CN104974850A - Plum glyceryl triacetate extract and application thereof in cigarettes - Google Patents
Plum glyceryl triacetate extract and application thereof in cigarettes Download PDFInfo
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- CN104974850A CN104974850A CN201510336648.0A CN201510336648A CN104974850A CN 104974850 A CN104974850 A CN 104974850A CN 201510336648 A CN201510336648 A CN 201510336648A CN 104974850 A CN104974850 A CN 104974850A
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Abstract
The invention discloses a plum glyceryl triacetate extract and the application thereof in cigarettes. Plums of which kernels are removed are used as raw materials, fruit flesh is made into fruit paste, the made fruit paste is placed in a round-bottomed flask, glyceryl triacetate is used as an extractant, firstly extraction is performed in a heating regurgitation manner, and then ultrasonic extraction is performed so as to obtain the plum glyceryl triacetate extract. The extract is compounded into a solution of which the concentration is 2-5% by using glyceryl triacetate as a solvent, the solution is uniformly sprayed to filter stick tows according to the proportion being 7-8% of the weight of acetate fiber tows, cigarette filter sticks are made, and the cigarettes of which the filter sticks contain effective components of the plums are made through a conventional cigarette rolling and connecting process. The extract can give fresh natural acid fragrance and fruity fragrance to the cigarettes, the smoke of the cigarettes promotes salivation and is sweet after taste, the miscellaneous gas and the aftertaste are improved, and the sucking quality of the cigarettes is improved. The plum glyceryl triacetate extract disclosed by the invention has the advantages that the production technology is simple, the operability and the normalization are strong, the raw materials are easy to obtain, the cost is low, industrial production is convenient to realize, and the plum glyceryl triacetate extract has a favorable application prospect.
Description
Technical field
The invention belongs to cigarette material technical field, be specifically related to a kind of plum glycerine triacetate extract.Meanwhile, the invention still further relates to the described application of plum glycerine triacetate extract in cigarette.
Background technology
Plum is flat, taste is sweet, sour, has in acid with sweet fragrance.Plum extract contains the organic acids such as abundant citric acid and oxysuccinic acid and multivitamin and fatty oil, mineral substance, can alleviate, Ginseng Extract; Also containing multiple materials useful to human body such as flavone glycoside, triterpenoid saponin, polyphenol and alkene.Organic acid contained by plum is the natural organic acids such as citric acid, oxysuccinic acid, Weibull, bitter folic acid, succsinic acid, tartrate mainly, there is multiple physiological regulation function, the main composition of plum, have promote the production of body fluid to quench thirst, preventing phlegm from forming and stopping coughing, the cool blood of hemostasis, anti-inflammatory analgetic, removing blood rubbish, delay senility, antibacterial and antineoplastic action.Plum juice was put in cigarette shreds in the past and had obvious castering action, but also negative impact served by band simultaneously, the residue that the pectin contained in such as plum and protein produce in cigarette burning process, make lingual surface has the astringent sense of trace and particulate state to remain, bring to cigarette and bad suck mouthfeel.
Along with smoking and healthy problem more and more receive publicity, the tar content of Chinese-style cigarette is progressively reduced.But cigarette tar content reduction also can bring cigarette nature fragrance and sweet sense inevitably to lose, for this reason, how while coke tar in cigarette reduces, to promote cigarette nature fragrance and sweet sense, become the focus that each tobacco productive corporation is researched and developed.Effectively can improve cigarette smoking quality by perfuming cigarette is reinforced, but there is again certain deficiency in this mode, and by adding some in filter stick, there is flavouring, increasing the additive of sweet effect and become the more potential compensation application mode of one.Research worker has carried out some correlative study work, and has applied for patent.The such as application of moringa seeds extract in cigarette filter rod and cigarette filter rod (CN 103271441A) thereof, a kind of filter stick fiber base material additive and application (CN 103126073A) reducing tar content in main cigarette stream smoke, a kind of cool taste mint type cigarette filter stick additive preparation method and application (CN 104161303 A) thereof, additive of cigarette filter stick and its preparation method and application (CN102860582 A) etc., but the filter stick additive described in above-mentioned patent mainly first by extract or allocate additive again in glycerine triacetate dissolve add in cigarette, or the additive some being insoluble in glycerine triacetate is applied directly in cigarette filter rod.On the one hand, there is complicated process of preparation in this interpolation application mode, the dissolving power of glycerine triacetate to additive is limited, much to cigarette, there is flavouring, increase the defect that the additive of sweet effect is difficult to be dissolved in glycerine triacetate, limit the application of spices in cigarette filter rod.On the other hand, if be not that medium carries out filter stick perfuming by glycerine triacetate, but additive is applied directly in cigarette filter rod, larger difficulty can be brought, significantly increase production cost to production of cigarettes, be unfavorable for applying on a large scale.For the problems referred to above, how to adopt suitable Technology, preparation is applicable to the additive of cigarette filter stick of Production requirement, to meet the demand of tobacco industry in cigarette flavouring, harm reduction, just becomes the technical barrier that this area waits to solve.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, a kind of plum extract prepared using glycerine triacetate as extraction agent is provided, this extract is applied to cigarette and can gives the pure and fresh acid of cigarette fragrant and fruital, flue gas sophistication and promote, and promotes the production of body fluid back sweet, mix gas and pleasant impression improvement in oral cavity.
