CN104800283A - Tooth flushing fluid and preparation method thereof - Google Patents
Tooth flushing fluid and preparation method thereof Download PDFInfo
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- CN104800283A CN104800283A CN201510212628.2A CN201510212628A CN104800283A CN 104800283 A CN104800283 A CN 104800283A CN 201510212628 A CN201510212628 A CN 201510212628A CN 104800283 A CN104800283 A CN 104800283A
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Abstract
The invention relates to tooth flushing fluid and a preparation method thereof. The tooth flushing fluid comprises the following substances in parts by weight: 5-13 parts of mint, 15-20 parts of honeysuckle, 15-20 parts of chrysanthemum, 2-8 parts of xylitol, 0.2-0.6 parts of water-soluble chitosan, 0.5-0.8 parts of zinc gluconate, and 100-200 parts of purified water. In the formula, the components such as honeysuckle, chrysanthemum and xylitol have the effects of clearing away heat and toxic materials, diminishing inflammation and preventing tooth decay; chitosan has the effect of selectively and highly inhibiting growth of oral streptococcus and meanwhile cannot influence growth of other beneficial bacteria; a chitosan zinc complex can be formed by chitosan and zinc in the tooth microenvironment, so that the antibacterial effect can be greatly improved. The components in the formula disclosed by the invention conform to the principle of homology of medicine and food; all the components are food-grade; the tooth flushing fluid is ideal tooth flushing fluid.
Description
Technical field
The invention belongs to dental care products field, relate to particularly a kind of can the mothproof collutory swallowed of heat-clearing and toxic substances removing, antiinflammatory, do not affect again the growth of probiotics while the alternative ground level of this oral liquid suppresses noxious bacteria.
Background technology
In recent years; the sickness rate of oral pathology is high; along with the raising of living standards of the people and health perception; the control of oral disease and the protection of tooth more and more important; it is inconvenient to there is use in the mouth care means that traditional employing toothpaste is brushed teeth; cleaning not in time, not thoroughly, have the drawbacks such as wearing and tearing to tooth, is difficult to the oral cavity cleaning requirement meeting people.
Collutory is as one oral cavity cleaning and nursing product easily, generally be contained in portable Packaging Bottle, can use at any time, overcome mouth care not in time, toothpaste uses inconvenient, the clean drawback such as not thorough, and then very popular, particularly travel crowd, office crowd.But show according to the study, collutory is on the market mostly containing alcoholic content, and the alcohol content in some collutory is up to 26%, and ethanol itself can destroy maintenance oral film, makes xerostomia, and then causes halitosis, oral cavity also can be made to produce uncomfortable prickling sensation.
The appearance of herbal mouthwash overcomes above problem, and containing enriching vitamin, they or there is sterilization, anti-caries, can effective anti-bacteria, the function of protection oral cavity cleaning and heath.
Application for a patent for invention (application number is 201210562322.6, applying date 2012-12-21) discloses a kind of sterilization pathogenic fire reducing collutory and preparation method thereof.With parts by weight, the present invention is composed of the following components: Flos Lonicerae: 20 ~ 30, Herba Saxifragae: 10 ~ 20, berberine: 1 ~ 3, Radix Glycyrrhizae: 20 ~ 30, the Radix Angelicae Dahuricae: 3 ~ 5, Herba Menthae: 4 ~ 6, Rhizoma Alpiniae Officinarum: 2 ~ 4, sodium citrate: 1 ~ 3, propylene glycol: 20 ~ 30, potassium sorbate: 1 ~ 3, glycerol: 20 ~ 40, deionized water: 600 ~ 800.Compared with prior art, the present invention has following beneficial effect: (1) has effect of well sterilization pathogenic fire reducing; (2) may be used for cleaning oral cavity and tooth, nontoxic, harmless, without any side effects.This patent application has the function relating to sterilization pathogenic fire reducing aspect, but not for antibacterial aspect.
In sum, one can heat-clearing and toxic substances removing, antiinflammatory mothproof, while also alternative ground level suppresses noxious bacteria, the development not affecting again the dental irrigation liquid of the growth of probiotics is necessary.
