CN109589282B - Hair wet tissue feed liquid with sun-proof and color-protecting functions and preparation method thereof - Google Patents
Hair wet tissue feed liquid with sun-proof and color-protecting functions and preparation method thereof Download PDFInfo
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/9789—Magnoliopsida [dicotyledons]
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
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- A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
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- A—HUMAN NECESSITIES
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/004—Preparations used to protect coloured hair
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Abstract
The invention relates to the technical field of daily chemical products, in particular to a hair wet tissue feed liquid with sun-proof and color-protecting functions and a preparation method thereof. A hair wet towel feed liquid with sunscreen and color protection functions comprises film forming agent, active substance, humectant, pH regulator, 1, 3-butanediol, essence, antiseptic, ethanol, and deionized water. The hair wet tissue liquid with the sun-proof and color-protecting functions can help hair reduce hair damage caused by sun-drying and slow down hair dyeing and color losing. The product can help to supplement the lipid on the surface layer of the hair, protect the hair flakes and prevent the hair flakes from tilting, so that dye molecules are prevented from falling off, the hair color losing condition is relieved, the hair is protected from being damaged, and the product has an ultraviolet absorption function and reduces the damage of ultraviolet rays to the hair.
Description
Technical Field
The invention belongs to the technical field of daily chemical products, and particularly relates to a hair wet tissue feed liquid with a sun-proof and color-protecting function and a preparation method thereof.
Background
Nowadays, the pace of life of people is faster and faster, and at the same time, the requirements on the image of the people, especially the hair, are higher and higher. More and more products applied to hair sun protection are prepared from chemical sun protection agents, and are compounded with a small amount of or no physical sun protection agent to prepare a low-viscosity emulsifying system or an oleyl alcohol system.
However, the existing products such as hair sunscreen aerosol cans have high requirements on packaging, storage and transportation of the products due to the propellant, an explosion-proof device is required to be arranged, and the products cannot be carried on an airplane. Shampoo rinse-off products, however, have a short leave-on time on the hair and a low residual amount, and have little practical sunscreen effect. Therefore, the invention aims to provide the hair wet tissue liquid with the sun-proof and color-protecting effects, which can help the hair to reduce the hair damage caused by the sun, slow down the hair dyeing and color losing situation, has no special requirements on transportation and storage, has no problems when being used on planes, is free of washing and quick-drying, is convenient to carry, and is disposable.
Disclosure of Invention
In order to solve the above problems, the first aspect of the present invention provides a hair wet towel feed liquid with sunscreen and color protection functions, comprising the following components: film forming agent, active matter, humectant, pH regulator, 1, 3-butanediol, essence, preservative, ethanol and deionized water.
As a preferable technical scheme, the hair wet tissue feed liquid comprises the following components in parts by weight: 0.01-5 parts of film forming agent, 2-10 parts of active matter, 0.05-2 parts of humectant, 0.1-0.5 part of pH regulator, 0.5-2 parts of 1, 3-butanediol, 0-1 part of essence, 0.5-2 parts of preservative, 0-15 parts of ethanol and 60-90 parts of deionized water.
As a preferable technical scheme, the hair wet tissue feed liquid comprises the following components in parts by weight: 0.1-3 parts of film forming agent, 3-8 parts of active matter, 0.1-0.4 part of humectant, 0.2-0.4 part of pH regulator, 1-1.5 parts of 1, 3-butanediol, 0.2-0.8 part of essence, 0.8-1.2 parts of preservative, 2-10 parts of ethanol and 70-80 parts of deionized water.
As a preferable technical scheme, the hair wet tissue feed liquid comprises the following components in parts by weight: 0.2-1.5 parts of film forming agent, 4-6 parts of active matter, 0.1-0.2 part of humectant, 0.2-0.3 part of pH regulator, 1.0-1.5 parts of 1, 3-butanediol, 0.3-0.6 part of essence, 0.9-1.2 parts of preservative, 3-8 parts of ethanol and 72-78 parts of deionized water.
As a preferable technical scheme, the film forming agent is selected from one or more of polyethylene glycol derivatives, polyvinylpyrrolidone, acrylamide propyl trimethyl ammonium chloride/acrylamide copolymers, acrylic copolymers, acrylate copolymers, modified silicone oil, tremella polysaccharides, sodium hyaluronate, tamarind seed gum, beta-glucan, trehalose, gum arabic and sodium cellulose sulfate.
As a preferred technical scheme, the active matter is selected from one or more of sunflower seed extract, haematococcus pluvialis extract, quercus robur fruit extract, cinnamide propyl trimethyl ammonium chloride and methoxy cinnamide propyl hydroxy sulfobetaine.
As a preferable technical scheme, the weight ratio of the active substance, the film forming agent and the humectant is 1 (0.005-0.5) to 0.02-0.2.
