CN104478289A - Fireproof and pressure-resistant artificial quartz stone plate and preparation method thereof - Google Patents
Fireproof and pressure-resistant artificial quartz stone plate and preparation method thereof Download PDFInfo
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- CN104478289A CN104478289A CN201410775823.1A CN201410775823A CN104478289A CN 104478289 A CN104478289 A CN 104478289A CN 201410775823 A CN201410775823 A CN 201410775823A CN 104478289 A CN104478289 A CN 104478289A
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Abstract
The invention discloses a fireproof and pressure-resistant artificial quartz stone plate and a preparation method thereof. The fireproof and pressure-resistant artificial quartz stone plate is composed of the following components in parts by weight: 30-80 parts of 8-100-mesh quartz stone, 20-50 parts of 325-1250-mesh quartz powder, 5-15 parts of broken glass, 5-10 parts of unsaturated polyester resin, 10-20 parts of 50-100-mesh white afrodite powder, 10-20 parts of 100-150-mesh andalusite powder, 3-8 parts of fibers, 0.3-0.5 part of an adjuvant and 0.1-2 parts of pigment. The artificial quartz stone plate disclosed by the invention not only has excellent fireproof performance, but also has stronger breaking strength, compressive strength and bending strength; in addition, the preparation cost is low, and the preparation method is simple and is suitable for industrial production.
Description
Technical field
The invention belongs to material of construction preparing technical field, specifically, refer to a kind of fire prevention resistance to compression artificial quartz stone plate and preparation method thereof.
Background technology
Artificial quartz in lump rises in Spain, cry match sharp stone when 2005 enter China, after artificial quartz in lump is by increasing consumer acceptance, China in 2006 starts someone and researches and develops artificial quartz in lump, within 2007, successively has a lot of producer to be proposed domestic artificial quartz in lump.
Artificial quartz in lump is the synthesis stone manufactured by artificial means, there is high strength, high rigidity, high temperature resistant, protection against corrosion, the unrivaled advantage of lithotome such as anti-aging, easy to clean, wear-resisting, radiationless, these advantages allow artificial quartz in lump become the upstart of architectural decoration, are widely applied to cabinet, bathroom, the ground of office and megastore, wall decoration and household industry.However, also there is certain drawback in artificial quartz stone plate, and such as fire resistance is not good, easily ftracture, and these drawbacks significantly limit the application of artificial quartz in lump at various complex condition.
Summary of the invention
Technical problem to be solved by this invention is not enough for prior art, a kind of fire prevention resistance to compression artificial quartz stone plate and preparation method thereof is provided, the fire resistance of the existing excellence of artificial quartz stone plate adopting the present invention to prepare, has again stronger Resisting fractre intensity, ultimate compression strength and flexural strength.
The technical scheme that the present invention solves the problems of the technologies described above is as follows: a kind of fire prevention resistance to compression artificial quartz stone plate, be made up of the component of following parts by weight: 8 ~ 100 order quartzites 30 ~ 80 parts, 325 ~ 1250 order silica powders 20 ~ 50 parts, glass cullet 5 ~ 15 parts, unsaturated polyester 5 ~ 10 parts, 50 ~ 100 10 ~ 20 parts, order white afrodite powder, 100 ~ 150 10 ~ 20 parts, order andaluzite powder, fiber 3 ~ 8 parts, auxiliary agent 0.3 ~ 0.5 part, pigment 0.3 ~ 0.8 part.
On the basis of technique scheme, the present invention can also do following improvement.
Further, described unsaturated polyester is one or more in epoxy resin, resol, acryl resin and urethane resin.
Further, described fiber is one or more in glass fibre, carbon fiber, basalt fibre, sapphire whisker, silicon carbide fiber and boron fibre.
Further, described auxiliary agent is the mixture of silane coupling agent and peroxide-2-ethyl hexanoic acid tert-butyl, and the part by weight of described silane coupling agent and peroxide-2-ethyl hexanoic acid tert-butyl is 3:1.
Further, described pigment be titanium dioxide, iron oxide yellow powder, iron oxide red, iron black powder, Lan Shuizhong one or more.
A kind of preparation method of resistance to compression artificial quartz stone plate of preventing fires, comprise following processing step: the component taking following parts by weight: 8 ~ 100 order quartzites 30 ~ 80 parts, 325 ~ 1250 order silica powders 20 ~ 50 parts, glass cullet 5 ~ 15 parts, unsaturated polyester 5 ~ 10 parts, 50 ~ 100 10 ~ 20 parts, order white afrodite powder, 100 ~ 150 10 ~ 20 parts, order andaluzite powder, fiber 3 ~ 8 parts, auxiliary agent 0.3 ~ 0.5 part, pigment 0.1 ~ 2 part, by above-mentioned each component Homogeneous phase mixing, the material mixed evenly is tiled on making sheet mould, then making sheet mould is sent into vacuum chamber, vacuumize, vibratory compaction, send into curing oven solidification again, sheet material after solidification is come out of the stove the demoulding, after stacking cooling, delivering to surely thick polishing machine carries out surely thick, after surface finish polished finish, artificial quartz in lump can be obtained.
