CN105030618A - Mouth wash and preparation method thereof - Google Patents
Mouth wash and preparation method thereof Download PDFInfo
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- CN105030618A CN105030618A CN201510530027.6A CN201510530027A CN105030618A CN 105030618 A CN105030618 A CN 105030618A CN 201510530027 A CN201510530027 A CN 201510530027A CN 105030618 A CN105030618 A CN 105030618A
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Abstract
The invention belongs to the field of articles for oral cleaning, and particularly relates to a mouth wash and a preparation method thereof. The mouth wash is prepared from the following components in percent by weight: 10-15% of peony root bark powder solution, 0.5-5% of peony seed oil, 0.1-5% of lemon juice, 0.1-5% of watermelon peel juice, 0.5-5% of green tea, 0.01-0.5% of mint and the balance of water. The mouth wash has the beneficial effects that the mouth wash provided by the invention adopts pure plant raw materials, wherein the peony root bark has the effects of alleviating pain, cooling, resisting allergy, diminishing inflammation, immunizing and the like, the peony seed oil has a unique effect on treating dental ulcer, the green tea has the effects of preventing decayed teeth, protecting teeth and strengthening teeth, the mint and lemon have the effects of resisting bacteria and diminishing inflammation, and the watermelon peel has the effects of preventing and treating mouth and tongue sores, so that the prepared pure plant mouth wash has the effects of safely removing bacteria and refreshing breath.
Description
Technical field
The invention belongs to dental care products field, be specifically related to a kind of collutory and preparation method thereof.
Background technology
Along with the raising of people's quality of life, oral cavity cleaning becomes the important component part of daily life.The common method of current oral cavity cleaning mainly contains two kinds, and one is brushed teeth, and one is gargled.Brush teeth be mainly limited to get up morning after and evening sleep before, gargle, there is conveniently feature.
Collutory kind is a lot of in the market, is mostly chemicals, or the compound recipe of chemicals and Chinese herbal medicine.Due to collutory can be kept at deutostoma intracavity of gargling to remain, can wrongly take and drink in body when even gargling careless, this preparation containing chemical drugs can have side effects to human body, and therefore developing safer collutory new product becomes a kind of trend.
Summary of the invention
In order to solve the problems referred to above that prior art exists, the invention provides a kind of collutory and preparation method thereof.
The technical solution adopted in the present invention is:
A kind of collutory, be made up of following compositions in weight percentage: the root of Paeonia suffruticosa Ardr. corium farinosum solution of 10-15%, the peony seed oil of 0.5-5%, the Fructus Citri Limoniae juice of 0.1-5%, the watermelon husk juice of 0.1-5%, the green tea of 0.5-5%, the Herba Menthae of 0.01-0.5%, surplus is water.Preferably, described root of Paeonia suffruticosa Ardr. corium farinosum solution be root of Paeonia suffruticosa Ardr. corium farinosum water-soluble after, through distilling the distillate that obtains.
Preferably, be made up of following compositions in weight percentage: the root of Paeonia suffruticosa Ardr. corium farinosum solution of 10-15%, the peony seed oil of 1-3%, the Fructus Citri Limoniae juice of 0.5-2%, the watermelon husk juice of 0.5-2%, the green tea of 1-3%, the Herba Menthae of 0.05-0.2%, surplus is water.
Preferably, be made up of following compositions in weight percentage: the root of Paeonia suffruticosa Ardr. corium farinosum solution of 12-15%, the peony seed oil of 1.5-2%, the Fructus Citri Limoniae juice of 0.8-1.5%, the watermelon husk juice of 0.8-1.5%, the green tea of 1.5-2%, the Herba Menthae of 0.08-0.12%, surplus is water
Preferably, be made up of following compositions in weight percentage: the root of Paeonia suffruticosa Ardr. corium farinosum solution of 13%, the peony seed oil of 2%, the Fructus Citri Limoniae juice of 1%, the watermelon husk juice of 1%, the green tea of 2%, the Herba Menthae of 0.1%, surplus is water.
