CN105132161A - Tomato glycerol triacetate extract and application thereof in cigarettes - Google Patents
Tomato glycerol triacetate extract and application thereof in cigarettes Download PDFInfo
- Publication number
- CN105132161A CN105132161A CN201510336339.3A CN201510336339A CN105132161A CN 105132161 A CN105132161 A CN 105132161A CN 201510336339 A CN201510336339 A CN 201510336339A CN 105132161 A CN105132161 A CN 105132161A
- Authority
- CN
- China
- Prior art keywords
- tomato
- extract
- cigarette
- glycerol triacetate
- glycerine triacetate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Preparation Of Fruits And Vegetables (AREA)
Abstract
The invention discloses a tomato glycerol triacetate extract and an application thereof in cigarettes. The tomato glycerol triacetate extract is prepared by the steps: washing cleanly fresh ripe tomatoes, draining, pounding into a paste as a raw material, taking glycerol triacetate as an extraction agent, firstly, extracting by a heating reflux method, and extracting by ultrasonic waves to prepare the tomato glycerol triacetate extract. With glycerol triacetate as a solvent, the extract is made into a solution with the concentration of 2-4%, the solution is evenly sprayed onto filter rod tows with the proportion of 7-9% of the weight of the acetate fiber tows, then cigarette filter rods are prepared, and the cigarettes having the filter rods containing tomato effective ingredients are prepared through a conventional cigarette rolling process. The extract can significantly enhance the smoke fresh and sweet feeling, is harmonious and rich in smoke incense, has irritation and miscellaneous odor reduced, and improves the quality of smoking. The tomato glycerol triacetate extract has the advantages of simple production process, strong operability and normalization, easily available raw materials, low cost, easy realization of industrialized production, and good application prospect.
Description
Technical field
The invention belongs to cigarette material technical field, be specifically related to a kind of tomato glycerine triacetate extract.Meanwhile, the invention still further relates to the described application of tomato glycerine triacetate extract in cigarette.
Background technology
Tomato is one of fruits and vegetables of enriching the most of nutrition, and its taste is sour, sweet, cold nature, has and relieves heat and thirst, the cool blood of yin-nourishing, the effect promoted the production of body fluid to quench thirst.Containing abundant Lyeopene and each biostearin in tomato, the synergy of the two makes it have good resistance of oxidation and bacteriostasis.Also containing the volatile component that a large amount of amino acid, organic acid, carotene, recuding sugars and compositions is nitrogenous compound and ester compound in tomato, there is special fragrance.The scholar of Germany detects 54 kinds of aroma volatile by instrument and organoleptic analysis from tomato.
Increasing natural phant is processed to smoking material and doses in cigarette, to reach the effect improving cigarette odor-absorbing He enrich cigarette flavor.Organic acid, monose, polysaccharide and multivitamin, lipid acid, Lyeopene and-carotene etc. that tomato is rich in are of value to the mouthfeel of cigarette and the health of smoker, cigarette can be made the adding of tomato fragrantly fine and smoothly to coordinate, flue gas is soft, assorted gas and pungency reduces, the sweet sense increase of flue gas.Meanwhile, the fragrance of tomato is fresh and clean, harmonious mellow, can coordinate to increase the fine and smooth sweet sense of flue gas with cigarette perfume simultaneously, improve organoleptic quality and flue gas suction taste.
