CN105296191A - Efficient decontaminating and color-protecting laundry detergent and preparation method therefor - Google Patents
Efficient decontaminating and color-protecting laundry detergent and preparation method therefor Download PDFInfo
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- CN105296191A CN105296191A CN201510810209.9A CN201510810209A CN105296191A CN 105296191 A CN105296191 A CN 105296191A CN 201510810209 A CN201510810209 A CN 201510810209A CN 105296191 A CN105296191 A CN 105296191A
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Abstract
The present invention relates to an efficient decontaminating and color-protecting laundry detergent and a preparation method therefor. The invention belongs to the field of detergents, particularly the efficient decontaminating and color-protecting laundry detergent and the preparation method therefor. The present invention aims to solve the problem that a good color-protecting effect cannot be achieved as a result of poor decontamination capability of the marketed laundry detergent and clothes which are washed by many times are dark in color and grow old. The efficient decontaminating and color-protecting laundry detergent provided by the invention comprises a liquid A and a liquid B, wherein the liquid B and liquid A can be used in a volume ratio of 1:(1-3). The efficient decontaminating and color-protecting laundry detergent provided by the invention is strong in decontamination capability and mild and stimulation-free and has a better color-protecting effect. The efficient decontaminating and color-protecting laundry detergent provided by the invention is used for washing household clothes.
Description
Technical field
The invention belongs to detergent applications, particularly relate to a kind of high-effective cleansing and protect look washing liquid and preparation method thereof field.
Background technology
Along with the expansion of social scope, the emphasis of people to look improves constantly, especially dressing aspect.And washing liquid soil removability is on the market poor, good effect of color protection can not be reached, wash rear easily causing and send out wrinkle, send out old, and the fabric scope of protecting look washing liquid applicable be little.
Summary of the invention
The washing liquid soil removability that the object of the invention is to solve on the market is poor, good effect of color protection can not be reached and repeatedly easily cause the problem being faint in color and sending out old after washing, providing a kind of high-effective cleansing and the washing liquid protecting look and preparation method thereof by the new concept of " decontamination-protect look-dyeing-protect look further ".
High-effective cleansing of the present invention and protect look washing liquid and comprise A liquid and B liquid;
Described A liquid is decontamination colour protecting liquid, it consists of the following composition by weight percentage: fatty alcohol-polyoxyethylene ether (3) sodium sulfate 10% ~ 20%, methyl sodiosul foaliphatate 1% ~ 10%, lauric acid amide of ethanol 5% ~ 10%, alkyl glycoside 1% ~ 5%, polyvinylpyrrolidone 0.1% ~ 5%, propylene glycol 1% ~ 6%, Trisodium Citrate 1% ~ 4%, sodium xylene sulfonate 1% ~ 3%, defoamer AFE-31680.1% ~ 0.3%, fluorescent brightener CBS-X0.01% ~ 0.1%, sodium-chlor 1% ~ 3%, Kathon CG 0.1% ~ 0.5%, the deionized water of spices 0.1% ~ 0.5% and surplus,
Described B liquid is dyeing colour protecting liquid, and it consists of the following composition by weight percentage: the deionized water of dyestuff 10% ~ 20%, dye leveller 1% ~ 5%, wetting agent 1% ~ 5%, sodium-chlor 1% ~ 5%, spices 0.1% ~ 0.5% and surplus.
Polyvinylpyrrolidone in described A liquid is colour protecting agent, sticks on clothing after washing, and can play good colour fixation for follow-up B liquid dyeing;
Dye leveller in described B liquid is fatty alcohol-polyoxyethylene ether.
Sodium-chlor in described B liquid generation ion soluble in water, is combined with the coloring matter of dress material and produces comparatively stable material, be not easily hydrolyzed, become good laking agent.
Dyestuff in described B liquid is bright red, grass green, dark blue, reddish brown, black, and coffee is dark blue, military green, blue, orange, blackish green, dark-grey or royal purple.
Described B liquid dyeing colour protecting liquid adds different spices, is used for eliminating the pungency taste of staining fluid.