On the basis of technique scheme, the present invention can also do following improvement.
Further, pressure during described vibratory compaction is 1.8 ~ 3MPa, and molding time is 2 ~ 3 minutes.
Further, the temperature of described solidification is 85 ~ 95 DEG C, and the time is 40 ~ 45 minutes.
The invention has the beneficial effects as follows:
(1) the present invention adopt white afrodite powder and andaluzite powder, be good refractory materials, they can improve the refractory temperature of artificial quartz stone plate of the present invention, extend fire resistance period.
(2) the present invention in the fabrication process, adds fiber, and artificial quartz stone plate can be made to have stronger Resisting fractre intensity, ultimate compression strength and flexural strength.
(3) low cost of manufacture of the present invention, preparation method simply, are suitable for suitability for industrialized production.
Embodiment
Be described principle of the present invention and feature below in conjunction with specific embodiment, example, only for explaining the present invention, is not intended to limit scope of the present invention.
Embodiment 1:
Take following component: 8 ~ 100 order quartzite 30kg, 325 ~ 1250 order silica powder 50kg, glass cullet 5kg, epoxy resin 10kg, 50 ~ 100 order white afrodite powder 10kg, 100 ~ 150 order andaluzite powder 20kg, glass fibre 3kg, part by weight is γ-(2,3-glycidoxy) propyl trimethoxy silicane and the peroxide-2-ethyl hexanoic acid tert-butyl mixture 0.5kg of 3:1, pigment 0.1kg, described pigment is made up of according to mass ratio 15:1 titanium dioxide and Lan Shui; By above-mentioned each component raw material Homogeneous phase mixing, the material mixed is sent in material distributing machine cloth system template die, then making sheet mould is sent into vacuum chamber, when when vacuumizing, air pressure reaches-0.1MPa, under 1.8 ~ 3MPa pressure vibrate 2 ~ 3 minutes shaping, send into curing oven solidification again, solidification value 85 ~ 95 DEG C, time is 40 ~ 45 minutes, sheet material after solidification is come out of the stove the demoulding, after stacking cooling, delivers to surely thick polishing machine and carries out surely thick, after surface finish polished finish, " white board " artificial quartz in lump can be obtained.
Embodiment 2:
Take following component: 8 ~ 100 order quartzite 80kg, 325 ~ 1250 order silica powder 20kg, glass cullet 15kg, resol 5kg, 50 ~ 100 order white afrodite powder 20kg, 100 ~ 150 order andaluzite powder 10kg, boron fibre 8kg, part by weight is the γ-(2 of 3:1,3-glycidoxy) propyl trimethoxy silicane and peroxide-2-ethyl hexanoic acid tert-butyl mixture 0.3kg, pigment 2kg, described pigment is made up of according to mass ratio 222:8:2:1:24 titanium dioxide, iron oxide yellow powder, iron oxide red, iron black powder and Lan Shui; By above-mentioned each component raw material Homogeneous phase mixing, the material mixed is sent in material distributing machine cloth system template die, then making sheet mould is sent into vacuum chamber, when when vacuumizing, air pressure reaches-0.1MPa, under 1.8 ~ 3MPa pressure vibrate 2 ~ 3 minutes shaping, send into curing oven solidification again, solidification value 85 ~ 95 DEG C, time is 40 ~ 45 minutes, sheet material after solidification is come out of the stove the demoulding, after stacking cooling, delivers to surely thick polishing machine and carries out surely thick, after surface finish polished finish, " Royal Pink " artificial quartz in lump can be obtained.
