CN105030618B - A kind of mouthwash and preparation method thereof - Google Patents
A kind of mouthwash and preparation method thereof Download PDFInfo
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- CN105030618B CN105030618B CN201510530027.6A CN201510530027A CN105030618B CN 105030618 B CN105030618 B CN 105030618B CN 201510530027 A CN201510530027 A CN 201510530027A CN 105030618 B CN105030618 B CN 105030618B
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Abstract
The invention belongs to dental care products field, and in particular to a kind of mouthwash and preparation method thereof.The mouthwash, it is made up by weight percentage of following components：10 15% moutan root bark powder solution, 0.5 5% peony seed oil, 0.1 5% lemon juice, 0.1 5% watermelon husk juice, 0.5 5% green tea, 0.01 0.5% peppermint, surplus is water.Beneficial effects of the present invention are：The mouthwash that invention provides uses pure plant raw material, utilize the effect such as the easing pain of moutan root bark, antipyretic, antiallergy, anti-inflammatory, immune, peony seed oil treats the special effect of canker sore, the effect of pre- anti-caries of green tea, shield tooth, hard tooth, and the antimicrobial and anti-inflammation efficacy of peppermint and lemon, the effect of preventing and treating aphthae with watermelon peel, is made in pure plant mouthwash, reaches the safe degerming and effect of fresh breath.
Description
Technical field
The invention belongs to dental care products field, and in particular to a kind of mouthwash and preparation method thereof.
Background technology
With the improvement of people's life quality, oral cleaning turns into the important component of daily life.Oral cavity is clear at present
Clean common method mainly has two kinds, and one kind is to brush teeth, and one kind is to gargle.Brush teeth be mainly limited to morning get up after and at night sleep
Before feel, and gargling then has the characteristics of convenient and swift.
Gargle various types in the market, are mostly chemicals, or the compound of chemicals and Chinese herbal medicine.
Due to that gargle can be kept to remain in deutostoma intracavitary of gargling, in addition gargle imprudence when can wrongly take drink into vivo, it is this containing chemistry
The preparation of medicine can produce side effect to human body, therefore develop safer mouthwash new product and turn into a kind of trend.
The content of the invention
In order to solve above mentioned problem existing for prior art, the invention provides a kind of mouthwash and preparation method thereof.
The technical solution adopted in the present invention is：
A kind of mouthwash, it is made up by weight percentage of following components：10-15% moutan root bark powder solution, 0.5-5%
Peony seed oil, 0.1-5% lemon juice, 0.1-5% watermelon husk juice, 0.5-5% green tea, 0.01-0.5% peppermint,
Surplus is water.Preferably, the moutan root bark powder solution is after moutan root bark powder is dissolved in water, through distilling obtained distillate.
Preferably, it is made up by weight percentage of following components：10-15% moutan root bark powder solution, 1-3% tree peony
Seed oil, 0.5-2% lemon juice, 0.5-2% watermelon husk juice, 1-3% green tea, 0.05-0.2% peppermint, surplus is water.
Preferably, it is made up by weight percentage of following components：12-15% moutan root bark powder solution, 1.5-2%'s is male
Red seed oil, 0.8-1.5% lemon juice, 0.8-1.5% watermelon husk juice, 1.5-2% green tea, 0.08-0.12% peppermint,
Surplus is water
Preferably, it is made up by weight percentage of following components：13% moutan root bark powder solution, 2% peony seed oil,
1% lemon juice, 1% watermelon husk juice, 2% green tea, 0.1% peppermint, surplus are water.
The preparation method of above-mentioned mouthwash, comprises the following steps：
Step 1, the bast for stripping tree peony root air-dries, and air-dried tree peony root bast is ground into powdered, obtains male
Red root skin powder, the moutan root bark powder are dissolved in water, and carry out steam distillation, obtain distillate；It is preferred that the bast by tree peony root
Portion air-dries in air-drying box, air-dried tree peony root bast is ground into powder beater powdered.
Step 2, the distillate of gained and peony seed oil are added to the water, stirred, obtain basal liquid；
Step 3, green tea and peppermint are ground into end respectively, add suitable quantity of water dissolving, 60-100 DEG C is heated 40-60min, cold
But to room temperature, filtering, respectively obtain green tea filtrate and peppermint filtrate is standby；
Step 4, by described filtrate, lemon juice and watermelon husk juice, it is added in described basal liquid, is well mixed, adds
Water polishing is 100% to total amount, obtains the mouthwash.
