CN107237180A - A kind of method of natural plant dye exhaust dyeing cellulosic fabric - Google Patents
A kind of method of natural plant dye exhaust dyeing cellulosic fabric Download PDFInfo
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- CN107237180A CN107237180A CN201710497744.2A CN201710497744A CN107237180A CN 107237180 A CN107237180 A CN 107237180A CN 201710497744 A CN201710497744 A CN 201710497744A CN 107237180 A CN107237180 A CN 107237180A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/445—Use of auxiliary substances before, during or after dyeing or printing
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/58—Material containing hydroxyl groups
- D06P3/60—Natural or regenerated cellulose
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
Abstract
The invention discloses a kind of method of natural plant dye exhaust dyeing cellulosic fabric, natural plant dye is added to the water, natural plants dye liquor is made into;Cationic dye fixing agent is dissolved in natural plants dye liquor, dyeing working solution is made into;Cellulosic fabric to be contaminated is immersed in the dyeing working solution of preparation, and carries out on padding machine roll compacting, then immerses and is contaminated in gardenia blue dyeing working solution, then the roll compacting on padding machine, complete to treat the coloring of dye cellulosic fabric;After the completion of coloring, coloured fiber cellulose fabric is dried, the coloured fiber cellulose fabric for completing drying washed with detergent, except removal floating color;Cellulosic fabric drying after will be scrubbed, completes the dyeing of natural plant dye.The beneficial effects of the invention are as follows the upper dye amount that can improve natural dye, while also improving its washing color fastness, and influence will not be produced on the color and luster of natural dye.
Description
Technical field
The invention belongs to technical field of textile chemistry, it is related to a kind of side of natural plant dye exhaust dyeing cellulosic fabric
Method.
Background technology
In recent years, as the improvement of people's living standards, the textile of environmental protection is liked by consumer, thus it is right
The research that natural fiber is contaminated on natural dye is received significant attention, and the staining technique of cotton fiber is contaminated especially on natural plant dye.
Natural plant dye is extracted from plant, is a kind of sustainable living resources, with nontoxic, nothing
The advantages of pollution and biodegradable.But the reason for being due to the structure of its dye molecule in itself, natural plant dye it is bright-coloured
The not high, form and aspect of degree are uneven, fastness to weathering deviation.In dyeing course, upper dye amount and water-fastness color of the dyestuff on cotton fiber
Fastness is poor, limits its application on the textile.
In order to improve the upper dye amount and washing color fastness of natural dye, generally, the hydrophily such as protein and cellulose is fine
Wesy without mordant dyeing color, first contaminate after mordant dyeing color and first matchmaker's after stain dyeing.Because part metals ion has color, such as iron ion and copper
Ion, therefore mordant dyeing technique in part can cause the color and luster of natural dye after dyeing to change.In addition, on natural plant dye
Dyeing cotton fabric, is typically that, to contaminate mode, compared with pad dyeing process, its dyeing temperature is high, and the time is long.These colouring methods
The requirement of ecological, environmental protective can not be met with technology warp.Therefore, develop it is new save, efficiently, environmental protection, the staining technique of health compeled
In the eyebrows and eyelashes.
Dye fixing agent can improve dyestuff in the auxiliary agent used in textile color moisture resistant fastness, be in textile dye
Fixation treatment is carried out after color.Common cation surface activating quaternary ammonium salt color fixing agent, its dye fixative theory is in water soluble anion
After dyeing, it is combined using the quaternary ammonium salt with cationic with the sulfonic group anion on dyestuff so that dyestuff quilt
Set on the textile, so as to reach tint retention, improves color fastness, especially washing color fastness.
The content of the invention
It is an object of the invention to provide a kind of method of natural plant dye exhaust dyeing cellulosic fabric, solve existing
With the presence of the dyeing of natural plant dye dyeing on dye amount is low and washing color fastness is poor the problem of.
The technical solution adopted in the present invention is to follow the steps below:
Step 1:Natural plant dye is added to the water, the natural plants dye liquor of 20-50g/L concentration is made into;
Step 2:Cationic dye fixing agent is dissolved in natural plants dye liquor, is made into containing the 2-5g/L dyes of positive ion
The dyeing working solution of color fixing agent;
Step 3:Cellulosic fabric to be contaminated is immersed in the dyeing working solution of preparation, and roll compacting is carried out on padding machine, then
Immerse and contaminated in gardenia blue dyeing working solution, then the roll compacting on padding machine, liquid carrying rate is 70%-100%, and dye cellulose is treated in completion
The coloring of fabric;
Step 4:After the completion of coloring, coloured fiber cellulose fabric is dried, drying temperature is 70-100 DEG C;
Step 5:The coloured fiber cellulose fabric for completing drying is washed with detergent, except removal floating color;
Step 6:Cellulosic fabric drying after will be scrubbed, completes the dyeing of natural plant dye.
