two;
3rd step, powder two mixing that the powder one first step obtained and second step obtain, add the distilled water relative to mixed-powder quality 5 times amount, the honey of 0.8 times, stir acquisition herb liquid.
Embodiment 3
A kind of method utilizing the agricultural chemicals of natural pond liquid preparation control fragrant-flowered garlic maggot, to in the natural pond liquid crossed after 200 mesh sieves, add after flocculant stirs and leave standstill 8h, then get supernatant, in supernatant, add herb liquid mix and obtain agricultural chemicals, the volume ratio of described supernatant and herb liquid is 3:1.
In herb liquid, the quality of each raw medicinal material is: humulus grass 20kg, rhizoma atractylodis 5kg, honeysuckle 20kg, kitchen garden 13kg, juglandis folia 12kg, sword brake herb 8kg, swallow tail 12kg, cannalike dona rhizome 10kg and pinkflower ecdysanthera root and leaf 16kg.
The changing food waste that utilizes that natural pond liquid takes from Chongqing City's black stone changing food waste treatment plant normal gas producing more than 3 months carries out the fermentation vat fermented.
PAMC addition in the liquid of natural pond is 0.1% of natural pond liquid quality.
Described flocculant is aluminium polychloride and polyacrylamide, and aluminium polychloride addition in the liquid of natural pond is 3.2g/L, and polyacrylamide addition in the liquid of natural pond is 0.01g/L.
The preparation method of herb liquid comprises the following steps: step one: by described raw medicinal material, mixes in described ratio, adds appropriate water, and water consumption is 8 times of raw material gross weight, soaks 2 hours;
Step 2: first for soaked raw medicinal material intense fire is fried open, fire of larding speech with literary allusions is continuous to be decocted, decoct after 1 hour, filter to get filtrate one and filter residue, the water of described filter residue weight 3 times is added in filter residue, decoct after 1 hour, cross leaching filtrate and obtain filtrate two, filtrate one and filtrate two are mixed and is herb liquid of the present invention.
1, test method
At Qingdao Vegetable Base, test leek kind is that the only son and heir is red, and test She20Ge community, 5 process, each process 4 repetition, each small plot experiment ground area is 0.5 mu.
In 5 process, 1-3 process is respectively the agricultural chemicals using embodiment 1-3 to prepare,
Wherein processing 4 is that control group 1 directly adopts natural pond liquid process;
Process 5 is blank group 2, and blank need not any method process;
Pouring mode is along root pouring.
2, investigation content
Strain rate of being injured is investigated: with each 10 piers of center of housing estate 2 row, statistics healthy tree and strain number (yellow, soft with blade tip, lodging is as the criterion) of being injured.Before dispenser and after dispenser 5,12,20,30d respectively investigates 1 time, investigate 5 times altogether.
Insect population radix is investigated: the insect population radix of random searching check plot before dispenser.
Survival insect population investigation: the last heart in the cell of investigating for 1 time digs 5 pier leek, statistics bulb inside and outside survival maggot number.Record insect population number, calculates Revision insect recluced rate.
Attacked trees rate (%)=total strain number of strain number × 100/ investigation of being injured;
Control efficiency (%)=(check plot be injured strain rate-treatment region be injured strain rate) × 100/ check plot is injured strain rate;
Insect population control efficiency (%)=(check plot borer population-treatment region alive borer population alive) × 100/ check plot borer population alive;
Each process control fragrant-flowered garlic maggot field control effectiveness test result is see table 1, and after each embodiment uses, the per mu yield (kg) of leek is see table 2
Each process control fragrant-flowered garlic maggot field control effectiveness test result of table 1
Each embodiment of table 2 uses the output (kg) of rear 1 mu of leek
1st batch of non-medication 2nd batch 3rd batch 4th batch
Embodiment 1 1286 2720 2708 2695
Embodiment 2 1279 2746 2723 2678
Embodiment 3 1320 2802 2759 2714
Control group 1 1295 1856 1947 1854
Control group 2 1335 1267 1204 1092
Can be found out by above-mentioned data, prevent and treat fragrant-flowered garlic maggot effect clearly, and leek plant strain growth be vigorous, significantly increases production.Use the treatment effect after agricultural chemicals of the present invention all clearly, the control group process insect population control efficiency wherein only using natural pond liquid reaches 88.69%.But fragrant-flowered garlic maggot effect highly significant administered by embodiment 1 agricultural chemicals, even can kill fragrant-flowered garlic maggot completely.
After applying pesticides, the per mu yield of leek is than obviously increasing production by the per mu yield of fragrant-flowered garlic maggot evil before, and volume increase reaches more than 100%, than the leek per mu yield volume increase more than 40% of only using natural pond liquid.The synergy of visible agricultural chemicals of the present invention obviously strengthens.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, within the spirit and principles in the present invention all, any amendment done, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.

