CN104892978A - 含异氰脲酸三烯丙酯的交联剂和组合物 - Google Patents
含异氰脲酸三烯丙酯的交联剂和组合物 Download PDFInfo
- Publication number
- CN104892978A CN104892978A CN201510181301.3A CN201510181301A CN104892978A CN 104892978 A CN104892978 A CN 104892978A CN 201510181301 A CN201510181301 A CN 201510181301A CN 104892978 A CN104892978 A CN 104892978A
- Authority
- CN
- China
- Prior art keywords
- type
- taic
- trans
- cis
- triallyl isocyanurate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- KOMNUTZXSVSERR-UHFFFAOYSA-N 1,3,5-tris(prop-2-enyl)-1,3,5-triazinane-2,4,6-trione Chemical compound C=CCN1C(=O)N(CC=C)C(=O)N(CC=C)C1=O KOMNUTZXSVSERR-UHFFFAOYSA-N 0.000 title claims abstract description 39
- 238000000034 method Methods 0.000 title description 27
- 238000004519 manufacturing process Methods 0.000 title description 11
- 150000004045 organic chlorine compounds Chemical class 0.000 claims abstract description 17
- 239000000126 substance Substances 0.000 claims abstract description 16
- 239000000203 mixture Substances 0.000 claims abstract description 12
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- 229920001971 elastomer Polymers 0.000 claims description 2
- 239000000806 elastomer Substances 0.000 claims description 2
- 229920005992 thermoplastic resin Polymers 0.000 claims description 2
- 239000012535 impurity Substances 0.000 abstract description 8
- 150000001875 compounds Chemical class 0.000 abstract 3
- 239000003518 caustics Substances 0.000 abstract 2
- ZFSLODLOARCGLH-UHFFFAOYSA-N isocyanuric acid Chemical compound OC1=NC(O)=NC(O)=N1 ZFSLODLOARCGLH-UHFFFAOYSA-N 0.000 description 18
- OSDWBNJEKMUWAV-UHFFFAOYSA-N Allyl chloride Chemical group ClCC=C OSDWBNJEKMUWAV-UHFFFAOYSA-N 0.000 description 16
- UOORRWUZONOOLO-OWOJBTEDSA-N (E)-1,3-dichloropropene Chemical group ClC\C=C\Cl UOORRWUZONOOLO-OWOJBTEDSA-N 0.000 description 12
- ZVCDLGYNFYZZOK-UHFFFAOYSA-M sodium cyanate Chemical compound [Na]OC#N ZVCDLGYNFYZZOK-UHFFFAOYSA-M 0.000 description 11
- 238000004458 analytical method Methods 0.000 description 7
- 238000006243 chemical reaction Methods 0.000 description 7
- 230000000052 comparative effect Effects 0.000 description 5
- 238000005260 corrosion Methods 0.000 description 5
- 230000007797 corrosion Effects 0.000 description 5
- 238000004821 distillation Methods 0.000 description 5
- 239000003566 sealing material Substances 0.000 description 5
- 239000007788 liquid Substances 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- IOLCXVTUBQKXJR-UHFFFAOYSA-M potassium bromide Chemical compound [K+].[Br-] IOLCXVTUBQKXJR-UHFFFAOYSA-M 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 3
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 3
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 3
- 230000032683 aging Effects 0.000 description 3
- 238000001514 detection method Methods 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 2
- JHXVRRJXCDAINK-UHFFFAOYSA-N NC(=O)N.N#CC#N Chemical compound NC(=O)N.N#CC#N JHXVRRJXCDAINK-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- XXROGKLTLUQVRX-UHFFFAOYSA-N allyl alcohol Chemical compound OCC=C XXROGKLTLUQVRX-UHFFFAOYSA-N 0.000 description 2
