KR102080958B1 - 폴리에테르 카보네이트 폴리올의 제조방법 - Google Patents
폴리에테르 카보네이트 폴리올의 제조방법 Download PDFInfo
- Publication number
- KR102080958B1 KR102080958B1 KR1020157006213A KR20157006213A KR102080958B1 KR 102080958 B1 KR102080958 B1 KR 102080958B1 KR 1020157006213 A KR1020157006213 A KR 1020157006213A KR 20157006213 A KR20157006213 A KR 20157006213A KR 102080958 B1 KR102080958 B1 KR 102080958B1
- Authority
- KR
- South Korea
- Prior art keywords
- reactor
- carbonate
- groups
- alkylene oxide
- functional
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
- C08G64/20—General preparatory processes
- C08G64/30—General preparatory processes using carbonates
- C08G64/305—General preparatory processes using carbonates and alcohols
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
- C08G64/18—Block or graft polymers
- C08G64/183—Block or graft polymers containing polyether sequences
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
- C08G64/20—General preparatory processes
- C08G64/32—General preparatory processes using carbon dioxide
- C08G64/34—General preparatory processes using carbon dioxide and cyclic ethers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2603—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2603—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen
- C08G65/2606—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
- C08G65/2645—Metals or compounds thereof, e.g. salts
- C08G65/2663—Metal cyanide catalysts, i.e. DMC's
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/48—Polyethers
- C08G18/4833—Polyethers containing oxyethylene units
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Toxicology (AREA)
- Polyesters Or Polycarbonates (AREA)
- Polyethers (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP12181905.6 | 2012-08-27 | ||
| EP12181905.6A EP2703425A1 (de) | 2012-08-27 | 2012-08-27 | Verfahren zur Herstellung von Polyethercarbonatpolyolen |
| PCT/EP2013/067578 WO2014033070A1 (de) | 2012-08-27 | 2013-08-23 | Verfahren zur herstellung von polyethercarbonatpolyolen |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR20150048769A KR20150048769A (ko) | 2015-05-07 |
| KR102080958B1 true KR102080958B1 (ko) | 2020-02-24 |
Family
ID=46982415
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020157006213A Expired - Fee Related KR102080958B1 (ko) | 2012-08-27 | 2013-08-23 | 폴리에테르 카보네이트 폴리올의 제조방법 |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US9273183B2 (https=) |
| EP (2) | EP2703425A1 (https=) |
| JP (1) | JP6339078B2 (https=) |
| KR (1) | KR102080958B1 (https=) |
| CN (1) | CN104540875B (https=) |
| BR (1) | BR112015003540A2 (https=) |
| CA (1) | CA2882891A1 (https=) |
| ES (1) | ES2587654T3 (https=) |
| MX (1) | MX2015002108A (https=) |
| PL (1) | PL2888308T3 (https=) |
| SG (1) | SG11201500914TA (https=) |
| WO (1) | WO2014033070A1 (https=) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2865700A1 (de) | 2013-10-23 | 2015-04-29 | Bayer MaterialScience AG | Verfahren zur Herstellung von Polyethercarbonatpolyolen |
| KR102333890B1 (ko) * | 2014-07-03 | 2021-12-02 | 코베스트로 도이칠란트 아게 | 폴리에테르 카르보네이트 폴리올의 제조 방법 |
| EP3023447A1 (de) * | 2014-11-18 | 2016-05-25 | Covestro Deutschland AG | Verfahren zur Herstellung von Polyethercarbonatpolyolen |
| EP3050907A1 (de) | 2015-01-28 | 2016-08-03 | Covestro Deutschland AG | Verfahren zur Herstellung von Polyethercarbonatpolyolen |
| EP3098250A1 (de) | 2015-05-26 | 2016-11-30 | Covestro Deutschland AG | Verfahren zur herstellung von polyethercarbonatpolyolen |
