CN113235315A - Environment-friendly dyeing slurry, preparation method thereof and muslin yarn dyeing process - Google Patents

Environment-friendly dyeing slurry, preparation method thereof and muslin yarn dyeing process Download PDF

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Publication number
CN113235315A
CN113235315A CN202110516761.2A CN202110516761A CN113235315A CN 113235315 A CN113235315 A CN 113235315A CN 202110516761 A CN202110516761 A CN 202110516761A CN 113235315 A CN113235315 A CN 113235315A
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China
Prior art keywords
dyeing
mass
accounts
natural
environment
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Pending
Application number
CN202110516761.2A
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Chinese (zh)
Inventor
徐兆梅
余志成
马行天
马廷方
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hangzhou Wansli Silk Digital Printing Co ltd
Hangzhou Boyang New Material Technology Co ltd
Zhejiang University of Technology ZJUT
Zhejiang Sci Tech University ZSTU
Zhejiang University of Science and Technology ZUST
Original Assignee
Hangzhou Wansli Silk Digital Printing Co ltd
Hangzhou Boyang New Material Technology Co ltd
Zhejiang University of Technology ZJUT
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Application filed by Hangzhou Wansli Silk Digital Printing Co ltd, Hangzhou Boyang New Material Technology Co ltd, Zhejiang University of Technology ZJUT filed Critical Hangzhou Wansli Silk Digital Printing Co ltd
Priority to CN202110516761.2A priority Critical patent/CN113235315A/en
Publication of CN113235315A publication Critical patent/CN113235315A/en
Pending legal-status Critical Current

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    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/34General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/02Material containing basic nitrogen
    • D06P3/04Material containing basic nitrogen containing amide groups

Abstract

The application discloses environment-friendly dyeing pulp, a preparation method thereof and a fragrant cloud yarn dyeing process, wherein the environment-friendly dyeing pulp mainly comprises natural plant dye, a natural thickener and water, wherein the natural plant dye accounts for 1-20% by mass, the natural thickener accounts for 1-20% by mass, and the water accounts for 75-98% by mass. The dyeing process of the gambiered Canton gauze comprises the steps of dyeing a refined real silk fabric in environment-friendly dyeing slurry; and drying after dyeing to obtain a semi-finished product.