Along with smoking and healthy problem more and more receive publicity, the tar content of Chinese-style cigarette is progressively reduced.But cigarette tar content reduction also can bring cigarette nature fragrance and sweet sense inevitably to lose, for this reason, how while coke tar in cigarette reduces, to promote cigarette nature fragrance and sweet sense, become the focus that each tobacco productive corporation is researched and developed.Effectively can improve cigarette smoking quality by perfuming cigarette is reinforced, but there is again certain deficiency in this mode, and by adding some in filter stick, there is flavouring, increasing the additive of sweet effect and become the more potential compensation application mode of one.Research worker has carried out some correlative study work, and has applied for patent.The such as application of moringa seeds extract in cigarette filter rod and cigarette filter rod (CN103271441A) thereof, a kind of filter stick fiber base material additive and application (CN103126073A) reducing tar content in main cigarette stream smoke, a kind of cool taste mint type cigarette filter stick additive preparation method and application (CN104161303A) thereof, additive of cigarette filter stick and its preparation method and application (CN102860582A) etc., but the filter stick additive described in above-mentioned patent mainly first by extract or allocate additive again in glycerine triacetate dissolve add in cigarette, or the additive some being insoluble in glycerine triacetate is applied directly in cigarette filter rod.On the one hand, there is complicated process of preparation in this interpolation application mode, the dissolving power of glycerine triacetate to additive is limited, much to cigarette, there is flavouring, increase the defect that the additive of sweet effect is difficult to be dissolved in glycerine triacetate, limit the application of spices in cigarette filter rod.On the other hand, if be not that medium carries out filter stick perfuming by glycerine triacetate, but additive is applied directly in cigarette filter rod, larger difficulty can be brought, significantly increase production cost to production of cigarettes, be unfavorable for applying on a large scale.For the problems referred to above, how to adopt suitable Technology, preparation is applicable to the additive of cigarette filter stick of Production requirement, to meet the demand of tobacco industry in cigarette flavouring, harm reduction, just becomes the technical barrier that this area waits to solve.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, there is provided a kind of Fructus Lycopersici esculenti extract prepared using glycerine triacetate as extraction agent, this extract is applied to cigarette can effectively strengthen cigarette sweet moisture feeling and exquisiteness, and cigarette perfume increases, pungency and assorted gas alleviate, and comfortableness promotes.
The present invention also aims to provide the described embody rule of tomato glycerine triacetate extract in production of cigarettes.
Object of the present invention is achieved by following technical proposals.
* except as otherwise noted, the percentage ratio adopted in the present invention is mass percent.
A kind of tomato glycerine triacetate extract, is obtained by the method for following steps:
(1) tomato of fresh mature is cleaned, drains, smash into pasty state to pieces, for subsequent use;
(2) take 5 ~ 10 parts of tomato purees by weight and be placed in round-bottomed flask, add 20 ~ 50 parts of glycerol triacetate for tobacco as extraction agent, soaking at room temperature, after 3 ~ 5 hours, carries out refluxing extraction under 50 ~ 100 DEG C of conditions, 4 ~ 8 hours extraction times, to be cooled for subsequent use to room temperature;
(3) step (2) gains are placed in ultrasonic extraction equipment, under 300 ~ 700W, 40kHZ condition, extract 20 ~ 55 minutes, cross the settled solution obtained after filtering filter residue and be required tomato glycerine triacetate extract.
The described application of tomato glycerine triacetate extract in cigarette, it is characterized in that: take glycerine triacetate as solvent, described tomato glycerine triacetate extract is mixed with the solution that concentration is 2 ~ 4%, be sprayed onto on tow by the ratio uniform of acetate silk weight 7 ~ 9%, make cigarette filter rod, and this filter stick is applied to cigarette.
Compared with prior art, the present invention has the following advantages:
1. the tomato glycerine triacetate extract prepared by the present invention, can dissolve each other in any proportion with glycerine triacetate, extract can be uniformly distributed in filter stick tow, solves the limited or undissolvable problem of dissolving that tomato exists by prior art when filter stick additive is mixed and is fitted in softening agent.
2. adopt glycerine triacetate to be that extraction agent extracts filter stick additive, can not have a negative impact to the security of cigarette, the effective efficiency composition being dissolved in glycerine triacetate in tomato fully can be extracted, avoid adopt other solvent carry out extracting again redissolve to glycerine triacetate time, the loss of effective efficiency composition.
3. gained tomato glycerine triacetate extract effectively can give prominence to the fresh and sweet note of cigarette, increase cigarette cigarette is fragrant, has abirritate and assorted gas simultaneously, promotes effect of organoleptic quality.
4. material used herein is food grade, has higher safety in utilization.
5. production technique of the present invention is simple, operability and standardization strong, raw material is easy to get, with low cost, is convenient to realize suitability for industrialized production, has a good application prospect.
Embodiment
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is described in further detail.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not limited to the technical solution.
Embodiment 1
The tomato of fresh mature is cleaned, drains, smash to pieces and make pasty state, take 5 parts of tomato purees according to weight part and be placed in round-bottomed flask, add 30 parts of glycerol triacetate for tobacco as extraction agent, soaking at room temperature is after 5 hours, refluxing extraction is carried out under 60 DEG C of conditions, extraction time is 8 hours, to be cooledly to room temperature, the tomato after described refluxing extraction and glycerine triacetate are placed in ultrasonic extraction equipment (400W, 40kHZ), extract 25 minutes, cross the settled solution obtained after filtering filter residue, be required tomato glycerine triacetate extract.