Above-mentioned high-effective cleansing is prepared according to the following steps with the preparation method protecting look washing liquid:
The preparation method of A liquid is prepared according to the following steps:
One, get 3g ~ 6g propylene glycol to join in 12g ~ 16g fatty alcohol-polyoxyethylene ether (3) sodium sulfate, stir to obtain mixed solution;
Two, in container, add 40g ~ 100g deionized water and be warmed up to 50 DEG C ~ 70 DEG C, the mixed solution that step one is obtained is added again successively in container, methyl sodiosul foaliphatate 3g ~ 5g, lauric acid amide of ethanol 7g ~ 10g, alkyl glycoside 1g ~ 3g and polyvinylpyrrolidone 2g ~ 4g, stirring reaction 20min ~ 40min, adding citric acid sodium 3g ~ 5g afterwards, stirs 10min ~ 20min;
Three, temperature of reaction is down to 40 DEG C ~ 45 DEG C, in container, adds sodium xylene sulfonate 1.0g ~ 2.0g, fluorescent brightener CBS-X0.01g ~ 0.1g and defoamer AFE-31680.1g ~ 0.2g successively, stir 10min ~ 20min; Add sodium-chlor 1g ~ 3g again, stir 10min ~ 20min; Then adjust pH with citric acid, make pH=7 ~ 8;
Four, temperature of reaction is down to 30 DEG C ~ 35 DEG C, adds 0.1g ~ 0.5g Kathon CG and 0.1g ~ 0.5g spices stirs 10min ~ 30min again, obtained solution is A liquid;
The preparation method of B liquid is prepared according to the following steps:
In container, add 40g ~ 100g deionized water be warming up to 30 DEG C ~ 35 DEG C, add 10g ~ 20g dyestuff, 2g ~ 4g dye leveller and 2g ~ 4g wetting agent successively and stir 10min ~ 30min, add 2g ~ 4g sodium-chlor and 0.1g ~ 0.5g spices stirring 10min ~ 30min again, obtained solution is B liquid;
A liquid of the present invention is applicable to various fabric.Add different dyestuffs in B liquid of the present invention and be applicable to different colours and the clothing easily faded.In washing liquid of the present invention, A liquid separates with B liquid and uses, and during use, first gets appropriate A liquid washing clothes of the present invention, then adds B immersion bubble clothing, and after rinsing airing, clothes recovers vivid color.The volume ratio of wherein said B liquid and A liquid is 1:(1 ~ 3).
The present invention is relative to its advantage of prior art:
1. washing liquid decontamination index carbon black R (ratio) that the preparation method utilizing decontamination of the present invention to protect look washing liquid obtains is 1.18 and 1.21, albumen R (ratio) 2.82 and 2.63, sebum R (ratio) 1.21 and 1.24, and ordinary liquid laundry detergent decontamination index is respectively carbon black R (ratio) 1.07, albumen R (ratio) 1.14, sebum R (ratio) 1.12.Washing liquid soil removability of the present invention is stronger by contrast.
2. high-effective cleansing of the present invention and to protect look washing liquid soil removability strong, effect of color protection is good, gentle non-stimulated, easily degrades, and the polyvinylpyrrolidone in A liquid makes B liquid dye firmly, thus makes clothing recover bright and new glossy, reaches better effect of color protection.
3. the present invention adopts the new concept of " decontamination-protect look-dyeing-protect look further ", and obtain Liquid laundry composition AB liquid, its cheaper starting materials is easy to get, and cost is reduced greatly.
Embodiment
Technical solution of the present invention is not limited to following cited embodiment, also comprises the arbitrary combination between each embodiment.
Embodiment one: the high-effective cleansing of present embodiment and protect look washing liquid, is characterized in that: described high-effective cleansing and protect look washing liquid and comprise A liquid and B liquid;
Described A liquid is decontamination colour protecting liquid, it consists of the following composition by weight percentage: fatty alcohol-polyoxyethylene ether (3) sodium sulfate 10% ~ 20%, methyl sodiosul foaliphatate 1% ~ 10%, lauric acid amide of ethanol 5% ~ 10%, alkyl glycoside 1% ~ 5%, polyvinylpyrrolidone 0.1% ~ 5%, propylene glycol 1% ~ 6%, Trisodium Citrate 1% ~ 4%, sodium xylene sulfonate 1% ~ 3%, defoamer AFE-31680.1% ~ 0.3%, fluorescent brightener CBS-X0.01% ~ 0.1%, sodium-chlor 1% ~ 3%, Kathon CG 0.1% ~ 0.5%, the deionized water of spices 0.1% ~ 0.5% and surplus,
Described B liquid is dyeing colour protecting liquid, and it consists of the following composition by weight percentage: the deionized water of dyestuff 10% ~ 20%, dye leveller 1% ~ 5%, wetting agent 1% ~ 5%, sodium-chlor 1% ~ 5%, spices 0.1% ~ 0.5% and surplus.
