CN104289156A - Method for softening traditional Chinese medicinal material before slicing - Google Patents
Method for softening traditional Chinese medicinal material before slicing Download PDFInfo
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- CN104289156A CN104289156A CN201410580504.5A CN201410580504A CN104289156A CN 104289156 A CN104289156 A CN 104289156A CN 201410580504 A CN201410580504 A CN 201410580504A CN 104289156 A CN104289156 A CN 104289156A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J3/00—Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/23—Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
- A61K36/232—Angelica
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/481—Astragalus (milkvetch)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/484—Glycyrrhiza (licorice)
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Abstract
The invention belongs to the processing field of traditional Chinese medicine decoction pieces, particularly relating to a method for softening a traditional Chinese medicinal material before slicing. According to the method for softening the traditional Chinese medicinal material before slicing, complete infiltration of water into the drug can be realized, water supply volume in softening of the traditional Chinese medicinal material is reduced, production water is saved, and substance loss amount in the softening process of the traditional Chinese medicinal herbs is reduced. According to the method for softening the traditional Chinese medicinal material before slicing, superiorities of two ways, namely, pressure-reduced cold soaking and pressure-boosted cold soaking, are combined, special equipment is not needed, production site is saved, heating and special pressure boosting and reducing equipment are unnecessary, a common vacuum packaging machine and common air compression equipment are only necessary, so that the production cost is low.
Description
Technical field
The invention belongs to prepared slices of Chinese crude drugs manufacture field, be specifically related to the softening method before the section of a kind of Chinese medicine.
Background technology
Softening method before traditional Chinese medicine section, there is the softening water of medicinal material all to be absorbed by medicinal material, a part of water soluble ingredient is caused not run off by absorption water, after causing cutting, the labeled component content of medicine materical crude slice declines compared with the labeled component content of medicinal material, the permeable most difficulty of the medicine done in actual production is larger, especially bubble profit tenderizer, infiltration tenderizer are not accomplished " medicine is permeable to the greatest extent ", and in production, the consumption of water is also comparatively large, and needs special softening production site; Softening before modern Chinese medicine cutting have vacuum to heat tenderizer, decompression cold soaking tenderizer, pressurization cold soaking tenderizer all needs the equipment of specialty, use and heat, pressurized equipment, energy resource consumption is comparatively large, and Productive statistics equipment cost is high, heat to soften and be not suitable for effective component case of thermal instability, containing the medicinal material of volatile ingredient; Pressurization cold soaking and decompression cold soaking all need special equipment, production equipment drops into higher, another shortcoming produces Chinese medicine to be closed in the container of a rigidity, softening water causes medicinal material excessively softening as being full of container, moisture too high, cutting medicine materical crude slice is not easily dry, and water soluble ingredient also can be caused to run off; If soften actual water requirement with medicinal material, medicinal material then can be caused softening uneven, during pieces of cutting, fragment relic is more, difficulty for the improvement of rigid container is larger, because decompression cold soaking needs certain vacuum to get rid of air in medicinal material gap, be easy to infiltration and allow moisture medicinal material tissue, so must rigid container be used; Pressurization cold soaking utilizes equipment that hydraulic pressure is entered medicinal material organization internal, also rigid device must be used, though two kinds of methods can improve softening rate, but two kinds of equipment all well solve and allow demineralized water needed for medicinal material be evenly distributed in the problem on medicinal material surface, and the water rate control of softening process, medicinal material soften consistent problem does not follow Chinese medicine very well and preserve the permeable most softening principle of drug effect medicine.
Summary of the invention
The object of the invention is to provide for problems of the prior art the softening method that a kind of medicinal material bating effect is good, softening process water consumption is low, softening process medicinal material active ingredient number of dropouts is few.
A softening method before Chinese medicine section, is characterized in that:
The Chinese medicine trimmed is put into soft packaging bag, in soft packaging bag, injects the water of Chinese medicine quality 0.1 ~ 0.8 times, then soft packaging bag sealing is vacuumized, make vacuum in soft packaging bag be less than 0.08Mpa; Soft packaging bag after sealing is put into pressure vessel, regulates pressure to 1.0 ~ 3.0 Mpa, maintain this pressure, treat that the moisture in soft packaging bag penetrates into Chinese medicine inside completely, soft packaging bag is taken out to pressure vessel pressure release;
After being taken out by soft packaging bag, open soft packaging bag, and the Chinese medicine after softening is spread out slightly dry in the air, its transepidermal water is evaporated, after medicinal material water content is down to 25% ~ 35% and epidermis tightens up, carries out cutting operation.