The preparation method of above-mentioned collutory, comprises the steps:
Step 1, the phloem stripping root of Paeonia suffruticosa Ardr. is air-dry, is ground into Powdered, obtains root of Paeonia suffruticosa Ardr. corium farinosum by air-dry root of Paeonia suffruticosa Ardr. phloem, and described root of Paeonia suffruticosa Ardr. corium farinosum is dissolved in water, and carries out vapor distillation, obtains distillate; Preferably that the phloem of root of Paeonia suffruticosa Ardr. is air-dry in air-drying box, air-dry root of Paeonia suffruticosa Ardr. phloem powder beater is ground into Powdered.
Step 2, is added to the water the distillate of gained and peony seed oil, stirs, obtain basal liquid;
Step 3, grinds to form end respectively by green tea and Herba Menthae, adds suitable quantity of water and dissolves, 60-100 DEG C of heating 40-60min, and be cooled to room temperature, filtration, obtains green tea filtrate respectively and Herba Menthae filtrate is for subsequent use;
Step 4, by described filtrate, Fructus Citri Limoniae juice and watermelon husk juice, join in described basal liquid, mix homogeneously, and the polishing that adds water is 100% to total amount, obtains described collutory.
Preferably, in step 1, described root of Paeonia suffruticosa Ardr. corium farinosum be dissolved in water, amount of water is 5-10 times of moutan root bark opaque amount, adds 0.5-1% sodium sulfate and 0.5-1% ethanol, and after leaving standstill, with steam distillation, collect distillate, described percentage ratio is all weight percentage.Select moutan root bark extract to be that collutory prepared by raw material, technique is simple, is easy to operation, can be used in commercial production.
Preferably, in step 4, Fructus Citri Limoniae and Exocarpium Citrulli are put into juice extractor respectively, squeeze juice, obtain Fructus Citri Limoniae juice and watermelon husk juice respectively.
Be rich in paeonol composition in root of Paeonia suffruticosa Ardr. corium farinosum, and paeonol have the effects such as analgesia, antipyretic, antiinflammatory, antibacterial, antioxidation, adds root of Paeonia suffruticosa Ardr. corium farinosum and can play reducing swelling and alleviating pain, prevent and treat dental caries, cover halitosis, the effects such as cleaning oral cavity in collutory of the present invention.
Peony seed oil has good curative effect for treatment oral ulcer.
Fructus Citri Limoniae, Fructus Citri Limoniae contains nicotinic acid and abundant organic acid, and its taste is extremely sour, has the multiple efficacies such as anti-inflammation, removing heat-phlegm, enhancing body immunity.
Exocarpium Citrulli, cool in nature, sweet in the mouth.Clearing away summer-heat is antipyretic, quenches the thirst, diuresis.For skin ulcer raw in summer-heat excessive thirst, oliguria, edema, mouth, tongue, lip.
Green tea, fluorinated volume is higher, belongs to alkaline drink, can suppress the minimizing that human body is calcareous, can tooth protection, hard tooth, has good effect to caries prevention.
Herba Menthae, containing menthol, this material can fresh breath, also has antisepsis and sterilization, diuresis, reduces phlegm, stomach invigorating and the effect such as aid digestion.
Beneficial effect of the present invention is: collutory provided by the invention adopts pure plant material, utilize the effects such as the analgesia of moutan root bark, antipyretic, antiallergic, antiinflammatory, immunity, the special effect of peony seed oil treatment oral ulcer, effect of green tea caries prevention, tooth protection, hard tooth, and the antimicrobial and anti-inflammation efficacy of Herba Menthae and Fructus Citri Limoniae, with effect of Exocarpium Citrulli control aphtha of the mouth and tongue, make in pure plant mouth wash, reach the effect of the degerming and fresh breath of safety.Current collutory is on the market many containing ethanol, use every day alcoholic collutory to there is unsafe factor, and collutory provided by the invention adopt pure plant material, even if after drinking because of carelessness, also can not cause potential safety hazard, the effect of the degerming and fresh breath of safety can be reached.