Claims (10)

1. one kind utilizes the method for the agricultural chemicals of natural pond liquid preparation control fragrant-flowered garlic maggot, it is characterized in that, to in the natural pond liquid crossed after 200 mesh sieves, add after flocculant stirs and leave standstill 5-8h, then supernatant is got, in supernatant, add herb liquid mix and obtain agricultural chemicals, the volume ratio of described supernatant and herb liquid is 3:1-4:3.
2. method according to claim 1, is characterized in that, the Chinese medicine in described herb liquid comprises following raw medicinal material: humulus grass, rhizoma atractylodis, honeysuckle, kitchen garden, juglandis folia, sword brake herb, swallow tail, cannalike dona rhizome and pinkflower ecdysanthera root and leaf.
3. method according to claim 1 and 2, it is characterized in that, in described herb liquid, the mass parts of each raw medicinal material is: humulus grass 15-20 part, rhizoma atractylodis 5-10 part, honeysuckle 20-26 part, kitchen garden 13-18 part, juglandis folia 5-12 part, sword brake herb 3-8 part, swallow tail 12-21 part, cannalike dona rhizome 7-14 part and pinkflower ecdysanthera root and leaf 12-16 part.
4. according to the arbitrary described method of claim 1-3, it is characterized in that, in described herb liquid, the mass parts of each raw medicinal material is: humulus grass 15 parts, rhizoma atractylodis 8 parts, honeysuckle 26 parts, kitchen garden 18 parts, juglandis folia 11 parts, sword brake herb 3 parts, 16 parts, swallow tail, cannalike dona rhizome 14 parts and pinkflower ecdysanthera root and leaf 12 parts.
5. according to the arbitrary described method of claim 1-3, it is characterized in that, in described herb liquid, the mass parts of each raw medicinal material is: humulus grass 18 parts, rhizoma atractylodis 10 parts, honeysuckle 23 parts, kitchen garden 15 parts, juglandis folia 5 parts, sword brake herb 6 parts, 21 parts, swallow tail, cannalike dona rhizome 7 parts and pinkflower ecdysanthera root and leaf 14 parts.
6. according to the arbitrary described method of claim 1-3, it is characterized in that, in described herb liquid, the mass parts of each raw medicinal material is: humulus grass 20 parts, rhizoma atractylodis 5 parts, honeysuckle 20 parts, kitchen garden 13 parts, juglandis folia 12 parts, sword brake herb 8 parts, 12 parts, swallow tail, cannalike dona rhizome 10 parts and pinkflower ecdysanthera root and leaf 16 parts.
7., according to the arbitrary described method of claim 1-6, it is characterized in that, described natural pond liquid takes from the fermentation vat of normal gas producing more than 3 months.
8., according to the arbitrary described method of claim 1-7, it is characterized in that, described flocculant is aluminium polychloride and polyacrylamide, and aluminium polychloride addition in the liquid of natural pond is 3.2-3.3g/L, and polyacrylamide addition in the liquid of natural pond is 0.01-0.015g/L.
9. according to the arbitrary described method of claim 1-8, it is characterized in that, the preparation method of described herb liquid comprises the following steps: the first step, and humulus grass, swallow tail, rhizoma atractylodis and honeysuckle are mixed to get mixture one in proportion, is that the ethanol of 70% ~ 80% is as solvent with determining alcohol, adopt percolation with the speed of 0.3-0.8ml per minute slowly diacolation, collect percolate, reduced pressure concentration is also dry, obtains and gets dry extract, be ground into powder one, the quality of the ethanol added is 3 ~ 5 times of mixture one quality;
Second step, mixes in proportion by kitchen garden, juglandis folia, sword brake herb, cannalike dona rhizome and pinkflower ecdysanthera root and leaf, obtains mixture two, adds the distilled water relative to mixture two quality 9 ~ 10 times, decocts 2 ~ 4 hours, filters, obtains the first filtered fluid; Filter residue is added the distilled water relative to filter residue quality 3 ~ 5 times, decoct 1 ~ 2 hour, filter, obtain the second filtered fluid; Merge the first filtered fluid and the second filtered fluid, reduced pressure concentration, dry, obtain and get dry extract, be ground into powder two;
3rd step, powder two mixing that the powder one first step obtained and second step obtain, add the honey of the distilled water relative to mixed-powder quality 3 ~ 5 times amount, 0.5 ~ 0.8 times amount, stir acquisition herb liquid.
10., according to the arbitrary described method of claim 1-8, it is characterized in that, the preparation method of described herb liquid comprises the following steps:
Step one: by described raw medicinal material, mixes in described ratio, adds appropriate water, and water consumption is 6-10 times of raw material gross weight, soaks 1-2 hour;
Step 2: first for soaked raw medicinal material intense fire is fried open, fire of larding speech with literary allusions is continuous to be decocted, decoct after 1-2 hour, filter to get filtrate one and filter residue, described filter residue weight 3-4 water is doubly added in filter residue, decoct after 0.5-1 hour, cross leaching filtrate and obtain filtrate two, filtrate one and filtrate two are mixed and is herb liquid of the present invention.
CN201610057665.5A 2016-01-28 2016-01-28 A method of preparing the pesticide of prevention bradysia odoriphaga using biogas slurry Expired - Fee Related CN105475385B (en)

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