The present invention has following beneficial effect:
This patent can accomplish that medicine is permeable most, water consumption during minimizing medicinal material softens, save industrial water, the advantage of decompression cold soaking and pressurization cold soaking two kinds of methods is combined, without the need to Special Equipment, save production site, do not need to add gentle special pressurization, pressure regulating equipment, only need general vacuum packing machine and normal air compression device, production cost is low; Because demineralized water all exhausts by medicinal material, do not have sewage to produce and drastically reduce the area the loss of active ingredients from traditional Chinese medicinal; Adopt the technology hydraulic pressure of softening medicinal material being invested medicinal material surface, make each portion of medicinal material evenly softening, deducted the work of turning in softening process; To the demineralized water press-in medicinal material tissue on medicinal material surface be attached to, and shorten the softening time, improve effect; Because the present invention adopts, medicinal material is closed in soften in soft package material, without the need to places such as fermentation vats, production site can with packing shop or cutting place public, decrease the handling workload in production, medicinal material softens output and does not limit by production site, the softening time is short, prevents medicinal material at the moldy metamorphism of softening process; Therefore the softening process parameter that cutting medicinal material is formulated utilizes the art of this patent to be easy to realize, and for direct labor without the need to Special Training, just can produce, be easy to this technology be applied in the suitability for industrialized production of prepared slices of Chinese crude drugs cutting.
Detailed description of the invention
Comparative example 1
Use drip washing damp method to soften Radix Angelicae Sinensis medicinal material: fibrous root, impurity, the silt of removing Radix Angelicae Sinensis medicinal material, banked up after getting the Radix Angelicae Sinensis medicinal material water wash that 250g trims, utilize the moisture infiltration medicinal material of environment inner, make it soften.
Embodiment 1
Remove fibrous root, impurity, the silt of Radix Angelicae Sinensis medicinal material, get the Radix Angelicae Sinensis medicinal material that 250g trims and put into soft packaging bag, Radix Angelicae Sinensis quality of medicinal material 0.3 times of water is injected in soft packaging bag, the air in soft packaging bag is removed by air-extractor, make vacuum in soft packaging bag be less than 0.08Mpa, then soft packaging bag is sealed; Soft packaging bag after sealing is put into pressure vessel, to pressure vessel insufflation gas be forced into 1.15 Mpa carry out pressurization soften, within every 3 hours, to Radix Angelicae Sinensis medicinal material, inspection is run through with bending method to pressure vessel pressure release, within 42 hours, reaches required softness number; Soft packaging bag is taken out to pressure vessel pressure release, opens soft packaging bag, the Radix Angelicae Sinensis medicinal material after softening is spread out and slightly dries in the air, its transepidermal water is evaporated, after medicinal material water content is down to 25% ~ 35% and epidermis tightens up, carry out cutting operation.
Embodiment 2
Remove fibrous root, impurity, the silt of Radix Angelicae Sinensis medicinal material, get the Radix Angelicae Sinensis medicinal material that 250g trims and put into soft packaging bag, Radix Angelicae Sinensis quality of medicinal material 0.35 times of water is injected in soft packaging bag, the air in soft packaging bag is removed by air-extractor, make vacuum in soft packaging bag be less than 0.08Mpa, then soft packaging bag is sealed; Soft packaging bag after sealing is put into pressure vessel, being forced into 1.25Mpa to pressure vessel insufflation gas, to carry out pressurization softening, within every 3 hours, runs through inspection, within 36 hours, reach required softness number to pressure vessel pressure release with bending method to Radix Angelicae Sinensis medicinal material; Soft packaging bag is taken out to pressure vessel pressure release, opens soft packaging bag, the Radix Angelicae Sinensis medicinal material after softening is spread out and slightly dries in the air, its transepidermal water is evaporated, after medicinal material water content is down to 25% ~ 35% and epidermis tightens up, carry out cutting operation.
Embodiment 3
Remove fibrous root, impurity, the silt of Radix Angelicae Sinensis medicinal material, get the Radix Angelicae Sinensis medicinal material that 250g trims and put into soft packaging bag, Radix Angelicae Sinensis quality of medicinal material 0.4 times of water is injected in soft packaging bag, the air in soft packaging bag is removed by air-extractor, make vacuum in soft packaging bag be less than 0.08Mpa, then soft packaging bag is sealed; Soft packaging bag after sealing is put into pressure vessel, being forced into 1.35Mpa to pressure vessel insufflation gas, to carry out pressurization softening, within every 3 hours, runs through inspection, within 36 hours, reach required softness number to pressure vessel pressure release with bending method to Radix Angelicae Sinensis medicinal material; Soft packaging bag is taken out to pressure vessel pressure release, opens soft packaging bag, the Radix Angelicae Sinensis medicinal material after softening is spread out and slightly dries in the air, its transepidermal water is evaporated, after medicinal material water content is down to 25% ~ 35% and epidermis tightens up, carry out cutting operation.
