CN104540875B - 制备聚醚碳酸酯多元醇的方法 - Google Patents

制备聚醚碳酸酯多元醇的方法 Download PDF

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Publication number
CN104540875B
CN104540875B CN201380044333.8A CN201380044333A CN104540875B CN 104540875 B CN104540875 B CN 104540875B CN 201380044333 A CN201380044333 A CN 201380044333A CN 104540875 B CN104540875 B CN 104540875B
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CN
China
Prior art keywords
carbonate
reactor
compound
kinds
carbon dioxide
Prior art date
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Expired - Fee Related
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CN201380044333.8A
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English (en)
Chinese (zh)
Other versions
CN104540875A (zh
Inventor
T.E.米勒
C.居特勒
M.沃哈克
J.霍夫曼
A.M.苏布哈尼
W.莱特纳
I.佩克曼
A.沃尔夫
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Covestro Deutschland AG
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Covestro Deutschland AG
Bayer MaterialScience AG
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Publication of CN104540875A publication Critical patent/CN104540875A/zh
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
    • C08G64/20—General preparatory processes
    • C08G64/30—General preparatory processes using carbonates
    • C08G64/305—General preparatory processes using carbonates and alcohols
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
    • C08G64/20—General preparatory processes
    • C08G64/32—General preparatory processes using carbon dioxide
    • C08G64/34—General preparatory processes using carbon dioxide and cyclic ethers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2603—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2603—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen
    • C08G65/2606—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2645—Metals or compounds thereof, e.g. salts
    • C08G65/2663—Metal cyanide catalysts, i.e. DMC's
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • C08G18/4833—Polyethers containing oxyethylene units

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Toxicology (AREA)
  • Polyesters Or Polycarbonates (AREA)
  • Polyethers (AREA)
CN201380044333.8A 2012-08-27 2013-08-23 制备聚醚碳酸酯多元醇的方法 Expired - Fee Related CN104540875B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP12181905.6 2012-08-27
EP12181905.6A EP2703425A1 (de) 2012-08-27 2012-08-27 Verfahren zur Herstellung von Polyethercarbonatpolyolen
PCT/EP2013/067578 WO2014033070A1 (de) 2012-08-27 2013-08-23 Verfahren zur herstellung von polyethercarbonatpolyolen

Publications (2)

Publication Number Publication Date
CN104540875A CN104540875A (zh) 2015-04-22
CN104540875B true CN104540875B (zh) 2017-09-29

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Country Status (12)

Country Link
US (1) US9273183B2 (https=)
EP (2) EP2703425A1 (https=)
JP (1) JP6339078B2 (https=)
KR (1) KR102080958B1 (https=)
CN (1) CN104540875B (https=)
BR (1) BR112015003540A2 (https=)
CA (1) CA2882891A1 (https=)
ES (1) ES2587654T3 (https=)
MX (1) MX2015002108A (https=)
PL (1) PL2888308T3 (https=)
SG (1) SG11201500914TA (https=)
WO (1) WO2014033070A1 (https=)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2865700A1 (de) 2013-10-23 2015-04-29 Bayer MaterialScience AG Verfahren zur Herstellung von Polyethercarbonatpolyolen
KR102333890B1 (ko) * 2014-07-03 2021-12-02 코베스트로 도이칠란트 아게 폴리에테르 카르보네이트 폴리올의 제조 방법
EP3023447A1 (de) * 2014-11-18 2016-05-25 Covestro Deutschland AG Verfahren zur Herstellung von Polyethercarbonatpolyolen
EP3050907A1 (de) 2015-01-28 2016-08-03 Covestro Deutschland AG Verfahren zur Herstellung von Polyethercarbonatpolyolen
EP3098250A1 (de) 2015-05-26 2016-11-30 Covestro Deutschland AG Verfahren zur herstellung von polyethercarbonatpolyolen
EP3219741A1 (de) * 2016-03-18 2017-09-20 Covestro Deutschland AG Verfahren zur herstellung von polyethercarbonatpolyolen
US10040903B2 (en) 2016-09-13 2018-08-07 Covestro Llc Polymer polyol quality
EP3538588B1 (en) 2016-11-11 2023-01-25 Dow Global Technologies LLC Polycarbonate based polyols
EP3502162A1 (de) * 2017-12-19 2019-06-26 Covestro Deutschland AG Verfahren zur herstellung von polyetheresterpolyolen
EP3760663A1 (de) * 2019-07-05 2021-01-06 Covestro Deutschland AG Verfahren zur herstellung von polyetherestercarbonatpolyolen
EP3916055A1 (de) * 2020-05-26 2021-12-01 Covestro Deutschland AG Polycarbonat-zusammensetzungen enthaltend polyethercarbonatpolyole
GB202017531D0 (en) * 2020-11-05 2020-12-23 Econic Tech Limited (poly)ol block copolymer

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101151296A (zh) * 2005-03-29 2008-03-26 巴斯福股份公司 使用亲co2化合物或取代物形成聚醚碳酸酯多元醇的方法
CN101611074A (zh) * 2007-01-30 2009-12-23 巴斯夫欧洲公司 制备聚醚碳酸酯多元醇的方法
WO2010100052A1 (de) * 2009-03-03 2010-09-10 Basf Se Verbackungsresistentes polyalkylencarbonat