Embodiment 3:
Take following component: 8 ~ 100 order quartzite 60kg, 325 ~ 1250 order silica powder 35kg, glass cullet 8kg, urethane resin 7kg, 50 ~ 100 order white afrodite powder 15kg, 100 ~ 150 order andaluzite powder 15kg, basalt fibre 5kg, part by weight is the γ-(2 of 3:1,3-glycidoxy) propyl trimethoxy silicane and peroxide-2-ethyl hexanoic acid tert-butyl mixture 0.4kg, pigment 0.5kg, described pigment is made up of according to mass ratio 330:20:1:2:9 titanium dioxide, iron oxide yellow powder, iron oxide red, iron black powder and Lan Shui; By above-mentioned each component raw material Homogeneous phase mixing, the material mixed is sent in material distributing machine cloth system template die, then making sheet mould is sent into vacuum chamber, when when vacuumizing, air pressure reaches-0.1MPa, under 1.8 ~ 3MPa pressure vibrate 2 ~ 3 minutes shaping, send into curing oven solidification again, solidification value 85 ~ 95 DEG C, time is 40 ~ 45 minutes, sheet material after solidification is come out of the stove the demoulding, after stacking cooling, delivers to surely thick polishing machine and carries out surely thick, after surface finish polished finish, " yellow quartz " artificial quartz in lump can be obtained.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, within the spirit and principles in the present invention all, any amendment done, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (8)
1. a fire prevention resistance to compression artificial quartz stone plate, it is characterized in that, be made up of the component of following parts by weight: 8 ~ 100 order quartzites 30 ~ 80 parts, 325 ~ 1250 order silica powders 20 ~ 50 parts, glass cullet 5 ~ 15 parts, unsaturated polyester 5 ~ 10 parts, 50 ~ 100 10 ~ 20 parts, order white afrodite powder, 100 ~ 150 10 ~ 20 parts, order andaluzite powder, fiber 3 ~ 8 parts, auxiliary agent 0.3 ~ 0.5 part, pigment 0.1 ~ 2 part.
2. one fire prevention resistance to compression artificial quartz stone plate according to claim 1, is characterized in that, described unsaturated polyester is one or more in epoxy resin, resol, acryl resin and urethane resin.
3. one fire prevention resistance to compression artificial quartz stone plate according to claim 1, is characterized in that, described fiber is one or more in glass fibre, carbon fiber, basalt fibre, sapphire whisker, silicon carbide fiber and boron fibre.
4. one fire prevention resistance to compression artificial quartz stone plate according to claim 1, it is characterized in that, described auxiliary agent is the mixture of silane coupling agent and peroxide-2-ethyl hexanoic acid tert-butyl, and the part by weight of described silane coupling agent and peroxide-2-ethyl hexanoic acid tert-butyl is 3:1.
5. one fire prevention resistance to compression artificial quartz stone plate according to claim 1, is characterized in that, described pigment be titanium dioxide, iron oxide yellow powder, iron oxide red, iron black powder, Lan Shuizhong one or more.
6. the preparation method of resistance to compression artificial quartz stone plate that prevents fires, it is characterized in that, comprise following processing step: the component taking following parts by weight: 8 ~ 100 order quartzites 30 ~ 80 parts, 325 ~ 1250 order silica powders 20 ~ 50 parts, glass cullet 5 ~ 15 parts, unsaturated polyester 5 ~ 10 parts, 50 ~ 100 10 ~ 20 parts, order white afrodite powder, 100 ~ 150 10 ~ 20 parts, order andaluzite powder, fiber 3 ~ 8 parts, auxiliary agent 0.3 ~ 0.5 part, pigment 0.1 ~ 2 part, by above-mentioned each component Homogeneous phase mixing, the material mixed evenly is tiled on making sheet mould, then making sheet mould is sent into vacuum chamber, vacuumize, vibratory compaction, send into curing oven solidification again, sheet material after solidification is come out of the stove the demoulding, after stacking cooling, delivering to surely thick polishing machine carries out surely thick, after surface finish polished finish, artificial quartz in lump can be obtained.
7. the preparation method of a kind of resistance to compression artificial quartz stone plate of preventing fires according to claim 6, it is characterized in that, pressure during described vibratory compaction is 1.8 ~ 3MPa, and molding time is 2 ~ 3 minutes.
8. the preparation method of a kind of resistance to compression artificial quartz stone plate of preventing fires according to claim 6, is characterized in that, the temperature of described solidification is 85 ~ 95 DEG C, and the time is 40 ~ 45 minutes.