Preferably, in step 1, the moutan root bark powder is dissolved in water, amount of water is the 5-10 of moutan root bark silty amount
Times, add 0.5-1% sodium sulphate and 0.5-1% alcohol, after standing, with steam distillation, collect distillate, the percentage is equal
It is weight percentage.It is that raw material prepares mouthwash from moutan root bark extract, technique is simple, easily operated, can be used in work
Industry produces.
Preferably, in step 4, lemon and watermelon peel are respectively put into juice extractor, squeeze juice, respectively obtain lemon juice and
Watermelon husk juice.
Paeonol composition is rich in moutan root bark powder, and there is Paeonol analgesia, antipyretic, anti-inflammatory, antibacterial, anti-oxidant etc. to make
With moutan root bark powder is added in mouthwash of the present invention can play swelling and pain relieving, preventing and treating carious tooth, cover halitosis, clean oral cavity
Deng effect.
Peony seed oil has the effect of fine for treatment canker sore.
Lemon, lemon contain nicotinic acid and abundant organic acid, and its taste is extremely sour, have anti-inflammation, clearing heat and eliminating phlegm, enhancing people
The multiple efficacies such as body immunity.
Watermelon peel, it is cool in nature, it is sweet.Clear heat is antipyretic, quenches the thirst, diuresis.For hot summer weather polydipsia, oliguresis, oedema, mouth,
Raw sore in tongue, lip.
Green tea, fluorinated volume is higher, belongs to alkaline drink, can suppress the calcareous reduction of human body, tooth, hard tooth can be protected, to pre-
Anti-caries have good effect.
Peppermint, containing menthol, the material can fresh breath, also disappear with antisepsis and sterilization, diuresis, resolving sputum, stomach invigorating and helping
Change and other effects.
Beneficial effects of the present invention are：Mouthwash provided by the invention uses pure plant raw material, utilizes the town of moutan root bark
The effect such as bitterly, antipyretic, antiallergy, anti-inflammatory, immune, peony seed oil treat the special effect of canker sore, the pre- anti-caries of green tea, shield tooth,
The effect of hard tooth, and the antimicrobial and anti-inflammation efficacy of peppermint and lemon, and the effect of watermelon peel preventing and treating aphthae, pure plant is made
In mouthwash, reach the safe degerming and effect of fresh breath.Mouthwash on the market contains alcohol more at present, and daily use contains
There is unsafe factor in the mouthwash of alcohol, and mouthwash provided by the invention uses pure plant raw material, even if imprudence is drunk
Afterwards, potential safety hazard will not be also caused, the safe degerming and effect of fresh breath can be reached.
Brief description of the drawings
Fig. 1 is suppression situation of the control group culture medium to oral bacteria；
Fig. 2 is suppression situation of the culture medium of the mouthwash provided containing embodiment 1 to oral bacteria；
Fig. 3 is suppression situation of the culture medium of the mouthwash provided containing embodiment 4 to oral bacteria；
Fig. 4 is suppression situation of the culture medium of the mouthwash provided containing embodiment 5 to oral bacteria.
Embodiment
Embodiment 1
The bast for stripping tree peony root is air-dried in air-drying box, and air-dried tree peony root bast is ground into powder with powder beater
Last shape, obtain moutan root bark powder；50g moutan root barks powder is added in 500ml water and dissolved, 10g adds sodium sulphate and 10ml alcohol,
After standing, with steam distillation, distillate 116ml is collected.The distillate of gained and 20g peony seed oils are added to the water, stirred
Uniformly, basal liquid is obtained.20g green tea and 1g peppermints are ground into end, add suitable quantity of water dissolving, 60-100 DEG C of heating 40-
60min, room temperature is cooled to, filters, it is standby to obtain filtrate；Lemon and watermelon peel are respectively put into juice extractor, squeeze juice, obtained
Lemon juice and watermelon husk juice, it is standby.By green tea and peppermint filtrate, 10g lemon juices and 10g watermelon husk juices are added to described basis
In liquid, it is well mixed, adds water polishing, obtain the mouthwash.
