CN104490684A - Fresh and cool type photooxidation-resistant cream and preparation method thereof - Google Patents
Fresh and cool type photooxidation-resistant cream and preparation method thereof Download PDFInfo
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Abstract
The invention discloses fresh and cool type photooxidation-resistant cream and a preparation method thereof. The fresh and cool type photooxidation-resistant cream is prepared from the following various components in parts by weight: 0.2-2 parts of resveratrol, 0.03-0.3 part of ellagic acid, 0.04-0.3 part of anthocyanin, 0.01-1 part of lycopene, 0.02-2 parts of vitamin C, 0.02-0.2 part of arbutin, 5-10 parts of glycerin, 0.25-2.5 parts of stearic acid, 2-7 parts of glycerin monostearate, 2-6 parts of propylene glycol, 0.02-0.3 part of rose essence oil, 0.3-0.5 part of triethanolamine, 0.2-5 parts of alcohol, 0.3-3 parts of olive oil and the balance of deionized water, totaling 100 parts. The fresh and cool type photooxidation-resistant cream disclosed by the invention is pure natural, non-irritating, convenient to use, mild, moistened, fresh, cool, ventilated, good in moisturizing effect and photooxidation-resistant, has the effects of improving the skin color, whitening, resisting skin aging, inhibiting accumulation of melanin and helping self-improvement of the skin.
Description
Technical field
The present invention relates to daily cosmetics field, be specifically related to a kind of light anti-photooxidation frost, also relate to the preparation method of this light anti-photooxidation frost.
Background technology
Summer is sunny, and ultraviolet is strong, and comparatively large to the injury of skin, skin understands lesional epidermis cell after accepting ultraviolet overexposure; Activation Tyrosinase accelerates pigment synthesis and blackening, and the moisture-keeping functions destroying skin makes skin become dry, makes the elastic fibers in skin corium impaired, microgroove is produced, under ultraviolet acute irradiation, also can cause skin inflammation, burn.When having abnormal case, then can become pigmentosa skin carcinoma, therefore, summer, antitan agent was necessary.Sunscreen product, all refer to the addition of and can intercept or absorb ultraviolet sunscreen to arrive sun-proof effect, the ultraviolet sunscreen of current absorption generally refers to Anthranilates, now, people pursue the theory of natural green environmental protection, therefore pure natural, the cosmetics of environmental protection have become a large focus of nowadays cosmetic industry, and the development containing natural sun-screening agents sun care preparations will have wide market prospect.After existing sunscreen cream uses, feel greasy to you, skin is airtight, not clearly.
Summary of the invention
The first object of the present invention provides a kind of light anti-photooxidation frost, it is salubrious, non-stimulated, sun-proof result is good and anti-photooxidation, whitening.
Light anti-photooxidation frost of the present invention, be prepared from by following each component by weight: resveratrol 0.2-2 part, ellagic acid 0.03-0.3 part, anthocyanidin 0.04-0.3 part, lycopene 0.01-1 part, vitamin C 0.02-2 part, arbutin 0.02-0.2 part, glycerol 5-10 part, stearic acid 0.25-2.5 part, glyceryl monostearate 2-7 part, propylene glycol 2-6 part, rose ethereal oil 0.02-0.3 part, triethanolamine 0.3-0.5 part, ethanol 0.2-5 part, olive oil 0.3-3 part, deionized water adds to 100 parts.
As preferred scheme, light anti-photooxidation frost of the present invention, be prepared from by following each component by weight: resveratrol 0.8-1.2 part, ellagic acid 0.18-0.23 part, anthocyanidin 0.17-0.22 part, lycopene 0.85-0.95 part, vitamin C 0.9-1.1 part, arbutin 0.08-0.13 part, glycerol 6-8 part, stearic acid 1.7-2.3 part, glyceryl monostearate 4-6 part, propylene glycol 4.7-5.5 part, rose ethereal oil 0.19-0.21 part, triethanolamine 0.35-0.45 part, ethanol 3.5-4.5 part, olive oil 1.5-2.5 part, deionized water adds to 100 parts.
