CN105353064B - 辛酰氯的气相色谱检测方法 - Google Patents
辛酰氯的气相色谱检测方法 Download PDFInfo
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- CN105353064B CN105353064B CN201510924481.XA CN201510924481A CN105353064B CN 105353064 B CN105353064 B CN 105353064B CN 201510924481 A CN201510924481 A CN 201510924481A CN 105353064 B CN105353064 B CN 105353064B
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/86—Signal analysis
- G01N30/8603—Signal analysis with integration or differentiation
- G01N30/8606—Integration
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
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Abstract
Description
峰编号 | 保留时间 | 峰面积 | 百分比含量 |
1 | 6.293 | 53556 | 0.0137 |
2 | 7.777 | 391296454 | 99.7888 |
3 | 7.893 | 603945 | 0.1540 |
4 | 8.107 | 66913 | 0.0171 |
5 | 8.353 | 82290 | 0.0210 |
6 | 8.710 | 21424 | 0.0055 |
峰编号 | 保留时间 | 峰面积 | 百分比含量 |
1 | 6.287 | 54170 | 0.0140 |
2 | 7.770 | 386078189 | 99.7484 |
3 | 7.887 | 401660 | 0.1038 |
4 | 8.100 | 412067 | 0.1065 |
5 | 8.347 | 84790 | 0.0219 |
6 | 8.703 | 21066 | 0.0054 |
名称 | 第一次检测值 | 第二次检测值 | 平均值 |
工业生产辛酰氯 | 99.7888 | 99.7484 | 99.7686 |
Claims (4)
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CN105353064A CN105353064A (zh) | 2016-02-24 |
CN105353064B true CN105353064B (zh) | 2017-03-22 |
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Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN107422056B (zh) * | 2017-08-17 | 2020-04-24 | 山东裕欣药业有限公司 | 一种特戊酸碘甲酯的气相色谱检测方法及其制备方法 |
CN111929369A (zh) * | 2019-05-13 | 2020-11-13 | 定远县云森科技有限公司 | 一种气相色谱法测定高压硫化异丁烯中硫含量的方法 |
CN110441446B (zh) * | 2019-09-06 | 2022-06-10 | 湖南新领航检测技术有限公司 | 一种有效检测2-氯丙酰氯纯度的方法 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101774908A (zh) * | 2010-02-06 | 2010-07-14 | 山东神工化工集团股份有限公司峄兴分公司 | 一种生产间氯苯甲酰氯的方法 |
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- 2015-12-14 CN CN201510924481.XA patent/CN105353064B/zh active Active
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN101774908A (zh) * | 2010-02-06 | 2010-07-14 | 山东神工化工集团股份有限公司峄兴分公司 | 一种生产间氯苯甲酰氯的方法 |
Non-Patent Citations (4)
Title |
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4-乙基辛酸及其同系物的合成与其应用研究;刘玉平;《中国博士学位论文全文数据库(工程科技Ⅰ辑)》;20120315(第03期);第18-19页 * |
ANALYSIS OF THE LIQUID FRACTION AFTER ESTERIFICATION OF SAWDUST WITH OCTANOYL CHLORIDE-PRODUCTION OF ESTERIFIED HEMICELLULOSES;S. Thiebaud et al;《Bioresource Technology》;19980228;第63卷(第2期);第139-145页 * |
气相色谱法分析氯乙酰氯;沈波 等;《浙江化工》;19971231;第28卷(第3期);第48-49页 * |
氯乙酰氯的气相色谱分析;刘文 等;《山东化工》;19981231(第5期);第B016-1页 * |
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