CN104544461A - 饮料专用焦糖色素及其制备方法 - Google Patents
饮料专用焦糖色素及其制备方法 Download PDFInfo
- Publication number
- CN104544461A CN104544461A CN201410844881.5A CN201410844881A CN104544461A CN 104544461 A CN104544461 A CN 104544461A CN 201410844881 A CN201410844881 A CN 201410844881A CN 104544461 A CN104544461 A CN 104544461A
- Authority
- CN
- China
- Prior art keywords
- glucose
- liquid
- caramel colorant
- syrup
- finished product
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- MIDXCONKKJTLDX-UHFFFAOYSA-N 3,5-dimethylcyclopentane-1,2-dione Chemical compound CC1CC(C)C(=O)C1=O MIDXCONKKJTLDX-UHFFFAOYSA-N 0.000 title claims abstract description 111
- 235000013736 caramel Nutrition 0.000 title claims abstract description 111
- 235000013361 beverage Nutrition 0.000 title claims abstract description 25
- 238000002360 preparation method Methods 0.000 title claims abstract description 20
- 239000000049 pigment Substances 0.000 title abstract description 4
- 239000007788 liquid Substances 0.000 claims abstract description 151
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims abstract description 138
- 239000008103 glucose Substances 0.000 claims abstract description 138
- 230000002378 acidificating effect Effects 0.000 claims abstract description 34
- 150000001450 anions Chemical class 0.000 claims abstract description 34
- 150000001768 cations Chemical class 0.000 claims abstract description 34
- PQUCIEFHOVEZAU-UHFFFAOYSA-N Diammonium sulfite Chemical compound [NH4+].[NH4+].[O-]S([O-])=O PQUCIEFHOVEZAU-UHFFFAOYSA-N 0.000 claims abstract description 25
- 238000007670 refining Methods 0.000 claims abstract description 18
- 239000003456 ion exchange resin Substances 0.000 claims abstract description 17
- 229920003303 ion-exchange polymer Polymers 0.000 claims abstract description 17
- 239000002994 raw material Substances 0.000 claims abstract description 16
- 238000001914 filtration Methods 0.000 claims abstract description 10
- 239000000203 mixture Substances 0.000 claims abstract description 10
- 239000003513 alkali Substances 0.000 claims abstract description 9
- 235000005911 diet Nutrition 0.000 claims abstract description 9
- 230000000378 dietary effect Effects 0.000 claims abstract description 9
- 238000010438 heat treatment Methods 0.000 claims abstract description 9
- 239000003086 colorant Substances 0.000 claims description 98
- 239000000047 product Substances 0.000 claims description 58
- 239000006188 syrup Substances 0.000 claims description 49
- 235000020357 syrup Nutrition 0.000 claims description 49
- 235000008504 concentrate Nutrition 0.000 claims description 40
- 239000012141 concentrate Substances 0.000 claims description 40
- 238000007599 discharging Methods 0.000 claims description 32
- 229930091371 Fructose Natural products 0.000 claims description 17
- 239000005715 Fructose Substances 0.000 claims description 17
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 claims description 17
- 230000000694 effects Effects 0.000 claims description 17
- 238000006317 isomerization reaction Methods 0.000 claims description 17
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims description 16
- 238000007445 Chromatographic isolation Methods 0.000 claims description 16
- WHUUTDBJXJRKMK-UHFFFAOYSA-N Glutamic acid Natural products OC(=O)C(N)CCC(O)=O WHUUTDBJXJRKMK-UHFFFAOYSA-N 0.000 claims description 16
- KDXKERNSBIXSRK-YFKPBYRVSA-N L-lysine Chemical compound NCCCC[C@H](N)C(O)=O KDXKERNSBIXSRK-YFKPBYRVSA-N 0.000 claims description 16
- QIVBCDIJIAJPQS-VIFPVBQESA-N L-tryptophane Chemical compound C1=CC=C2C(C[C@H](N)C(O)=O)=CNC2=C1 QIVBCDIJIAJPQS-VIFPVBQESA-N 0.000 claims description 16
- KDXKERNSBIXSRK-UHFFFAOYSA-N Lysine Natural products NCCCCC(N)C(O)=O KDXKERNSBIXSRK-UHFFFAOYSA-N 0.000 claims description 16
- 239000004472 Lysine Substances 0.000 claims description 16
- QIVBCDIJIAJPQS-UHFFFAOYSA-N Tryptophan Natural products C1=CC=C2C(CC(N)C(O)=O)=CNC2=C1 QIVBCDIJIAJPQS-UHFFFAOYSA-N 0.000 claims description 16
- 235000001014 amino acid Nutrition 0.000 claims description 16
- 150000001413 amino acids Chemical class 0.000 claims description 16
- 238000006243 chemical reaction Methods 0.000 claims description 16
- 239000011552 falling film Substances 0.000 claims description 16
- 239000000706 filtrate Substances 0.000 claims description 16
- 238000005194 fractionation Methods 0.000 claims description 16
- 235000013922 glutamic acid Nutrition 0.000 claims description 16
- 239000004220 glutamic acid Substances 0.000 claims description 16
- CSNNHWWHGAXBCP-UHFFFAOYSA-L magnesium sulphate Substances [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 claims description 16
- 238000004587 chromatography analysis Methods 0.000 claims description 14
- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 claims description 9
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 claims description 9
- 150000001875 compounds Chemical class 0.000 claims description 9
- 239000013078 crystal Substances 0.000 claims description 9
- JLPULHDHAOZNQI-ZTIMHPMXSA-N 1-hexadecanoyl-2-(9Z,12Z-octadecadienoyl)-sn-glycero-3-phosphocholine Chemical group CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCCCCCC\C=C/C\C=C/CCCCC JLPULHDHAOZNQI-ZTIMHPMXSA-N 0.000 claims description 8
- ATRRKUHOCOJYRX-UHFFFAOYSA-N Ammonium bicarbonate Chemical compound [NH4+].OC([O-])=O ATRRKUHOCOJYRX-UHFFFAOYSA-N 0.000 claims description 8
- 229910000013 Ammonium bicarbonate Inorganic materials 0.000 claims description 8
- WHUUTDBJXJRKMK-VKHMYHEASA-N L-glutamic acid Chemical compound OC(=O)[C@@H](N)CCC(O)=O WHUUTDBJXJRKMK-VKHMYHEASA-N 0.000 claims description 8
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 8
- 235000012538 ammonium bicarbonate Nutrition 0.000 claims description 8
- 239000001099 ammonium carbonate Substances 0.000 claims description 8
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims description 8
- 239000003054 catalyst Substances 0.000 claims description 8
- 239000000919 ceramic Substances 0.000 claims description 8
- 239000008367 deionised water Substances 0.000 claims description 8
- 229910021641 deionized water Inorganic materials 0.000 claims description 8
- 238000001704 evaporation Methods 0.000 claims description 8
- 230000008020 evaporation Effects 0.000 claims description 8
- 239000012535 impurity Substances 0.000 claims description 8
- 229910052943 magnesium sulfate Inorganic materials 0.000 claims description 8
- 239000000463 material Substances 0.000 claims description 8
- 239000012528 membrane Substances 0.000 claims description 8
- 230000035484 reaction time Effects 0.000 claims description 8
- AKHNMLFCWUSKQB-UHFFFAOYSA-L sodium thiosulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=S AKHNMLFCWUSKQB-UHFFFAOYSA-L 0.000 claims description 8
- 229940083466 soybean lecithin Drugs 0.000 claims description 8
- 238000010792 warming Methods 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical group O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 238000000034 method Methods 0.000 abstract description 3
- 239000002699 waste material Substances 0.000 abstract description 2
- 239000011347 resin Substances 0.000 abstract 4
- 229920005989 resin Polymers 0.000 abstract 4
- 150000002500 ions Chemical class 0.000 abstract 2
- 238000009835 boiling Methods 0.000 abstract 1
- 238000013375 chromatographic separation Methods 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 238000002156 mixing Methods 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
- 150000002303 glucose derivatives Chemical class 0.000 description 6
- 238000002955 isolation Methods 0.000 description 6
- 230000003287 optical effect Effects 0.000 description 6
- 238000005457 optimization Methods 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 4
- XLSZMDLNRCVEIJ-UHFFFAOYSA-N 4-methylimidazole Chemical compound CC1=CNC=N1 XLSZMDLNRCVEIJ-UHFFFAOYSA-N 0.000 description 2
- 238000004040 coloring Methods 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 229930006000 Sucrose Natural products 0.000 description 1
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000012970 cakes Nutrition 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 235000019219 chocolate Nutrition 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 235000012907 honey Nutrition 0.000 description 1
- 230000000968 intestinal effect Effects 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 235000021110 pickles Nutrition 0.000 description 1
- 235000014347 soups Nutrition 0.000 description 1
- 235000013555 soy sauce Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
- 238000009923 sugaring Methods 0.000 description 1
- 235000021419 vinegar Nutrition 0.000 description 1
- 239000000052 vinegar Substances 0.000 description 1
Landscapes
- Non-Alcoholic Beverages (AREA)
Abstract
Description
Claims (5)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201410844881.5A CN104544461B (zh) | 2014-12-31 | 2014-12-31 | 饮料专用焦糖色素及其制备方法 |
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CN201410844881.5A CN104544461B (zh) | 2014-12-31 | 2014-12-31 | 饮料专用焦糖色素及其制备方法 |
Publications (2)
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CN104544461A true CN104544461A (zh) | 2015-04-29 |
CN104544461B CN104544461B (zh) | 2016-08-24 |
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CN201410844881.5A Active CN104544461B (zh) | 2014-12-31 | 2014-12-31 | 饮料专用焦糖色素及其制备方法 |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105062132A (zh) * | 2015-09-10 | 2015-11-18 | 千禾味业食品股份有限公司 | 一种亚硫酸铵法焦糖色生产工艺 |
