CN104364244B - 制备单‑n‑烷基哌嗪的方法 - Google Patents

制备单‑n‑烷基哌嗪的方法 Download PDF

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Publication number
CN104364244B
CN104364244B CN201380028959.XA CN201380028959A CN104364244B CN 104364244 B CN104364244 B CN 104364244B CN 201380028959 A CN201380028959 A CN 201380028959A CN 104364244 B CN104364244 B CN 104364244B
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catalyst
reaction
weight
formula
deoa
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CN201380028959.XA
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English (en)
Chinese (zh)
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CN104364244A (zh
Inventor
切迪德 R·布
J-P·梅尔德
U·艾贝尔
R·多斯塔莱克
B·施泰因
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/02—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms containing only hydrogen and carbon atoms in addition to the ring hetero elements
    • C07D295/023—Preparation; Separation; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/04—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
    • C07D295/08—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly bound oxygen or sulfur atoms
    • C07D295/084—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly bound oxygen or sulfur atoms with the ring nitrogen atoms and the oxygen or sulfur atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings
    • C07D295/088—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly bound oxygen or sulfur atoms with the ring nitrogen atoms and the oxygen or sulfur atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings to an acyclic saturated chain
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/02—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms containing only hydrogen and carbon atoms in addition to the ring hetero elements
    • C07D295/027—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms containing only hydrogen and carbon atoms in addition to the ring hetero elements containing only one hetero ring
    • C07D295/03—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms containing only hydrogen and carbon atoms in addition to the ring hetero elements containing only one hetero ring with the ring nitrogen atoms directly attached to acyclic carbon atoms

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
CN201380028959.XA 2012-06-01 2013-05-23 制备单‑n‑烷基哌嗪的方法 Expired - Fee Related CN104364244B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP12170569 2012-06-01
EP12170569.3 2012-06-01
PCT/EP2013/060658 WO2013178534A1 (de) 2012-06-01 2013-05-23 Verfahren zur herstellung eines mono-n-alkyl-piperazins

Publications (2)

Publication Number Publication Date
CN104364244A CN104364244A (zh) 2015-02-18
CN104364244B true CN104364244B (zh) 2017-10-24

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CN201380028959.XA Expired - Fee Related CN104364244B (zh) 2012-06-01 2013-05-23 制备单‑n‑烷基哌嗪的方法

Country Status (7)

Country Link
EP (1) EP2855442B1 (enExample)
JP (1) JP6242876B2 (enExample)
CN (1) CN104364244B (enExample)
ES (1) ES2573287T3 (enExample)
HU (1) HUE029629T2 (enExample)
IN (1) IN2014DN09198A (enExample)
WO (1) WO2013178534A1 (enExample)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014184048A1 (de) * 2013-05-16 2014-11-20 Basf Se Verfahren zur herstellung von n-alkyl-piperazinen
WO2017125358A1 (de) 2016-01-20 2017-07-27 Basf Se Verfahren zur homogen-katalysierten herstellung von mono-n-substituierten-piperazinen

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2009080507A1 (de) * 2007-12-21 2009-07-02 Basf Se Verfahren zur herstellung eines amins
US20110137030A1 (en) * 2009-12-03 2011-06-09 Basf Se Catalyst and process for preparing an amine
WO2011157710A1 (de) * 2010-06-15 2011-12-22 Basf Se Verfahren zur herstellung eines zyklischen tertiären methylamins
WO2012055893A1 (de) * 2010-10-29 2012-05-03 Basf Se Verfahren zur herstellung von 1,4-bishydroxyethyl-piperazin

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL296139A (enExample) 1963-08-02
NL169595C (nl) 1970-05-21 1982-08-02 Shell Int Research Werkwijze voor de bereiding van aminen en van smeerolien en vloeibare motorbrandstoffen die deze bevatten.
DE3605005A1 (de) 1986-02-18 1987-08-20 Basf Ag Verfahren zur herstellung von n-methylpiperazin
DE3611230A1 (de) 1986-04-04 1987-10-08 Basf Ag Polybutyl- und polyisobutylamine, verfahren zu deren herstellung und diese enthaltende kraft- und schmierstoffzusammensetzungen
DE4008322A1 (de) 1990-03-15 1991-09-19 Basf Ag Verfahren zur herstellung von n-arylsubstituierten 2-aminoalkyl-2-hydroxyalkylaminen und n-arylsubstituierten piperazinen
DE10153411A1 (de) 2001-10-30 2003-05-15 Basf Ag Verfahren zur Auftrennung von wasserhaltigen Rohamingemischen aus der Aminsynthese
DE10153410A1 (de) 2001-10-30 2003-05-15 Basf Ag Verfahren zur Auftrennung von wasserhaltigen Rohamingemischen aus der Aminsynthese
US7196033B2 (en) 2001-12-14 2007-03-27 Huntsman Petrochemical Corporation Advances in amination catalysis
US8063252B2 (en) 2006-07-14 2011-11-22 Basf Se Process for preparing amines and zirconium dioxide- and nickel-containing catalysts for use therein
EP2225027B1 (de) 2007-12-21 2012-05-23 Basf Se Verfahren zur herstellung eines amins
WO2009080508A1 (de) 2007-12-21 2009-07-02 Basf Se Verfahren zur herstellung eines amins
CN103189365B (zh) 2010-10-14 2015-01-07 巴斯夫欧洲公司 制备环状叔胺的方法
CN102101847B (zh) 2010-12-06 2012-09-12 周玉莲 N-甲基-n′-(2-氯乙基)哌嗪的制备方法
CN102304101A (zh) 2011-05-26 2012-01-04 绍兴兴欣化工有限公司 哌嗪与n-烷基哌嗪联产工艺

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2009080507A1 (de) * 2007-12-21 2009-07-02 Basf Se Verfahren zur herstellung eines amins
US20110137030A1 (en) * 2009-12-03 2011-06-09 Basf Se Catalyst and process for preparing an amine
WO2011157710A1 (de) * 2010-06-15 2011-12-22 Basf Se Verfahren zur herstellung eines zyklischen tertiären methylamins
WO2012055893A1 (de) * 2010-10-29 2012-05-03 Basf Se Verfahren zur herstellung von 1,4-bishydroxyethyl-piperazin

Also Published As

Publication number Publication date
IN2014DN09198A (enExample) 2015-07-10
EP2855442A1 (de) 2015-04-08
JP2015519349A (ja) 2015-07-09
CN104364244A (zh) 2015-02-18
EP2855442B1 (de) 2016-03-23
WO2013178534A1 (de) 2013-12-05
JP6242876B2 (ja) 2017-12-06
HUE029629T2 (en) 2017-03-28
ES2573287T3 (es) 2016-06-07

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