Take glycerine triacetate as solvent, described tomato glycerine triacetate extract is mixed with the solution that concentration is 2%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 8%, make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains tomato effective constituent.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the cigarette of adding above-mentioned tomato glycerine triacetate extract is mixed, and gas weakens, pungency reduces, and fresh and sweet note shows, pleasant impression and comfortableness are improved.
Embodiment 2
The tomato of fresh mature is cleaned, drains, smash to pieces and make pasty state, take 6 parts of tomato purees according to weight part and be placed in round-bottomed flask, add 40 parts of glycerol triacetate for tobacco as extraction agent, soaking at room temperature is after 4 hours, refluxing extraction is carried out under 80 DEG C of conditions, extraction time is 5 hours, to be cooledly to room temperature, the tomato after described refluxing extraction and glycerine triacetate are placed in ultrasonic extraction equipment (700W, 40kHZ), extract 20 minutes, cross after filtering filter residue and obtain settled solution, required tomato glycerine triacetate extract can be obtained.
Take glycerine triacetate as solvent, tomato glycerine triacetate extract is mixed with the solution that concentration is 3%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7.5%, make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains tomato effective constituent.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the cigarette pungency and the assorted gas that add above-mentioned tomato glycerine triacetate extract alleviate, and the cigarette of fresh and sweet sense is fragrant significantly to be increased, and oral cavity is residual obviously improves with comfort level.
Embodiment 3
The tomato of fresh mature is cleaned, drains, smash to pieces and make pasty state, take 8 parts of tomato purees according to weight part and be placed in round-bottomed flask, add 32 parts of glycerol triacetate for tobacco as extraction agent, soaking at room temperature is after 5 hours, refluxing extraction is carried out under 70 DEG C of conditions, extraction time is 6 hours, to be cooledly to room temperature, the tomato after described refluxing extraction and glycerine triacetate are placed in ultrasonic extraction equipment (500W, 40kHZ), extract 50 minutes, cross after filtering filter residue and obtain settled solution, required tomato glycerine triacetate extract can be obtained.
Take glycerine triacetate as solvent, tomato glycerine triacetate extract is mixed with the solution that concentration is 4%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7% and make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains tomato effective constituent.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the cigarette pungency and the assorted gas that add above-mentioned tomato glycerine triacetate extract alleviate, and sweet sense is obvious, and the fragrant rich increase of cigarette, comfort level obviously promotes.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any amendments done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.
Claims (2)
1. a tomato glycerine triacetate extract, is obtained by the method for following steps:
(1) tomato of fresh mature is cleaned, drains, smash into pasty state to pieces, for subsequent use;
(2) take 5 ~ 10 parts of tomato purees by weight and be placed in round-bottomed flask, add 20 ~ 50 parts of glycerol triacetate for tobacco as extraction agent, soaking at room temperature, after 3 ~ 5 hours, carries out refluxing extraction under 50 ~ 100 DEG C of conditions, 4 ~ 8 hours extraction times, to be cooled for subsequent use to room temperature;
(3) step (2) gains are placed in ultrasonic extraction equipment, under 300 ~ 700W, 40kHZ condition, extract 20 ~ 55 minutes, cross the settled solution obtained after filtering filter residue and be required tomato glycerine triacetate extract.