- HXBPYFMVGFDZFT-UHFFFAOYSA-N allyl isocyanate Chemical compound C=CCN=C=O HXBPYFMVGFDZFT-UHFFFAOYSA-N 0.000 description 2
- 229910001628 calcium chloride Inorganic materials 0.000 description 2
- 239000001110 calcium chloride Substances 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- SBUXRMKDJWEXRL-ROUUACIJSA-N cis-body Chemical compound O=C([C@H]1N(C2=O)[C@H](C3=C(C4=CC=CC=C4N3)C1)CC)N2C1=CC=C(F)C=C1 SBUXRMKDJWEXRL-ROUUACIJSA-N 0.000 description 2
- 230000002596 correlated effect Effects 0.000 description 2
- 239000012776 electronic material Substances 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000004065 semiconductor Substances 0.000 description 2
- 238000005987 sulfurization reaction Methods 0.000 description 2
- SBUXRMKDJWEXRL-ZWKOTPCHSA-N trans-body Chemical compound O=C([C@@H]1N(C2=O)[C@H](C3=C(C4=CC=CC=C4N3)C1)CC)N2C1=CC=C(F)C=C1 SBUXRMKDJWEXRL-ZWKOTPCHSA-N 0.000 description 2
- BJELTSYBAHKXRW-UHFFFAOYSA-N 2,4,6-triallyloxy-1,3,5-triazine Chemical compound C=CCOC1=NC(OCC=C)=NC(OCC=C)=N1 BJELTSYBAHKXRW-UHFFFAOYSA-N 0.000 description 1
- 241000370738 Chlorion Species 0.000 description 1
- IMLUAMAZHQFDNT-UHFFFAOYSA-N ClC(C(C)(CCCCl)Cl)Cl Chemical compound ClC(C(C)(CCCCl)Cl)Cl IMLUAMAZHQFDNT-UHFFFAOYSA-N 0.000 description 1
- -1 DIONEX Ion Chemical class 0.000 description 1
- GSNUFIFRDBKVIE-UHFFFAOYSA-N DMF Natural products CC1=CC=C(C)O1 GSNUFIFRDBKVIE-UHFFFAOYSA-N 0.000 description 1
- 239000006087 Silane Coupling Agent Substances 0.000 description 1
- 239000004809 Teflon Substances 0.000 description 1
- 229920006362 Teflon® Polymers 0.000 description 1
- 239000000538 analytical sample Substances 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- MGNCLNQXLYJVJD-UHFFFAOYSA-N cyanuric chloride Chemical compound ClC1=NC(Cl)=NC(Cl)=N1 MGNCLNQXLYJVJD-UHFFFAOYSA-N 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000004973 liquid crystal related substance Substances 0.000 description 1
- 238000004949 mass spectrometry Methods 0.000 description 1
- SNMVRZFUUCLYTO-UHFFFAOYSA-N n-propyl chloride Chemical compound CCCCl SNMVRZFUUCLYTO-UHFFFAOYSA-N 0.000 description 1
- 239000012044 organic layer Substances 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 230000002285 radioactive effect Effects 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000001877 single-ion monitoring Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/30—Only oxygen atoms
- C07D251/34—Cyanuric or isocyanuric esters
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
- Sealing Material Composition (AREA)
Abstract
Description
TAIC的种类 | 氯离子浓度(ppm) |
比较例1 | 150 |
实施例1 | ND(小于1ppm) |
Claims (2)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2009125334A JP5509674B2 (ja) | 2009-05-25 | 2009-05-25 | トリアリルイソシアヌレート及びその製造方法 |
JP2009-125334 | 2009-05-25 | ||
CN201080022780.XA CN102448944B (zh) | 2009-05-25 | 2010-05-20 | 异氰脲酸三烯丙酯及其制造方法 |
Related Parent Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201080022780.XA Division CN102448944B (zh) | 2009-05-25 | 2010-05-20 | 异氰脲酸三烯丙酯及其制造方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN104892978A true CN104892978A (zh) | 2015-09-09 |
CN104892978B CN104892978B (zh) | 2018-11-13 |
Family
ID=43222628