Description

Environment-friendly dyeing slurry, preparation method thereof and muslin yarn dyeing process
Technical Field
The application relates to the technical field of silk fabric dyeing, in particular to environment-friendly dyeing slurry, a preparation method thereof and a gambiered Canton gauze dyeing process.
Background
The gambiered san yarn is a pure plant and mineral dyeing and finishing silk fabric in the current world textile, is an ancient plant dyeing fabric manufactured by hand weaving and dyeing and finishing in the south of five Ridges, has a history of over one hundred years, has the characteristics of smoothness, quickness in cooling, sterilization, insect expelling and health care effect on skin due to unique manufacturing process, rare quantity, long manufacturing period and exquisite required technology, and is worn smoothly, quickly cooled, degerming, insect expelling and health care effect on skin.
The gamboge yarn is also called 'gamboge yarn', and is made up by using the special-purpose plant dioscorea cirrhosa juice (containing gelatin and tannic acid) of Guangdong through the processes of several times of soaking, drying in the sun and coating on the cooked raw silk to make the fabric obtain a layer of yellow-brown colloidal substance, then covering with river silt richly containing several mineral substances, repeatedly drying in the sun, washing with water and fermenting.
The gambiered plant yarn is manufactured by the steps of silk blank making, refining, gambiered plant juice soaking, airing, repeated soaking and airing processes for multiple times, silk boiling, repeated washing and airing of the gambiered plant juice, re-boiling, mud filtering, airing, mist spreading, tentering, and packaging and warehousing. The whole airing process needs dozens of processes of three washing, nine boiling and eighteen airing. The main process flow is as follows:
silk fabric preparation → 1 time of soaking the crow's foot water → 6 times of sprinkling the crow's foot water → 6 times of sealing the crow's foot water → 1 time of boiling the silk fabric → 12 times of sealing the crow's foot water → 1 time of boiling the silk fabric → 1 time of sealing the crow's foot water → silk rolling → river mud → water washing → 1 time of sealing the crow's foot water → spreading → silk rolling → check and size scale → finished product warehousing.
The defects of the process are that the process is complicated, the water consumption is large, the waste water is large, the yield is low and the industrialization is limited, which are important obstacles that the gambiered plant cannot be popularized.
Disclosure of Invention
The embodiment of the application aims to provide the environment-friendly dyeing pulp, the preparation method thereof and the gambiered plant yarn dyeing process, so as to solve the problems of complicated working procedures, large water consumption, more waste water, low yield and limited industrialization in the related technology.
According to a first aspect of embodiments of the present application, an environment-friendly dyeing slurry is provided, which mainly comprises natural plant dyes, a natural thickener and water, wherein the natural plant dyes account for 1% to 20% by mass, the natural thickener accounts for 1% to 20% by mass, and the water accounts for 75% to 98% by mass.
According to a second aspect of embodiments of the present application, there is provided a method for preparing an environment-friendly dyeing slurry, comprising:
the natural plant dye and the natural thickener are sequentially poured into water and stirred and mixed, wherein the natural plant dye accounts for 1-20% by mass, the natural thickener accounts for 1-20% by mass, and the water accounts for 75-98% by mass.
According to a third aspect of embodiments of the present application, there is provided a gambiered Canton yarn dyeing process, the process comprising:
dyeing the refined real silk fabric in environment-friendly dyeing slurry;
drying after dyeing to obtain a semi-finished product;
the environment-friendly dyeing pulp mainly comprises natural plant dye, natural thickener and water, wherein the natural plant dye accounts for 1-20% by mass, the natural thickener accounts for 1-20% by mass, and the water accounts for 75-98% by mass.
Further, the dyeing is pad dyeing, rotary screen printing and dyeing, flat-cylinder jig dyeing, rope-loading dip dyeing or beam dip dyeing.
According to a fourth aspect of embodiments of the present application, there is provided a dyeing process for a gambiered Canton yarn, the process comprising:
carrying out first padding on the refined silk fabric in environment-friendly dyeing slurry;
drying after the first padding;
after drying, carrying out secondary padding in the environment-friendly dyeing slurry;
after the second padding, performing coiling rotary cold reactor reaction for color fixation;
drying after color fixing to obtain a semi-finished product;
the environment-friendly dyeing pulp mainly comprises natural plant dye, natural thickener and water, wherein the natural plant dye accounts for 1-20% by mass, the natural thickener accounts for 1-20% by mass, and the water accounts for 75-98% by mass.
Further, the stirring time is 1 hour or more.
Further, the first padding of the refined real silk fabric in the mixed dyeing slurry comprises the following steps:
and inputting the mixed dyeing slurry into a dye liquor tank of a uniform padder to pad the refined real silk fabric.
Further, the padding vehicle speed of the uniform padder is 20-40 m/min.
Further, after drying, the second padding is carried out in the environment-friendly dyeing slurry, and the method comprises the following steps:
and (4) pulling the dried refined real silk fabric back to the evenness calender again, and carrying out secondary padding in the environment-friendly dyeing slurry.
Further, the time of the cold reactor is 16-24 hours.
The technical scheme provided by the embodiment of the application can have the following beneficial effects:
according to the embodiment, the environment-friendly dyeing slurry provided by the embodiment of the application mainly comprises the natural plant dye, the natural thickening agent and water, the color fastness of the fragrant cloud yarn fabric dyed by the environment-friendly dyeing slurry can reach or exceed the traditional fragrant cloud yarn detection index, and the detection data are shown in table 1.
Compared with the traditional key technology of the fragrant cloud yarn, the technology provided by the embodiment of the application reduces a plurality of procedures, liberates a large amount of manpower, does not occupy natural grasslands for drying silk, greatly improves the production efficiency, and has stable quality and high yield in mechanical production.