As a preferred technical scheme, the essence is selected from one or more of lavender essence, rose essence, osmanthus flower essence, lily essence, chamomile essence, green apple essence, strawberry essence, papaya essence, hami melon essence, cherry essence and juicy peach essence.
As a preferable technical scheme, the preservative is selected from one or more of cetylpyridinium chloride, benzalkonium chloride, chlorphenesin, poly (aminopropyl) biguanide, chlorhexidine digluconate, benzethonium chloride, phenoxyethanol, benzoic acid, sodium benzoate, caprylyl hydroximic acid, sodium dehydroacetate, gluconolactone, pentanediol, hexanediol and p-hydroxyacetophenone.
A preparation method of a hair wet tissue feed liquid with sun-proof and color-protecting functions comprises the following steps:
(1) pre-dispersing a film forming agent by using 1, 3-butanediol, adding deionized water, heating and stirring until the film forming agent is completely dissolved to obtain a mixture A;
(2) cooling the mixture A to below 45 ℃, and sequentially adding an active substance, a humectant, a preservative and essence to obtain a mixture B;
(3) and cooling the mixture B to room temperature, adding a pH regulator, and finally adding ethanol to obtain the hair wet tissue feed liquid with the sun-screening and color-protecting functions.
Has the advantages that: the hair wet tissue liquid with the sun-proof and color-protecting functions can help hair reduce hair damage caused by sun-drying and slow down hair dyeing and color losing. The product can help to supplement the lipid on the surface layer of the hair, protect the hair flakes and prevent the hair flakes from tilting, so that dye molecules are prevented from falling off, the hair color losing condition is relieved, the hair is protected from being damaged, and the product has an ultraviolet absorption function and reduces the damage of ultraviolet rays to the hair.
Detailed Description
The technical features of the technical solutions provided by the present invention are further clearly and completely described below with reference to the specific embodiments, and the scope of protection is not limited thereto.
The words "preferred", "more preferred", and the like, in the present invention refer to embodiments of the invention that may provide certain benefits, under certain circumstances. However, other embodiments may be preferred, under the same or other circumstances. Furthermore, the recitation of one or more preferred embodiments does not imply that other embodiments are not useful, nor is it intended to exclude other embodiments from the scope of the invention.
When a range of values is disclosed herein, the range is considered to be continuous and includes both the minimum and maximum values of the range, as well as each value between such minimum and maximum values. Further, when a range refers to an integer, each integer between the minimum and maximum values of the range is included. Further, when multiple range-describing features or characteristics are provided, the ranges may be combined. In other words, unless otherwise indicated, all ranges disclosed herein are to be understood to encompass any and all subranges subsumed therein. For example, a stated range from "1 to 10" should be considered to include any and all subranges between the minimum value of 1 and the maximum value of 10. Exemplary subranges of the range 1 to 10 include, but are not limited to, 1 to 6.1, 3.5 to 7.8, 5.5 to 10, and the like.
In order to solve the above problems, the first aspect of the present invention provides a hair wet towel feed liquid with sunscreen and color protection functions, comprising the following components: film forming agent, active matter, humectant, pH regulator, 1, 3-butanediol, essence, preservative, ethanol and deionized water.
In a preferred embodiment, the hair wet tissue solution comprises the following components in parts by weight: 0.01-5 parts of film forming agent, 2-10 parts of active matter, 0.05-2 parts of humectant, 0.1-0.5 part of pH regulator, 0.5-2 parts of 1, 3-butanediol, 0-1 part of essence, 0.5-2 parts of preservative, 0-15 parts of ethanol and 60-90 parts of deionized water.
In a preferred embodiment, the hair wet tissue solution comprises the following components in parts by weight: 0.1-3 parts of film forming agent, 3-8 parts of active matter, 0.1-0.4 part of humectant, 0.2-0.4 part of pH regulator, 1-1.5 parts of 1, 3-butanediol, 0.2-0.8 part of essence, 0.8-1.2 parts of preservative, 2-10 parts of ethanol and 70-80 parts of deionized water.
In a preferred embodiment, the hair wet tissue solution comprises the following components in parts by weight: 0.2-1.5 parts of film forming agent, 4-6 parts of active matter, 0.1-0.2 part of humectant, 0.2-0.3 part of pH regulator, 1.0-1.5 parts of 1, 3-butanediol, 0.3-0.6 part of essence, 0.9-1.2 parts of preservative, 3-8 parts of ethanol and 72-78 parts of deionized water.
Film forming agent
The film forming agent is a high molecular polymer generally, and different polymers bring different use effects. According to their origin and properties, they can be classified into protein film formers, acrylic resin film formers, polyethylene copolymers, copolymers of various hydrocarbons, silicone polymers, silicone acrylates, and the like.