| EP3219741A1 (de) * | 2016-03-18 | 2017-09-20 | Covestro Deutschland AG | Verfahren zur herstellung von polyethercarbonatpolyolen |
| US10040903B2 (en) | 2016-09-13 | 2018-08-07 | Covestro Llc | Polymer polyol quality |
| EP3538588B1 (en) | 2016-11-11 | 2023-01-25 | Dow Global Technologies LLC | Polycarbonate based polyols |
| EP3502162A1 (de) * | 2017-12-19 | 2019-06-26 | Covestro Deutschland AG | Verfahren zur herstellung von polyetheresterpolyolen |
| EP3760663A1 (de) * | 2019-07-05 | 2021-01-06 | Covestro Deutschland AG | Verfahren zur herstellung von polyetherestercarbonatpolyolen |
| EP3916055A1 (de) * | 2020-05-26 | 2021-12-01 | Covestro Deutschland AG | Polycarbonat-zusammensetzungen enthaltend polyethercarbonatpolyole |
| GB202017531D0 (en) * | 2020-11-05 | 2020-12-23 | Econic Tech Limited | (poly)ol block copolymer |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2003029325A1 (de) | 2001-09-27 | 2003-04-10 | Basf Aktiengesellschaft | Verfahren zur herstellung aliphatischer polycarbonate |
| WO2008092767A1 (de) | 2007-01-30 | 2008-08-07 | Basf Se | Verfahren zur herstellung von polyethercarbonatpolyolen |
Family Cites Families (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1063525A (en) | 1963-02-14 | 1967-03-30 | Gen Tire & Rubber Co | Organic cyclic oxide polymers, their preparation and tires prepared therefrom |
| US3829505A (en) | 1970-02-24 | 1974-08-13 | Gen Tire & Rubber Co | Polyethers and method for making the same |
| US3941849A (en) | 1972-07-07 | 1976-03-02 | The General Tire & Rubber Company | Polyethers and method for making the same |
| GB8528071D0 (en) | 1985-11-14 | 1985-12-18 | Shell Int Research | Polycarbonates |
| US5158922A (en) | 1992-02-04 | 1992-10-27 | Arco Chemical Technology, L.P. | Process for preparing metal cyanide complex catalyst |
| US5470813A (en) | 1993-11-23 | 1995-11-28 | Arco Chemical Technology, L.P. | Double metal cyanide complex catalysts |
| US5712216A (en) | 1995-05-15 | 1998-01-27 | Arco Chemical Technology, L.P. | Highly active double metal cyanide complex catalysts |
| US5482908A (en) | 1994-09-08 | 1996-01-09 | Arco Chemical Technology, L.P. | Highly active double metal cyanide catalysts |
| US5545601A (en) | 1995-08-22 | 1996-08-13 | Arco Chemical Technology, L.P. | Polyether-containing double metal cyanide catalysts |
| US5767323A (en) * | 1995-12-22 | 1998-06-16 | Arco Chemical Technology, L.P. | Process for preparing polyoxyalkylene polyether polyols having low levels of transition metals through double metal cyanide complex polyoxyalkylation |
| US5627120A (en) | 1996-04-19 | 1997-05-06 | Arco Chemical Technology, L.P. | Highly active double metal cyanide catalysts |
| US5714428A (en) | 1996-10-16 | 1998-02-03 | Arco Chemical Technology, L.P. | Double metal cyanide catalysts containing functionalized polymers |
| DE19905611A1 (de) | 1999-02-11 | 2000-08-17 | Bayer Ag | Doppelmetallcyanid-Katalysatoren für die Herstellung von Polyetherpolyolen |
| DE19958355A1 (de) | 1999-12-03 | 2001-06-07 | Bayer Ag | Verfahren zur Herstellung von DMC-Katalysatoren |
| AU2001260217A1 (en) | 2000-04-20 | 2001-11-07 | Bayer Aktiengesellschaft | Method for producing double metal cyanide (dmc) catalysts |
| US6713593B2 (en) * | 2000-10-11 | 2004-03-30 | Pohang Iron & Steel Co., Ltd. | Copolymer comprising alkylene carbonate and method of preparing same |
| DE10219028A1 (de) | 2002-04-29 | 2003-11-06 | Bayer Ag | Herstellung und Verwendung von hochmolekularen aliphatischen Polycarbonaten |