It is to be understood that both the foregoing general description and the following detailed description are exemplary and explanatory only and are not restrictive of the application.
Detailed Description
Exemplary embodiments will be described in detail herein. The embodiments described in the following exemplary embodiments do not represent all embodiments consistent with the present application. Rather, they are merely examples of apparatus and methods consistent with certain aspects of the present application, as detailed in the appended claims.
The terminology used herein is for the purpose of describing particular embodiments only and is not intended to be limiting of the application. As used in this application and the appended claims, the singular forms "a", "an", and "the" are intended to include the plural forms as well, unless the context clearly indicates otherwise. It should also be understood that the term "and/or" as used herein refers to and encompasses any and all possible combinations of one or more of the associated listed items.
Example 1:
the embodiment provides an environment-friendly dyeing pulp, which mainly comprises natural plant dye, a natural thickener and water, wherein the natural plant dye accounts for 1% by mass, the natural thickener accounts for 1% by mass, and the water accounts for 98% by mass.
The corresponding preparation method of the environment-friendly dyeing slurry can comprise the following steps:
the natural plant dye and the natural thickener are sequentially poured into water and stirred and mixed, wherein the natural plant dye accounts for 1% by mass, the natural thickener accounts for 1% by mass, and the water accounts for 98% by mass.
Example 2:
the embodiment provides an environment-friendly dyeing pulp, which mainly comprises natural plant dyes, a natural thickener and water, wherein the natural plant dyes account for 20% by mass, the natural thickener accounts for 5% by mass, and the water accounts for 75% by mass.
The corresponding preparation method of the environment-friendly dyeing slurry can comprise the following steps:
the natural plant dye and the natural thickener are sequentially poured into water and stirred and mixed, the natural plant dye accounts for 20% by mass, the natural thickener accounts for 5% by mass, and the water accounts for 75% by mass.
Example 3:
the embodiment provides an environment-friendly dyeing pulp, which mainly comprises a natural plant dye, a natural thickener and water, wherein the natural plant dye accounts for 20% by mass, the natural thickener accounts for 1% by mass, and the water accounts for 79% by mass.
The corresponding preparation method of the environment-friendly dyeing slurry can comprise the following steps:
the natural plant dye and the natural thickener are sequentially poured into water and stirred and mixed, wherein the natural plant dye accounts for 20% by mass, the natural thickener accounts for 1% by mass, and the water accounts for 79% by mass.
Example 4:
the embodiment provides an environment-friendly dyeing pulp, which mainly comprises natural plant dyes, a natural thickener and water, wherein the natural plant dyes account for 1% by mass, the natural thickener accounts for 20% by mass, and the water accounts for 79% by mass.
The corresponding preparation method of the environment-friendly dyeing slurry can comprise the following steps:
the natural plant dye and the natural thickener are sequentially poured into water and stirred and mixed, wherein the natural plant dye accounts for 1% by mass, the natural thickener accounts for 20% by mass, and the water accounts for 79% by mass.
Example 5:
the embodiment provides an environment-friendly dyeing pulp, which mainly comprises a natural plant dye, a natural thickener and water, wherein the natural plant dye accounts for 5% by mass, the natural thickener accounts for 20% by mass, and the water accounts for 75% by mass.
The corresponding preparation method of the environment-friendly dyeing slurry can comprise the following steps:
the natural plant dye and the natural thickener are sequentially poured into water and stirred and mixed, the natural plant dye accounts for 5% by mass, the natural thickener accounts for 20% by mass, and the water accounts for 75% by mass.
Example 6:
the embodiment provides an environment-friendly dyeing pulp, which mainly comprises a natural plant dye, a natural thickener and water, wherein the natural plant dye accounts for 6% by mass, the natural thickener accounts for 1% by mass, and the water accounts for 93% by mass.
The corresponding preparation method of the environment-friendly dyeing slurry can comprise the following steps:
the natural plant dye and the natural thickener are sequentially poured into water and stirred and mixed, wherein the natural plant dye accounts for 6% by mass, the natural thickener accounts for 1% by mass, and the water accounts for 93% by mass.
Example 7:
the embodiment provides an environment-friendly dyeing pulp, which mainly comprises a natural plant dye, a natural thickener and water, wherein the natural plant dye accounts for 15% by mass, the natural thickener accounts for 2% by mass, and the water accounts for 83% by mass.
The corresponding preparation method of the environment-friendly dyeing slurry can comprise the following steps:
the natural plant dye and the natural thickener are sequentially poured into water and stirred and mixed, wherein the natural plant dye accounts for 15% by mass, the natural thickener accounts for 2% by mass, and the water accounts for 83% by mass.
Example 8:
the embodiment provides an environment-friendly dyeing pulp, which mainly comprises a natural plant dye, a natural thickener and water, wherein the natural plant dye accounts for 3% by mass, the natural thickener accounts for 1% by mass, and the water accounts for 97% by mass.
The corresponding preparation method of the environment-friendly dyeing slurry can comprise the following steps:
the natural plant dye and the natural thickener are sequentially poured into water and stirred and mixed, the natural plant dye accounts for 5% by mass, the natural thickener accounts for 20% by mass, and the water accounts for 75% by mass.
According to the 8 embodiments, the environment-friendly dyeing slurry provided by the embodiment of the application mainly comprises the natural plant dye, the natural thickening agent and water, and the color fastness of the fragrant cloud yarn fabric dyed by the environment-friendly dyeing slurry can reach or exceed the traditional fragrant cloud yarn detection index. The test data are shown in table 1.
Example 9:
