CN105229084B - 分离蓝色的花青素苷级分的方法 - Google Patents

分离蓝色的花青素苷级分的方法 Download PDF

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Publication number
CN105229084B
CN105229084B CN201480013986.4A CN201480013986A CN105229084B CN 105229084 B CN105229084 B CN 105229084B CN 201480013986 A CN201480013986 A CN 201480013986A CN 105229084 B CN105229084 B CN 105229084B
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CN
China
Prior art keywords
fraction
anthocyanin
fractions
anthocyanins
blue
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
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CN201480013986.4A
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English (en)
Chinese (zh)
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CN105229084A (zh
Inventor
R·J·罗宾斯
J·C·约翰逊
T·M·柯林斯
N·艾哈迈迪阿尼
M·M·朱斯蒂
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Jr Co
Wm Regley
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Mars Inc
Ohio State University
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
    • A23L2/02Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof containing fruit or vegetable juices
    • A23L2/04Extraction of juices
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
    • A23L2/52Adding ingredients
    • A23L2/58Colouring agents
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
    • A23L2/70Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
    • A23L2/78Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by ion-exchange
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L5/00Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
    • A23L5/40Colouring or decolouring of foods
    • A23L5/42Addition of dyes or pigments, e.g. in combination with optical brighteners
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D15/00Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08Selective adsorption, e.g. chromatography
    • B01D15/26Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/36Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction, e.g. ion-exchange, ion-pair, ion-suppression or ion-exclusion
    • B01D15/361Ion-exchange
    • B01D15/362Cation-exchange
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D15/00Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08Selective adsorption, e.g. chromatography
    • B01D15/42Selective adsorption, e.g. chromatography characterised by the development mode, e.g. by displacement or by elution
    • B01D15/424Elution mode
    • B01D15/426Specific type of solvent
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D311/00Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
    • C07D311/02Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
    • C07D311/04Benzo[b]pyrans, not hydrogenated in the carbocyclic ring
    • C07D311/58Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07HSUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H17/00Compounds containing heterocyclic radicals directly attached to hetero atoms of saccharide radicals
    • C07H17/04Heterocyclic radicals containing only oxygen as ring hetero atoms
    • C07H17/06Benzopyran radicals
    • C07H17/065Benzo[b]pyrans
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L5/00Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
    • A23L5/40Colouring or decolouring of foods
    • A23L5/42Addition of dyes or pigments, e.g. in combination with optical brighteners
    • A23L5/43Addition of dyes or pigments, e.g. in combination with optical brighteners using naturally occurring organic dyes or pigments, their artificial duplicates or their derivatives
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B61/00Dyes of natural origin prepared from natural sources, e.g. vegetable sources

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Nutrition Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Biotechnology (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Molecular Biology (AREA)
  • Biochemistry (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Cosmetics (AREA)
CN201480013986.4A 2013-03-15 2014-03-14 分离蓝色的花青素苷级分的方法 Expired - Fee Related CN105229084B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201361790842P 2013-03-15 2013-03-15
US61/790,842 2013-03-15
PCT/US2014/027319 WO2014152417A2 (en) 2013-03-15 2014-03-14 Method of isolating blue anthocyanin fractions

Publications (2)

Publication Number Publication Date
CN105229084A CN105229084A (zh) 2016-01-06
CN105229084B true CN105229084B (zh) 2017-09-01

Family

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Country Link
US (2) US9598581B2 (https=)
EP (1) EP2986675B1 (https=)
JP (1) JP5981675B2 (https=)
CN (1) CN105229084B (https=)
AU (1) AU2014239875B2 (https=)
BR (1) BR112015021402B1 (https=)
CA (1) CA2904650C (https=)
GB (1) GB2527453B (https=)
MX (1) MX362026B (https=)
RU (1) RU2629257C2 (https=)
WO (1) WO2014152417A2 (https=)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2527453B (en) 2013-03-15 2017-03-15 Mars Inc Method of isolating blue anthocyanin fractions
CN104961783B (zh) * 2015-04-17 2018-07-10 浙江惠松制药有限公司 一种有效提取花青素和花色苷的方法
RU2721836C2 (ru) * 2015-06-30 2020-05-22 Марс, Инкорпорейтед Композиции красителей и способы их использования
EP3562313B1 (en) 2016-12-29 2021-12-01 Mars, Incorporated Edible ink formulations including scalenohedral calcium carbonate particles
EP3813553A4 (en) 2018-06-28 2022-03-16 Wm. Wrigley Jr. Company TITANIUM-FREE OPACITY COMPOSITIONS
ES3001095T3 (es) 2018-06-28 2025-03-04 Mars Inc Formulaciones mejoradas de tintas comestibles que incluyen carbonato de calcio
WO2020047276A1 (en) 2018-08-31 2020-03-05 Mars, Incorporated Anthocyanin-based colorant compositions and methods of use thereof
WO2021067627A1 (en) 2019-10-01 2021-04-08 Mars, Incorporated Enzymatic treatment of anthocyanins
EP3939437A1 (en) * 2020-07-17 2022-01-19 GNT Group B.V. A composition comprising spirulina extract