Embodiment two: present embodiment and embodiment one unlike, fatty alcohol-polyoxyethylene ether (3) sodium sulfate described in A liquid is 12% ~ 16% by weight percentage.Other steps are identical with embodiment one with parameter.
Embodiment three: present embodiment and embodiment one unlike, the methyl sodiosul foaliphatate described in A liquid is 5% ~ 8% by weight percentage.Other steps are identical with embodiment one with parameter.
Embodiment four: present embodiment and embodiment one unlike, the lauric acid amide of ethanol described in A liquid is 6% ~ 8% by weight percentage.Other steps are identical with embodiment one with parameter.
Embodiment five: present embodiment and embodiment one unlike, the alkyl glycoside described in A liquid is 2% ~ 4% by weight percentage.Other steps are identical with embodiment one with parameter.
Embodiment six: present embodiment and embodiment one unlike, the polyvinylpyrrolidone described in A liquid is 2% ~ 4% by weight percentage.Other steps are identical with embodiment one with parameter.
Embodiment seven: present embodiment and embodiment one unlike, the dye leveller described in B liquid is fatty alcohol-polyoxyethylene ether.Other steps are identical with embodiment one with parameter.
Embodiment eight: present embodiment and embodiment one unlike, the dyestuff described in B liquid is 15% ~ 18% by weight percentage.Other steps are identical with embodiment one with parameter.
Embodiment nine: present embodiment and embodiment one unlike, the dye leveller described in B liquid is 2% ~ 4% by weight percentage.Other steps are identical with embodiment one with parameter.
Embodiment ten: present embodiment and embodiment one unlike, the wetting agent described in B liquid is 2% ~ 4% by weight percentage.Other steps are identical with embodiment one with parameter.
Embodiment 11: present embodiment and embodiment one unlike, the sodium-chlor described in B liquid is 2% ~ 4% by weight percentage.Other steps are identical with embodiment one with parameter.
Embodiment 12: present embodiment and embodiment one unlike, the spices in B liquid is 0.1% ~ 0.3% by weight percentage.Other steps are identical with embodiment one with parameter.
Embodiment 13: present embodiment and embodiment one are bright red, grass green, dark blue, reddish brown, black, coffee, dark blue, military green, blueness, orange, blackish green, dark-grey or royal purple unlike, the dyestuff in B liquid.Other steps are identical with embodiment one with parameter.
Embodiment 14: high-effective cleansing and the preparation method protecting look washing liquid of present embodiment, is characterized in that described high-effective cleansing is prepared according to the following steps with the preparation method protecting look washing liquid:
The preparation method of A liquid is prepared according to the following steps:
One, get 3g ~ 6g propylene glycol to join in 12g ~ 16g fatty alcohol-polyoxyethylene ether (3) sodium sulfate, stir to obtain mixed solution;
Two, in container, add 40g ~ 100g deionized water and be warmed up to 50 DEG C ~ 70 DEG C, the mixed solution that step one is obtained is added again successively in container, methyl sodiosul foaliphatate 3g ~ 5g, lauric acid amide of ethanol 7g ~ 10g, alkyl glycoside 1g ~ 3g and polyvinylpyrrolidone 2g ~ 4g, stirring reaction 20min ~ 40min, adding citric acid sodium 3g ~ 5g afterwards, stirs 10min ~ 20min;
Three, temperature of reaction is down to 40 DEG C ~ 45 DEG C, in container, adds sodium xylene sulfonate 1.0g ~ 2.0g, fluorescent brightener CBS-X0.01g ~ 0.1g and defoamer AFE-31680.1g ~ 0.2g successively, stir 10min ~ 20min; Add sodium-chlor 1g ~ 3g again, stir 10min ~ 20min; Then adjust pH with citric acid, make pH=7 ~ 8;
Four, temperature of reaction is down to 30 DEG C ~ 35 DEG C, adds 0.1g ~ 0.5g Kathon CG and 0.1g ~ 0.5g spices stirs 10min ~ 30min again, obtained solution is A liquid;
The preparation method of B liquid is prepared according to the following steps:
In container, add 40g ~ 100g deionized water be warming up to 30 DEG C ~ 35 DEG C, add 10g ~ 20g dyestuff, 2g ~ 4g dye leveller and 2g ~ 4g wetting agent successively and stir 10min ~ 30min, add 2g ~ 4g sodium-chlor and 0.1g ~ 0.5g spices stirring 10min ~ 30min again, obtained solution is B liquid;
Embodiment 15: present embodiment and embodiment 14 unlike, the dye leveller described in B liquid is fatty alcohol-polyoxyethylene ether.Other steps are identical with embodiment 14 with parameter.