| JP4145123B2 (ja) | 2002-11-18 | 2008-09-03 | 株式会社オンダ製作所 | 継手 |
| US7671228B2 (en) * | 2005-03-29 | 2010-03-02 | Basf Corporation | Method of forming a polyethercarbonate polyol using a CO2-philic compound or substituent |
| KR101455878B1 (ko) * | 2006-11-15 | 2014-11-03 | 바스프 에스이 | 연질 폴리우레탄 발포체의 제조 방법 |
| CN101054441A (zh) * | 2007-05-09 | 2007-10-17 | 中南大学 | 可控降解二氧化碳/环氧化物/内酯的三元共聚物及其制备方法 |
| DE102008000360A1 (de) * | 2008-02-21 | 2009-08-27 | Evonik Goldschmidt Gmbh | Neue Alkoxysilylgruppen tragende Polyetheralkohole durch Alkoxylierung epoxidfunktioneller Alkoxysilane an Doppelmetallcyanid (DMC)-Katalysatoren, sowie Verfahren zu deren Herstellung |
| CN103333330A (zh) * | 2008-09-08 | 2013-10-02 | 诺沃梅尔公司 | 聚碳酸酯多元醇组合物和方法 |
| WO2010100052A1 (de) * | 2009-03-03 | 2010-09-10 | Basf Se | Verbackungsresistentes polyalkylencarbonat |
| KR20120069681A (ko) * | 2009-09-17 | 2012-06-28 | 아사히 가라스 가부시키가이샤 | 폴리에테르류의 제조 방법 |
| KR20120128130A (ko) | 2010-01-20 | 2012-11-26 | 바이엘 인텔렉쳐 프로퍼티 게엠베하 | 폴리에테르 카르보네이트 폴리올의 제조를 위한 이중 금속 시아나이드 촉매의 활성화 방법 |
| MX2012011003A (es) * | 2010-03-24 | 2012-10-15 | Bayer Ip Gmbh | Procedimiento para la preparacion de polioletercarbonatos. |
| EP2441788A1 (de) * | 2010-10-14 | 2012-04-18 | Bayer MaterialScience AG | Verfahren zur Herstellung von Polyetherpolyolen |
| DE102010043409A1 (de) * | 2010-11-04 | 2012-05-10 | Bayer Materialscience Aktiengesellschaft | Verfahren zur Herstellung von Polycarbonatpolyolen durch immortale Polymerisation von cyclischen Carbonaten |
-
2012
- 2012-08-27 EP EP12181905.6A patent/EP2703425A1/de not_active Withdrawn
-
2013
- 2013-08-23 KR KR1020157006213A patent/KR102080958B1/ko not_active Expired - Fee Related
- 2013-08-23 EP EP13756070.2A patent/EP2888308B1/de not_active Not-in-force
- 2013-08-23 SG SG11201500914TA patent/SG11201500914TA/en unknown
- 2013-08-23 CA CA2882891A patent/CA2882891A1/en not_active Abandoned
- 2013-08-23 BR BR112015003540A patent/BR112015003540A2/pt not_active IP Right Cessation
- 2013-08-23 CN CN201380044333.8A patent/CN104540875B/zh not_active Expired - Fee Related
- 2013-08-23 MX MX2015002108A patent/MX2015002108A/es unknown
- 2013-08-23 WO PCT/EP2013/067578 patent/WO2014033070A1/de not_active Ceased
- 2013-08-23 PL PL13756070T patent/PL2888308T3/pl unknown
- 2013-08-23 JP JP2015528974A patent/JP6339078B2/ja not_active Expired - Fee Related
- 2013-08-23 US US14/424,171 patent/US9273183B2/en not_active Expired - Fee Related
- 2013-08-23 ES ES13756070.2T patent/ES2587654T3/es active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2003029325A1 (de) | 2001-09-27 | 2003-04-10 | Basf Aktiengesellschaft | Verfahren zur herstellung aliphatischer polycarbonate |
| WO2008092767A1 (de) | 2007-01-30 | 2008-08-07 | Basf Se | Verfahren zur herstellung von polyethercarbonatpolyolen |
Also Published As
| Publication number | Publication date |
|---|---|
| EP2703425A1 (de) | 2014-03-05 |
| BR112015003540A2 (pt) | 2017-07-04 |
| EP2888308B1 (de) | 2016-08-17 |
| CN104540875B (zh) | 2017-09-29 |
| US9273183B2 (en) | 2016-03-01 |
| CN104540875A (zh) | 2015-04-22 |
| US20150225503A1 (en) | 2015-08-13 |
| WO2014033070A1 (de) | 2014-03-06 |
| SG11201500914TA (en) | 2015-04-29 |
| PL2888308T3 (pl) | 2017-08-31 |
| JP6339078B2 (ja) | 2018-06-06 |
| MX2015002108A (es) | 2015-05-11 |
| EP2888308A1 (de) | 2015-07-01 |
| ES2587654T3 (es) | 2016-10-26 |
| CA2882891A1 (en) | 2014-03-06 |
| KR20150048769A (ko) | 2015-05-07 |
| JP2015526575A (ja) | 2015-09-10 |
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