In a preferred embodiment, the film forming agent of the present invention is selected from one or more of polyethylene glycol derivatives, polyvinylpyrrolidone, acrylamide propyl trimethyl ammonium chloride/acrylamide copolymers, acrylic copolymers, acrylate copolymers, modified silicone oil, tremella polysaccharides, sodium hyaluronate, tamarind seed gum, beta-glucan, trehalose, gum arabic, and sodium cellulose sulfate.
In a preferred embodiment, the film-forming agent is prepared by compounding PEG-8 polydimethylsiloxane and polyethylene glycol-90M according to the weight ratio of 1 (0.01-0.03); the polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou Mei; the PEG-8 polydimethylsiloxane was purchased from Hongyui chemical Co., Ltd, Guangzhou.
The inventor of the application adds the PEG-8 polydimethylsiloxane into the formula, and finds that the film-forming property is poor when the PEG-8 polydimethylsiloxane is generally used after the hair quality is damaged, so that the PEG-90M is compounded according to a certain proportion, and the product can be used for repairing the damaged hair quality and nursing the healthy hair quality. The inventor conjectures that after the two are compounded, the polyethylene glycol-90M can form a film on the surface of the hair firstly, and simultaneously, the polyethylene glycol-90M and PEG-8 polydimethylsiloxane are mutually cooperated to form a network structure to be uniformly spread on the hair to form a firm protective film, so that hair scales can be smoothed, the loss of dye molecules in the hair perming and dyeing process is reduced, the color fading is slowed down, and when the weight ratio of the PEG-8 polydimethylsiloxane to the polyethylene glycol-90M is 1 (0.01-0.03), the product has a better effect.
Active substance
In a preferred embodiment, the active according to the invention is selected from one or more of sunflower seed extract, haematococcus pluvialis extract, quercus robur fruit extract, cinnamide propyl trimethyl ammonium chloride, methoxy cinnamide propyl hydroxysultaine.
In a preferred embodiment, the weight ratio of the active substance, the film forming agent and the humectant is 1 (0.005-0.5) to (0.02-0.2).
In a preferred embodiment, the active of the invention is Haematococcus pluvialis extract, purchased from Shanghai Biotech limited.
The inventor of the application adds the active substance into a formula to improve the problem of withered and yellow hair of hair caused by long-time solarization, and the inventor finds that when the weight ratio of the active substance to the film-forming agent to the humectant is 1 (0.005-0.5) to (0.02-0.2), the active substance, the film-forming agent and the humectant can play a better role in sun screening and color protecting, and the hair is enabled to be more smooth and bright. And secondly, due to the existence of the active agent, the active agent can be uniformly dispersed on the surface of the hair under the synergistic action with other components, so that the irradiation of sunlight is comprehensively resisted, and the loss of dye molecules caused by the warping of hair flakes is reduced. The 1, 3-butanediol is mainly used for dispersing a film forming agent and has a moisturizing effect, and in addition, the addition of the ethanol can ensure that the feed liquid can be quickly volatilized on the hair, so that the natural air drying speed of the hair is accelerated.
Moisture-retaining agent
The moisturizer is a hydrophilic skin moisturizing substance, has the capacity of combining water in a lower humidity range and replenishing water to the skin, and can maintain the skin in a balanced state with the water content higher than the normal water content by controlling the water exchange between a product and the ambient air, thereby playing the role of relieving the dryness of the skin.
In a preferred embodiment, the humectant of the present invention is selected from one or more of glycerin, polyalkylene glycol, urea, D or DL panthenol, hexane-1, 2, 6-triol, guanidine or its derivatives, alkylene glycol.
In a preferred embodiment, the humectant of the present invention is ethylhexyl glycerin, available from wuhan eosin science and technology ltd.
The inventor finds that the humectant is added into the formula to prevent the hair from drying easily, and the humectant is cooperated with the rest components in the formula to promote the hair to be more bright and natural.
pH regulator
The acidity regulator is also called pH regulator, and is used to maintain or change the pH value of the product. It is mainly useful to control the acidifying agent, the alkaling agent and the salts with buffering action required by the product.
In a preferred embodiment, the pH regulator of the present invention is selected from one or more of sodium hydroxide, sodium citrate, sodium dihydrogen phosphate, disodium hydrogen phosphate, sodium acetate, citric acid, phosphoric acid, acetic acid, hydrochloric acid, and arginine.
In a preferred embodiment, the pH modifier of the invention is arginine and has a repair effect on damaged hair, and is purchased from mitani zeuginese biotechnology limited.
Essence
The essence is a raw material for endowing cosmetics with certain fragrance, is one of key raw materials in the manufacturing process, is prepared by blending and mixing various spices, and has certain type of fragrance, namely fragrance type.