Further, natural plant dye is gardenia blue, turmeric, green tea.
Further, cellulosic fabric is cotton, fiber crops, viscose fabric.
The beneficial effects of the invention are as follows the upper dye amount that can improve natural dye, while its washing color fastness is also improved,
And influence will not be produced on the color and luster of natural dye.
Embodiment
With reference to specific embodiment, the present invention is described in detail.
Embodiment 1:20g is taken, 30g, 40g, 50g natural dye gardenia blue is dissolved in 1L water, add 4g cations dye
Expect color fixing agent, be made into dyeing working solution.6g cottons are immersed in gardenia blue dyeing working solution and adsorb dyestuff, are rolled on padding machine
Pressure, then dip-dye in gardenia blue dyeing working solution, then roll compacting (i.e. two leachings two are rolled) on padding machine are immersed, make the cotton after exhaust dyeing
Liquid carrying rate be 90% (i.e. 11.4g), then at 90 DEG C drying.Dyed cotton fabric after drying is washed containing 2g/L nonionics
In the 500ml cleaning solutions for washing agent, in washing 15min at 70 DEG C, finally dry, complete cotton dyeing.
The K/S values of the dyed cotton fabric after washing and drying are detected using colour photometer, to characterize the upper dye amount of natural dye, and are examined
The washing color fastness of washing poststaining cotton is surveyed, the results are shown in Table 1.K/S values are higher, show that color is deeper, dyestuff it is upper
Dye amount is higher;K/S values are smaller, show that color is more shallow, and the upper dye amount of dyestuff is lower.Washing color fastness is with dyestuff to multifilament cloth
The staining degree of middle cotton, is evaluated according to national standard.
Show that the K/S values of its cotton dyed are maximum, i.e. natural dye when dye dosage is 40g (40g/L) in table 1
Upper dye amount at most, washing color fastness reaches 4 grades.
K/S value and the shadow of washing color fastness of the different natural dye gardenia blue dye dosages of table 1. to cotton exhaust dyeing
Ring
Dye dosage (g) | K/S values | Washing color fastness (level) |
20 | 4.61 | 3 |
30 | 6.32 | 3-4 |
40 | 11.58 | 4 |
50 | 9.96 | 3-4 |
Embodiment 2:Take 40g natural dye gardenia blue to be dissolved in 1L water, add 0g, 2g, 3g, 4g, 5g cation
Dye fixing agent, is made into dyeing working solution.6g cottons are immersed in gardenia blue dyeing working solution and adsorb dyestuff, are rolled on padding machine
Pressure, then dip-dye in gardenia blue dyeing working solution, then roll compacting (i.e. two leachings two are rolled) on padding machine are immersed, make the cotton after exhaust dyeing
Liquid carrying rate be 90%, then at 90 DEG C dry.Dyed cotton fabric after drying is being contained into 2g/L nonionic detergent
In 500ml cleaning solutions, in washing 15min at 70 DEG C, finally dry, complete cotton dyeing.
The K/S values of the dyed cotton fabric after washing and drying are detected using colour photometer, to characterize the upper dye amount of natural dye, and are examined
The washing color fastness of washing poststaining cotton is surveyed, the results are shown in Table 2.K/S values are higher, show that color is deeper, dyestuff it is upper
Dye amount is higher;K/S values are smaller, show that color is more shallow, and the upper dye amount of dyestuff is lower.Washing color fastness is with dyestuff to multifilament cloth
The staining degree of middle cotton, is evaluated according to national standard.
Show that the K/S values of its cotton dyed are maximum, i.e. day when cationic dye fixing agent is 4g (4g/L) in table 2
At most, washing color fastness reaches 4 grades to the upper dye amount of right dyestuff.When being not added with cationic dye fixing agent, dye amount on its dyestuff
Seldom, washing color fastness is very poor.
K/S value and the influence of washing color fastness of the different cationic dye fixing agent consumptions of table 2. to cotton exhaust dyeing
Embodiment 3:Take 40g natural dye gardenia blue to be dissolved in 1L water, add 4g cationic dye fixing agent, match somebody with somebody
Into dyeing working solution.6g cottons are immersed in gardenia blue dyeing working solution and adsorb dyestuff, the roll compacting on padding machine, then immerse cape jasmine
Contaminated in indigo plant dyeing working solution, then roll compacting (i.e. two leachings two are rolled) on padding machine, distinguish the liquid carrying rate of the cotton after exhaust dyeing
For 70%, 80%, 90%, 100%, the then drying at 90 DEG C.Dyed cotton fabric after drying is washed containing 2g/L nonionics
In the 500ml cleaning solutions for washing agent, in washing 15min at 70 DEG C, finally dry, complete cotton dyeing.