the embodiment provides a dyeing process for gambiered Canton gauze, which comprises the following steps:
carrying out first padding → first padding and then drying → drying on the refined silk fabric in environment-friendly dyeing slurry, then carrying out second padding → second padding and then carrying out coiling rotary cold batch reaction color fixation → drying after color fixation to obtain a semi-finished product; the environment-friendly dyeing slurry mainly comprises natural plant dye, a natural thickener and water, wherein the natural plant dye accounts for 6% by mass, the natural thickener accounts for 1% by mass, and the water accounts for 93% by mass.
Specifically, the padding dyeing steps are as follows:
1, sewing the refined real silk fabric with a piece of fabric, and putting the piece of fabric on a uniform padder for pad dyeing.
And 2, blending the dyeing slurry according to a ratio (the mass percent of the natural plant dye is 6%, the mass percent of the natural thickener is 1%, the mass percent of the water is 93%, firstly discharging water, then sequentially and uniformly putting the natural plant dye mixture and the natural thickener into a stirrer, uniformly stirring, and feeding the blended dyeing slurry into a dye bath tank of a uniform padder, wherein the stirring time is more than or equal to 1 hour).
And 3, pad dyeing the sewn refined silk fabric with dyeing slurry in a pad dyeing machine at the pad dyeing speed of 20-40 m/min, dyeing, rolling and sending the fabric to a drying and setting machine for drying.
And 4, pulling the dried refined real silk fabric back to the evenness calender again, pad dyeing the dyeing slurry, and performing cold-batch color fixation after rolling for 16-24 hours.
5, after cold piling, drying again by using a drying and setting machine, wherein the drying temperature is 120-.
And 6, finally, checking and warehousing.
And (3) carrying out color fastness detection on the fabric processed in the previous step, wherein the color fastness data are shown in table 1.
Table 1: color fastness data
Color fastness detection item The present application relates to a gambiered Canton color fastness grade Color fastness grade of traditional gambiered Canton gauze
Color fastness to soaping 3 3
Color fastness to sunlight 4 4
Colour fastness to perspiration 3-4 3
Color fastness to wet rubbing 2-3 2-3
Color fastness to dry rubbing 4-5 4
Example 10:
the embodiment provides a dyeing process for gambiered Canton gauze, which comprises the following steps:
dyeing the refined real silk fabric in dyeing slurry → drying after dyeing to obtain a semi-finished product; the dyeing slurry mainly comprises natural plant dye, a natural thickener and water, wherein the natural plant dye accounts for 15% by mass, the natural thickener accounts for 2% by mass, and the water accounts for 83% by mass.
Specifically, this example shows a cloud yarn rotary screen printing, which includes:
and 1, refining the real silk fabric, sewing, and putting the fabric on a rotary screen printing machine for printing and dyeing.
And 2, blending the dyeing slurry according to a ratio (the mass percent of the natural plant dye is 15%, the mass percent of the natural thickener is 2%, the mass percent of the water is 83%, firstly, discharging water, then, sequentially and uniformly putting the natural plant dye mixture and the natural thickener into a stirrer, uniformly stirring, and enabling the stirring time to be more than or equal to 1 hour), and inputting the blended dyeing slurry into a color slurry tank of the rotary screen printing machine.
And 3, using two circular screens with the same pattern by using a circular screen printing machine, wherein the pattern simulates cracks of the traditional gambiered plant silk yarn, and directly drying the fabric after printing and dyeing twice, wherein the drying temperature is 120-.
And 4, finishing the dyeing semi-finished product after steaming and color fixing.
And 5, checking and warehousing.
Example 11:
the embodiment provides a dyeing process for gambiered Canton gauze, which comprises the following steps:
dyeing the white blank silk refined and degummed by the real silk in dyeing slurry → drying after dyeing to obtain a semi-finished product; the dyeing slurry mainly comprises natural plant dye, a natural thickener and water, wherein the natural plant dye accounts for 3% by mass, the natural thickener accounts for 1% by mass, and the water accounts for 97% by mass.
Specifically, this example shows a cloud yarn flat-vat jig dyeing (rope-mounted dip dyeing, beam dip dyeing are suitable), the flat-vat jig dyeing step comprising:
1, sewing the real silk electric spun silk, rolling the silk and putting the silk in a flat vat to prepare for dyeing.
And 2, blending the dyeing slurry according to a ratio (the mass percent of the natural plant dye is 3%, the mass percent of the natural thickener is 1%, the mass percent of the water is 97%, firstly discharging water, then sequentially and uniformly putting the natural plant dye mixture and the natural thickener into a stirrer, uniformly stirring, and stirring for more than or equal to 1 hour), and inputting the blended dyeing slurry into a flat-vat color slurry tank.
And 3, starting the flat cylinder for dyeing, and continuously performing jig dyeing for 3-4 times back and forth.
4, taking out and drying at the drying temperature of 120 ℃ and the vehicle speed of 130 ℃ of 30-40 m/min.
And 5, checking and warehousing.
Compared with the traditional key technology of the fragrant cloud yarn, the technology provided by the embodiment of the application reduces a plurality of procedures, liberates a large amount of manpower, does not occupy natural grasslands for drying silk, greatly improves the production efficiency, and has stable quality and high yield in mechanical production.
Other embodiments of the present application will be apparent to those skilled in the art from consideration of the specification and practice of the disclosure disclosed herein. This application is intended to cover any variations, uses, or adaptations of the invention following, in general, the principles of the application and including such departures from the present disclosure as come within known or customary practice within the art to which the invention pertains. It is intended that the specification and examples be considered as exemplary only, with a true scope and spirit of the application being indicated by the following claims.
It will be understood that the present application is not limited to the precise arrangements that have been described above and that various modifications and changes may be made without departing from the scope thereof. The scope of the application is limited only by the appended claims.

