CN104529248A - Artificial quartz stone panel and preparation method thereof - Google Patents
Artificial quartz stone panel and preparation method thereof Download PDFInfo
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- CN104529248A CN104529248A CN201410778529.6A CN201410778529A CN104529248A CN 104529248 A CN104529248 A CN 104529248A CN 201410778529 A CN201410778529 A CN 201410778529A CN 104529248 A CN104529248 A CN 104529248A
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Abstract
The invention discloses an artificial quartz stone panel and a preparation method thereof. The artificial quartz sand panel is prepared from the following components in parts by weight: 30-90 parts of 3-80mesh quartz stones, 20-60 parts of 325mesh quartz powder, 5-15 parts of cullet, 3-10 parts of shells, 3-10 parts of fibers, 3-10 parts of 30-50mesh tourmaline, 3-12 parts of 50-100mesh sillimanite powder, 3-12 parts of 100-200mesh zirconium silicate powder, 5-10 parts of unsaturated resin, 0.3-0.5 part of auxiliaries and 0.3-0.8 part of pigments. According to the artificial quartz stone panel disclosed by the invention, in the preparation process, the fibers and tourmaline are added, so that the compressive property and the antibacterial property of the artificial quartz stone panel are improved and meanwhile, the sillimanite powder and the zirconium silicate powder are added, so that the fireproof performance of the artificial quartz stone panel is improved.
Description
Technical field
The invention belongs to material of construction preparing technical field, specifically, refer to a kind of artificial quartz stone plate and preparation method thereof.
Background technology
Artificial quartz in lump is as the substitute of lithotome, have high strength, high rigidity, high temperature resistant, protection against corrosion, anti-aging, easy to clean, wear-resisting, material is consummate, the unrivaled advantage of lithotome such as radiationless, now be widely used in the daily life of industrial production and the people, as the decorative material material of floor tile, metope etc.
But the artificial quartz in lump that prior art manufactures, exist density unevenness, hardness low, easily tie powder ball, yielding, easily aging, easily enter look, color and pattern single, not there is the defects such as anti-microbial effect, limit its larger application on a large scale, urgently to be resolved hurrily.
Summary of the invention
Technical problem to be solved by this invention is not enough for prior art, a kind of artificial quartz stone plate and preparation method thereof is provided, the artificial quartz stone plate wear resistance adopting the present invention to prepare is good, has antibacterial and fire-proof function, expands the range of application of artificial quartz in lump.
The technical scheme that the present invention solves the problems of the technologies described above is as follows: artificial quartz stone plate, be made up of the component of following parts by weight: 3 ~ 80 order quartzites 30 ~ 90 parts, 325 order silica powders 20 ~ 60 parts, glass cullet 5 ~ 15 parts, 3 ~ 10 parts, shell, fiber 3 ~ 10 parts, 30 ~ 50 3 ~ 10 parts, order tourmalinite, 50 ~ 100 3 ~ 12 parts, order sillimanite powder, 100 ~ 200 order zirconium silicate powders 3 ~ 12 parts, unsaturated polyester 5 ~ 10 parts, auxiliary agent 0.3 ~ 0.5 part, pigment 0.3 ~ 0.8 part.
On the basis of technique scheme, the present invention can also do following improvement.
Further, be made up of the component of following parts by weight: 3 ~ 80 order quartzites 70 parts, 325 order silica powders 40 parts, glass cullet 8 parts, 6 parts, shell, fiber 5 parts, 30 ~ 50 5 parts, order tourmalinite, 50 ~ 100 5 parts, order sillimanite powder, 100 ~ 200 order zirconium silicate powders 5 parts, unsaturated polyester 8 parts, auxiliary agent 0.4 part, pigment 0.5 part.
Further, described fiber is one or more in glass fibre, carbon fiber, basalt fibre, sapphire whisker, silicon carbide fiber and boron fibre.
Further, described unsaturated polyester is one or more in epoxy resin, resol, acryl resin and urethane resin.
Further, described auxiliary agent is the mixture of silane coupling agent and peroxide-2-ethyl hexanoic acid tert-butyl, and the part by weight of described silane coupling agent and peroxide-2-ethyl hexanoic acid tert-butyl is 3:1.
Further, described pigment be titanium dioxide, iron oxide yellow powder, iron oxide red, iron black powder, chrome green powder, Lan Shuizhong one or more.