The K/S values of the dyed cotton fabric after washing and drying are detected using colour photometer, to characterize the upper dye amount of natural dye, and are examined
The washing color fastness of washing poststaining cotton is surveyed, the results are shown in Table 3.K/S values are higher, show that color is deeper, dyestuff it is upper
Dye amount is higher;K/S values are smaller, show that color is more shallow, and the upper dye amount of dyestuff is lower.Washing color fastness is with dyestuff to multifilament cloth
The staining degree of middle cotton, is evaluated according to national standard.
Although showing that all washing color fastness all reach 4 grades in table 3, when liquid carrying rate is 90%, what it was dyed
The K/S values of cotton are maximum, i.e. the upper dye amount of natural dye is most.
K/S value and the influence of washing color fastness of the different liquid carrying rates of table 3. to cotton exhaust dyeing
Liquid carrying rate (%) | K/S values | Washing color fastness (level) |
70 | 7.58 | 4 |
80 | 9.19 | 4 |
90 | 11.58 | 4 |
100 | 11.21 | 4 |
Embodiment 4:Take 40g natural dye gardenia blue to be dissolved in 1L water, add 4g cationic dye fixing agent, match somebody with somebody
Into dyeing working solution.6g cottons are immersed in gardenia blue dyeing working solution and adsorb dyestuff, the roll compacting on padding machine, then immerse cape jasmine
Contaminated in indigo plant dyeing working solution, then roll compacting (i.e. two leachings two are rolled) on padding machine, the liquid carrying rate for making the cotton after exhaust dyeing is
90%.Then dried at 70 DEG C, 80 DEG C, 90 DEG C, 100 DEG C.Dyed cotton fabric after drying is being contained into 2g/L non-ionic detergents
In the 500ml cleaning solutions of agent, in washing 15min at 70 DEG C, finally dry, complete cotton dyeing.
The K/S values of the dyed cotton fabric after washing and drying are detected using colour photometer, to characterize the upper dye amount of natural dye, and are examined
The washing color fastness of washing poststaining cotton is surveyed, the results are shown in Table 4.K/S values are higher, show that color is deeper, dyestuff it is upper
Dye amount is higher;K/S values are smaller, show that color is more shallow, and the upper dye amount of dyestuff is lower.Washing color fastness is with dyestuff to multifilament cloth
The staining degree of middle cotton, is evaluated according to national standard.
Show that the K/S values of its cotton dyed are maximum, i.e. natural dye when pad dyeing post-baking temperature is 90 DEG C in table 4
Upper dye amount at most, washing color fastness reaches 4 grades.
K/S value and the influence of washing color fastness of the different drying temperatures to cotton exhaust dyeing after the pad dyeing of table 4.
Temperature (DEG C) | K/S values | Washing color fastness (level) |
70 | 7.62 | 3-4 |
80 | 9.43 | 3-4 |
90 | 11.58 | 4 |
100 | 11.41 | 4 |
Embodiment 5:Take 40g natural dye gardenia blue to be dissolved in 1L water, add 4g cationic dye fixing agent, match somebody with somebody
Into dyeing working solution.6g cottons are immersed in gardenia blue dyeing working solution and adsorb dyestuff, the roll compacting on padding machine, then immerse cape jasmine
Contaminated in indigo plant dyeing working solution, then roll compacting (i.e. two leachings two are rolled) on padding machine, the liquid carrying rate for making the cotton after exhaust dyeing is
90%, then dried at 90 DEG C, i.e. dyestuff and cation Guyang agent simultaneously dyeing (dye fixing is synchronous).Separately take 40g day
Right dyestuff gardenia blue is dissolved in 1L water, is made into dyeing working solution.4g cationic dye fixing agent is taken, fixation work is made into
Liquid.6g cottons are immersed in the gardenia blue dyeing working solution without cationic dye fixing agent and adsorb dyestuff, are rolled on padding machine
Pressure, then dip-dye in gardenia blue dyeing working solution, then roll compacting (i.e. two leachings two are rolled) on padding machine are immersed, make the cotton after exhaust dyeing
Liquid carrying rate be 90%, then at 90 DEG C dry.By in the stained clot-h immersion fixation working solution after drying, two leachings two are rolled, band
Liquid rate is 90%, is then dried at 90 DEG C, i.e., fixation after first dyeing.Dyed cotton fabric after drying is being contained into 2g/L nonionics
In the 500ml cleaning solutions of detergent, in washing 15min at 70 DEG C, finally dry, complete cotton dyeing.