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201510181301.3A Active CN104892978B (zh) | 2009-05-25 | 2010-05-20 | 含异氰脲酸三烯丙酯的交联剂和组合物 |
CN201080022780.XA Active CN102448944B (zh) | 2009-05-25 | 2010-05-20 | 异氰脲酸三烯丙酯及其制造方法 |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201080022780.XA Active CN102448944B (zh) | 2009-05-25 | 2010-05-20 | 异氰脲酸三烯丙酯及其制造方法 |
Country Status (7)
Country | Link |
---|---|
US (1) | US8674092B2 (zh) |
EP (2) | EP2899184A1 (zh) |
JP (1) | JP5509674B2 (zh) |
KR (4) | KR101917639B1 (zh) |
CN (2) | CN104892978B (zh) |
TW (2) | TWI508952B (zh) |
WO (1) | WO2010137518A1 (zh) |
Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2010137519A1 (ja) * | 2009-05-25 | 2010-12-02 | 日本化成株式会社 | トリアリルイソシアヌレートの貯蔵方法 |
KR101956545B1 (ko) * | 2009-05-25 | 2019-03-11 | 미쯔비시 케미컬 주식회사 | 트리알릴이소시아누레이트, 트리알릴시아누레이트 및 트리알릴이소시아누레이트의 제조방법 |
CN102775364B (zh) * | 2012-07-31 | 2015-01-07 | 合肥工业大学 | 一种交联剂三烯丙基异氰尿酸酯的制备方法 |
CN102887868B (zh) * | 2012-09-18 | 2014-12-31 | 江苏科利新材料有限公司 | 一种三烯丙基异氰尿酸酯的制备方法 |
ES2632783T3 (es) | 2014-12-19 | 2017-09-15 | Evonik Degussa Gmbh | Sistemas de redes de cubierta para láminas de encapsulación que comprenden compuestos de bis-(alquenilamidas) |
EP3034528B1 (de) | 2014-12-19 | 2017-06-21 | Evonik Degussa GmbH | Covernetzersysteme für Verkapselungsfolien umfassend Harnstoffverbindungen |
CN106810505A (zh) * | 2017-03-02 | 2017-06-09 | 江苏华星新材料科技股份有限公司 | 一种异氰脲酸制备三烯丙基异氰脲酸酯的工艺 |
CN109694460B (zh) * | 2018-12-11 | 2021-04-20 | 万华化学集团股份有限公司 | 多官能度不饱和异氰酸酯三聚体及其制备和在分散体稳定剂中的应用 |
CN111253329B (zh) * | 2020-04-14 | 2022-11-29 | 湖南方锐达科技有限公司 | 一种三烯丙基异氰脲酸酯的制备工艺 |
CN111848532A (zh) * | 2020-07-23 | 2020-10-30 | 山东海益化工科技有限公司 | 三烯丙基异三聚氰酸酯生产工艺 |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS4826022A (zh) * | 1971-08-04 | 1973-04-05 | ||
JPS4826022B1 (zh) * | 1970-05-03 | 1973-08-03 | ||
JPS5444688A (en) * | 1977-09-12 | 1979-04-09 | Nippon Kasei Chem | Manufacture of isocyanic acid triallyl |
JPS62286936A (ja) * | 1986-06-04 | 1987-12-12 | Showa Denko Kk | アリルクロライドの製造方法 |
JPH11255753A (ja) * | 1998-03-10 | 1999-09-21 | Nissei Kagaku Kogyo Kk | 高品位トリアリルイソシアヌレートとその製造方法 |
WO2008006661A2 (en) * | 2006-07-12 | 2008-01-17 | Evonik Degussa Gmbh | Process for preparing triallyl isocyanurate (taic) |
Family Cites Families (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3065231A (en) | 1958-08-06 | 1962-11-20 | Allied Chem | Production of triallyl isocyanurate |
US3376301A (en) * | 1960-08-24 | 1968-04-02 | Gulf Oil Corp | Method of producing triallylic isocyanurates |
US3322761A (en) * | 1965-07-14 | 1967-05-30 | Allied Chem | Purification of triallyl isocyanurate |
JPS4722588B1 (zh) * | 1970-03-02 | 1972-06-24 | ||
US3965231A (en) | 1975-04-07 | 1976-06-22 | Modern Builders Supply Co. | Means and method for defeathering blocks |
JPS5822118B2 (ja) * | 1978-03-31 | 1983-05-06 | 日本化成株式会社 | イソシアヌル酸トリアリルの製造法 |
JPS5835515B2 (ja) | 1977-09-12 | 1983-08-03 | 日本化成株式会社 | イソシアヌル酸エステルの製造法 |
JPS5835515A (ja) | 1981-08-28 | 1983-03-02 | Canon Inc | 液晶表示装置 |
JPH0826022A (ja) * | 1994-07-18 | 1996-01-30 | Mitsubishi Motors Corp | ヘッドランプ点灯回路 |
JP2006036876A (ja) | 2004-07-26 | 2006-02-09 | Du Pont Mitsui Polychem Co Ltd | 太陽電池封止材及びそれを用いた太陽電池モジュール |