Summary of the invention
For defect of the prior art, the present invention propose one can heat-clearing and toxic substances removing, antiinflammatory mothproof, while also alternative ground level suppresses noxious bacteria, do not affect again the dental irrigation liquid of the growth of probiotics.
In order to realize above-mentioned technical purpose, the technical scheme of employing is:
A kind of dental irrigation liquid, its formula comprises following material according to weight: Herba Menthae 5 ~ 13 parts; Flos Lonicerae 15 ~ 20 parts; Flos Chrysanthemi 15 ~ 20 parts; Xylitol 2 ~ 8 parts; Water-soluble chitosan 0.2 ~ 0.6 part; Zinc gluconate 0.5 ~ 0.8 part; Purified water 100 ~ 200 parts.
Preferably, dental irrigation liquid of the present invention, comprises following material according to weight: Herba Menthae 6 ~ 12 parts; Flos Lonicerae 15 ~ 18 parts; Flos Chrysanthemi 15 ~ 18 parts; Xylitol 2 ~ 6 parts; Water-soluble chitosan 0.2 ~ 0.6 part; Zinc gluconate 0.5 ~ 0.8 part; Purified water 100 ~ 200 parts.
Preferably, dental irrigation liquid of the present invention comprises following material according to weight: Herba Menthae 6 ~ 10 parts; Flos Lonicerae 16 ~ 18 parts; Flos Chrysanthemi 16 ~ 18 parts; Xylitol 2 ~ 5 parts; Water-soluble chitosan 0.2 ~ 0.6 part; Zinc gluconate 0.5 ~ 0.8 part; Purified water 100 ~ 200 parts.
On the other hand, present invention also offers a kind of preparation method of dental irrigation liquid, comprise the following steps:
(1), according to formula each material is weighed, stand-by;
(2), by Flos Lonicerae, Flos Chrysanthemi clean, dry, wear into fine powder, after crossing 80 ~ 100 mesh sieves, add 60 ~ 80% of purified water gross weight, heating in water bath in the flask being placed in sealing, water bath heating temperature controls at 35 ~ 50 DEG C, and heat time heating time is 5 ~ 7 hours, filter, collect filtrate; Liquid to be filtered adds xylitol after being cooled to room temperature and stirs;
(3), in remaining 20% ~ 40% purified water add Herba Menthae, water-soluble chitosan and zinc gluconate successively, be uniformly mixed;
(4), by step (2) mix with (3) gained solution, stir.
Preferably, in described step (2), the temperature of heating in water bath is 40 ~ 45 DEG C, and heat time heating time is 6 ~ 7 hours.
Compared with prior art, the present invention has following beneficial effect:
1. the prescription compatibility of Flos Lonicerae, Flos Chrysanthemi and xylitol, heat-clearing and toxic substances removing, antiinflammatory are mothproof;
2. chitosan has the effect optionally highly suppressing Streptococcus oralis growth, does not affect the growth of other beneficial bacterias simultaneously.Like this because chitosan and zinc form chitosan-zn complex in tooth microenvironment, its fungistatic effect improves more greatly.
3. be added with Herba Menthae in mouthwash formula of the present invention, can fresh breath.
4. collutory of the present invention is for swallowing collutory, and formula components meets the principle of integration of edible and medicinal herbs, and all the components is food, and enters performance efficacy of drugs capable of being combined in the microenvironment of tooth.
Detailed description of the invention
In order to make the object, technical solutions and advantages of the present invention definitely, below the preferred embodiments of the present invention are described in detail.
embodiment 1
(1), according to formula each material is weighed, stand-by;
Described dental irrigation liquid, weighs following material according to weight: Herba Menthae 7 parts; Flos Lonicerae 18 parts; Flos Chrysanthemi 18 parts; Xylitol 6 parts; Water-soluble chitosan 0.2 part; Zinc gluconate 0.8 part; Purified water 150 parts.