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20040022904A1 (en) * 2002-07-31 2004-02-05 Mars Incorporated Novel confectionery composition
WO2009100165A2 (en) * 2008-02-06 2009-08-13 The Ohio State University Research Foundation High-purity fractionation of anthocyanins from fruits and vegetables
WO2012043173A1 (ja) * 2010-09-27 2012-04-05 理研ビタミン株式会社 クチナシ青色素の製造方法

Family Cites Families (49)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3361631A (en) 1963-09-30 1968-01-02 Sandoz Ag Method of sugar coating pharmaceutical tablets
DE1482489A1 (de) 1965-01-13 1970-03-12 Boehringer Mannheim Gmbh Vollautomatisches Dragierverfahren
NL6601426A (https=) 1965-02-12 1966-08-15
US4172902A (en) 1978-05-26 1979-10-30 The United States Of America As Represented By The Secretary Of Agriculture Stable foods and beverages containing the anthocyanin, peonidin 3-(dicaffeylsophoroside)-5-glucoside
JPS6025181B2 (ja) 1982-10-04 1985-06-17 フロイント産業株式会社 パンコ−チング装置
US4681766A (en) 1986-01-07 1987-07-21 Warner-Lambert Company Coatings for chewing gums containing gum arabic and a soluble calcium salt
JPH083047B2 (ja) 1986-06-21 1996-01-17 サントリー株式会社 天然青色系色素組成物及びそれを用いた着色剤
DK0719093T3 (da) 1993-09-15 2000-06-05 Wrigley W M Jun Co Tyggegummi med hårdt overtræk og forbedret holdbarhed og med blandede polyocoatinger
JPH07188572A (ja) 1993-12-27 1995-07-25 Kyodo Nyugyo Kk マロ−由来の天然色素
DE69724231T3 (de) 1996-01-22 2012-09-20 Chr. Hansen A/S In wasser dispergierbare zusammensetzungen, die ein natuerliches hydrophobes pigment enthalten, verfahren zu ihrer herstellung und ihre verwendung
US6541048B2 (en) 1999-09-02 2003-04-01 Wm. Wrigley Jr. Company Coated chewing gum products containing an acid blocker and process of preparing
CA2378464A1 (en) 2000-03-16 2001-09-20 San-Ei Gen F.F.I., Inc. Fading inhibitors
CN1276954C (zh) 2000-05-26 2006-09-27 三荣源有限公司 脱臭的十字花科植物色素
US6572900B1 (en) 2000-06-09 2003-06-03 Wm. Wrigley, Jr. Company Method for making coated chewing gum products including a high-intensity sweetener
ATE323744T1 (de) 2001-07-26 2006-05-15 Hansens Lab Lebensmittelfärbende substanzen auf anthocyaninbasis
US6881430B2 (en) 2001-07-26 2005-04-19 Chr. Hansen A/S Food coloring substances and method for their preparation
JP4590034B2 (ja) 2002-01-31 2010-12-01 三菱商事フードテック株式会社 硬質糖衣製剤、糖衣液及び硬質糖衣製剤の製造方法
WO2003064538A1 (en) * 2002-02-01 2003-08-07 San-Ei Gen F.F.I., Inc. Purified purple corn color and method of preparing the same
DE10227151B4 (de) 2002-06-18 2007-03-15 Wild Flavors Berlin Gmbh & Co. Kg Extrakt aus Nebenprodukten der Nussverarbeitung, Verfahren zu dessen Herstellung und dessen Verwendung
US7378118B2 (en) 2002-08-14 2008-05-27 Wm. Wrigley Jr. Company Methods for manufacturing coated confectionary products
US20040105919A1 (en) 2002-12-02 2004-06-03 Mars, Incorporated Processing system having a process injection apparatus
WO2005007088A2 (en) * 2003-07-03 2005-01-27 Unibar Corporation Stabilized anthocyanin extract from garcinia indica
US7279189B2 (en) 2004-07-02 2007-10-09 Colormaker, Inc. Stabilized natural blue and green colorants
EP2484773A3 (en) 2004-07-10 2015-01-21 The Research Foundation of State University of New York Process for producing anthocyanins
CN102864195B (zh) 2004-10-29 2014-11-12 三得利控股株式会社 利用编码花色苷3′位芳香族酰基转移酶的基因的花色苷色素稳定化和蓝化方法
WO2006066389A1 (en) 2004-12-22 2006-06-29 Colarôme Inc. Natural water-insoluble encapsulation compositions and processes for preparing same
RU2302423C2 (ru) * 2005-06-10 2007-07-10 Закрытое акционерное общество "Научно-производственное объединение "ТЕХКОН" Способ выделения биологически активных антоцианов
WO2008111589A1 (ja) * 2007-03-12 2008-09-18 National University Corporation Kagawa University 精製アントシアニンの製造方法
FR2914311B1 (fr) 2007-03-28 2011-02-11 Diana Naturals Modification de la nuance colorante d'anthocyanes pour l'obtention de substances colorantes
EP2070422A1 (en) 2007-12-05 2009-06-17 Südzucker Aktiengesellschaft Mannheim/Ochsenfurt Confectionery products promoting dental health
US8575334B2 (en) 2008-02-06 2013-11-05 The Ohio State University Research Foundation High-purity fractionation of anthocyanins from fruits and vegetables
US8557319B2 (en) 2008-03-28 2013-10-15 Wild Flavors, Inc. Stable natural color process, products and use thereof
FR2930557B1 (fr) 2008-04-29 2013-08-30 Lvmh Rech Matieres colorantes d'origine vegetale et leur utilisation pour colorer des compositions, en particulier des compositions cosmetiques
US20090298952A1 (en) 2008-05-07 2009-12-03 Brimmer Karen S Platable soluble dyes
US8642340B2 (en) 2008-12-18 2014-02-04 Dianaplantsciences, Inc. Plant cell culture for production of natural products with reduced glucosinolate contamination
PL2385766T3 (pl) 2009-01-07 2018-07-31 Chr. Hansen Natural Colors A/S Kompozycja zawierająca węglan wapnia jako biały pigment
WO2010114568A1 (en) * 2009-04-03 2010-10-07 Dianaplantsciences, Inc. Methods for creating color variation in anthocyanins produced by cell culture
GB0908397D0 (en) 2009-05-15 2009-06-24 Univ Leeds Natural hair dyes
WO2011065977A1 (en) 2009-11-25 2011-06-03 Sensient Colors Inc. Natural blue-shade colorants and methods of making and using same
US9427007B2 (en) 2010-11-05 2016-08-30 Chr. Hansen Natural Colors A/S Multiple emulsions for colorants
US20130165531A1 (en) * 2011-06-13 2013-06-27 E.P.C. (Beijing) Plant Pharmaceutical Technology Co., Ltd. Anthocyanin based colorant compositions
EP2545787B1 (de) 2011-07-11 2016-04-13 RUDOLF WILD GmbH & CO. KG Anthocyanhaltige Zusammensetzung
BR112014000838A2 (pt) 2011-07-15 2017-02-14 Nestec Sa grau alimentício de encapsulado azul e processo para produção do mesmo
WO2013106179A1 (en) 2011-12-19 2013-07-18 Sensient Colors Llc Color compositions and methods of making color compositions comprising starch as a matrix
US20130184359A1 (en) 2012-01-13 2013-07-18 Karim Nafisi-Movaghar Processes for Extracting Colors from Hibiscus Plants
EP2882306A1 (en) 2012-08-09 2015-06-17 Nestec S.A. Anthocyanin colouring composition
HK1214835A1 (zh) 2013-03-15 2016-08-05 马斯公司 含花青素苷的天然蓝色着色剂
GB2527453B (en) 2013-03-15 2017-03-15 Mars Inc Method of isolating blue anthocyanin fractions
CA2903474C (en) 2013-03-15 2021-04-20 Mars, Incorporated Stabilization of natural blue anthocyanin-containing colorants and products made