Accompanying drawing explanation
Fig. 1 is the suppression situation of matched group culture medium to oral cavity bacterium;
Fig. 2 is that the culture medium of the collutory provided containing embodiment 1 is to the suppression situation of oral cavity bacterium;
Fig. 3 is that the culture medium of the collutory provided containing embodiment 4 is to the suppression situation of oral cavity bacterium;
Fig. 4 is that the culture medium of the collutory provided containing embodiment 5 is to the suppression situation of oral cavity bacterium.
Detailed description of the invention
Embodiment 1
The phloem stripping root of Paeonia suffruticosa Ardr. is air-dry in air-drying box, is ground into Powdered, obtains root of Paeonia suffruticosa Ardr. corium farinosum by air-dry root of Paeonia suffruticosa Ardr. phloem powder beater; 50g root of Paeonia suffruticosa Ardr. corium farinosum added in 500ml water and dissolve, 10g adds sodium sulfate and 10ml ethanol, after leaving standstill, with steam distillation, collects distillate 116ml.The distillate of gained and 20g peony seed oil are added to the water, stir, obtain basal liquid.20g green tea and 1g Herba Menthae are ground to form end, adds suitable quantity of water and dissolve, 60-100 DEG C of heating 40-60min, is cooled to room temperature, filters, obtain filtrate for subsequent use; Fructus Citri Limoniae and Exocarpium Citrulli are put into juice extractor respectively, squeeze juice, obtain Fructus Citri Limoniae juice and watermelon husk juice, for subsequent use.By green tea and Herba Menthae filtrate, 10g Fructus Citri Limoniae juice and 10g watermelon husk juice join in described basal liquid, mix homogeneously, and add water polishing, obtain described collutory.
Embodiment 2
The phloem stripping root of Paeonia suffruticosa Ardr. is air-dry in air-drying box, is ground into Powdered, obtains root of Paeonia suffruticosa Ardr. corium farinosum by air-dry root of Paeonia suffruticosa Ardr. phloem powder beater; 45g root of Paeonia suffruticosa Ardr. corium farinosum is added in 300ml water and dissolves, add 5g sodium sulfate and 5ml ethanol, after leaving standstill, with steam distillation, collect distillate 105ml.The distillate of gained and 15g peony seed oil are added to the water, stir, obtain basal liquid.15g green tea and 0.8g Herba Menthae are ground to form end, adds suitable quantity of water and dissolve, 60 DEG C of heating 40min, are cooled to room temperature, filter, obtain filtrate for subsequent use; Fructus Citri Limoniae and Exocarpium Citrulli are put into juice extractor respectively, squeeze juice, obtain Fructus Citri Limoniae juice and watermelon husk juice, for subsequent use.By green tea and Herba Menthae filtrate, 8g Fructus Citri Limoniae juice and 8g watermelon husk juice join in described basal liquid, mix homogeneously, and add water polishing, obtain described collutory.
Embodiment 3
The phloem stripping root of Paeonia suffruticosa Ardr. is air-dry in air-drying box, is ground into Powdered, obtains root of Paeonia suffruticosa Ardr. corium farinosum by air-dry root of Paeonia suffruticosa Ardr. phloem powder beater; 60g root of Paeonia suffruticosa Ardr. corium farinosum is added in 300ml water and dissolves, add 8g sodium sulfate and 6ml ethanol, after leaving standstill, with steam distillation, collect distillate 140ml.The distillate of gained and 20g peony seed oil are added to the water, stir, obtain basal liquid.20g green tea and 1.2g Herba Menthae are ground to form end, adds suitable quantity of water and dissolve, 100 DEG C of heating 60min, are cooled to room temperature, filter, obtain filtrate for subsequent use; Fructus Citri Limoniae and Exocarpium Citrulli are put into juice extractor respectively, squeeze juice, obtain Fructus Citri Limoniae juice and watermelon husk juice, for subsequent use.By green tea and Herba Menthae filtrate, 15g Fructus Citri Limoniae juice and 15g watermelon husk juice join in described basal liquid, mix homogeneously, and add water polishing, obtain described collutory.