In some embodiments, the essence of the present invention is selected from one or more of lavender essence, rose essence, osmanthus essence, lily essence, chamomile essence, green apple essence, strawberry essence, papaya essence, hami melon essence, cherry essence, and juicy peach essence.
In a preferred embodiment, the fragrance of the present invention is a rose fragrance, purchased from Guangzhou Baoshidi perfumery, Inc.
Preservative
The preservative of the present invention refers to a natural or synthetic chemical ingredient used in foods, medicines, paints, biological specimens, etc. to retard spoilage caused by microbial growth or chemical changes.
In some embodiments, the preservative of the present invention is selected from one or more of cetylpyridinium chloride, benzalkonium chloride, chlorphenesin, polyallylguanide, chlorhexidine digluconate, benzethonium chloride, phenoxyethanol, benzoic acid, sodium benzoate, caprylyl hydroxamic acid, sodium dehydroacetate, gluconolactone, pentanediol, hexanediol, and p-hydroxyacetophenone.
In a preferred embodiment, the preservative of the present invention is caprylhydroxamic acid, purchased from golden Carlo, Inc. of Shanghai.
The second aspect of the invention provides a preparation method of a hair wet tissue feed liquid with sun-proof and color-protecting functions, which comprises the following steps:
(1) pre-dispersing a film forming agent by using 1, 3-butanediol, adding deionized water, heating and stirring until the film forming agent is completely dissolved to obtain a mixture A;
(2) cooling the mixture A to below 45 ℃, and sequentially adding an active substance, a humectant, a preservative and essence to obtain a mixture B;
(3) and cooling the mixture B to room temperature, adding a pH regulator, and finally adding ethanol to obtain the hair wet tissue feed liquid with the sun-screening and color-protecting functions.
The present invention will now be described in detail by way of examples, and the starting materials used are commercially available unless otherwise specified.
Examples
Example 1
Embodiment 1 provides a hair wet tissue feed liquid with sun-screening and color-protecting functions, which comprises the following components: 0.01 part of film forming agent, 2 parts of active matter, 0.05 part of humectant, 0.1 part of pH regulator, 0.5 part of 1, 3-butanediol, 0 part of essence, 0.5 part of preservative, 0 part of ethanol and 60 parts of deionized water.
The film-forming agent is obtained by compounding PEG-8 polydimethylsiloxane and polyethylene glycol-90M according to the weight ratio of 1: 0.01; the polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou Mei; the PEG-8 polydimethylsiloxane was purchased from Hongyui chemical Co., Ltd, Guangzhou.
The active substance is Haematococcus pluvialis extract, and is purchased from Shanghai Gayu Biotech Co.
The humectant was ethylhexylglycerin, purchased from wuhan eosin science co.
The pH adjusting agent is arginine, purchased from Wuxi Jiuxin Biotech limited.
The essence is rose essence, and is purchased from Guangzhou Baoshidi essence and spice Co.
The preservative is caprylyl hydroxamic acid, purchased from golden mosaic, inc.
A preparation method of a hair wet tissue feed liquid with sun-proof and color-protecting functions comprises the following steps:
(1) pre-dispersing a film forming agent by using 1, 3-butanediol, adding deionized water, heating and stirring until the film forming agent is completely dissolved to obtain a mixture A;
(2) cooling the mixture A to below 45 ℃, and sequentially adding an active substance, a humectant, a preservative and essence to obtain a mixture B;
(3) and cooling the mixture B to room temperature, adding a pH regulator, and finally adding ethanol to obtain the hair wet tissue feed liquid with the sun-screening and color-protecting functions.
Example 2
Embodiment 2 provides a hair wet tissue feed liquid with sun-screening and color-protecting functions, which comprises the following components: 5 parts of film forming agent, 10 parts of active matter, 2 parts of humectant, 0.5 part of pH regulator, 2 parts of 1, 3-butanediol, 1 part of essence, 2 parts of preservative, 15 parts of ethanol and 90 parts of deionized water.
The film-forming agent is obtained by compounding PEG-8 polydimethylsiloxane and polyethylene glycol-90M according to the weight ratio of 1: 0.03; the polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou Mei; the PEG-8 polydimethylsiloxane was purchased from Hongyui chemical Co., Ltd, Guangzhou.
The active substance is Haematococcus pluvialis extract, and is purchased from Shanghai Gayu Biotech Co.
The humectant was ethylhexylglycerin, purchased from wuhan eosin science co.
The pH adjusting agent is arginine, purchased from Wuxi Jiuxin Biotech limited.
The essence is rose essence, and is purchased from Guangzhou Baoshidi essence and spice Co.
The preservative is caprylyl hydroxamic acid, purchased from golden mosaic, inc.