As preferred scheme, light anti-photooxidation frost of the present invention, is prepared from by following each component of parts by weights meter: resveratrol 1 part, ellagic acid 0.2 part, anthocyanidin 0.2 part, lycopene 0.9 part, vitamin C 1 part, arbutin 0.1 part, glycerol 7 parts, stearic acid 2 parts, glyceryl monostearate 5 parts, propylene glycol 5 parts, rose ethereal oil 0.2 part, triethanolamine 0.4 part, ethanol 4 parts, 2 parts, olive oil, deionized water adds to 100 parts.
Another object of the present invention is to provide the preparation method of described light anti-photooxidation frost, comprises following steps:
(1) get the stearic acid of proportional quantity, glyceryl monostearate and mixed with propylene glycol post-heating to dissolve, form oily solution A;
(2) get after the resveratrol of proportional quantity, ellagic acid, anthocyanidin, lycopene, vitamin C and arbutin be dissolved in the ethanol of proportional quantity, the glycerol and the mixed with olive oil that add proportional quantity stir heating 78-80 DEG C simultaneously, evaporate into after without alcohol taste until ethanol and stop heating, form oily solution B;
(3) after described oily solution B is added stirring in described oily solution A, the triethanolamine adding proportional quantity stirs, form paste, finally add the rose ethereal oil of proportional quantity, add the deionized water of proportional quantity, after continuing to stir, after cooling down, namely obtain described light anti-photooxidation frost.
Described light anti-photooxidation frost of the present invention can be used as various clearly, antioxidative cosmetics use, preferably as sunscreen cream.
Compared with prior art; the light anti-photooxidation frost of the present invention has the following advantages: containing bioactive ingredients resveratrol, ellagic acid, anthocyanidin, lycopene, vitamin C and arbutin; Skin Cell can be protected from ultraviolet injury and repair photic damage, and suppressing the formation of melanocyte in skin.By it in use well effect can be played with other substrate compatibilities in white body.Pure natural of the present invention is non-stimulated, easy to use, gentle moist, clearly breathes freely; moistening effect is good, can anti-photooxidation, bright color, whitening; the accumulation of anti aging effect and check melanin, the skin of energy protection & restoration irriate restores calm, and helps skin self-improvement.
Detailed description of the invention
Following examples for illustration of the present invention, but are not used for limiting the scope of the invention.
Embodiment 1: a kind of light anti-photooxidation frost
The light anti-photooxidation frost of the present embodiment, each component following by weight is prepared from: resveratrol 1g, ellagic acid 0.2g, anthocyanidin 0.2g, lycopene 0.9g, vitamin C 1g, arbutin 0.1g, glycerol 7g, stearic acid 2g, glyceryl monostearate 5g, propylene glycol 5g, rose ethereal oil 0.2g, triethanolamine 0.4g, ethanol 4g, olive oil 2g, deionized water adds to 100g.
The preparation method of the light anti-photooxidation frost of the present embodiment, comprises the following steps:
(1), after getting the dissolving of the stearic acid of proportional quantity, glyceryl monostearate and mixed with propylene glycol post-heating, oily solution A is formed;
(2) get after the resveratrol of proportional quantity, ellagic acid, anthocyanidin, lycopene, vitamin C and arbutin be dissolved in the ethanol of proportional quantity, the glycerol and the mixed with olive oil that add proportional quantity stir heating 78-80 DEG C simultaneously, evaporate into after without alcohol taste until ethanol and stop heating, form oily solution B;
(3) after described oily solution B is added stirring in described oily solution A, the triethanolamine adding proportional quantity stirs, form paste, finally add the rose ethereal oil of proportional quantity, add the deionized water of proportional quantity, after continuing to stir, after cooling down, namely obtain described light anti-photooxidation frost.