Embodiment 2
The bast for stripping tree peony root is air-dried in air-drying box, and air-dried tree peony root bast is ground into powder with powder beater
Last shape, obtain moutan root bark powder；45g moutan root barks powder is added in 300ml water and dissolved, adds 5g sodium sulphate and 5ml alcohol, it is quiet
Postpone, with steam distillation, collect distillate 105ml.The distillate of gained and 15g peony seed oils are added to the water, stirring is equal
It is even, obtain basal liquid.15g green tea and 0.8g peppermints are ground into end, suitable quantity of water dissolving is added, 60 DEG C of heating 40min, is cooled to
Room temperature, filtering, it is standby to obtain filtrate；Lemon and watermelon peel are respectively put into juice extractor, squeeze juice, obtain lemon juice and watermelon
Skin juice, it is standby.By green tea and peppermint filtrate, 8g lemon juices and 8g watermelon husk juices are added in described basal liquid, are well mixed,
Add water polishing, obtain the mouthwash.
Embodiment 3
The bast for stripping tree peony root is air-dried in air-drying box, and air-dried tree peony root bast is ground into powder with powder beater
Last shape, obtain moutan root bark powder；60g moutan root barks powder is added in 300ml water and dissolved, adds 8g sodium sulphate and 6ml alcohol, it is quiet
Postpone, with steam distillation, collect distillate 140ml.The distillate of gained and 20g peony seed oils are added to the water, stirring is equal
It is even, obtain basal liquid.20g green tea and 1.2g peppermints are ground into end, add suitable quantity of water dissolving, 100 DEG C of heating 60min, cooling
To room temperature, filtering, it is standby to obtain filtrate；Lemon and watermelon peel are respectively put into juice extractor, squeeze juice, obtain lemon juice and west
Melon skin juice, it is standby.By green tea and peppermint filtrate, 15g lemon juices and 15g watermelon husk juices are added in described basal liquid, mixing
Uniformly, add water polishing, obtain the mouthwash.
Embodiment 4
The bast for stripping tree peony root is air-dried in air-drying box, and air-dried tree peony root bast is ground into powder with powder beater
Last shape, obtain moutan root bark powder；It will be dissolved in 43g moutan root barks powder addition 300ml water, addition sodium sulphate and alcohol, after standing,
With steam distillation, distillate is collected, gained distillate accounts for the 10% of whole mouthwash gross mass.By the distillate of gained and
10g peony seed oils are added to the water, and stir, and obtain basal liquid.10g green tea and 0.5g peppermints are ground into end, added appropriate
Water dissolves, and 100 DEG C of heating 40min, is cooled to room temperature, filters, it is standby to obtain filtrate；Lemon and watermelon peel are respectively put into and squeezed the juice
Machine, squeeze juice, lemon juice and watermelon husk juice are obtained, it is standby.By green tea and peppermint filtrate, 5g lemon juices and 5g watermelon husk juices add
Enter into described basal liquid, be well mixed, add water polishing, obtain the mouthwash.
Embodiment 5
The bast for stripping tree peony root is air-dried in air-drying box, and air-dried tree peony root bast is ground into powder with powder beater
Last shape, obtain moutan root bark powder；64g moutan root barks powder is added in 500ml water and dissolved, adds 5g sodium sulphate and 5ml alcohol, it is quiet
Postpone, with steam distillation, collect distillate, gained distillate accounts for the 15% of whole mouthwash gross mass.By the distillation of gained
Liquid and 30g peony seed oils are added to the water, and stir, obtain basal liquid.30g green tea and 2g peppermints are ground into end, added suitable
Water dissolving is measured, 80 DEG C of heating 50min, room temperature is cooled to, filters, it is standby to obtain filtrate；Lemon and watermelon peel are respectively put into squeezing
Juice machine, squeeze juice, lemon juice and watermelon husk juice are obtained, it is standby.By green tea and peppermint filtrate, 20g lemon juices and 20g watermelon peels
Juice is added in described basal liquid, is well mixed, is added water polishing, obtain the mouthwash.