The present invention also aims to provide the described embody rule of plum glycerine triacetate extract in production of cigarettes.
Object of the present invention is achieved by following technical proposals.
* except as otherwise noted, the percentage ratio adopted in the present invention is mass percent.
A kind of plum glycerine triacetate extract, is obtained by the method for following steps:
(1) by after plum stoning, pulp smashs into puree to pieces, for subsequent use;
(2) take 5 ~ 10 portions of plum purees according to weight part and be placed in round-bottomed flask, add 30 ~ 60 parts of glycerol triacetate for tobacco as extraction agent, soaking at room temperature, after 4 ~ 7 hours, carries out refluxing extraction under 60 ~ 100 DEG C of conditions, 5 ~ 8 hours extraction times, to be cooled for subsequent use to room temperature;
(3) step (2) gains are placed in ultrasonic extractor, under 400 ~ 700W, 40kHZ condition, extract 20 ~ 55 minutes, cross the settled solution obtained after filtering filter residue and be required plum glycerine triacetate extract.
The described application of plum glycerine triacetate extract in cigarette, it is characterized in that: take glycerine triacetate as solvent, described plum glycerine triacetate extract is mixed with the solution that concentration is 2 ~ 5%, be sprayed onto on tow by the ratio uniform of acetate silk weight 7 ~ 8%, make cigarette filter rod, and this filter stick is applied to cigarette.
Compared with prior art, the present invention has the following advantages:
1. the plum glycerine triacetate extract prepared by the present invention, can dissolve each other in any proportion with glycerine triacetate, extract can be uniformly distributed in filter stick tow, solves the limited or undissolvable problem of dissolving that plum exists by prior art when filter stick additive is mixed and is fitted in softening agent.
2. adopt glycerine triacetate to be that extraction agent extracts filter stick additive, can not have a negative impact to the security of cigarette, the effective efficiency composition being dissolved in glycerine triacetate in plum fully can be extracted, avoid adopt other solvent carry out extracting again redissolve to glycerine triacetate time, the loss of effective efficiency composition.
3. gained plum glycerine triacetate extract can be given the pure and fresh acid of cigarette fragrant and fruital, flue gas sophistication and promotes, and promotes the production of body fluid back sweet, mix gas and pleasant impression improvement in oral cavity.
4. material used herein is food grade, has higher safety in utilization.
5. production technique of the present invention is simple, operability and standardization strong, raw material is easy to get, with low cost, is convenient to realize suitability for industrialized production, has a good application prospect.
Embodiment
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is described in further detail.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not limited to the technical solution.
Embodiment 1
After plum stoning, with stamp mill, pulp is made puree, take 5 portions of plum purees by weight and be placed in round-bottomed flask, add 30 parts of glycerol triacetate for tobacco as extraction agent, soaking at room temperature is after 7 hours, refluxing extraction is carried out under 60 DEG C of conditions, extraction time is 8 hours, to be cooledly to room temperature, the plum after described refluxing extraction and glycerine triacetate are placed in ultrasonic extraction equipment (400W, 40kHZ), extract 25 minutes, cross after filtering filter residue and obtain settled solution, be required plum glycerine triacetate extract.
Take glycerine triacetate as solvent, plum glycerine triacetate extract is mixed with the solution that concentration is 2%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 8%, make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains plum effective constituent.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the cigarette flue gas adding above-mentioned plum glycerine triacetate extract promotes the production of body fluid back obviously sweet, and increase fruital and the fragrant note of acid, flue gas sophistication promotes to some extent, and pleasant impression improves.
Embodiment 2
After plum stoning, with stamp mill, pulp is made puree, take 8 parts of plum particles by weight and be placed in round-bottomed flask, add 45 parts of glycerol triacetate for tobacco as extraction agent, soaking at room temperature is after 4 hours, refluxing extraction is carried out under 80 DEG C of conditions, extraction time is 5 hours, to be cooledly to room temperature, the plum after described refluxing extraction and glycerine triacetate are placed in ultrasonic extraction equipment (600W, 40kHZ), extract 20 minutes, cross after filtering filter residue and obtain settled solution, required plum glycerine triacetate extract can be obtained.
Take glycerine triacetate as solvent, plum glycerine triacetate extract is mixed with the solution that concentration is 3%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7.5%, make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains plum effective constituent.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the cigarette flue gas adding above-mentioned plum glycerine triacetate extract sweet sense of promoting the production of body fluid back strengthens, and flue gas sophistication increases, and fragrant pure and fresh elegant, the pleasant impression of cigarette and assorted gas obviously improve.