The preparation method of artificial quartz stone plate, comprise following processing step: the component taking following parts by weight: 3 ~ 80 order quartzites 30 ~ 90 parts, 325 order silica powders 20 ~ 60 parts, glass cullet 5 ~ 15 parts, 3 ~ 10 parts, shell, fiber 3 ~ 10 parts, 30 ~ 50 3 ~ 10 parts, order tourmalinite, 50 ~ 100 3 ~ 12 parts, order sillimanite powder, 100 ~ 200 order zirconium silicate powders 3 ~ 12 parts, unsaturated polyester 5 ~ 10 parts, auxiliary agent 0.3 ~ 0.5 part, pigment 0.3 ~ 0.8 part, by above-mentioned each component Homogeneous phase mixing, the material mixed evenly is tiled on making sheet mould, then making sheet mould is sent into vacuum chamber, vacuumize, vibratory compaction, send into curing oven solidification again, sheet material after solidification is come out of the stove the demoulding, after stacking cooling, delivering to surely thick polishing machine carries out surely thick, after surface finish polished finish, artificial quartz in lump can be obtained.
On the basis of technique scheme, the present invention can also do following improvement.
Further, the temperature of described solidification is 90 ~ 95 DEG C, and the time is 30 ~ 40 minutes.
Further, pressure during described vibratory compaction is 2.5 ~ 3.5MPa, and molding time is 2 ~ 3 minutes.
The invention has the beneficial effects as follows:
(1) resistance to compression: the present invention with the addition of fiber, can improve tensile strength and the ultimate compression strength of artificial quartz stone plate of the present invention.
(2) antibacterial: tourmalinite is ring texture silicate minerals, there is the special performances such as piezoelectricity, pyroelectric, far-infrared radiation and anion releasing, the present invention with the addition of tourmalinite in the feed, effectively can increase the germ resistance of artificial quartz stone plate, and antibiotic effect is for a long time special.
(3) prevent fires: sillimanite powder and zirconium silicate powder are good refractory materialss, and fusing point and hardness are very high, and they can improve the refractory temperature of artificial quartz stone plate of the present invention, extend fire resistance period, increase ultimate compression strength.
(4) preparation method of the present invention is simple, is suitable for suitability for industrialized production.
Embodiment
Be described principle of the present invention and feature below in conjunction with specific embodiment, example, only for explaining the present invention, is not intended to limit scope of the present invention.
Embodiment 1:
Take 3 ~ 80 order quartzite 30kg, 325 order silica powder 60kg, glass cullet 5kg, shell 10kg, glass fibre 3kg, 30 ~ 50 order tourmalinite 10kg, 50 ~ 100 order sillimanite powder 3kg, 100 ~ 200 order zirconium silicate powder 12kg, epoxy resin 5kg, part by weight is the γ-methacryloxypropyl trimethoxy silane (KH570) of 3:1 and the 0.5kg of peroxide-2-ethyl hexanoic acid tert-butyl mixture, pigment 0.3kg, and described pigment is made up of according to mass ratio 15:1 titanium dioxide and Lan Shui; By above-mentioned each component Homogeneous phase mixing, the material mixed evenly is tiled on making sheet mould, then making sheet mould is sent into vacuum chamber, when when vacuumizing, air pressure reaches-0.1MPa, under 2.5 ~ 3.5MPa pressure vibrate 2 ~ 3 minutes shaping, then send into curing oven solidification, solidification value 90 ~ 95 DEG C, time is 30 ~ 40 minutes, sheet material after solidification is come out of the stove the demoulding, after stacking cooling, delivers to surely thick polishing machine and carries out surely thick, " white shell plate " artificial quartz in lump after surface finish polished finish, can be obtained.
Embodiment 2:
Take 3 ~ 80 order quartzite 90kg, 325 order silica powder 20kg, glass cullet 15kg, shell 3kg, carbon fiber 10kg, 30 ~ 50 order tourmalinite 3kg, 50 ~ 100 order sillimanite powder 12kg, 100 ~ 200 order zirconium silicate powder 3kg, resol 10kg, part by weight is the γ-aminopropyl triethoxysilane (KH550) of 3:1 and the 0.3kg of peroxide-2-ethyl hexanoic acid tert-butyl mixture, pigment 0.8kg, and described pigment is made up of according to mass ratio 1421:40:1:3:178 titanium dioxide, iron oxide yellow powder, iron oxide red, iron black powder and Lan Shui; By above-mentioned each component Homogeneous phase mixing, the material mixed evenly is tiled on making sheet mould, then making sheet mould is sent into vacuum chamber, when when vacuumizing, air pressure reaches-0.1MPa, under 2.5 ~ 3.5MPa pressure vibrate 2 ~ 3 minutes shaping, then send into curing oven solidification, solidification value 90 ~ 95 DEG C, time is 30 ~ 40 minutes, sheet material after solidification is come out of the stove the demoulding, after stacking cooling, delivers to surely thick polishing machine and carries out surely thick, " pale yellow shell plate " artificial quartz in lump after surface finish polished finish, can be obtained.