Embodiment 6
The bast for stripping tree peony root is air-dried in air-drying box, and air-dried tree peony root bast is ground into powder with powder beater
Last shape, obtain moutan root bark powder；40g moutan root barks powder is added in 300ml water and dissolved, adds 5g sodium sulphate and 8ml alcohol, it is quiet
Postpone, with steam distillation, collect distillate.The distillate of gained and 5g peony seed oils are added to the water, stirred, is obtained
Basal liquid.5g green tea and 0.1g peppermints are ground into end, suitable quantity of water dissolving is added, 60 DEG C of heating 60min, is cooled to room temperature, mistake
Filter, it is standby to obtain filtrate；Lemon and watermelon peel are respectively put into juice extractor, squeeze juice, obtain lemon juice and watermelon husk juice, it is standby
With.By green tea and peppermint filtrate, 1g lemon juices and 1g watermelon husk juices are added in described basal liquid, are well mixed, are added water to mend
Together, the mouthwash is obtained.
Embodiment 7
The bast for stripping tree peony root is air-dried in air-drying box, and air-dried tree peony root bast is ground into powder with powder beater
Last shape, obtain moutan root bark powder；70g moutan root barks powder is added in 600ml water and dissolved, adds 10g sodium sulphate and 9ml alcohol,
After standing, with steam distillation, distillate is collected.The distillate of gained and 50g peony seed oils are added to the water, stirred,
Obtain basal liquid.50g green tea and 5g peppermints are ground into end, suitable quantity of water dissolving is added, 100 DEG C of heating 60min, is cooled to room
Temperature, filtering, it is standby to obtain filtrate；Lemon and watermelon peel are respectively put into juice extractor, squeeze juice, obtain lemon juice and watermelon peel
Juice, it is standby.By green tea and peppermint filtrate, 50g lemon juices and 50g watermelon husk juices are added in described basal liquid, are well mixed,
Add water polishing, obtain the mouthwash.
The culture medium of the mouthwash containing the gained of embodiment 1,4,5 is configured, and using distilled water as control, the checking present invention is right
Effect of the mouthwash of offer to oral bacteria.
1st, beef extract 0.225g, peptone 0.75g, Nacl0.375g, agar 1.5g, distilled water 75ml is weighed to be heated to boiling
Boiling to agar is completely dissolved, and adjusts PH to 7.4-7.6.The culture medium of preparation and clean flat board are placed in high-pressure steam sterilizing pan
121 DEG C, sterilize 30min.Suitably cool down and be down flat plate after desinfection chamber superclean bench.First gargled with distilled water, then with sterile tooth
After label gently scrape oral cavity wall, rule on the culture medium of cooled and solidified.The culture medium for being inoculated with oral bacteria is placed in 37 DEG C of perseverance
It is incubated overnight in incubator.
2nd, culture medium is prepared according to the formula of table 1, is heated to boiling to agar and is completely dissolved, adjust PH to 7.4-7.6, envelope
Mouthful, numbering.The culture medium of preparation and clean flat board are placed in 121 DEG C of high-pressure steam sterilizing pan, and sterilize 30min.Appropriate cooling after
Desinfection chamber superclean bench is down flat plate.
| Beef extract/g | Peptone/g | Agar/g | Nacl/g | Distilled water/ml | Mouthwash/ml | |
| Distilled water | 0.225 | 0.75 | 1.5 | 0.375 | 75 | 0 |
| Embodiment 1 | 0.225 | 0.75 | 1.5 | 0.375 | 65 | 10 |
| Embodiment 4 | 0.225 | 0.75 | 1.5 | 0.375 | 65 | 10 |
| Embodiment 5 | 0.225 | 0.75 | 1.5 | 0.375 | 65 | 10 |
3rd, after treating culture medium cooling, S lines are gently drawn on culture medium with the oral bacteria cultivated in oese picking 1.
The culture medium sealing completed will be inoculated with, be placed in culture overnight in 37 DEG C of insulating box, observation oral bacteria is on each culture medium
Growing state.
Control group and different embodiments gargle water culture medium counterpart chamber bacterium suppression situation as shown in Figures 1 to 4, from figure
It can be seen that mouthwash provided by the invention, has obvious inhibitory action to oral bacteria in 1-4.The present invention utilizes tree peony root
The effect such as the easing pain, be antipyretic of skin, antiallergy, anti-inflammatory, immune, peony seed oil treat the special effect of canker sore, the pre- anti-caries of green tea,
The effect of protecting tooth, hard tooth, and the antimicrobial and anti-inflammation efficacy of peppermint and lemon, and the effect of watermelon peel preventing and treating aphthae, be made
In pure plant mouthwash, reach the safe degerming and effect of fresh breath.Mouthwash on the market contains alcohol more at present, daily
Unsafe factor be present using alcoholic mouthwash, and mouthwash provided by the invention uses pure plant raw material, even if not small
After the heart is drunk, potential safety hazard will not be also caused, the safe degerming and effect of fresh breath can be reached.