Embodiment 4
The phloem stripping root of Paeonia suffruticosa Ardr. is air-dry in air-drying box, is ground into Powdered, obtains root of Paeonia suffruticosa Ardr. corium farinosum by air-dry root of Paeonia suffruticosa Ardr. phloem powder beater; 43g root of Paeonia suffruticosa Ardr. corium farinosum added in 300ml water and dissolve, add sodium sulfate and ethanol, after leaving standstill, with steam distillation, collect distillate, gained distillate accounts for 10% of whole collutory gross mass.The distillate of gained and 10g peony seed oil are added to the water, stir, obtain basal liquid.10g green tea and 0.5g Herba Menthae are ground to form end, adds suitable quantity of water and dissolve, 100 DEG C of heating 40min, are cooled to room temperature, filter, obtain filtrate for subsequent use; Fructus Citri Limoniae and Exocarpium Citrulli are put into juice extractor respectively, squeeze juice, obtain Fructus Citri Limoniae juice and watermelon husk juice, for subsequent use.By green tea and Herba Menthae filtrate, 5g Fructus Citri Limoniae juice and 5g watermelon husk juice join in described basal liquid, mix homogeneously, and add water polishing, obtain described collutory.
Embodiment 5
The phloem stripping root of Paeonia suffruticosa Ardr. is air-dry in air-drying box, is ground into Powdered, obtains root of Paeonia suffruticosa Ardr. corium farinosum by air-dry root of Paeonia suffruticosa Ardr. phloem powder beater; 64g root of Paeonia suffruticosa Ardr. corium farinosum added in 500ml water and dissolve, add 5g sodium sulfate and 5ml ethanol, after leaving standstill, with steam distillation, collect distillate, gained distillate accounts for 15% of whole collutory gross mass.The distillate of gained and 30g peony seed oil are added to the water, stir, obtain basal liquid.30g green tea and 2g Herba Menthae are ground to form end, adds suitable quantity of water and dissolve, 80 DEG C of heating 50min, are cooled to room temperature, filter, obtain filtrate for subsequent use; Fructus Citri Limoniae and Exocarpium Citrulli are put into juice extractor respectively, squeeze juice, obtain Fructus Citri Limoniae juice and watermelon husk juice, for subsequent use.By green tea and Herba Menthae filtrate, 20g Fructus Citri Limoniae juice and 20g watermelon husk juice join in described basal liquid, mix homogeneously, and add water polishing, obtain described collutory.
Embodiment 6
The phloem stripping root of Paeonia suffruticosa Ardr. is air-dry in air-drying box, is ground into Powdered, obtains root of Paeonia suffruticosa Ardr. corium farinosum by air-dry root of Paeonia suffruticosa Ardr. phloem powder beater; 40g root of Paeonia suffruticosa Ardr. corium farinosum is added in 300ml water and dissolves, add 5g sodium sulfate and 8ml ethanol, after leaving standstill, with steam distillation, collect distillate.The distillate of gained and 5g peony seed oil are added to the water, stir, obtain basal liquid.5g green tea and 0.1g Herba Menthae are ground to form end, adds suitable quantity of water and dissolve, 60 DEG C of heating 60min, are cooled to room temperature, filter, obtain filtrate for subsequent use; Fructus Citri Limoniae and Exocarpium Citrulli are put into juice extractor respectively, squeeze juice, obtain Fructus Citri Limoniae juice and watermelon husk juice, for subsequent use.By green tea and Herba Menthae filtrate, 1g Fructus Citri Limoniae juice and 1g watermelon husk juice join in described basal liquid, mix homogeneously, and add water polishing, obtain described collutory.
Embodiment 7
The phloem stripping root of Paeonia suffruticosa Ardr. is air-dry in air-drying box, is ground into Powdered, obtains root of Paeonia suffruticosa Ardr. corium farinosum by air-dry root of Paeonia suffruticosa Ardr. phloem powder beater; 70g root of Paeonia suffruticosa Ardr. corium farinosum is added in 600ml water and dissolves, add 10g sodium sulfate and 9ml ethanol, after leaving standstill, with steam distillation, collect distillate.The distillate of gained and 50g peony seed oil are added to the water, stir, obtain basal liquid.50g green tea and 5g Herba Menthae are ground to form end, adds suitable quantity of water and dissolve, 100 DEG C of heating 60min, are cooled to room temperature, filter, obtain filtrate for subsequent use; Fructus Citri Limoniae and Exocarpium Citrulli are put into juice extractor respectively, squeeze juice, obtain Fructus Citri Limoniae juice and watermelon husk juice, for subsequent use.By green tea and Herba Menthae filtrate, 50g Fructus Citri Limoniae juice and 50g watermelon husk juice join in described basal liquid, mix homogeneously, and add water polishing, obtain described collutory.