Embodiment 3:
Take 3 ~ 80 order quartzite 70kg, 325 order silica powder 40kg, glass cullet 8kg, shell 6kg, boron fibre 5kg, 30 ~ 50 order tourmalinite 5kg, 50 ~ 100 order sillimanite powder 5kg, 100 ~ 200 order zirconium silicate powder 5kg, urethane resin 8kg, part by weight is the γ-glycidyl ether oxygen propyl trimethoxy silicane of 3:1 and the 0.4kg of peroxide-2-ethyl hexanoic acid tert-butyl mixture, pigment 0.5kg, and described pigment is made up of according to mass ratio 980:1:2:3:118 titanium dioxide, iron oxide yellow powder, iron black powder, chrome green powder and Lan Shui; By above-mentioned each component Homogeneous phase mixing, the material mixed evenly is tiled on making sheet mould, then making sheet mould is sent into vacuum chamber, when when vacuumizing, air pressure reaches-0.1MPa, under 2.5 ~ 3.5MPa pressure vibrate 2 ~ 3 minutes shaping, send into curing oven solidification again, solidification value 90 ~ 95 DEG C, time is 30 ~ 40 minutes, sheet material after solidification is come out of the stove the demoulding, after stacking cooling, delivers to surely thick polishing machine and carries out surely thick, " spring's colours fill the garden shell plate " artificial quartz in lump after surface finish polished finish, can be obtained.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, within the spirit and principles in the present invention all, any amendment done, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (9)
1. artificial quartz stone plate, is characterized in that, is made up of the component of following parts by weight: 3 ~ 80 order quartzites 30 ~ 90 parts, 325 order silica powders 20 ~ 60 parts, glass cullet 5 ~ 15 parts, 3 ~ 10 parts, shell, fiber 3 ~ 10 parts, 30 ~ 50 3 ~ 10 parts, order tourmalinite, 50 ~ 100 3 ~ 12 parts, order sillimanite powder, 100 ~ 200 order zirconium silicate powders 3 ~ 12 parts, unsaturated polyester 5 ~ 10 parts, auxiliary agent 0.3 ~ 0.5 part, pigment 0.3 ~ 0.8 part.
2. artificial quartz stone plate according to claim 1, is characterized in that, is made up of the component of following parts by weight: 3 ~ 80 order quartzites 70 parts, 325 order silica powders 40 parts, glass cullet 8 parts, 6 parts, shell, fiber 5 parts, 30 ~ 50 5 parts, order tourmalinite, 50 ~ 100 5 parts, order sillimanite powder, 100 ~ 200 order zirconium silicate powders 5 parts, unsaturated polyester 8 parts, auxiliary agent 0.4 part, pigment 0.5 part.
3. artificial quartz stone plate according to claim 1 and 2, is characterized in that, described fiber is one or more in glass fibre, carbon fiber, basalt fibre, sapphire whisker, silicon carbide fiber and boron fibre.
4. artificial quartz stone plate according to claim 1 and 2, is characterized in that, described unsaturated polyester is one or more in epoxy resin, resol, acryl resin and urethane resin.
5. artificial quartz stone plate according to claim 1 and 2, it is characterized in that, described auxiliary agent is the mixture of silane coupling agent and peroxide-2-ethyl hexanoic acid tert-butyl, and the part by weight of described silane coupling agent and peroxide-2-ethyl hexanoic acid tert-butyl is 3:1.
6. artificial quartz stone plate according to claim 1 and 2, is characterized in that, described pigment be titanium dioxide, iron oxide yellow powder, iron oxide red, iron black powder, chrome green powder, Lan Shuizhong one or more.