Embodiment 2: a kind of light anti-photooxidation frost
The light anti-photooxidation frost of the present embodiment, each component following by weight is prepared from: resveratrol 0.8g, ellagic acid 0.18g, anthocyanidin 0.17g, lycopene 0.85g, vitamin C 0.9g, arbutin 0.08g, glycerol 6g, stearic acid 1.7g, glyceryl monostearate 4g, propylene glycol 4.7g, rose ethereal oil 0.19g, triethanolamine 0.35g, ethanol 3.5g, olive oil 1.5g, deionized water adds to 100g.
Described in the present embodiment, the preparation method of light anti-photooxidation frost is identical with embodiment 1.
Embodiment 3: a kind of light anti-photooxidation frost
The light anti-photooxidation frost of the present embodiment, each component following by weight is prepared from: resveratrol 1.2g, ellagic acid 0.23g, anthocyanidin 0.22g, lycopene 0.95g, vitamin C 1.1g, arbutin 0.13g, glycerol 8g, stearic acid 2.3g, glyceryl monostearate 6g, propylene glycol 5.5g, rose ethereal oil 0.21g, triethanolamine 0.45g, ethanol 4.5g, olive oil 2.5g, deionized water adds to 100g.
Described in the present embodiment, the preparation method of light anti-photooxidation frost is identical with embodiment 1.
Embodiment 4: a kind of light anti-photooxidation frost
The light anti-photooxidation frost of the present embodiment, each component following by weight is prepared from: resveratrol 2g, ellagic acid 0.3g, anthocyanidin 0.3g, lycopene 1g, Catergen g, arbutin 0.2g, glycerol 10g, stearic acid 2.5g, glyceryl monostearate 7g, propylene glycol 6g, rose ethereal oil 0.3g, triethanolamine 0.5g, ethanol 5g, olive oil 3g, deionized water adds to 100g.
Described in the present embodiment, the preparation method of light anti-photooxidation frost is identical with embodiment 1.
Embodiment 5: a kind of light anti-photooxidation frost
The light anti-photooxidation frost of the present embodiment, each component following by weight is prepared from: resveratrol 0.2g, ellagic acid 0.03g, anthocyanidin 0.04g, lycopene 0.01g, vitamin C 0.02g, arbutin 0.02g, glycerol 5g, stearic acid 0.25g, glyceryl monostearate 2g, propylene glycol 2g, rose ethereal oil 0.02g, triethanolamine 0.3g, ethanol 0.2g, olive oil 0.3g, deionized water adds to 100g.
Described in the present embodiment, the preparation method of light anti-photooxidation frost is identical with embodiment 1.
For verifying the excellent properties of light anti-photooxidation frost of the present invention further, inventor expands the test of a large amount of Performance Detection further to it, and length limit, and only exemplifies the part test of part most cogency herein.
Experimental example 1: free radical scavenging is tested
The spectrophotometry principle of 1, test principle: DPPH in dehydrated alcohol and ethanol-water system, presents darkviolet according to DHHP, has absorption maximum respectively under 517nm and 525nm.Free radical scavenger can make purple retreat gradually, goes out the content of DHHP according to the change detection of absorbance, and reaction free radical scavenger is to the Scavenging activity of DHHP.
2, test specimen:
Sample 1-3: the sample prepared by embodiment of the present invention 1-3.
Reference substance 1-5: the composition of reference example 3 and preparation method, wherein:
Reference substance 1: delete resveratrol, ellagic acid, anthocyanidin and lycopene, adjustment vitamin C is 1.83g, and arbutin is 2g, and remaining composition is identical with embodiment 3 with consumption;
Reference substance 2: delete resveratrol, ellagic acid, vitamin C and arbutin, adjustment anthocyanidin is 1.83g, and lycopene is 2g, and remaining composition is identical with embodiment 3 with consumption;
Reference substance 3: delete anthocyanidin, lycopene, vitamin C and arbutin, adjustment resveratrol is 1.83g, and ellagic acid is 2g, and remaining composition is identical with embodiment 3 with consumption;
Reference substance 4: delete resveratrol, ellagic acid, anthocyanidin, lycopene, vitamin C and arbutin, replace with the aloe extraction liquid that uses in CN104042486 for 3g and vitamin E be 0.6g, remaining composition is identical with embodiment 3 with consumption;
Reference substance 5: delete glycerol, stearic acid, glyceryl monostearate, propylene glycol, rose ethereal oil, triethanolamine, ethanol and olive oil, replace with the Oleum Rosae Rugosae 0.5g used in CN103550091, stearic acid 10g, glyceryl monostearate 5g, hexadecanol 5g, Semen pruni armeniacae oil 0.5g, titanium dioxide 20g and antiseptic 10g, the composition of active component is identical with embodiment 3 with weight.