A method for preparing a hair wet tissue feed liquid with sun-proof and color-protecting functions, which comprises the same steps as example 1.
Example 3
Embodiment 3 provides a hair wet tissue feed liquid with sun-screening and color-protecting functions, which comprises the following components: 0.1 part of film forming agent, 3 parts of active matter, 0.1 part of humectant, 0.2 part of pH regulator, 1 part of 1, 3-butanediol, 0.2 part of essence, 0.8 part of preservative, 2 parts of ethanol and 70 parts of deionized water.
The film forming agent is obtained by compounding PEG-8 polydimethylsiloxane and polyethylene glycol-90M according to the weight ratio of 1: 0.02; the polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou Mei; the PEG-8 polydimethylsiloxane was purchased from Hongyui chemical Co., Ltd, Guangzhou.
The active substance is Haematococcus pluvialis extract, and is purchased from Shanghai Gayu Biotech Co.
The humectant was ethylhexylglycerin, purchased from wuhan eosin science co.
The pH adjusting agent is arginine, purchased from Wuxi Jiuxin Biotech limited.
The essence is rose essence, and is purchased from Guangzhou Baoshidi essence and spice Co.
The preservative is caprylyl hydroxamic acid, purchased from golden mosaic, inc.
A method for preparing a hair wet tissue feed liquid with sun-proof and color-protecting functions, which comprises the same steps as example 1.
Example 4
Embodiment 4 provides a hair wet tissue feed liquid with sun-screening and color-protecting functions, which comprises the following components: 3 parts of film forming agent, 8 parts of active matter, 0.4 part of humectant, 0.4 part of pH regulator, 1.5 parts of 1, 3-butanediol, 0.8 part of essence, 1.2 parts of preservative, 10 parts of ethanol and 80 parts of deionized water.
The film forming agent is obtained by compounding PEG-8 polydimethylsiloxane and polyethylene glycol-90M according to the weight ratio of 1: 0.02; the polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou Mei; the PEG-8 polydimethylsiloxane was purchased from Hongyui chemical Co., Ltd, Guangzhou.
The active substance is Haematococcus pluvialis extract, and is purchased from Shanghai Gayu Biotech Co.
The humectant was ethylhexylglycerin, purchased from wuhan eosin science co.
The pH adjusting agent is arginine, purchased from Wuxi Jiuxin Biotech limited.
The essence is rose essence, and is purchased from Guangzhou Baoshidi essence and spice Co.
The preservative is caprylyl hydroxamic acid, purchased from golden mosaic, inc.
A method for preparing a hair wet tissue feed liquid with sun-proof and color-protecting functions, which comprises the same steps as example 1.
Example 5
Embodiment 5 provides a hair wet tissue feed liquid with sun-screening and color-protecting functions, which comprises the following components: 0.5 part of film forming agent, 5 parts of active matter, 0.1 part of humectant, 0.22 part of pH regulator, 1 part of 1, 3-butanediol, 0.5 part of essence, 1 part of preservative, 5 parts of ethanol and 75 parts of deionized water.
The film forming agent is obtained by compounding PEG-8 polydimethylsiloxane and polyethylene glycol-90M according to the weight ratio of 1: 0.02; the polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou Mei; the PEG-8 polydimethylsiloxane was purchased from Hongyui chemical Co., Ltd, Guangzhou.
The active substance is Haematococcus pluvialis extract, and is purchased from Shanghai Gayu Biotech Co.
The humectant was ethylhexylglycerin, purchased from wuhan eosin science co.
The pH adjusting agent is arginine, purchased from Wuxi Jiuxin Biotech limited.
The essence is rose essence, and is purchased from Guangzhou Baoshidi essence and spice Co.
The preservative is caprylyl hydroxamic acid, purchased from golden mosaic, inc.
A method for preparing a hair wet tissue feed liquid with sun-proof and color-protecting functions, which comprises the same steps as example 1.
Comparative example 1
Comparative example 1 provides a hair wet wipe feed solution with sunscreen and color protection functions, comprising the following components: 0 part of film forming agent, 5 parts of active matter, 0.1 part of humectant, 0.22 part of pH regulator, 1 part of 1, 3-butanediol, 0.5 part of essence, 1 part of preservative, 5 parts of ethanol and 75 parts of deionized water.
The film forming agent is obtained by compounding PEG-8 polydimethylsiloxane and polyethylene glycol-90M according to the weight ratio of 1: 0.02; the polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou Mei; the PEG-8 polydimethylsiloxane was purchased from Hongyui chemical Co., Ltd, Guangzhou.
The active substance is Haematococcus pluvialis extract, and is purchased from Shanghai Gayu Biotech Co.
The humectant was ethylhexylglycerin, purchased from wuhan eosin science co.