CN108948784A (zh) * | 2018-08-23 | 2018-12-07 | 湖南汇升生物科技有限公司 | 一种焦糖色生产工艺 |
CN110079121A (zh) * | 2019-04-22 | 2019-08-02 | 千禾味业食品股份有限公司 | 一种提升双倍焦糖色耐酸性的生产工艺 |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5648866A (en) * | 1979-09-28 | 1981-05-02 | Ajinomoto Co Inc | Evaluation of caramel |
CN103981241A (zh) * | 2014-05-19 | 2014-08-13 | 山东省鲁洲食品集团有限公司 | 一种利用结晶糖母液为原料生产果葡糖浆的方法 |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP5648866B2 (ja) * | 2012-10-02 | 2015-01-07 | カシオ計算機株式会社 | 撮影システム、撮影方法、撮影装置、及びプログラム |
-
2014
- 2014-12-31 CN CN201410844881.5A patent/CN104544461B/zh active Active
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5648866A (en) * | 1979-09-28 | 1981-05-02 | Ajinomoto Co Inc | Evaluation of caramel |
CN103981241A (zh) * | 2014-05-19 | 2014-08-13 | 山东省鲁洲食品集团有限公司 | 一种利用结晶糖母液为原料生产果葡糖浆的方法 |
Non-Patent Citations (1)
Title |
---|
张国瑛,等: "焦糖色素生产及应用的进展", 《食品工业科技》, no. 4, 31 December 2007 (2007-12-31), pages 232 - 236 * |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105062132A (zh) * | 2015-09-10 | 2015-11-18 | 千禾味业食品股份有限公司 | 一种亚硫酸铵法焦糖色生产工艺 |
CN108948784A (zh) * | 2018-08-23 | 2018-12-07 | 湖南汇升生物科技有限公司 | 一种焦糖色生产工艺 |
CN110079121A (zh) * | 2019-04-22 | 2019-08-02 | 千禾味业食品股份有限公司 | 一种提升双倍焦糖色耐酸性的生产工艺 |
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Publication number | Publication date |
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CN104544461B (zh) | 2016-08-24 |
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Denomination of invention: Beverage special caramel pigment and preparation method thereof Effective date of registration: 20190513 Granted publication date: 20160824 Pledgee: Agricultural Development Bank of China Qixian County branch Pledgor: HENAN FEITIAN AGRICULTURAL DEVELOPMENT Co.,Ltd. Registration number: 2019990000419 |
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Date of cancellation: 20200421 Granted publication date: 20160824 Pledgee: Agricultural Development Bank of China Qixian County branch Pledgor: HENAN FEITIAN AGRICULTURAL DEVELOPMENT Co.,Ltd. Registration number: 2019990000419 |
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Denomination of invention: Beverage special caramel pigment and preparation method thereof Effective date of registration: 20200506 Granted publication date: 20160824 Pledgee: Agricultural Development Bank of China Qixian County branch Pledgor: HENAN FEITIAN AGRICULTURAL DEVELOPMENT Co.,Ltd. Registration number: Y2020990000426 |
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Date of cancellation: 20201118 Granted publication date: 20160824 Pledgee: Agricultural Development Bank of China Qixian County branch Pledgor: HENAN FEITIAN AGRICULTURAL DEVELOPMENT Co.,Ltd. Registration number: Y2020990000426 |
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Denomination of invention: Caramel pigment for beverage and its preparation Effective date of registration: 20201118 Granted publication date: 20160824 Pledgee: Agricultural Development Bank of China Qixian County branch Pledgor: HENAN FEITIAN AGRICULTURAL DEVELOPMENT Co.,Ltd. Registration number: Y2020990001356 |
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Denomination of invention: Caramel pigment for beverage and its preparation method Effective date of registration: 20211025 Granted publication date: 20160824 Pledgee: Agricultural Development Bank of China Qixian County branch Pledgor: HENAN FEITIAN AGRICULTURAL DEVELOPMENT Co.,Ltd. Registration number: Y2021990001014 |
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Address after: 456750 north of Gongye Road, Tiexi District, Qi County, Hebi City, Henan Province Patentee after: Henan Feitian Biotechnology Co.,Ltd. Address before: 456750 north of Gongye Road, Tiexi District, Qi County, Hebi City, Henan Province Patentee before: HENAN FEITIAN AGRICULTURAL DEVELOPMENT Co.,Ltd. |
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Denomination of invention: Caramel pigment for beverages and its preparation method Effective date of registration: 20221210 Granted publication date: 20160824 Pledgee: Agricultural Development Bank of China Qixian County branch Pledgor: Henan Feitian Biotechnology Co.,Ltd. Registration number: Y2022990000827 |
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Denomination of invention: Beverage specific caramel pigment and its preparation method Effective date of registration: 20230913 Granted publication date: 20160824 Pledgee: Agricultural Development Bank of China Qixian County branch Pledgor: Henan Feitian Biotechnology Co.,Ltd. Registration number: Y2023980056241 |
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