CN104478295A - Compressive and fireproof artificial quartz stone sheet and preparation method thereof - Google Patents
Compressive and fireproof artificial quartz stone sheet and preparation method thereof Download PDFInfo
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- CN104478295A CN104478295A CN201410778678.2A CN201410778678A CN104478295A CN 104478295 A CN104478295 A CN 104478295A CN 201410778678 A CN201410778678 A CN 201410778678A CN 104478295 A CN104478295 A CN 104478295A
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Abstract
The invention discloses a compressive and fireproof artificial quartz stone sheet and a preparation method thereof. The artificial quartz stone sheet comprises the following components in parts by weight: 50-80 parts of (6-100)-mesh quartz stone, 40- 60 parts of 325-mesh quartz powder, 5-10 parts of broken glass, 5-10 parts of fiber, 5-10 parts of unsaturated resin, 5-15 parts of (50-100)-mesh sillimanite powder, 5-15 parts of (100-200)-mesh zirconium silicate powder, 0.3-0.5 part of an additive and 0.3-0.8 part of a pigment. During the preparation, the sillimanite powder, zirconium silicate powder and fiber are added so as to improve the compressive property and fireproof property of the artificial quartz stone sheet and meanwhile, the preparation cost is low, the preparation method is simple and is suitable for industrial production.
Description
Technical field
The invention belongs to material of construction preparing technical field, specifically, refer to a kind of resistance to compression, fireproof artificial quartz stone sheet material and preparation method thereof.
Background technology
Artificial quartz stone plate is compared with artificial marble sheet material, there is the features such as sinuousness is high, compressive strength is high, Mohs' hardness is high, water-intake rate is low, gradually like by domestic and international users, be widely applied to cabinet, bathroom, the ground of office and megastore, wall decoration and household industry.However, also there is certain drawback in artificial quartz stone plate, and such as fire resistance is not good, easily ftracture, and these drawbacks significantly limit the application of artificial quartz in lump at various complex condition.
Summary of the invention
Technical problem to be solved by this invention is not enough for prior art, provides a kind of resistance to compression, fireproof artificial quartz stone sheet material and preparation method thereof, and the artificial quartz stone plate adopting the present invention to prepare has resistance to compression, fire prevention effect.
The technical scheme that the present invention solves the problems of the technologies described above is as follows: resistance to compression, fireproof artificial quartz stone sheet material, be made up of the component of following parts by weight: 6 ~ 100 order quartzites 50 ~ 80 parts, 325 order silica powders 40 ~ 60 parts, glass cullet 5 ~ 10 parts, fiber 5 ~ 10 parts, unsaturated polyester 5 ~ 10 parts, 50 ~ 100 5 ~ 15 parts, order sillimanite powder, 100 ~ 200 order zirconium silicate powders 5 ~ 15 parts, auxiliary agent 0.3 ~ 0.5 part, pigment 0.3 ~ 0.8 part.
On the basis of technique scheme, the present invention can also do following improvement.
Further, be made up of the component of following parts by weight: 6 ~ 100 order quartzites 60 parts, 325 order silica powders 50 parts, glass cullet 8 parts, fiber 8 parts, unsaturated polyester 8 parts, 50 ~ 100 10 parts, order sillimanite powder, 100 ~ 200 order zirconium silicate powders 10 parts, auxiliary agent 0.4 part, pigment 0.5 part.
Further, described fiber is brucite fiber, and length is 3 ~ 10mm.
Further, described unsaturated polyester is one or more in epoxy resin, resol, acryl resin and urethane resin.
Further, described auxiliary agent is the mixture of silane coupling agent and peroxide-2-ethyl hexanoic acid tert-butyl, and the part by weight of described silane coupling agent and peroxide-2-ethyl hexanoic acid tert-butyl is 3:1.
Further, described pigment be titanium dioxide, iron oxide yellow powder, iron oxide red, iron black powder, chrome green powder, Lan Shuizhong one or more.
Resistance to compression, fireproof artificial quartz stone preparation of plates method, comprise following processing step: the component taking following parts by weight: 6 ~ 100 order quartzites 50 ~ 80 parts, 325 order silica powders 40 ~ 60 parts, glass cullet 5 ~ 10 parts, fiber 5 ~ 10 parts, unsaturated polyester 5 ~ 10 parts, 50 ~ 100 5 ~ 15 parts, order sillimanite powder, 100 ~ 200 order zirconium silicate powders 5 ~ 15 parts, auxiliary agent 0.3 ~ 0.5 part, pigment 0.3 ~ 0.8 part, by above-mentioned each component Homogeneous phase mixing, the material mixed evenly is tiled on making sheet mould, then making sheet mould is sent into vacuum chamber, vacuumize, vibratory compaction, send into curing oven solidification again, sheet material after solidification is come out of the stove the demoulding, after stacking cooling, delivering to surely thick polishing machine carries out surely thick, after surface finish polished finish, artificial quartz in lump can be obtained.
On the basis of technique scheme, the present invention can also do following improvement.
Further, pressure during described vibratory compaction is 2.5 ~ 3.5MPa, and molding time is 2 ~ 3 minutes.