3, test method: compound concentration is 1 × 10
-4the DPPH ethanol solution of mol/L.Get 2mLDPPH standard solution, be placed in test tube, add sample solution 2mL, after placing 30min, measure absorbance at 517nm.DPPH clearance rate is measured according to following formula:
Clearance rate=[1-(Ai-Aj)/Ac] × 100% of DHHP;
The absorbance of Ai:2mL testing sample solution+2mLDPPH solution;
The absorbance of Aj:2mL testing sample solution+2mL95% ethanol;
The absorbance of the absorbance+2mL95% ethanol of Ac:2mLDPPH solution.
Measure the testing sample of 0 month, 6 months, 12 months and 18 months, preservation condition: vial sealing is kept in Dark Place, indoor shady and cool place is conventional places.
4, experimental result
Within 4.10 months, detect the clearance rate of DHHP: in table 1.
Show 1:0 month clearance rate to DHHP
The result display of table 1, compared with reference substance 1-5, sample 1-3 shows excellent DHHP elimination effect, and wherein the clearance rate of sample 1 is best.
Within 4.26 months, detect the clearance rate of DHHP: in table 2.
Show 2:6 month clearance rate to DHHP
The result display of table 2, compared with reference substance 1-5, sample 1-3 shows good DHHP elimination effect, and wherein the clearance rate of sample 1 is best.
Within 4.312 months, detect the clearance rate of DHHP: in table 3.
Show 3:12 month clearance rate to DHHP
The result display of table 3, compared with reference substance 1-5, sample 1-3 shows good DHHP elimination effect, and wherein the clearance rate of sample 1 is best.
Within 4.418 months, detect the clearance rate of DHHP: in table 4.
Show 4:18 month clearance rate to DHHP
The result display of table 4, compared with reference substance 1-5, sample 1-3 shows certain DHHP elimination effect, and wherein the clearance rate of sample 1 is best.
To sum up result is known, and light anti-photooxidation frost of the present invention is in the probation of 0-18 month, and all remain good elimination effect to DHHP, and show excellent stability, wherein the elimination effect of the sunscreen cream of embodiment 1 is best, stability is best.
The mensuration of experimental example 2:SPF value
1, the preparation of sample: identical with experimental example 1.
2, experimental technique
The portable spectrometer that experiment adopts u s company to produce measures in indoor.During mensuration, in order to ensure the precision measured, the determination step that its operating process specifies in strict accordance with this instrument carries out.
(1) black cloth is padded on below sample and blank, reduces because desktop reflects the systematic error brought;
(2) spectrogrph is placed in the top of vessel, distance vessel upper surface 120mm, probe 20 °, visual field;
(3) testing sample being put into a diameter is 75mm, is highly in the culture dish of 14mm, and is struck off to eliminate the impact of testing sample surface on its spectral signature in testing sample surface with ruler.
Measure the testing sample of 0 month, 6 months, 12 months and 18 months, preservation condition: vial sealing is kept in Dark Place, indoor shady and cool place is conventional places.
3, experimental result
To the spf value measurement result of the testing sample of 0,6,12,18 month, in table 5.
Table 5: the spf value measuring 0,6,12,18 month
The result display of table 5, compared with reference substance 1-5, the SFP value of sample 1-3 is higher, meets the sun-proof requirement in long outdoor activities, and shows excellent stability in 0-18 month, best with sample 1.