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20040022904A1 (en) * 2002-07-31 2004-02-05 Mars Incorporated Novel confectionery composition
WO2009100165A2 (en) * 2008-02-06 2009-08-13 The Ohio State University Research Foundation High-purity fractionation of anthocyanins from fruits and vegetables
WO2012043173A1 (ja) * 2010-09-27 2012-04-05 理研ビタミン株式会社 クチナシ青色素の製造方法

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
Improved high performance liquid chromatographic separation of anthocyanin compounds from grapes using a novel mixed-mode ion-exchange reversed-phase column;Jason L. McCallum et.al;《Journal of Chromatography A》;20070302;第1148卷(第1期);38-45 *

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Publication number Publication date
EP2986675A2 (en) 2016-02-24
US20170204269A1 (en) 2017-07-20
EP2986675B1 (en) 2016-10-05
GB201517443D0 (en) 2015-11-18
CA2904650A1 (en) 2014-09-25
GB2527453B (en) 2017-03-15
RU2015144064A (ru) 2017-04-27
CA2904650C (en) 2016-07-12
GB2527453A (en) 2015-12-23
BR112015021402A2 (https=) 2017-08-22
US10119029B2 (en) 2018-11-06
AU2014239875A1 (en) 2015-11-05
BR112015021402B1 (pt) 2021-11-03
RU2629257C2 (ru) 2017-08-28
BR112015021402A8 (pt) 2021-09-08
WO2014152417A2 (en) 2014-09-25
AU2014239875B2 (en) 2016-02-04
JP5981675B2 (ja) 2016-08-31
US20160017150A1 (en) 2016-01-21
JP2016519177A (ja) 2016-06-30
MX2015011349A (es) 2016-06-06
HK1215040A1 (zh) 2016-08-12
WO2014152417A3 (en) 2014-11-20
CN105229084A (zh) 2016-01-06
US9598581B2 (en) 2017-03-21
MX362026B (es) 2019-01-04

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