The pH adjusting agent is arginine, purchased from Wuxi Jiuxin Biotech limited.
The essence is rose essence, and is purchased from Guangzhou Baoshidi essence and spice Co.
The preservative is caprylyl hydroxamic acid, purchased from golden mosaic, inc.
A method for preparing a hair wet tissue feed liquid with sun-proof and color-protecting functions, which comprises the same steps as example 1.
Comparative example 2
Comparative example 2 provides a hair wet wipe feed solution with sunscreen and color protection functions, comprising the following components: 20 parts of film forming agent, 5 parts of active matter, 0.1 part of humectant, 0.22 part of pH regulator, 1 part of 1, 3-butanediol, 0.5 part of essence, 1 part of preservative, 5 parts of ethanol and 75 parts of deionized water.
The film forming agent is obtained by compounding PEG-8 polydimethylsiloxane and polyethylene glycol-90M according to the weight ratio of 1: 0.02; the polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou Mei; the PEG-8 polydimethylsiloxane was purchased from Hongyui chemical Co., Ltd, Guangzhou.
The active substance is Haematococcus pluvialis extract, and is purchased from Shanghai Gayu Biotech Co.
The humectant was ethylhexylglycerin, purchased from wuhan eosin science co.
The pH adjusting agent is arginine, purchased from Wuxi Jiuxin Biotech limited.
The essence is rose essence, and is purchased from Guangzhou Baoshidi essence and spice Co.
The preservative is caprylyl hydroxamic acid, purchased from golden mosaic, inc.
A method for preparing a hair wet tissue feed liquid with sun-proof and color-protecting functions, which comprises the same steps as example 1.
Comparative example 3
Comparative example 3 provides a hair wet wipe feed solution with sunscreen and color protection functions, comprising the following components: 0.5 part of film forming agent, 0.05 part of active matter, 0.1 part of humectant, 0.22 part of pH regulator, 1 part of 1, 3-butanediol, 0.5 part of essence, 1 part of preservative, 5 parts of ethanol and 75 parts of deionized water.
The film forming agent is obtained by compounding PEG-8 polydimethylsiloxane and polyethylene glycol-90M according to the weight ratio of 1: 0.02; the polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou Mei; the PEG-8 polydimethylsiloxane was purchased from Hongyui chemical Co., Ltd, Guangzhou.
The active substance is Haematococcus pluvialis extract, and is purchased from Shanghai Gayu Biotech Co.
The humectant was ethylhexylglycerin, purchased from wuhan eosin science co.
The pH adjusting agent is arginine, purchased from Wuxi Jiuxin Biotech limited.
The essence is rose essence, and is purchased from Guangzhou Baoshidi essence and spice Co.
The preservative is caprylyl hydroxamic acid, purchased from golden mosaic, inc.
A method for preparing a hair wet tissue feed liquid with sun-proof and color-protecting functions, which comprises the same steps as example 1.
Comparative example 4
Comparative example 4 provides a hair wet wipe feed solution with sunscreen and color protection functions, comprising the following components: 0.5 part of film forming agent, 30 parts of active matter, 0.1 part of humectant, 0.22 part of pH regulator, 1 part of 1, 3-butanediol, 0.5 part of essence, 1 part of preservative, 5 parts of ethanol and 75 parts of deionized water.
The film forming agent is obtained by compounding PEG-8 polydimethylsiloxane and polyethylene glycol-90M according to the weight ratio of 1: 0.02; the polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou Mei; the PEG-8 polydimethylsiloxane was purchased from Hongyui chemical Co., Ltd, Guangzhou.
The active substance is Haematococcus pluvialis extract, and is purchased from Shanghai Gayu Biotech Co.
The humectant was ethylhexylglycerin, purchased from wuhan eosin science co.
The pH adjusting agent is arginine, purchased from Wuxi Jiuxin Biotech limited.
The essence is rose essence, and is purchased from Guangzhou Baoshidi essence and spice Co.
The preservative is caprylyl hydroxamic acid, purchased from golden mosaic, inc.
A method for preparing a hair wet tissue feed liquid with sun-proof and color-protecting functions, which comprises the same steps as example 1.
Comparative example 5
Comparative example 5 provides a hair wet wipe feed solution with sunscreen and color protection functions, comprising the following components: 0.5 part of film forming agent, 5 parts of active matter, 0.01 part of humectant, 0.22 part of pH regulator, 1 part of 1, 3-butanediol, 0.5 part of essence, 1 part of preservative, 5 parts of ethanol and 75 parts of deionized water.
The film forming agent is obtained by compounding PEG-8 polydimethylsiloxane and polyethylene glycol-90M according to the weight ratio of 1: 0.02; the polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou Mei; the PEG-8 polydimethylsiloxane was purchased from Hongyui chemical Co., Ltd, Guangzhou.