To sum up result is known, and light anti-photooxidation frost of the present invention is in the probation of 0-18 month, and sun-proof performance is good, and SFP value is all higher, and shows excellent stability at 0-12 month.Wherein, the SFP value of the light anti-photooxidation frost of embodiment 1 is the highest, stability is best.
Experimental example 3: suppress the effect that in human body melanocyte, melanin generates
1, the preparation of sample: identical with experimental example 1.
2, experimental technique
(1) testing sample PBS is diluted 1 times.
(2) trophophase B16 cell routine of taking the logarithm digests, and adjustment number of cells is 5 × 10
4individual/ml, is seeded in 96 orifice plates, every hole 90 μ L, CO
2after incubator hatches 24 hours, every hole adds dissolves and the testing sample filtered with DMSO, sets up the blank group of culture medium and cell;
(3) culture plate is placed in incubator and hatched 72 as a child, abandon supernatant, PBS washes two times, then adds the 1%Triton-100 of 100 μ L, shakes after 5 minutes, place after 1 hour for-20 DEG C, room temperature is melted makes the complete cracking of cell, and then every hole adds the 0.1% levodopa solution (PBS joins) of 100 μ L, hatches 1 hour in incubator, to cultivate datum hole zeroing, under microplate reader, survey the absorbance of 460nm.
Measure the testing sample of 0 month, 6 months, 12 months and 18 months, preservation condition: vial sealing is kept in Dark Place, indoor shady and cool place is conventional places.
3, experimental result
Measure the melanocyte suppression ratio of 0,6,12,18 month testing sample, in table 6.
Table 6: the melanocyte suppression ratio (%) of different time testing sample
The result display of table 6, compared with reference substance 1-5, sample 1-3 is remarkable to the inhibition of melanocyte, and shows excellent stability in 0-12 month, best with sample 1.
To sum up result is known, and light anti-photooxidation frost of the present invention is in the probation of 0-18 month, remarkable to the inhibition of melanocyte, and shows excellent stability at 0-12 month.Wherein, the check melanin cell effect of the light anti-photooxidation frost of embodiment 1 is best, stability is best.
Experimental example 4: trial effect is tested
1, the preparation of sample: identical with experimental example 1.
2, experimental technique
Use population ages 17 ~ 40 years old.Hair perplexs: dandruff, head pruritus, scalp pomade.
Number on probation: schoolgirl 144 people, is divided into 8 experimental grouies at random.
Each experimental group uses a kind of sample on probation.Each use soybean grain size, is coated in face to all absorbing.
3, result on trial
Light anti-photooxidation frost result on trial, in table 7.
Table 7: result on trial (%)
Known according to table 7, compared with reference substance 1-5, the satisfaction of sample 1-3 is high, and sample 1 is best.Therefore, light anti-photooxidation frost user satisfaction of the present invention is very high, and the result of use of embodiment 1 is best.
Although above the present invention is described in detail with a general description of the specific embodiments, on basis of the present invention, can make some modifications or improvements it, this will be apparent to those skilled in the art.Therefore, these modifications or improvements without departing from theon the basis of the spirit of the present invention, all belong to the scope of protection of present invention.
Claims (4)
1. a light anti-photooxidation frost, it is characterized in that, be prepared from by following each component by weight: resveratrol 0.2-2 part, ellagic acid 0.03-0.3 part, anthocyanidin 0.04-0.3 part, lycopene 0.01-1 part, vitamin C 0.02-2 part, arbutin 0.02-0.2 part, glycerol 5-10 part, stearic acid 0.25-2.5 part, glyceryl monostearate 2-7 part, propylene glycol 2-6 part, rose ethereal oil 0.02-0.3 part, triethanolamine 0.3-0.5 part, ethanol 0.2-5 part, olive oil 0.3-3 part, deionized water adds to 100 parts.