7. the preparation method of artificial quartz stone plate, it is characterized in that, comprise following processing step: the component taking following parts by weight: 3 ~ 80 order quartzites 30 ~ 90 parts, 325 order silica powders 20 ~ 60 parts, glass cullet 5 ~ 15 parts, 3 ~ 10 parts, shell, fiber 3 ~ 10 parts, 30 ~ 50 3 ~ 10 parts, order tourmalinite, 50 ~ 100 3 ~ 12 parts, order sillimanite powder, 100 ~ 200 order zirconium silicate powders 3 ~ 12 parts, unsaturated polyester 5 ~ 10 parts, auxiliary agent 0.3 ~ 0.5 part, pigment 0.3 ~ 0.8 part, by above-mentioned each component Homogeneous phase mixing, the material mixed evenly is tiled on making sheet mould, then making sheet mould is sent into vacuum chamber, vacuumize, vibratory compaction, send into curing oven solidification again, sheet material after solidification is come out of the stove the demoulding, after stacking cooling, delivering to surely thick polishing machine carries out surely thick, after surface finish polished finish, artificial quartz in lump can be obtained.
8. the preparation method of artificial quartz stone plate according to claim 7, is characterized in that, pressure during described vibratory compaction is 2.5 ~ 3.5MPa, and molding time is 2 ~ 3 minutes.
9. the preparation method of artificial quartz stone plate according to claim 7, is characterized in that, the temperature of described solidification is 90 ~ 95 DEG C, and the time is 30 ~ 40 minutes.
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105837239A (en) * | 2016-05-05 | 2016-08-10 | 四川航天五源复合材料有限公司 | Phenolic resin containing basalt fiber refractory material |
| CN105948769A (en) * | 2016-05-05 | 2016-09-21 | 四川航天五源复合材料有限公司 | Basalt fiber quartz refractory material |
| CN105967697A (en) * | 2016-05-05 | 2016-09-28 | 四川航天五源复合材料有限公司 | Basalt fiber refractory material |
| CN105967698A (en) * | 2016-05-05 | 2016-09-28 | 四川航天五源复合材料有限公司 | Alkali basalt fiber refractory material |
| CN107382141A (en) * | 2017-08-21 | 2017-11-24 | 福建省正丰数控科技有限公司 | A kind of method that bed piece is cast using scrap glass |
| CN107777920A (en) * | 2017-09-30 | 2018-03-09 | 镇江市星耀智能装备有限公司 | A kind of high performance artificial slabstone |
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| CN101337805A (en) * | 2008-08-25 | 2009-01-07 | 张璐 | Artificial quartz in lump and fabrication technology thereof |
| CN102390953A (en) * | 2011-08-12 | 2012-03-28 | 新云石业（云浮）有限公司 | Raw material of antibacterial superhard artificial quartz stone plate, artificial quartz stone plate and preparation method thereof |
| CN102584115A (en) * | 2011-12-20 | 2012-07-18 | 汪洋 | Fireproof material, preparation method thereof and fireproof door |
| CN103613325A (en) * | 2013-11-22 | 2014-03-05 | 廖荣刚 | Pattern quartz composite board and production method thereof |
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| WO2000005283A1 (en) * | 1998-07-22 | 2000-02-03 | Elotex Ag | Method for producing aqueous dispersions of (co)polymers, dispersions obtained using said method, redispersible powders which can be obtained from said dispersions and use thereof |
| CN101337805A (en) * | 2008-08-25 | 2009-01-07 | 张璐 | Artificial quartz in lump and fabrication technology thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105837239A (en) * | 2016-05-05 | 2016-08-10 | 四川航天五源复合材料有限公司 | Phenolic resin containing basalt fiber refractory material |
| CN105948769A (en) * | 2016-05-05 | 2016-09-21 | 四川航天五源复合材料有限公司 | Basalt fiber quartz refractory material |
| CN105967697A (en) * | 2016-05-05 | 2016-09-28 | 四川航天五源复合材料有限公司 | Basalt fiber refractory material |
| CN105967698A (en) * | 2016-05-05 | 2016-09-28 | 四川航天五源复合材料有限公司 | Alkali basalt fiber refractory material |
| CN107382141A (en) * | 2017-08-21 | 2017-11-24 | 福建省正丰数控科技有限公司 | A kind of method that bed piece is cast using scrap glass |
| CN107777920A (en) * | 2017-09-30 | 2018-03-09 | 镇江市星耀智能装备有限公司 | A kind of high performance artificial slabstone |
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Application publication date: 20150422 |