(2), by Flos Lonicerae, Flos Chrysanthemi clean, dry, wear into fine powder, after crossing 80 mesh sieves, add 80% of purified water gross weight, heating in water bath in the flask being placed in sealing, water bath heating temperature controls at 35 ~ 50 DEG C, and heat time heating time is 5 ~ 7 hours, filter, collect filtrate; Liquid to be filtered adds xylitol after being cooled to room temperature and stirs;
(3), in remaining 20% purified water add Herba Menthae, water-soluble chitosan and zinc gluconate successively, be uniformly mixed;
(4), by step (2) mix with (3) gained solution, stir.
embodiment 2
(1), according to formula each material is weighed, stand-by;
Described dental irrigation liquid, weighs following material according to weight: Herba Menthae 10 parts; Flos Lonicerae 17 parts; Flos Chrysanthemi 17 parts; Xylitol 5 parts; Water-soluble chitosan 0.3 part; Zinc gluconate 0.7 part; Purified water 150 parts.
(2), by Flos Lonicerae, Flos Chrysanthemi clean, dry, wear into fine powder, after crossing 80 mesh sieves, add 60% of purified water gross weight, heating in water bath in the flask being placed in sealing, water bath heating temperature controls at 40 ~ 45 DEG C, and heat time heating time is 5 ~ 7 hours, filter, collect filtrate; Liquid to be filtered adds xylitol after being cooled to room temperature and stirs;
(3), in remaining 40% purified water add Herba Menthae, water-soluble chitosan and zinc gluconate successively, be uniformly mixed;
(4), by step (2) mix with (3) gained solution, stir.
embodiment 3
(1), according to formula each material is weighed, stand-by;
Described dental irrigation liquid, comprises following material according to weight: Herba Menthae 6 parts; Flos Lonicerae 15 parts; Flos Chrysanthemi 15 parts; Xylitol 3 parts; Water-soluble chitosan 0.2 part; Zinc gluconate 0.8 part; Purified water 120.
(2), by Flos Lonicerae, Flos Chrysanthemi clean, dry, wear into fine powder, after crossing 80 mesh sieves, add 60% of purified water gross weight, heating in water bath in the flask being placed in sealing, water bath heating temperature controls at 35 ~ 50 DEG C, and heat time heating time is 6 ~ 7 hours, filter, collect filtrate; Liquid to be filtered adds xylitol after being cooled to room temperature and stirs;
(3), in remaining 40% purified water add Herba Menthae, water-soluble chitosan and zinc gluconate successively, be uniformly mixed;
(4), by step (2) mix with (3) gained solution, stir.
effect example
48 experimenters are divided into four groups, existing collutory in kind of the formula mouth wash of three in embodiment 1-3 and city is tested.Experimenter's every day, early, middle and late all use after the meal specified collutory, continued three days.Each oral fluid of getting after the meal checks that collutory is to bacteria clearance, and viewing test person uses the breath freshening situation in latter three hours.The noxious bacteria clearance of each experimental group, breath freshening rate, heat-clearing and toxic substances removing rate all calculate by effective percentage.
| Noxious bacteria clearance | Breath freshening rate | Heat-clearing and toxic substances removing rate | |
| Embodiment 1 | 95.8％ | 100％ | 97.9％ |
| Embodiment 2 | 93.7％ | 100％ | 100％ |
| Embodiment 3 | 89.6％ | 93.7％ | 95.8％ |
| Matched group 1 | 25％ | 66.7％ | 27.1％ |
Above-described embodiment can adopt and pack easily, as provided single deal collutory in portable mode, namely with a packing box or container holds and can be carried easily by people.Also can be that one group of portable packaging of multi-pieces or container hold collutory.First-selected container includes lid container, easily tears packaging and the little plastic cup with peelable lid.
This collutory can be filled into be had in the container of sprayer unit, for use of spraying.This solution and other collutory maintain in mouth in the same way, this solution is contained as by gargling or shutting up, with buccal, tongue and/or facial muscle realize solution and rotate everywhere in mouth or rock, and object makes cleaning effect optimization and increases contact surface.Time, greatly between 2 seconds to 60 seconds, was better between about 5 seconds to 30 seconds.When using in the form of a spray, directly in entrance, by the absorption of oral mucosa, afterwards through swallowing, further can absorb through intestines and stomach again.
Content described in this description embodiment is only enumerating the way of realization of inventive concept; protection scope of the present invention should not be regarded as being only limitted to the concrete form that embodiment is stated, protection scope of the present invention also relates to those skilled in the art and conceives the equivalent technologies means that can expect according to the present invention.