Embodiment 16: present embodiment and embodiment 14 are bright red, grass green, dark blue, reddish brown, black, coffee, dark blue, military green, blueness, orange, blackish green, dark-grey or royal purple unlike, the dyestuff in B liquid.Other steps are identical with embodiment 14 with parameter.
Embodiment 1
The preparation of A liquid:
One, in container, add 53.8g deionized water and be warmed up to 60 DEG C, with propylene glycol 5g dissolved fat polyoxyethylenated alcohol (3) sodium sulfate, fatty alcohol-polyoxyethylene ether (3) sodium sulfate 16g, methyl sodiosul foaliphatate 4g, lauric acid amide of ethanol 8g, alkyl glycoside 2g and polyvinylpyrrolidone 3g is added successively again in container, stirring reaction 20min, adding citric acid sodium 4g afterwards, stirs 10min;
Two, temperature of reaction is down to 45 DEG C, in container, adds sodium xylene sulfonate 1.5g, fluorescent brightener CBS-X0.05g and defoamer AFE-31680.15g successively, stir 10min; Add sodium-chlor 2g again, stir 10min; Then adjust pH with citric acid, make pH=7;
Three, temperature of reaction is down to 35 DEG C, adds 0.2g Kathon CG, 0.3g spices stirs 20min again, and obtained solution is A liquid.
The preparation method of B liquid is prepared according to the following steps:
In container, add 75.7g deionized water be warming up to 30 DEG C ~ 35 DEG C, add 15g scarlet dye, 3g fatty alcohol-polyoxyethylene ether and 3g wetting agent PE-100 successively and stir 30min, add 3g sodium-chlor and 0.3g spices stirring 20min again, obtained solution is B liquid.
Embodiment 2
The preparation of A liquid:
One, in container, add 54.8g deionized water and be warmed up to 60 DEG C, with propylene glycol 4g dissolved fat polyoxyethylenated alcohol (3) sodium sulfate, fatty alcohol-polyoxyethylene ether (3) sodium sulfate 14g, methyl sodiosul foaliphatate 3g, lauric acid amide of ethanol 10g, alkyl glycoside 3g and polyvinylpyrrolidone 2g is added successively again in container, stirring reaction 20min, adding citric acid sodium 5g afterwards, stirs 10min;
Two, temperature of reaction is down to 45 DEG C, in container, adds sodium xylene sulfonate 1.5g, fluorescent brightener CBS-X0.05g and defoamer AFE-31680.15g successively, stir 10min; Add sodium-chlor 2g again, stir 10min; Then adjust pH with citric acid, make pH=7;
Three, temperature of reaction is down to 35 DEG C, adds 0.2g Kathon CG, 0.3g spices stirs 20min again, and obtained solution is A liquid.
The preparation method of B liquid is prepared according to the following steps:
In container, add 73.8g deionized water be warming up to 30 DEG C ~ 35 DEG C, add 18g scarlet dye, 2g fatty alcohol-polyoxyethylene ether and 3g wetting agent PE-100 successively and stir 30min, add 3g sodium-chlor and 0.2g spices stirring 20min again, obtained solution is B liquid.
Detergency test:
Detergency test method is with reference to QB/T1224 standard, and detergency test the results are shown in shown in following table.