The culture medium of the collutory of configuration containing embodiment 1,4,5 gained, and be contrast with distilled water, the present invention is to the effect of the collutory provided to oral cavity bacterium in checking.
1, take Carnis Bovis seu Bubali cream 0.225g, peptone 0.75g, Nacl0.375g, agar 1.5g, distilled water 75ml be heated to boil to agar and dissolve completely, adjustment PH to 7.4-7.6.The culture medium of preparation and clean flat board are placed in high-pressure steam sterilizing pan 121 DEG C, sterilizing 30min.Plate is down flat in sterilizing room superclean bench after suitable cooling.First gargle with distilled water, then after gently scraping oral cavity wall with sterile toothpick, the culture medium of cooled and solidified is rule.The culture medium of inoculation oral cavity bacterium is placed in the calorstat incubated overnight of 37 DEG C.
2, according to the formulated culture medium of table 1, be heated to boil and dissolve completely to agar, adjustment PH to 7.4-7.6, sealing, numbers.Culture medium and the clean flat board of preparation are placed in high-pressure steam sterilizing pan 121 DEG C, sterilizing 30min.Plate is down flat in sterilizing room superclean bench after suitable cooling.
| Carnis Bovis seu Bubali cream/g | Peptone/g | Agar/g | Nacl/g | Distilled water/ml | Collutory/ml | |
| Distilled water | 0.225 | 0.75 | 1.5 | 0.375 | 75 | 0 |
| Embodiment 1 | 0.225 | 0.75 | 1.5 | 0.375 | 65 | 10 |
| Embodiment 4 | 0.225 | 0.75 | 1.5 | 0.375 | 65 | 10 |
| Embodiment 5 | 0.225 | 0.75 | 1.5 | 0.375 | 65 | 10 |
3, after treating culture medium cooling, in culture medium, S line is drawn with the oral cavity bacterium cultivated in inoculating loop picking 1 gently.By the culture medium sealing inoculated, be placed in the calorstat cultivation overnight of 37 DEG C, observe the growing state of oral cavity bacterium in each culture medium.
Matched group and different embodiment collutory culture medium to the suppression situation of oral cavity bacterium as shown in Figures 1 to 4, can be found out collutory provided by the invention, have obvious inhibitory action to oral cavity bacterium from Fig. 1-4.The present invention utilizes the effects such as the analgesia of moutan root bark, antipyretic, antiallergic, antiinflammatory, immunity, the special effect of peony seed oil treatment oral ulcer, effect of green tea caries prevention, tooth protection, hard tooth, and the antimicrobial and anti-inflammation efficacy of Herba Menthae and Fructus Citri Limoniae, with effect of Exocarpium Citrulli control aphtha of the mouth and tongue, make in pure plant mouth wash, reach the effect of the degerming and fresh breath of safety.Current collutory is on the market many containing ethanol, use every day alcoholic collutory to there is unsafe factor, and collutory provided by the invention adopt pure plant material, even if after drinking because of carelessness, also can not cause potential safety hazard, the effect of the degerming and fresh breath of safety can be reached.
The present invention is not limited to above-mentioned preferred forms; anyone can draw other various forms of products under enlightenment of the present invention; no matter but any change is done in its shape or structure; every have identical with the application or akin technical scheme, all drops within protection scope of the present invention.
Claims (8)
1. a collutory, is characterized in that: be made up of following compositions in weight percentage: the root of Paeonia suffruticosa Ardr. corium farinosum solution of 10-15%, the peony seed oil of 0.5-5%, the Fructus Citri Limoniae juice of 0.1-5%, the watermelon husk juice of 0.1-5%, the green tea of 0.5-5%, the Herba Menthae of 0.01-0.5%, surplus is water.