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105481294A (en) * | 2015-12-02 | 2016-04-13 | 常州工程职业技术学院 | Method for producing hot-pressed composite plates by using papermaking white clay |
| CN105907033A (en) * | 2016-06-22 | 2016-08-31 | 金华知产婺源信息技术有限公司 | Preparation method of flame-retardant artificial stone containing nano perovskite oxide |
| CN105907034A (en) * | 2016-06-22 | 2016-08-31 | 金华知产婺源信息技术有限公司 | Preparation method of flame-retardant artificial stone containing nano perovskite oxide MTiO3 |
| CN105949709A (en) * | 2016-06-22 | 2016-09-21 | 金华知产婺源信息技术有限公司 | Preparation method of pleonaste-containing artificial stone |
| CN106007480A (en) * | 2016-06-22 | 2016-10-12 | 金华知产婺源信息技术有限公司 | Preparation method of flame-retardant artificial stone containing pleonaste |
| CN106116247A (en) * | 2016-06-24 | 2016-11-16 | 安徽弗仕通实业有限公司 | A kind of antidetonation swings the preparation technology of artificial floor tile |
| CN107892506A (en) * | 2017-11-07 | 2018-04-10 | 桂林奥尼斯特节能环保科技有限责任公司 | One kind fire prevention resistance to compression artificial quartz stone plate and its manufacture method |
| CN108911582A (en) * | 2018-08-07 | 2018-11-30 | 枣庄鑫金山智能机械股份有限公司 | A kind of production method of granolith |
| CN110714586A (en) * | 2019-10-18 | 2020-01-21 | 山东康洁利新材料有限公司 | Flame-retardant inorganic quartz stone plate and manufacturing method thereof |
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Cited By (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105481294B (en) * | 2015-12-02 | 2017-08-01 | 常州工程职业技术学院 | A kind of method that utilization paper white sludge produces hot press composite board material |
| CN105481294A (en) * | 2015-12-02 | 2016-04-13 | 常州工程职业技术学院 | Method for producing hot-pressed composite plates by using papermaking white clay |
| CN105907033B (en) * | 2016-06-22 | 2018-07-17 | 广西利升石业有限公司 | A kind of preparation method of the fire retardant man-made stone comprising nano-perovskite oxide |
| CN109133722A (en) * | 2016-06-22 | 2019-01-04 | 金华知产婺源信息技术有限公司 | A kind of preparation method of the artificial stone containing magnesium aluminate spinel |
| CN106007480A (en) * | 2016-06-22 | 2016-10-12 | 金华知产婺源信息技术有限公司 | Preparation method of flame-retardant artificial stone containing pleonaste |
| CN109133722B (en) * | 2016-06-22 | 2021-07-20 | 杭州百维艾特卫浴有限公司 | Preparation method of artificial stone containing magnesium aluminate spinel |
| CN105907034A (en) * | 2016-06-22 | 2016-08-31 | 金华知产婺源信息技术有限公司 | Preparation method of flame-retardant artificial stone containing nano perovskite oxide MTiO3 |
| CN108455902B (en) * | 2016-06-22 | 2021-01-01 | 余笑眉 | Preparation method of flame-retardant artificial stone containing nano perovskite oxide |
| CN105907033A (en) * | 2016-06-22 | 2016-08-31 | 金华知产婺源信息技术有限公司 | Preparation method of flame-retardant artificial stone containing nano perovskite oxide |
| CN106007480B (en) * | 2016-06-22 | 2018-08-07 | 金华知产婺源信息技术有限公司 | A kind of preparation method of the fire retardant man-made stone containing magnesium aluminate spinel |
| CN105907034B (en) * | 2016-06-22 | 2018-08-24 | 浙江南塑合成材料有限公司 | One kind includes nano-perovskite oxide M TiO3Fire retardant man-made stone preparation method |
| CN108455902A (en) * | 2016-06-22 | 2018-08-28 | 金华知产婺源信息技术有限公司 | A kind of preparation method of the fire retardant man-made stone comprising nano-perovskite oxide |
| CN108483993A (en) * | 2016-06-22 | 2018-09-04 | 金华知产婺源信息技术有限公司 | A kind of preparation method of the fire retardant man-made stone containing magnesium aluminate spinel |
| CN105949709B (en) * | 2016-06-22 | 2018-11-13 | 金华知产婺源信息技术有限公司 | A kind of preparation method of the artificial stone containing magnesium aluminate spinel |
| CN105949709A (en) * | 2016-06-22 | 2016-09-21 | 金华知产婺源信息技术有限公司 | Preparation method of pleonaste-containing artificial stone |
| CN106116247A (en) * | 2016-06-24 | 2016-11-16 | 安徽弗仕通实业有限公司 | A kind of antidetonation swings the preparation technology of artificial floor tile |
| CN107892506A (en) * | 2017-11-07 | 2018-04-10 | 桂林奥尼斯特节能环保科技有限责任公司 | One kind fire prevention resistance to compression artificial quartz stone plate and its manufacture method |
| CN108911582A (en) * | 2018-08-07 | 2018-11-30 | 枣庄鑫金山智能机械股份有限公司 | A kind of production method of granolith |
| CN110714586A (en) * | 2019-10-18 | 2020-01-21 | 山东康洁利新材料有限公司 | Flame-retardant inorganic quartz stone plate and manufacturing method thereof |
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Application publication date: 20150401 |