Further, the temperature of described solidification is 90 ~ 95 DEG C, and the time is 30 ~ 40 minutes.
The invention has the beneficial effects as follows:
(1) resistance to compression, fire prevention: sillimanite powder and zirconium silicate powder are good refractory materialss, and fusing point and hardness are very high, and they can improve the refractory temperature of artificial quartz stone plate of the present invention, extend fire resistance period, increases ultimate compression strength.Meanwhile, fiber also can improve the tensile strength of artificial quartz stone plate of the present invention.
(2) low cost of manufacture of the present invention, preparation method simply, are suitable for suitability for industrialized production.
Embodiment
Be described principle of the present invention and feature below in conjunction with specific embodiment, example, only for explaining the present invention, is not intended to limit scope of the present invention.
Embodiment 1:
Take 6 ~ 100 order quartzite 50kg, 325 order silica powder 60kg, glass cullet 5kg, brucite fiber 10kg, epoxy resin 5kg, 50 ~ 100 order sillimanite powder 15kg, 100 ~ 200 order zirconium silicate powder 5kg, part by weight is γ-(2,3-glycidoxy) propyl trimethoxy silicane and the peroxide-2-ethyl hexanoic acid tert-butyl mixture 0.5kg of 3:1, pigment 0.3kg, described pigment is made up of according to mass ratio 18:1 titanium dioxide and Lan Shui; By above-mentioned each component Homogeneous phase mixing, the material mixed evenly is tiled on making sheet mould, then making sheet mould is sent into vacuum chamber, when when vacuumizing, air pressure reaches-0.1MPa, under 2.5 ~ 3.5MPa pressure vibrate 2 ~ 3 minutes shaping, then send into curing oven solidification, solidification value 90 ~ 95 DEG C, time is 30 ~ 40 minutes, sheet material after solidification is come out of the stove the demoulding, after stacking cooling, delivers to surely thick polishing machine and carries out surely thick, after surface finish polished finish, " white board " artificial quartz in lump can be obtained.
Embodiment 2:
Take 6 ~ 100 order quartzite 80kg, 325 order silica powder 40kg, glass cullet 10kg, brucite fiber 5kg, resol 10kg, 50 ~ 100 order sillimanite powder 5kg, 100 ~ 200 order zirconium silicate powder 15kg, part by weight is the γ-(2 of 3:1,3-glycidoxy) propyl trimethoxy silicane and peroxide-2-ethyl hexanoic acid tert-butyl mixture 0.3kg, pigment 0.8kg, described pigment is made up of according to mass ratio 1076:47:1:310:125 titanium dioxide, iron oxide yellow powder, iron black powder, chrome green powder and Lan Shui; By above-mentioned each component Homogeneous phase mixing, the material mixed evenly is tiled on making sheet mould, then making sheet mould is sent into vacuum chamber, when when vacuumizing, air pressure reaches-0.1MPa, under 2.5 ~ 3.5MPa pressure vibrate 2 ~ 3 minutes shaping, then send into curing oven solidification, solidification value 90 ~ 95 DEG C, time is 30 ~ 40 minutes, sheet material after solidification is come out of the stove the demoulding, after stacking cooling, delivers to surely thick polishing machine and carries out surely thick, " pale yellow plate " artificial quartz in lump after surface finish polished finish, can be obtained.
Embodiment 3:
Take 6 ~ 100 order quartzite 60kg, 325 order silica powder 50kg, glass cullet 8kg, brucite fiber 8kg, urethane resin 8kg, 50 ~ 100 order sillimanite powder 10kg, 100 ~ 200 order zirconium silicate powder 10kg, part by weight is the γ-(2 of 3:1,3-glycidoxy) propyl trimethoxy silicane and peroxide-2-ethyl hexanoic acid tert-butyl mixture 0.4kg, pigment 0.5kg, described pigment is made up of according to mass ratio 980:1:2:3:118 titanium dioxide, iron oxide yellow powder, iron black powder, chrome green powder and Lan Shui; By above-mentioned each component Homogeneous phase mixing, the material mixed evenly is tiled on making sheet mould, then making sheet mould is sent into vacuum chamber, when when vacuumizing, air pressure reaches-0.1MPa, under 2.5 ~ 3.5MPa pressure vibrate 2 ~ 3 minutes shaping, then send into curing oven solidification, solidification value 90 ~ 95 DEG C, time is 30 ~ 40 minutes, sheet material after solidification is come out of the stove the demoulding, after stacking cooling, delivers to surely thick polishing machine and carries out surely thick, after surface finish polished finish, " spring's colours fill the garden " artificial quartz in lump can be obtained.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, within the spirit and principles in the present invention all, any amendment done, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (9)
1. resistance to compression, fireproof artificial quartz stone sheet material, it is characterized in that, be made up of the component of following parts by weight: 6 ~ 100 order quartzites 50 ~ 80 parts, 325 order silica powders 40 ~ 60 parts, glass cullet 5 ~ 10 parts, fiber 5 ~ 10 parts, unsaturated polyester 5 ~ 10 parts, 50 ~ 100 5 ~ 15 parts, order sillimanite powder, 100 ~ 200 order zirconium silicate powders 5 ~ 15 parts, auxiliary agent 0.3 ~ 0.5 part, pigment 0.3 ~ 0.8 part.