2. light anti-photooxidation frost according to claim 1, it is characterized in that, be prepared from by following each component by weight: resveratrol 0.8-1.2 part, ellagic acid 0.18-0.23 part, anthocyanidin 0.17-0.22 part, lycopene 0.85-0.95 part, vitamin C 0.9-1.1 part, arbutin 0.08-0.13 part, glycerol 6-8 part, stearic acid 1.7-2.3 part, glyceryl monostearate 4-6 part, propylene glycol 4.7-5.5 part, rose ethereal oil 0.19-0.21 part, triethanolamine 0.35-0.45 part, ethanol 3.5-4.5 part, olive oil 1.5-2.5 part, deionized water adds to 100 parts.
3. light anti-photooxidation frost according to claim 1 and 2, is characterized in that, be prepared from by following each component by weight: resveratrol 1 part, ellagic acid 0.2 part, anthocyanidin 0.2 part, lycopene 0.9 part, vitamin C 1 part, arbutin 0.1 part, glycerol 7 parts, stearic acid 2 parts, glyceryl monostearate 5 parts, propylene glycol 5 parts, rose ethereal oil 0.2 part, triethanolamine 0.4 part, ethanol 4 parts, 2 parts, olive oil, deionized water adds to 100 parts.
4. the preparation method of light anti-photooxidation frost according to any one of claim 1 to 3, is characterized in that, comprise following steps:
(1) get stearic acid, glyceryl monostearate and mixed with propylene glycol post-heating to dissolve, form oily solution A;
(2) get after resveratrol, ellagic acid, anthocyanidin, lycopene, vitamin C and arbutin be dissolved in ethanol, add glycerol and mixed with olive oil and stir and heat 78-80 DEG C simultaneously, evaporate into after without alcohol taste until ethanol and stop heating, formation oily solution B;
(3) after described oily solution B is added stirring in described oily solution A, add triethanolamine and stir, form paste, finally add rose ethereal oil, add deionized water, after continuing to stir, after cooling down, namely obtain described light anti-photooxidation frost.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105853332A (en) * | 2016-05-10 | 2016-08-17 | 赫尔森江苏医药有限公司 | Anti-electromagnetic skin care cream and process for manufacturing same |
| CN107137248A (en) * | 2017-04-19 | 2017-09-08 | 北海市韩能生物科技有限公司 | Cosmetics containing OPC |
| CN107280998A (en) * | 2017-06-16 | 2017-10-24 | 湖南御家化妆品制造有限公司 | Tyrosinase inhibiting composition and application thereof |
| CN113876676A (en) * | 2021-10-25 | 2022-01-04 | 贵州大学 | Dendrobium beautifying cream and preparation method thereof |
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| CN1798538A (en) * | 2003-06-03 | 2006-07-05 | 默克专利股份有限公司 | Photostable organic sunscreen composition |
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| CN103599021A (en) * | 2013-11-15 | 2014-02-26 | 上海应用技术学院 | Roselle extract as well as preparation method thereof and application thereof in whitening skincare cosmetics |
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| CN1282572A (en) * | 2000-07-12 | 2001-02-07 | 张俊峰 | Cosmetics series for treating face chloasma |
| CN1798538A (en) * | 2003-06-03 | 2006-07-05 | 默克专利股份有限公司 | Photostable organic sunscreen composition |
| CN101222856A (en) * | 2005-07-15 | 2008-07-16 | 帝斯曼知识产权资产管理有限公司 | Novel use of organic compounds |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105853332A (en) * | 2016-05-10 | 2016-08-17 | 赫尔森江苏医药有限公司 | Anti-electromagnetic skin care cream and process for manufacturing same |
| CN107137248A (en) * | 2017-04-19 | 2017-09-08 | 北海市韩能生物科技有限公司 | Cosmetics containing OPC |
| CN107280998A (en) * | 2017-06-16 | 2017-10-24 | 湖南御家化妆品制造有限公司 | Tyrosinase inhibiting composition and application thereof |
| CN113876676A (en) * | 2021-10-25 | 2022-01-04 | 贵州大学 | Dendrobium beautifying cream and preparation method thereof |
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Application publication date: 20150408 |
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