Embodiment 3
After plum stoning, with stamp mill, pulp is made puree, take 10 parts of plum particles by weight and be placed in round-bottomed flask, add 40 parts of glycerol triacetate for tobacco as extraction agent, soaking at room temperature is after 7 hours, refluxing extraction is carried out under 80 DEG C of conditions, extraction time is 8 hours, to be cooledly to room temperature, the plum after described refluxing extraction and glycerine triacetate are placed in ultrasonic extraction equipment (700W, 40kHZ), extract 55 minutes, cross after filtering filter residue and obtain settled solution, required plum glycerine triacetate extract can be obtained.
Take glycerine triacetate as solvent, plum glycerine triacetate extract is mixed with the solution that concentration is 4%, be sprayed onto on filter stick tow by the ratio uniform of acetate silk weight 7% and make cigarette filter rod, make by the cigarette seaming operation of routine the cigarette that filter stick contains plum effective constituent.Analyses Methods for Sensory Evaluation Results shows: compared with the control, and the cigarette flue gas adding above-mentioned plum glycerine triacetate extract sweet sense of promoting the production of body fluid is obvious, the fragrant rich increase of cigarette, has the fragrant and fruital of acid, and sophistication promotes, and assorted gas and pleasant impression improve.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any amendments done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.
Claims (2)
1. a plum glycerine triacetate extract, is obtained by the method for following steps:
(1) by after plum stoning, pulp smashs into puree to pieces, for subsequent use;
(2) take 5 ~ 10 portions of plum purees according to weight part and be placed in round-bottomed flask, add 30 ~ 60 parts of glycerol triacetate for tobacco as extraction agent, soaking at room temperature, after 4 ~ 7 hours, carries out refluxing extraction under 60 ~ 100 DEG C of conditions, 5 ~ 8 hours extraction times, to be cooled for subsequent use to room temperature;
(3) step (2) gains are placed in ultrasonic extractor, under 400 ~ 700W, 40kHZ condition, extract 20 ~ 55 minutes, cross the settled solution obtained after filtering filter residue and be required plum glycerine triacetate extract.
2. the application of plum glycerine triacetate extract according to claim 1 in cigarette, it is characterized in that: take glycerine triacetate as solvent, described plum glycerine triacetate extract is mixed with the solution that concentration is 2 ~ 5%, be sprayed onto on tow by the ratio uniform of acetate silk weight 7 ~ 8%, make cigarette filter rod, and this filter stick is applied to cigarette.
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| CN201510336648.0A CN104974850A (en) | 2015-06-17 | 2015-06-17 | Plum glyceryl triacetate extract and application thereof in cigarettes |
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| CN201510336648.0A CN104974850A (en) | 2015-06-17 | 2015-06-17 | Plum glyceryl triacetate extract and application thereof in cigarettes |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115584297A (en) * | 2022-11-07 | 2023-01-10 | 云南中烟工业有限责任公司 | Preparation method and application of plum fragrance extract |
Citations (5)
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| CN101199363A (en) * | 2007-11-13 | 2008-06-18 | 广西中烟工业公司 | Additive agent for reducing harmful constituents in flue gas and method for preparing same |
| CN103478888A (en) * | 2013-09-09 | 2014-01-01 | 湖南中烟工业有限责任公司 | Chewing tobacco with plum taste |
| CN104188089A (en) * | 2014-08-20 | 2014-12-10 | 云南中烟工业有限责任公司 | Application of green plum extractives in cigarettes |
| CN104305511A (en) * | 2014-08-20 | 2015-01-28 | 云南中烟工业有限责任公司 | Application of spices made of green plums to cigarettes |
| CN104432460A (en) * | 2014-08-20 | 2015-03-25 | 云南中烟工业有限责任公司 | Application of preserved plum extractives in cigarettes |
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2015
- 2015-06-17 CN CN201510336648.0A patent/CN104974850A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101199363A (en) * | 2007-11-13 | 2008-06-18 | 广西中烟工业公司 | Additive agent for reducing harmful constituents in flue gas and method for preparing same |
| CN103478888A (en) * | 2013-09-09 | 2014-01-01 | 湖南中烟工业有限责任公司 | Chewing tobacco with plum taste |
| CN104188089A (en) * | 2014-08-20 | 2014-12-10 | 云南中烟工业有限责任公司 | Application of green plum extractives in cigarettes |
| CN104305511A (en) * | 2014-08-20 | 2015-01-28 | 云南中烟工业有限责任公司 | Application of spices made of green plums to cigarettes |
| CN104432460A (en) * | 2014-08-20 | 2015-03-25 | 云南中烟工业有限责任公司 | Application of preserved plum extractives in cigarettes |
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| Title |
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| 中国科学技术学会: "《2009-2010烟草科学与技术学科发展报告》", 30 April 2010, 中国科学技术出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN115584297A (en) * | 2022-11-07 | 2023-01-10 | 云南中烟工业有限责任公司 | Preparation method and application of plum fragrance extract |
| CN115584297B (en) * | 2022-11-07 | 2024-01-19 | 云南中烟工业有限责任公司 | Preparation method and application of plum extract |
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Application publication date: 20151014 |