JP2007115840A (ja) | 2005-10-19 | 2007-05-10 | Kyocera Corp | 配線基板および配線基板の製造方法 |
-
2009
- 2009-05-25 JP JP2009125334A patent/JP5509674B2/ja active Active
-
2010
- 2010-05-20 KR KR1020177032802A patent/KR101917639B1/ko active IP Right Grant
- 2010-05-20 KR KR1020177005497A patent/KR20170026641A/ko active Search and Examination
- 2010-05-20 CN CN201510181301.3A patent/CN104892978B/zh active Active
- 2010-05-20 EP EP15155216.3A patent/EP2899184A1/en not_active Ceased
- 2010-05-20 CN CN201080022780.XA patent/CN102448944B/zh active Active
- 2010-05-20 EP EP10780473.4A patent/EP2436678B1/en active Active
- 2010-05-20 WO PCT/JP2010/058566 patent/WO2010137518A1/ja active Application Filing
- 2010-05-20 KR KR1020167020520A patent/KR101753159B1/ko active IP Right Grant
- 2010-05-20 KR KR1020117025330A patent/KR20120024559A/ko not_active Application Discontinuation
- 2010-05-24 TW TW099116523A patent/TWI508952B/zh active
- 2010-05-24 TW TW103145491A patent/TWI603961B/zh active
-
2011
- 2011-11-02 US US13/287,275 patent/US8674092B2/en active Active
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS4826022B1 (zh) * | 1970-05-03 | 1973-08-03 | ||
JPS4826022A (zh) * | 1971-08-04 | 1973-04-05 | ||
JPS5444688A (en) * | 1977-09-12 | 1979-04-09 | Nippon Kasei Chem | Manufacture of isocyanic acid triallyl |
JPS62286936A (ja) * | 1986-06-04 | 1987-12-12 | Showa Denko Kk | アリルクロライドの製造方法 |
JPH11255753A (ja) * | 1998-03-10 | 1999-09-21 | Nissei Kagaku Kogyo Kk | 高品位トリアリルイソシアヌレートとその製造方法 |
WO2008006661A2 (en) * | 2006-07-12 | 2008-01-17 | Evonik Degussa Gmbh | Process for preparing triallyl isocyanurate (taic) |
Also Published As
Publication number | Publication date |
---|---|
KR20160096209A (ko) | 2016-08-12 |
EP2899184A1 (en) | 2015-07-29 |
US20120095224A1 (en) | 2012-04-19 |
EP2436678B1 (en) | 2016-04-20 |
CN104892978B (zh) | 2018-11-13 |
KR101917639B1 (ko) | 2018-11-13 |
KR101753159B1 (ko) | 2017-07-03 |
KR20170127077A (ko) | 2017-11-20 |
JP5509674B2 (ja) | 2014-06-04 |
EP2436678A4 (en) | 2012-11-07 |
TW201111353A (en) | 2011-04-01 |
US8674092B2 (en) | 2014-03-18 |
EP2436678A1 (en) | 2012-04-04 |
CN102448944B (zh) | 2017-06-20 |
TW201512179A (zh) | 2015-04-01 |
WO2010137518A1 (ja) | 2010-12-02 |
KR20120024559A (ko) | 2012-03-14 |
CN102448944A (zh) | 2012-05-09 |
KR20170026641A (ko) | 2017-03-08 |
JP2010270087A (ja) | 2010-12-02 |
TWI508952B (zh) | 2015-11-21 |
TWI603961B (zh) | 2017-11-01 |
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Legal Events
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TA01 | Transfer of patent application right |
Effective date of registration: 20180712 Address after: Tokyo, Japan, Japan Applicant after: Mitsubishi Kasei Corporation Address before: Fukushima Applicant before: Nippon Kasei Chemical Company |
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GR01 | Patent grant | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right |
Effective date of registration: 20210226 Address after: Fukuoka Prefecture Patentee after: New Ling Co.,Ltd. Address before: Tokyo, Japan Patentee before: MITSUBISHI CHEMICAL Corp. |
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TR01 | Transfer of patent right |