The active substance is Haematococcus pluvialis extract, and is purchased from Shanghai Gayu Biotech Co.
The humectant was ethylhexylglycerin, purchased from wuhan eosin science co.
The pH adjusting agent is arginine, purchased from Wuxi Jiuxin Biotech limited.
The essence is rose essence, and is purchased from Guangzhou Baoshidi essence and spice Co.
The preservative is caprylyl hydroxamic acid, purchased from golden mosaic, inc.
A method for preparing a hair wet tissue feed liquid with sun-proof and color-protecting functions, which comprises the same steps as example 1.
Comparative example 6
Comparative example 6 provides a hair wet wipe feed solution with sunscreen and color protection functions, comprising the following components: 0.5 part of film forming agent, 5 parts of active matter, 15 parts of humectant, 0.22 part of pH regulator, 1 part of 1, 3-butanediol, 0.5 part of essence, 1 part of preservative, 5 parts of ethanol and 75 parts of deionized water.
The film forming agent is obtained by compounding PEG-8 polydimethylsiloxane and polyethylene glycol-90M according to the weight ratio of 1: 0.02; the polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou Mei; the PEG-8 polydimethylsiloxane was purchased from Hongyui chemical Co., Ltd, Guangzhou.
The active substance is Haematococcus pluvialis extract, and is purchased from Shanghai Gayu Biotech Co.
The humectant was ethylhexylglycerin, purchased from wuhan eosin science co.
The pH adjusting agent is arginine, purchased from Wuxi Jiuxin Biotech limited.
The essence is rose essence, and is purchased from Guangzhou Baoshidi essence and spice Co.
The preservative is caprylyl hydroxamic acid, purchased from golden mosaic, inc.
A method for preparing a hair wet tissue feed liquid with sun-proof and color-protecting functions, which comprises the same steps as example 1.
Comparative example 7
Comparative example 7 provides a hair wet wipe feed solution with sunscreen and color protection functions, comprising the following components: 0.5 part of film forming agent, 5 parts of active matter, 0.1 part of humectant, 0.22 part of pH regulator, 1 part of 1, 3-butanediol, 0.5 part of essence, 1 part of preservative, 5 parts of ethanol and 75 parts of deionized water.
The film-forming agent is obtained by compounding PEG-8 polydimethylsiloxane and polyethylene glycol-90M according to the weight ratio of 1: 1; the polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou Mei; the PEG-8 polydimethylsiloxane was purchased from Hongyui chemical Co., Ltd, Guangzhou.
The active substance is Haematococcus pluvialis extract, and is purchased from Shanghai Gayu Biotech Co.
The humectant was ethylhexylglycerin, purchased from wuhan eosin science co.
The pH adjusting agent is arginine, purchased from Wuxi Jiuxin Biotech limited.
The essence is rose essence, and is purchased from Guangzhou Baoshidi essence and spice Co.
The preservative is caprylyl hydroxamic acid, purchased from golden mosaic, inc.
A method for preparing a hair wet tissue feed liquid with sun-proof and color-protecting functions, which comprises the same steps as example 1.
Comparative example 8
Comparative example 8 provides a hair wipe feed solution with sunscreen and color protection functions, comprising the following components: 0.5 part of film forming agent, 5 parts of active matter, 0.1 part of humectant, 0.22 part of pH regulator, 1 part of 1, 3-butanediol, 0.5 part of essence, 1 part of preservative, 5 parts of ethanol and 75 parts of deionized water.
The film-forming agent is obtained by compounding PEG-8 polydimethylsiloxane and polyethylene glycol-90M according to the weight ratio of 5: 1; the polyethylene glycol-90M was purchased from chemical Co., Ltd, Guangzhou Mei; the PEG-8 polydimethylsiloxane was purchased from Hongyui chemical Co., Ltd, Guangzhou.
The active substance is Haematococcus pluvialis extract, and is purchased from Shanghai Gayu Biotech Co.
The humectant was ethylhexylglycerin, purchased from wuhan eosin science co.
The pH adjusting agent is arginine, purchased from Wuxi Jiuxin Biotech limited.
The essence is rose essence, and is purchased from Guangzhou Baoshidi essence and spice Co.
The preservative is caprylyl hydroxamic acid, purchased from golden mosaic, inc.
A method for preparing a hair wet tissue feed liquid with sun-proof and color-protecting functions, which comprises the same steps as example 1.
Evaluation of Performance
1. Hair flexibility test
The test method comprises the following steps: carrying out sensory evaluation on the hair tresses treated by the feed liquid, wherein the flexibility evaluation standard adopts 5 grades, and 1 grade represents very poor performance; 2 denotes the difference; score 3 indicates general; 4 points are well represented; score 5 indicates very good.