The K/S values of the dyed cotton fabric after washing and drying are detected using colour photometer, to characterize the upper dye amount of natural dye, and are examined
The washing color fastness of washing poststaining cotton is surveyed, the results are shown in Table 5.K/S values are higher, show that color is deeper, dyestuff it is upper
Dye amount is higher;K/S values are smaller, show that color is more shallow, and the upper dye amount of dyestuff is lower.Washing color fastness is with dyestuff to multifilament cloth
The staining degree of middle cotton, is evaluated according to national standard.
After being dyed in the ban in table 5 after fixation, the upper dye amount and washing color fastness of the cotton after dyeing all compare dye fixing
Synchronous staining method is poor, and the staining method of fixation is good after showing the synchronous staining method of dye fixing than first dyeing.
K/S value and the influence of washing color fastness of the coloured differently mode of table 5. to cotton exhaust dyeing
Staining method | K/S values | Washing color fastness (level) |
Fixation after first dyeing | 4.04 | 3 |
Dye fixing is synchronous | 11.58 | 4 |
It is also an advantage of the present invention that the natural dye of the present invention and dye fixing agent synchronously carry out exhaust dyeing, rather than
Fixation again after first dyeing, saves dyeing time and simplifies dyeing process, be the new dyeing technology of energy-saving consumption-reducing.The technology is not only carried
The upper rate amount of high natural dye, while also improving its washing color fastness, and will not produce influence to the color and luster of natural dye.
Described above is only the better embodiment to the present invention, not makees any formal limit to the present invention
System, any simple modification that every technical spirit according to the present invention is made to embodiment of above, equivalent variations and modification,
Belong in the range of technical solution of the present invention.
Claims (3)
1. a kind of method of natural plant dye exhaust dyeing cellulosic fabric, it is characterised in that follow the steps below:
Step 1:Natural plant dye is added to the water, the natural plants dye liquor of 20-50g/L concentration is made into;
Step 2:Cationic dye fixing agent is dissolved in natural plants dye liquor, is made into containing 2-5g/L cationic dyestuff fixations
The dyeing working solution of agent;
Step 3:Cellulosic fabric to be contaminated is immersed in the dyeing working solution of preparation, and carries out on padding machine roll compacting, then is immersed
Contaminated in gardenia blue dyeing working solution, then the roll compacting on padding machine, liquid carrying rate is 70-100%, completes to treat dye cellulosic fabric
Coloring;
Step 4:After the completion of coloring, coloured fiber cellulose fabric is dried, drying temperature is 70-100 DEG C;
Step 5:The coloured fiber cellulose fabric for completing drying is washed with detergent, except removal floating color;
Step 6:Cellulosic fabric drying after will be scrubbed, completes the dyeing of natural plant dye.
2. according to a kind of method of natural plant dye exhaust dyeing cellulosic fabric described in claim 1, it is characterised in that:Institute
Natural plant dye is stated for gardenia blue, turmeric, green tea.
3. according to a kind of method of natural plant dye exhaust dyeing cellulosic fabric described in claim 1, it is characterised in that:Institute
Cellulosic fabric is stated for cotton, fiber crops, viscose fabric.
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Cited By (13)
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CN108149493A (en) * | 2017-12-29 | 2018-06-12 | 罗莱生活科技股份有限公司 | A kind of preparation method of granatum dyestuff and the purposes of granatum dyestuff |
CN108517702A (en) * | 2018-04-24 | 2018-09-11 | 广东爱华毛织工艺有限公司 | A kind of method of natural plant dye dyeing cellulosic fibre |
CN108589334A (en) * | 2018-04-24 | 2018-09-28 | 武汉纺织大学 | A method of preparing the dark damp cellulose fibre of natural plant dye dyeing |
CN110184830A (en) * | 2019-06-17 | 2019-08-30 | 苏州东山汇旅游发展有限公司 | A kind of plant dyeing technique process using Pilochun (a green tea) |
CN110241632A (en) * | 2019-06-20 | 2019-09-17 | 泉州师范学院(石狮)生态智能织物工程技术研究院 | A method of fabric is dyed using riboflavin as dyestuff |
CN111021098A (en) * | 2019-12-25 | 2020-04-17 | 湖北鸿鑫化工有限公司 | Method for dyeing by using natural dye |
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Cited By (21)
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CN108149493A (en) * | 2017-12-29 | 2018-06-12 | 罗莱生活科技股份有限公司 | A kind of preparation method of granatum dyestuff and the purposes of granatum dyestuff |
CN108589334B (en) * | 2018-04-24 | 2021-07-06 | 武汉纺织大学 | Method for preparing natural plant dye dyed dark-color cellulose fiber |
CN108517702A (en) * | 2018-04-24 | 2018-09-11 | 广东爱华毛织工艺有限公司 | A kind of method of natural plant dye dyeing cellulosic fibre |
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