Family Cites Families (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1063525A (en) 1963-02-14 1967-03-30 Gen Tire & Rubber Co Organic cyclic oxide polymers, their preparation and tires prepared therefrom
US3829505A (en) 1970-02-24 1974-08-13 Gen Tire & Rubber Co Polyethers and method for making the same
US3941849A (en) 1972-07-07 1976-03-02 The General Tire & Rubber Company Polyethers and method for making the same
GB8528071D0 (en) 1985-11-14 1985-12-18 Shell Int Research Polycarbonates
US5158922A (en) 1992-02-04 1992-10-27 Arco Chemical Technology, L.P. Process for preparing metal cyanide complex catalyst
US5470813A (en) 1993-11-23 1995-11-28 Arco Chemical Technology, L.P. Double metal cyanide complex catalysts
US5712216A (en) 1995-05-15 1998-01-27 Arco Chemical Technology, L.P. Highly active double metal cyanide complex catalysts
US5482908A (en) 1994-09-08 1996-01-09 Arco Chemical Technology, L.P. Highly active double metal cyanide catalysts
US5545601A (en) 1995-08-22 1996-08-13 Arco Chemical Technology, L.P. Polyether-containing double metal cyanide catalysts
US5767323A (en) * 1995-12-22 1998-06-16 Arco Chemical Technology, L.P. Process for preparing polyoxyalkylene polyether polyols having low levels of transition metals through double metal cyanide complex polyoxyalkylation
US5627120A (en) 1996-04-19 1997-05-06 Arco Chemical Technology, L.P. Highly active double metal cyanide catalysts
US5714428A (en) 1996-10-16 1998-02-03 Arco Chemical Technology, L.P. Double metal cyanide catalysts containing functionalized polymers
DE19905611A1 (de) 1999-02-11 2000-08-17 Bayer Ag Doppelmetallcyanid-Katalysatoren für die Herstellung von Polyetherpolyolen
DE19958355A1 (de) 1999-12-03 2001-06-07 Bayer Ag Verfahren zur Herstellung von DMC-Katalysatoren
AU2001260217A1 (en) 2000-04-20 2001-11-07 Bayer Aktiengesellschaft Method for producing double metal cyanide (dmc) catalysts
US6713593B2 (en) * 2000-10-11 2004-03-30 Pohang Iron & Steel Co., Ltd. Copolymer comprising alkylene carbonate and method of preparing same
DE10147712A1 (de) 2001-09-27 2003-04-17 Basf Ag Verfahren zur Herstellung aliphatischer Polycarbonate
DE10219028A1 (de) 2002-04-29 2003-11-06 Bayer Ag Herstellung und Verwendung von hochmolekularen aliphatischen Polycarbonaten
JP4145123B2 (ja) 2002-11-18 2008-09-03 株式会社オンダ製作所 継手
KR101455878B1 (ko) * 2006-11-15 2014-11-03 바스프 에스이 연질 폴리우레탄 발포체의 제조 방법
CN101054441A (zh) * 2007-05-09 2007-10-17 中南大学 可控降解二氧化碳/环氧化物/内酯的三元共聚物及其制备方法
DE102008000360A1 (de) * 2008-02-21 2009-08-27 Evonik Goldschmidt Gmbh Neue Alkoxysilylgruppen tragende Polyetheralkohole durch Alkoxylierung epoxidfunktioneller Alkoxysilane an Doppelmetallcyanid (DMC)-Katalysatoren, sowie Verfahren zu deren Herstellung
CN103333330A (zh) * 2008-09-08 2013-10-02 诺沃梅尔公司 聚碳酸酯多元醇组合物和方法
KR20120069681A (ko) * 2009-09-17 2012-06-28 아사히 가라스 가부시키가이샤 폴리에테르류의 제조 방법
KR20120128130A (ko) 2010-01-20 2012-11-26 바이엘 인텔렉쳐 프로퍼티 게엠베하 폴리에테르 카르보네이트 폴리올의 제조를 위한 이중 금속 시아나이드 촉매의 활성화 방법
MX2012011003A (es) * 2010-03-24 2012-10-15 Bayer Ip Gmbh Procedimiento para la preparacion de polioletercarbonatos.
EP2441788A1 (de) * 2010-10-14 2012-04-18 Bayer MaterialScience AG Verfahren zur Herstellung von Polyetherpolyolen
DE102010043409A1 (de) * 2010-11-04 2012-05-10 Bayer Materialscience Aktiengesellschaft Verfahren zur Herstellung von Polycarbonatpolyolen durch immortale Polymerisation von cyclischen Carbonaten

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101151296A (zh) * 2005-03-29 2008-03-26 巴斯福股份公司 使用亲co2化合物或取代物形成聚醚碳酸酯多元醇的方法
CN101611074A (zh) * 2007-01-30 2009-12-23 巴斯夫欧洲公司 制备聚醚碳酸酯多元醇的方法
WO2010100052A1 (de) * 2009-03-03 2010-09-10 Basf Se Verbackungsresistentes polyalkylencarbonat

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
高聚物负载双金属催化剂催化二氧化碳-环氧丙烷-己内酯的三元共聚反应;刘素琴 等;《高分子材料科学与工程》;20060731;76-79 *

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Publication number Publication date
EP2703425A1 (de) 2014-03-05
BR112015003540A2 (pt) 2017-07-04
EP2888308B1 (de) 2016-08-17
US9273183B2 (en) 2016-03-01
CN104540875A (zh) 2015-04-22
US20150225503A1 (en) 2015-08-13
WO2014033070A1 (de) 2014-03-06
SG11201500914TA (en) 2015-04-29
PL2888308T3 (pl) 2017-08-31
JP6339078B2 (ja) 2018-06-06
MX2015002108A (es) 2015-05-11
EP2888308A1 (de) 2015-07-01
ES2587654T3 (es) 2016-10-26
CA2882891A1 (en) 2014-03-06
KR20150048769A (ko) 2015-05-07
KR102080958B1 (ko) 2020-02-24
JP2015526575A (ja) 2015-09-10

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