Known by upper table, the detersive power of the present embodiment 1 and embodiment 2 will much larger than the ordinary liquid laundry detergent on standard washing liquid and market.
Effect of color protection is tested:
The large red clothing of waste and old fugitive color is cut into the sample of 20 pieces of 15cm × 15cm, through identical spot effect, then processes 10 pieces of samples respectively with the product obtained by embodiment 1 and embodiment 2.
Implementation method: first get appropriate A liquid and wash, then carry out dyeing process with the B liquid of A liquid 1/3 amount.
Experimental result: contrast with former clothing, with the present embodiment 1 and the obtained above-mentioned sample protecting the process of look washing liquid of embodiment 2, recovers original bright and new glossy.
Claims (10)
1. a high-effective cleansing and protect look washing liquid and preparation method thereof, is characterized in that: described high-effective cleansing and protect look washing liquid and comprise A liquid and B liquid;
Described A liquid consists of the following composition by weight percentage: fatty alcohol-polyoxyethylene ether (3) sodium sulfate 10% ~ 20%, methyl sodiosul foaliphatate 1% ~ 10%, lauric acid amide of ethanol 5% ~ 10%, alkyl glycoside 1% ~ 5%, polyvinylpyrrolidone 0.1% ~ 5%, propylene glycol 1% ~ 6%, Trisodium Citrate 1% ~ 4%, sodium xylene sulfonate 1% ~ 3%, defoamer AFE-31680.1% ~ 0.3%, fluorescent brightener CBS-X0.01% ~ 0.1%, sodium-chlor 1% ~ 3%, Kathon CG 0.1% ~ 0.5%, the deionized water of spices 0.1% ~ 0.5% and surplus,
Described B liquid consists of the following composition by weight percentage: the deionized water of dyestuff 10% ~ 20%, dye leveller 1% ~ 5%, wetting agent 1% ~ 5%, sodium-chlor 1% ~ 5%, spices 0.1% ~ 0.5% and surplus;
Described B liquid and A liquid volume ratio are in use 1:(1 ~ 3).
2. a kind of high-effective cleansing according to claim 1 and protect look washing liquid, is characterized in that: fatty alcohol-polyoxyethylene ether (3) sodium sulfate described in A liquid is 12% ~ 16% by weight percentage.
3. a kind of high-effective cleansing according to claim 1 and protect look washing liquid, is characterized in that: the methyl sodiosul foaliphatate described in A liquid is 5% ~ 8% by weight percentage.
4. a kind of high-effective cleansing according to claim 1 and protect look washing liquid, is characterized in that: the lauric acid amide of ethanol described in A liquid is 6% ~ 8% by weight percentage.
5. a kind of high-effective cleansing according to claim 1 and protect look washing liquid, is characterized in that: the alkyl glycoside described in A liquid is 2% ~ 4% by weight percentage.
6. a kind of high-effective cleansing according to claim 1 and protect look washing liquid, is characterized in that: the polyvinylpyrrolidone described in A liquid is 2% ~ 4% by weight percentage.
7. a kind of high-effective cleansing according to claim 1 and protect look washing liquid, is characterized in that: the dye leveller described in B liquid is fatty alcohol-polyoxyethylene ether.
8. a kind of high-effective cleansing according to claim 1 and protect look washing liquid, is characterized in that: the dyestuff described in B liquid is 15% ~ 18% by weight percentage.
9. a kind of high-effective cleansing according to claim 1 and protect look washing liquid, is characterized in that: the dyestuff in B liquid is bright red, grass green, dark blue, reddish brown, black, coffee, dark blue, military green, blueness, orange, blackish green, dark-grey or royal purple.