2. collutory according to claim 1, is characterized in that: described root of Paeonia suffruticosa Ardr. corium farinosum solution be root of Paeonia suffruticosa Ardr. corium farinosum water-soluble after, through distilling the distillate that obtains.
3. collutory according to claim 2, it is characterized in that: be made up of following compositions in weight percentage: the root of Paeonia suffruticosa Ardr. corium farinosum solution of 10-15%, the peony seed oil of 1-3%, the Fructus Citri Limoniae juice of 0.5-2%, the watermelon husk juice of 0.5-2%, the green tea of 1-3%, the Herba Menthae of 0.05-0.2%, surplus is water.
4. collutory according to claim 2, it is characterized in that: be made up of following compositions in weight percentage: the root of Paeonia suffruticosa Ardr. corium farinosum solution of 12-15%, the peony seed oil of 1.5-2%, the Fructus Citri Limoniae juice of 0.8-1.5%, the watermelon husk juice of 0.8-1.5%, the green tea of 1.5-2%, the Herba Menthae of 0.08-0.12%, surplus is water.
5. collutory according to claim 2, is characterized in that: be made up of following compositions in weight percentage: the root of Paeonia suffruticosa Ardr. corium farinosum solution of 13%, the peony seed oil of 2%, the Fructus Citri Limoniae juice of 1%, the watermelon husk juice of 1%, the green tea of 2%, the Herba Menthae of 0.1%, surplus is water.
6. according to the preparation method of the collutory one of claim 1-5 Suo Shu, it is characterized in that: comprise the steps:
Step 1, the phloem stripping root of Paeonia suffruticosa Ardr. is air-dry, is ground into Powdered, obtains root of Paeonia suffruticosa Ardr. corium farinosum by air-dry root of Paeonia suffruticosa Ardr. phloem, and described root of Paeonia suffruticosa Ardr. corium farinosum is dissolved in water, and carries out vapor distillation, obtains distillate;
Step 2, is added to the water the distillate of gained and peony seed oil, stirs, obtain basal liquid;
Step 3, grinds to form end respectively by green tea and Herba Menthae, adds suitable quantity of water and dissolves, 60-100 DEG C of heating 40-60min, and be cooled to room temperature, filtration, obtains green tea filtrate respectively and Herba Menthae filtrate is for subsequent use;
Step 4, by described filtrate, Fructus Citri Limoniae juice and watermelon husk juice, join in described basal liquid, mix homogeneously, and the polishing that adds water is 100% to total amount, obtains described collutory.
7. the preparation method of collutory according to claim 6, it is characterized in that: in step 1, described root of Paeonia suffruticosa Ardr. corium farinosum is dissolved in water, amount of water is 5-10 times of moutan root bark opaque amount, add 0.5-1% sodium sulfate and 0.5-1% ethanol, after leaving standstill, with steam distillation, collect distillate, described percentage ratio is all weight percentage.
8. the preparation method of collutory according to claim 6, is characterized in that: in step 4, Fructus Citri Limoniae and Exocarpium Citrulli is put into juice extractor respectively, squeeze juice, obtains Fructus Citri Limoniae juice and watermelon husk juice respectively.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1927160A (en) * | 2006-08-25 | 2007-03-14 | 青岛大学医学院附属医院 | Gargle and its preparing process |
| CN101642422A (en) * | 2009-09-07 | 2010-02-10 | 甘肃中川牡丹研究所 | Poppy tree peony skin-moistening cream and preparation method thereof |
| CN104510918A (en) * | 2013-09-26 | 2015-04-15 | 刘常春 | Traditional Chinese medicine powder capable of curing oral ulcer quickly |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1927160A (en) * | 2006-08-25 | 2007-03-14 | 青岛大学医学院附属医院 | Gargle and its preparing process |
| CN101642422A (en) * | 2009-09-07 | 2010-02-10 | 甘肃中川牡丹研究所 | Poppy tree peony skin-moistening cream and preparation method thereof |
| CN104510918A (en) * | 2013-09-26 | 2015-04-15 | 刘常春 | Traditional Chinese medicine powder capable of curing oral ulcer quickly |
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