Claims (5)
1. a dental irrigation liquid, is characterized in that, its formula comprises following material according to weight:
2. dental irrigation liquid according to claim 1, is characterized in that, comprises following material according to weight:
3. dental irrigation liquid according to claim 1, is characterized in that, comprises following material according to weight:
4., as a preparation method for the dental irrigation liquid in claim 1-3 as described in any one, it is characterized in that, comprise the following steps:
(1), according to formula each material is weighed, stand-by;
(2), by Flos Lonicerae, Flos Chrysanthemi clean, dry, wear into fine powder, after crossing 80 ~ 100 mesh sieves, add 60 ~ 80% of purified water gross weight, heating in water bath in the flask being placed in sealing, water bath heating temperature controls at 35 ~ 50 DEG C, and heat time heating time is 5 ~ 7 hours, filter, collect filtrate; Liquid to be filtered adds xylitol after being cooled to room temperature and stirs;
(3), in remaining 20% ~ 40% purified water add Herba Menthae, water-soluble chitosan and zinc gluconate successively, be uniformly mixed;
(4), by step (2) mix with (3) gained solution, stir.
5. the preparation method of dental irrigation liquid according to claim 4, is characterized in that, in described step (2), the temperature of heating in water bath is 40 ~ 45 DEG C, and heat time heating time is 6 ~ 7 hours.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510212628.2A CN104800283A (en) | 2015-04-29 | 2015-04-29 | Tooth flushing fluid and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510212628.2A CN104800283A (en) | 2015-04-29 | 2015-04-29 | Tooth flushing fluid and preparation method thereof |
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| CN104800283A true CN104800283A (en) | 2015-07-29 |
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| CN201510212628.2A Pending CN104800283A (en) | 2015-04-29 | 2015-04-29 | Tooth flushing fluid and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105796379A (en) * | 2016-05-06 | 2016-07-27 | 青岛蓝百合生物科技有限公司 | Water soluble chitosan oral care solution and preparation method thereof |
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| CN1192898A (en) * | 1997-03-07 | 1998-09-16 | 杨云平 | Tooth-paste sheet and mfg. method thereof |
| WO2009106963A2 (en) * | 2008-02-26 | 2009-09-03 | Italmed S.R.L. | Dental composition for preventing and treating stomatitis and mouth ulcers |
| CN103431144A (en) * | 2013-08-30 | 2013-12-11 | 谢松芬 | Lotus leaf chewing gum and preparation method thereof |
| CN103876972A (en) * | 2012-12-23 | 2014-06-25 | 吕子玉 | Anti-allergic toothpaste containing traditional Chinese medicinal components |
| CN104434690A (en) * | 2014-12-11 | 2015-03-25 | 安徽安科余良卿药业有限公司 | Mouthwash and preparation method thereof |
-
2015
- 2015-04-29 CN CN201510212628.2A patent/CN104800283A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1192898A (en) * | 1997-03-07 | 1998-09-16 | 杨云平 | Tooth-paste sheet and mfg. method thereof |
| WO2009106963A2 (en) * | 2008-02-26 | 2009-09-03 | Italmed S.R.L. | Dental composition for preventing and treating stomatitis and mouth ulcers |
| CN103876972A (en) * | 2012-12-23 | 2014-06-25 | 吕子玉 | Anti-allergic toothpaste containing traditional Chinese medicinal components |
| CN103431144A (en) * | 2013-08-30 | 2013-12-11 | 谢松芬 | Lotus leaf chewing gum and preparation method thereof |
| CN104434690A (en) * | 2014-12-11 | 2015-03-25 | 安徽安科余良卿药业有限公司 | Mouthwash and preparation method thereof |
Non-Patent Citations (1)
| Title |
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| 刘艳如，等。: ""水溶性壳聚糖与锌的络合"", 《福建师范大学学报》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105796379A (en) * | 2016-05-06 | 2016-07-27 | 青岛蓝百合生物科技有限公司 | Water soluble chitosan oral care solution and preparation method thereof |
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Application publication date: 20150729 |
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