Embodiment 4
Remove fibrous root, impurity, the silt of Radix Angelicae Sinensis medicinal material, get the Radix Angelicae Sinensis medicinal material that 250g trims and put into soft packaging bag, 0.45 times of water of Radix Angelicae Sinensis quality of medicinal material is injected in soft packaging bag, the air in soft packaging bag is removed by air-extractor, make vacuum in soft packaging bag be less than 0.08Mpa, then soft packaging bag is sealed; Soft packaging bag after sealing is put into pressure vessel, being forced into 1.45Mpa to pressure vessel insufflation gas, to carry out pressurization softening, within every 3 hours, runs through inspection, within 30 hours, reach required softness number to pressure vessel pressure release with bending method to Radix Angelicae Sinensis medicinal material; Soft packaging bag is taken out to pressure vessel pressure release, opens soft packaging bag, the Radix Angelicae Sinensis medicinal material after softening is spread out and slightly dries in the air, its transepidermal water is evaporated, after medicinal material water content is down to 25% ~ 35% and epidermis tightens up, carry out cutting operation.
The effect that the method for table 1 comparative example 1 and embodiment 1 ~ 4 is softened Radix Angelicae Sinensis medicinal material
By shown in table 1, softening method of the present invention softens Radix Angelicae Sinensis medicinal material, softening water consumption is 1/5th of the traditional damp softening water consumption of drip washing, softening consumes time is compared conventional method and is greatly shortened, its alcohol extract of medicine materical crude slice after cutting, forulic acid, Ligustilide content are also high than conventional method, illustrate that the present invention decreases the loss of active ingredient in Radix Angelicae Sinensis medicinal material in softening link.
Comparative example 2
Use bubble profit method to soften Milkvetch Root: impurity, the silt of removing Milkvetch Root, get the licorice medicinal materials that 250g trims and be placed in bubble medicine cylinder, add water and medicinal material softened, stir up and down in good time, until medicinal material softening good after cutting.
Embodiment 5
Remove impurity, the silt of Milkvetch Root, get the Milkvetch Root that 250g trims and put into soft packaging bag, Milkvetch Root quality 0.3 times of water is injected in soft packaging bag, the air in soft packaging bag is removed by air-extractor, make vacuum in soft packaging bag be less than 0.08Mpa, then soft packaging bag is sealed; Soft packaging bag after sealing is put into pressure vessel, being forced into 1.15Mpa to pressure vessel insufflation gas, to carry out pressurization softening, within every 3 hours, runs through inspection, within 42 hours, reach required softness number to pressure vessel pressure release with bending method to Milkvetch Root; Soft packaging bag is taken out to pressure vessel pressure release, opens soft packaging bag, the Milkvetch Root after softening is opened and slightly dries in the air, its transepidermal water is evaporated, after medicinal material water content is down to 25% ~ 35% and epidermis tightens up, carry out cutting operation.
Embodiment 6
Remove impurity, the silt of Milkvetch Root, get the Milkvetch Root that 250g trims and put into soft packaging bag, Milkvetch Root quality 0.35 times of water is injected in soft packaging bag, the air in soft packaging bag is removed by air-extractor, make vacuum in soft packaging bag be less than 0.08Mpa, then soft packaging bag is sealed; Soft packaging bag after sealing is put into pressure vessel, being forced into 1.25Mpa to pressure vessel insufflation gas, to carry out pressurization softening, within every 3 hours, runs through inspection, within 36 hours, reach required softness number to pressure vessel pressure release with bending method to Milkvetch Root; Soft packaging bag is taken out to pressure vessel pressure release, opens soft packaging bag, the Milkvetch Root after softening is opened and slightly dries in the air, its transepidermal water is evaporated, after medicinal material water content is down to 25% ~ 35% and epidermis tightens up, carry out cutting operation.
Embodiment 7
Remove impurity, the silt of Milkvetch Root, get the Milkvetch Root that 250g trims and put into soft packaging bag, Milkvetch Root quality 0.4 times of water is injected in soft packaging bag, the air in soft packaging bag is removed by air-extractor, make vacuum in soft packaging bag be less than 0.08Mpa, then soft packaging bag is sealed; Soft packaging bag after sealing is put into pressure vessel, being forced into 1.35Mpa to pressure vessel insufflation gas, to carry out pressurization softening, within every 3 hours, runs through inspection, within 36 hours, reach required softness number to pressure vessel pressure release with bending method to Milkvetch Root; Soft packaging bag is taken out to pressure vessel pressure release, opens soft packaging bag, the Milkvetch Root after softening is opened and slightly dries in the air, its transepidermal water is evaporated, after medicinal material water content is down to 25% ~ 35% and epidermis tightens up, carry out cutting operation.