10. a kind of high-effective cleansing as claimed in claim 1 and the preparation method protecting look washing liquid, is characterized in that: this high-effective cleansing carries out according to the following steps with the preparation method protecting look washing liquid:
The preparation method of A liquid is prepared according to the following steps:
One, get 3g ~ 6g propylene glycol to join in 12g ~ 16g fatty alcohol-polyoxyethylene ether (3) sodium sulfate, stir to obtain mixed solution;
Two, in container, add 40g ~ 100g deionized water and be warmed up to 50 DEG C ~ 70 DEG C, mixed solution, methyl sodiosul foaliphatate 3g ~ 5g, lauric acid amide of ethanol 7g ~ 10g, alkyl glycoside 1g ~ 3g and polyvinylpyrrolidone 2g ~ 4g that step one is obtained is added again successively in container, stirring reaction 20min ~ 40min, adding citric acid sodium 3g ~ 5g afterwards, stirs 10min ~ 20min;
Three, temperature of reaction is down to 40 DEG C ~ 45 DEG C, in container, adds sodium xylene sulfonate 1.0g ~ 2.0g, white dyes 0.01g ~ 0.1g and defoamer 0.1g ~ 0.2g successively, stir 10min ~ 20min; Add sodium-chlor 1g ~ 3g again, stir 10min ~ 20min; Then adjust pH with citric acid, make pH=7 ~ 8;
Four, temperature of reaction is down to 30 DEG C ~ 35 DEG C, adds 0.1g ~ 0.5g Kathon CG and 0.1g ~ 0.5g spices stirs 10min ~ 30min again, obtained solution is A liquid;
The preparation method of B liquid is prepared according to the following steps:
In container, add 40g ~ 100g deionized water be warming up to 30 DEG C ~ 35 DEG C, add 10g ~ 20g dyestuff, 2g ~ 4g dye leveller and 2g ~ 4g wetting agent successively and stir 10min ~ 30min, add 2g ~ 4g sodium-chlor and 0.1g ~ 0.5g spices stirring 10min ~ 30min again, obtained solution is B liquid.
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| CN201510810209.9A CN105296191A (en) | 2015-11-19 | 2015-11-19 | Efficient decontaminating and color-protecting laundry detergent and preparation method therefor |
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| CN201510810209.9A CN105296191A (en) | 2015-11-19 | 2015-11-19 | Efficient decontaminating and color-protecting laundry detergent and preparation method therefor |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105907490A (en) * | 2016-05-17 | 2016-08-31 | 河南工程学院 | Acidic colour-protecting detergent composition |
| CN106190631A (en) * | 2016-07-05 | 2016-12-07 | 林恒 | A kind of environment friendly laundry liquid |
| CN109055036A (en) * | 2018-09-26 | 2018-12-21 | 深圳市裕农科技股份有限公司 | A kind of liquid detergent and preparation method thereof |
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| CN102644206A (en) * | 2012-05-14 | 2012-08-22 | 杭州航民美时达印染有限公司 | Polyamide nonwoven fabric dyeing process |
| CN103966033A (en) * | 2014-05-30 | 2014-08-06 | 于文 | Color-protecting laundry detergent and preparation method thereof |
| CN103981714A (en) * | 2014-05-21 | 2014-08-13 | 佛山市邦孚新材料科技有限公司 | Clothing dye-resistant color fixative as well as preparation method and application of clothing dye-resistant color fixative |
| CN104987960A (en) * | 2015-07-13 | 2015-10-21 | 于文 | Fabric fiber care type bio-enzyme laundry detergent and preparation method thereof |
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| WO1992018597A1 (en) * | 1991-04-12 | 1992-10-29 | The Procter & Gamble Company | Compact detergent composition containing polyvinylpyrrolidone |
| CN102644206A (en) * | 2012-05-14 | 2012-08-22 | 杭州航民美时达印染有限公司 | Polyamide nonwoven fabric dyeing process |
| CN103981714A (en) * | 2014-05-21 | 2014-08-13 | 佛山市邦孚新材料科技有限公司 | Clothing dye-resistant color fixative as well as preparation method and application of clothing dye-resistant color fixative |
| CN103966033A (en) * | 2014-05-30 | 2014-08-06 | 于文 | Color-protecting laundry detergent and preparation method thereof |
| CN104987960A (en) * | 2015-07-13 | 2015-10-21 | 于文 | Fabric fiber care type bio-enzyme laundry detergent and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105907490A (en) * | 2016-05-17 | 2016-08-31 | 河南工程学院 | Acidic colour-protecting detergent composition |
| CN106190631A (en) * | 2016-07-05 | 2016-12-07 | 林恒 | A kind of environment friendly laundry liquid |
| CN109055036A (en) * | 2018-09-26 | 2018-12-21 | 深圳市裕农科技股份有限公司 | A kind of liquid detergent and preparation method thereof |
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