Claims (10)

1. The environment-friendly dyeing pulp is characterized by mainly comprising natural plant dye, a natural thickener and water, wherein the natural plant dye accounts for 1-20% by mass, the natural thickener accounts for 1-20% by mass, and the water accounts for 75-98% by mass.
2. The preparation method of the environment-friendly dyeing slurry is characterized by comprising the following steps:
the natural plant dye and the natural thickener are sequentially poured into water and stirred and mixed, wherein the natural plant dye accounts for 1-20% by mass, the natural thickener accounts for 1-20% by mass, and the water accounts for 75-98% by mass.
3. A dyeing process of gambiered Canton gauze is characterized by comprising the following steps:
dyeing the refined real silk fabric in environment-friendly dyeing slurry;
drying after dyeing to obtain a semi-finished product;
the environment-friendly dyeing pulp mainly comprises natural plant dye, natural thickener and water, wherein the natural plant dye accounts for 1-20% by mass, the natural thickener accounts for 1-20% by mass, and the water accounts for 75-98% by mass.
4. The dyeing process of the gambiered Canton yarn as claimed in claim 3, wherein the dyeing is pad dyeing, rotary screen printing and dyeing, flat-cylinder jig dyeing, rope-mounted dip dyeing or beam dip dyeing.
5. A dyeing process of gambiered Canton gauze is characterized by comprising the following steps:
carrying out first padding on the refined silk fabric in environment-friendly dyeing slurry;
drying after the first padding;
after drying, carrying out secondary padding in the environment-friendly dyeing slurry;
after the second padding, performing coiling rotary cold reactor reaction for color fixation;
drying after color fixing to obtain a semi-finished product;
the environment-friendly dyeing pulp mainly comprises natural plant dye, natural thickener and water, wherein the natural plant dye accounts for 1-20% by mass, the natural thickener accounts for 1-20% by mass, and the water accounts for 75-98% by mass.
6. The cloud yarn dyeing process according to claim 5, wherein the stirring time is greater than or equal to 1 hour.
7. The dyeing process of fragrant musty yarn as claimed in claim 5, wherein the first padding of refined silk fabric in mixed dyeing slurry comprises:
and inputting the mixed dyeing slurry into a dye liquor tank of a uniform padder to pad the refined real silk fabric.
8. The dyeing process of gambiered muskmelon as claimed in claim 5, wherein the padding speed of the evenness padder is 20-40 m/min.
9. The dyeing process of the gambiered Canton gauze as claimed in claim 5, wherein the second padding is carried out in the environment-friendly dyeing slurry after drying, and comprises the following steps:
and (4) pulling the dried refined real silk fabric back to the evenness calender again, and carrying out secondary padding in the environment-friendly dyeing slurry.
10. The cloud yarn dyeing process according to claim 5, wherein the time of the cold pad-batch is 16-24 hours.
CN202110516761.2A 2021-05-12 2021-05-12 Environment-friendly dyeing slurry, preparation method thereof and muslin yarn dyeing process Pending CN113235315A (en)

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Application publication date: 20210810