The present invention is not limited to above-mentioned preferred forms, and anyone can show that other are various under the enlightenment of the present invention
The product of form, however, make any change in its shape or structure, it is every that there is skill identical or similar to the present application
Art scheme, is within the scope of the present invention.
Claims (7)
- A kind of 1. mouthwash, it is characterised in that：It is made up by weight percentage of following components：10-15% moutan root bark powder is molten Liquid, 0.5-5% peony seed oil, 0.1-5% lemon juice, 0.1-5% watermelon husk juice, 0.5-5% green tea, 0.01- 0.5% peppermint, surplus are water；The moutan root bark powder solution is after moutan root bark powder is dissolved in water, through distilling obtained distillation Liquid.
- 2. mouthwash according to claim 1, it is characterised in that：It is made up by weight percentage of following components：10-15% Moutan root bark powder solution, 1-3% peony seed oil, 0.5-2% lemon juice, 0.5-2% watermelon husk juice, 1-3%'s is green Tea, 0.05-0.2% peppermint, surplus are water.
- 3. mouthwash according to claim 1, it is characterised in that：It is made up by weight percentage of following components：12-15% Moutan root bark powder solution, 1.5-2% peony seed oil, 0.8-1.5% lemon juice, 0.8-1.5% watermelon husk juice, 1.5- 2% green tea, 0.08-0.12% peppermint, surplus are water.
- 4. mouthwash according to claim 1, it is characterised in that：It is made up by weight percentage of following components：13% Moutan root bark powder solution, 2% peony seed oil, 1% lemon juice, 1% watermelon husk juice, 2% green tea, 0.1% peppermint, Surplus is water.
- 5. the preparation method of the mouthwash according to one of claim 1-4, it is characterised in that：Comprise the following steps：Step 1, the bast for stripping tree peony root air-dries, and air-dried tree peony root bast is ground into powdered, obtains tree peony root Pi Fen, the moutan root bark powder are dissolved in water, and carry out steam distillation, obtain distillate；Step 2, the distillate of gained and peony seed oil are added to the water, stirred, obtain basal liquid；Step 3, green tea and peppermint are ground into end respectively, add suitable quantity of water dissolving, 60-100 DEG C of heating 40-60min, be cooled to Room temperature, filtering, respectively obtains green tea filtrate and peppermint filtrate is standby；Step 4, by described filtrate, lemon juice and watermelon husk juice, it is added in described basal liquid, is well mixed, adds water to mend It is together 100% to total amount, obtains the mouthwash.
- 6. the preparation method of mouthwash according to claim 5, it is characterised in that：In step 1, by the moutan root bark powder It is dissolved in water, amount of water is 5-10 times of moutan root bark silty amount, adds 0.5-1% sodium sulphate and 0.5-1% alcohol, is stood Afterwards, with steam distillation, distillate is collected, the percentage is weight percentage.
- 7. the preparation method of mouthwash according to claim 5, it is characterised in that：In step 4, by lemon and watermelon peel point Juice extractor is not put into, squeeze juice, respectively obtains lemon juice and watermelon husk juice.
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| CN201510530027.6A CN105030618B (en) | 2015-08-26 | 2015-08-26 | A kind of mouthwash and preparation method thereof |
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| CN201510530027.6A CN105030618B (en) | 2015-08-26 | 2015-08-26 | A kind of mouthwash and preparation method thereof |
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| CN105030618A CN105030618A (en) | 2015-11-11 |
| CN105030618B true CN105030618B (en) | 2018-02-02 |
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| CN100420432C (en) * | 2006-08-25 | 2008-09-24 | 青岛大学医学院附属医院 | Gargle and its preparing process |
| CN101642422B (en) * | 2009-09-07 | 2011-03-16 | 甘肃中川牡丹研究所 | Poppy tree peony skin-moistening cream and preparation method thereof |
| CN104510918A (en) * | 2013-09-26 | 2015-04-15 | 刘常春 | Traditional Chinese medicine powder capable of curing oral ulcer quickly |
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