2. resistance to compression according to claim 1, fireproof artificial quartz stone sheet material, it is characterized in that, be made up of the component of following parts by weight: 6 ~ 100 order quartzites 60 parts, 325 order silica powders 50 parts, glass cullet 8 parts, fiber 8 parts, unsaturated polyester 8 parts, 50 ~ 100 10 parts, order sillimanite powder, 100 ~ 200 order zirconium silicate powders 10 parts, auxiliary agent 0.4 part, pigment 0.5 part.
3. resistance to compression according to claim 1 and 2, fireproof artificial quartz stone sheet material, is characterized in that, described fiber is brucite fiber, and length is 3 ~ 10mm.
4. resistance to compression according to claim 1 and 2, fireproof artificial quartz stone sheet material, is characterized in that, described unsaturated polyester is one or more in epoxy resin, resol, acryl resin and urethane resin.
5. resistance to compression according to claim 1 and 2, fireproof artificial quartz stone sheet material, it is characterized in that, described auxiliary agent is the mixture of silane coupling agent and peroxide-2-ethyl hexanoic acid tert-butyl, and the part by weight of described silane coupling agent and peroxide-2-ethyl hexanoic acid tert-butyl is 3:1.
6. resistance to compression according to claim 1 and 2, fireproof artificial quartz stone sheet material, is characterized in that, described pigment be titanium dioxide, iron oxide yellow powder, iron oxide red, iron black powder, chrome green powder, Lan Shuizhong one or more.
7. resistance to compression, fireproof artificial quartz stone preparation of plates method, it is characterized in that, comprise following processing step: the component taking following parts by weight: 6 ~ 100 order quartzites 50 ~ 80 parts, 325 order silica powders 40 ~ 60 parts, glass cullet 5 ~ 10 parts, fiber 5 ~ 10 parts, unsaturated polyester 5 ~ 10 parts, 50 ~ 100 5 ~ 15 parts, order sillimanite powder, 100 ~ 200 order zirconium silicate powders 5 ~ 15 parts, auxiliary agent 0.3 ~ 0.5 part, pigment 0.3 ~ 0.8 part, by above-mentioned each component Homogeneous phase mixing, the material mixed evenly is tiled on making sheet mould, then making sheet mould is sent into vacuum chamber, vacuumize, vibratory compaction, send into curing oven solidification again, sheet material after solidification is come out of the stove the demoulding, after stacking cooling, delivering to surely thick polishing machine carries out surely thick, after surface finish polished finish, artificial quartz in lump can be obtained.
8. resistance to compression according to claim 7, fireproof artificial quartz stone preparation of plates method, it is characterized in that, pressure during described vibratory compaction is 2.5 ~ 3.5MPa, molding time is 2 ~ 3 minutes.
9. resistance to compression according to claim 7, fireproof artificial quartz stone preparation of plates method, is characterized in that, the temperature of described solidification is 90 ~ 95 DEG C, and the time is 30 ~ 40 minutes.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410778678.2A CN104478295A (en) | 2014-12-15 | 2014-12-15 | Compressive and fireproof artificial quartz stone sheet and preparation method thereof |
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| CN201410778678.2A CN104478295A (en) | 2014-12-15 | 2014-12-15 | Compressive and fireproof artificial quartz stone sheet and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115925321A (en) * | 2023-02-17 | 2023-04-07 | 江苏百代节能建材有限公司 | High-strength ecological stone slab and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH02199049A (en) * | 1989-01-26 | 1990-08-07 | Matsushita Electric Works Ltd | Artificial stone and production thereof |
| CN101337805A (en) * | 2008-08-25 | 2009-01-07 | 张璐 | Artificial quartz in lump and fabrication technology thereof |
| CN102584115A (en) * | 2011-12-20 | 2012-07-18 | 汪洋 | Fireproof material, preparation method thereof and fireproof door |
| CN103204660A (en) * | 2013-03-20 | 2013-07-17 | 安徽瑞翔石英制品有限公司 | High-hardness artificial quartz stone plate and production process thereof |
-
2014
- 2014-12-15 CN CN201410778678.2A patent/CN104478295A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH02199049A (en) * | 1989-01-26 | 1990-08-07 | Matsushita Electric Works Ltd | Artificial stone and production thereof |
| CN101337805A (en) * | 2008-08-25 | 2009-01-07 | 张璐 | Artificial quartz in lump and fabrication technology thereof |
| CN102584115A (en) * | 2011-12-20 | 2012-07-18 | 汪洋 | Fireproof material, preparation method thereof and fireproof door |
| CN103204660A (en) * | 2013-03-20 | 2013-07-17 | 安徽瑞翔石英制品有限公司 | High-hardness artificial quartz stone plate and production process thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115925321A (en) * | 2023-02-17 | 2023-04-07 | 江苏百代节能建材有限公司 | High-strength ecological stone slab and preparation method thereof |
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Application publication date: 20150401 |