2. Hair smoothness test
The test method comprises the following steps: 65 poor hair quality testers were selected, and five individuals in each group treated the hair by using the products described in the examples and comparative examples in a double-blind manner, and the evaluation of hair smoothness was given by 0-10 points, 10 points representing the most satisfactory performance of the testers per se, and 0 point representing the unsatisfactory performance.
3. Test for fading alleviation degree
The test method comprises the following steps: the dyed hair is treated with the products described in the examples and comparative examples and, after 48h of UV irradiation, the integrated difference in chromaticity dE is calculated1A value; after the dyed hair without any treatment is irradiated by UV for 48 hours, the comprehensive chromaticity difference dE is calculated2A value; calculating a fading mitigation degree, wherein the fading mitigation degree is (dE)2-dE1)×100/dE2。
Testing method of dE value: after dyeing the hair, the Lab value (comprising a) is measured0、b0、L0Parameters); measuring Lab values (including a, b and L parameters) after the hair is irradiated by UV for 48 hours; the dE value is calculated as:
TABLE 1
Claims (8)
1. A hair wet tissue feed liquid with sun-proof and color-protecting functions is characterized by comprising the following components: film forming agent, active matter, humectant, pH regulator, 1, 3-butanediol, essence, preservative, ethanol and deionized water;
the weight ratio of the active substance, the film forming agent and the humectant is 1 (0.005-0.5) to 0.02-0.2);
the film-forming agent is obtained by compounding PEG-8 polydimethylsiloxane and polyethylene glycol-90M according to the weight ratio of 1 (0.01-0.03).
2. The hair wet wipe feed liquid according to claim 1, which is characterized by comprising the following components in parts by weight: 0.01-5 parts of film forming agent, 2-10 parts of active matter, 0.05-2 parts of humectant, 0.1-0.5 part of pH regulator, 0.5-2 parts of 1, 3-butanediol, 0-1 part of essence, 0.5-2 parts of preservative, 0-15 parts of ethanol and 60-90 parts of deionized water.
3. The hair wet wipe feed liquid according to claim 2, which is characterized by comprising the following components in parts by weight: 0.1-3 parts of film forming agent, 3-8 parts of active matter, 0.1-0.4 part of humectant, 0.2-0.4 part of pH regulator, 1-1.5 parts of 1, 3-butanediol, 0.2-0.8 part of essence, 0.8-1.2 parts of preservative, 2-10 parts of ethanol and 70-80 parts of deionized water.
4. The hair wet wipe feed liquid according to claim 3, which is characterized by comprising the following components in parts by weight: 0.2-1.5 parts of film forming agent, 4-6 parts of active matter, 0.1-0.2 part of humectant, 0.2-0.3 part of pH regulator, 1.0-1.5 parts of 1, 3-butanediol, 0.3-0.6 part of essence, 0.9-1.2 parts of preservative, 3-8 parts of ethanol and 72-78 parts of deionized water.
5. The hair wet wipe feed of claim 1 wherein the active is selected from one or more of sunflower seed extract, haematococcus pluvialis extract, quercus robur fruit extract, cinnamide propyl trimethyl ammonium chloride, methoxy cinnamide propyl hydroxysultaine.
6. The hair wet wipe feed liquid of claim 1, wherein the essence is selected from one or more of lavender essence, rose essence, osmanthus essence, lily essence, chamomile essence, green apple essence, strawberry essence, papaya essence, hami melon essence, cherry essence, and juicy peach essence.
7. The wet wipe feed of claim 1 wherein the preservative is selected from one or more of cetylpyridinium chloride, benzalkonium chloride, chlorphenesin, polyallybiguanide, chlorhexidine digluconate, benzethonium chloride, phenoxyethanol, benzoic acid, sodium benzoate, caprylhydroxamic acid, sodium dehydroacetate, gluconolactone, pentanediol, hexanediol, and p-hydroxyacetophenone.
8. The method for preparing the hair wet wipe feed liquid according to claim 1, which is characterized by comprising the following steps:
(1) pre-dispersing a film forming agent by using 1, 3-butanediol, adding deionized water, heating and stirring until the film forming agent is completely dissolved to obtain a mixture A;
(2) cooling the mixture A to below 45 ℃, and sequentially adding an active substance, a humectant, a preservative and essence to obtain a mixture B;
(3) and cooling the mixture B to room temperature, adding a pH regulator, and finally adding ethanol to obtain the hair wet tissue feed liquid with the sun-screening and color-protecting functions.
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| CN111346037B (en) * | 2020-01-13 | 2021-08-06 | 章华化妆品科技有限公司 | Preparation and application of plant composition with ultraviolet light protection, color protection and hair care effects |
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