2. the application of tomato glycerine triacetate extract according to claim 1 in cigarette, it is characterized in that: take glycerine triacetate as solvent, described tomato glycerine triacetate extract is mixed with the solution that concentration is 2 ~ 4%, be sprayed onto on tow by the ratio uniform of acetate silk weight 7 ~ 9%, make cigarette filter rod, and this filter stick is applied to cigarette.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510336339.3A CN105132161A (en) | 2015-06-17 | 2015-06-17 | Tomato glycerol triacetate extract and application thereof in cigarettes |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510336339.3A CN105132161A (en) | 2015-06-17 | 2015-06-17 | Tomato glycerol triacetate extract and application thereof in cigarettes |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105132161A true CN105132161A (en) | 2015-12-09 |
Family
ID=54717740
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510336339.3A Pending CN105132161A (en) | 2015-06-17 | 2015-06-17 | Tomato glycerol triacetate extract and application thereof in cigarettes |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105132161A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101199363A (en) * | 2007-11-13 | 2008-06-18 | 广西中烟工业公司 | Additive agent for reducing harmful constituents in flue gas and method for preparing same |
| CN103960764A (en) * | 2014-05-15 | 2014-08-06 | 嘉兴市得百科新材料科技有限公司 | Tobacco flavor containing Virginia tobacco extract and preparing method thereof |
| CN104087414A (en) * | 2014-07-28 | 2014-10-08 | 嘉兴市得百科新材料科技有限公司 | Electronic cigarette liquid with blueberry flavor and preparation method thereof |
-
2015
- 2015-06-17 CN CN201510336339.3A patent/CN105132161A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101199363A (en) * | 2007-11-13 | 2008-06-18 | 广西中烟工业公司 | Additive agent for reducing harmful constituents in flue gas and method for preparing same |
| CN103960764A (en) * | 2014-05-15 | 2014-08-06 | 嘉兴市得百科新材料科技有限公司 | Tobacco flavor containing Virginia tobacco extract and preparing method thereof |
| CN104087414A (en) * | 2014-07-28 | 2014-10-08 | 嘉兴市得百科新材料科技有限公司 | Electronic cigarette liquid with blueberry flavor and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 中国科学技术学会: "《2009-2010烟草科学与技术学科发展报告》", 30 April 2010, 中国科学技术出版社 * |
| 杨玉芳等: "番茄提取物分析及其在卷烟加香中的应用", 《应用化工》 * |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106820251A (en) | A kind of herbal tea cigarette | |
| CN104450192A (en) | Tobacco flavor prepared by taking fructus terminaliae immaturus, dendrobium nobile, tobacco and the like as raw materials and application thereof | |
| CN108004023A (en) | Iris extract and its application in cigarette | |
| CN105105320A (en) | Moisture preserving and aroma enhancing tobacco flavor, and preparation method and application thereof | |
| CN109156895A (en) | A kind of reduction cigarette smoking dry sensation and irritating filter stick additive, preparation method and the usage | |
| CN101637303A (en) | Lemon extract, preparation method thereof and application thereof in cigarette flavoring | |
| CN105011363A (en) | Jujube glycerol triacetate extract and application thereof to cigarette | |
| CN108968136B (en) | Herbal tobacco composition, smoking segment and heating non-combustible cigarette rod | |
| CN105029700A (en) | Plant composite glycerol triacetate extract and application thereof in cigarettes | |
| CN104263517A (en) | Tobacco flavor prepared from black tomato, lavender and tobacco and application of tobacco flavor | |
| CN105011368A (en) | Glycerol triacetate extract of momordica grosvenori and application thereof to cigarette | |
| CN104694254B (en) | Red ginseng extract and its preparation method and application | |
| CN103462214A (en) | Method for improving quality of tobacco leaves by adding glucose, citric acid and vegetable hydrated protein | |
| CN105132162A (en) | Dendrobe glycerol triacetate extract and application thereof in cigarettes | |
| CN105029699A (en) | Mint glycerol triacetate extract and application thereof in cigarette | |
| CN110358630A (en) | A kind of clear spicy tobacco aromaticss, preparation method and the application in cigarette | |
| CN105132161A (en) | Tomato glycerol triacetate extract and application thereof in cigarettes | |
| CN110122921A (en) | A kind of preparation method of the quick-fried pearl of black tea | |
| CN104687243A (en) | Natural compound humectant with cigarette sensory humectation function | |
| CN105029696A (en) | Black tea glycerol triacetate extract and application thereof in cigarettes | |
| CN105132163A (en) | Moringa seed glycerol triacetate extract and application thereof in cigarettes | |
| CN104830534B (en) | A kind of preparation method of tomato extract and its application in production of cigarettes | |
| CN105011362A (en) | Glyceryl triacetate extract of Chinese hawthorn fruit and application thereof to cigarette | |
| CN104974850A (en) | Plum glyceryl triacetate extract and application thereof in cigarettes | |
| CN103184100A (en) | Method for extracting and preparing tobacco flavors by using pistacia weinmannifolia |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20151209 |