Embodiment 8
Remove impurity, the silt of Milkvetch Root, get the Milkvetch Root that 250g trims and put into soft packaging bag, Milkvetch Root quality 0.45 times of water is injected in soft packaging bag, the air in soft packaging bag is removed by air-extractor, make vacuum in soft packaging bag be less than 0.08Mpa, then soft packaging bag is sealed; Soft packaging bag after sealing is put into pressure vessel, being forced into 1.45Mpa to pressure vessel insufflation gas, to carry out pressurization softening, within every 3 hours, runs through inspection, within 30 hours, reach required softness number to pressure vessel pressure release with bending method to Milkvetch Root; Soft packaging bag is taken out to pressure vessel pressure release, opens soft packaging bag, the Milkvetch Root after softening is opened and slightly dries in the air, its transepidermal water is evaporated, after medicinal material water content is down to 25% ~ 35% and epidermis tightens up, carry out cutting operation.
The effect that the method for table 2 comparative example 2 and embodiment 5 ~ 8 is softened Milkvetch Root
By shown in table 2, softening method of the present invention softens Milkvetch Root, softening water consumption is that traditional bubble profit method softens 1/5th of water consumption, softening consumes time is compared conventional method and is greatly shortened, its water-soluble extractives of medicine materical crude slice after cutting, Astragaloside IV, calycosin heteroside content are also high than conventional method, illustrate that the present invention decreases the loss of active ingredient in Milkvetch Root in softening link.
Comparative example 3
Use bubble profit method to soften licorice medicinal materials: impurity, the silt of removing licorice medicinal materials, get the licorice medicinal materials that 250g trims and be placed in bubble medicine cylinder, add water and medicinal material softened, stir up and down in good time, until medicinal material softening good after cutting.
Embodiment 9
Remove impurity, the silt of licorice medicinal materials, get the licorice medicinal materials that 250g trims and put into soft packaging bag, licorice medicinal materials quality 0.3 times of water is injected in soft packaging bag, the air in soft packaging bag is removed by air-extractor, make vacuum in soft packaging bag be less than 0.08Mpa, then soft packaging bag is sealed; Soft packaging bag after sealing is put into pressure vessel, being forced into 1.15Mpa to pressure vessel insufflation gas, to carry out pressurization softening, within every 3 hours, runs through inspection, within 42 hours, reach required softness number to pressure vessel pressure release with bending method to licorice medicinal materials; Soft packaging bag is taken out to pressure vessel pressure release, opens soft packaging bag, the licorice medicinal materials after softening is spread out and slightly dries in the air, its transepidermal water is evaporated, after medicinal material water content is down to 25% ~ 35% and epidermis tightens up, carry out cutting operation.
Embodiment 10
Remove impurity, the silt of licorice medicinal materials, get the licorice medicinal materials that 250g trims and put into soft packaging bag, licorice medicinal materials quality 0.35 times of water is injected in soft packaging bag, the air in soft packaging bag is removed by air-extractor, make vacuum in soft packaging bag be less than 0.08Mpa, then soft packaging bag is sealed; Soft packaging bag after sealing is put into pressure vessel, being forced into 1.25Mpa to pressure vessel insufflation gas, to carry out pressurization softening, within every 3 hours, runs through inspection, within 36 hours, reach required softness number to pressure vessel pressure release with bending method to licorice medicinal materials; Soft packaging bag is taken out to pressure vessel pressure release, opens soft packaging bag, the licorice medicinal materials after softening is spread out and slightly dries in the air, its transepidermal water is evaporated, after medicinal material water content is down to 25% ~ 35% and epidermis tightens up, carry out cutting operation.
Embodiment 11
Remove impurity, the silt of licorice medicinal materials, get the licorice medicinal materials that 250g trims and put into soft packaging bag, licorice medicinal materials quality 0.4 times of water is injected in soft packaging bag, the air in soft packaging bag is removed by air-extractor, make vacuum in soft packaging bag be less than 0.08Mpa, then soft packaging bag is sealed; Soft packaging bag after sealing is put into pressure vessel, being forced into 1.35Mpa to pressure vessel insufflation gas, to carry out pressurization softening, within every 3 hours, runs through inspection, within 36 hours, reach required softness number to pressure vessel pressure release with bending method to licorice medicinal materials; Soft packaging bag is taken out to pressure vessel pressure release, opens soft packaging bag, the licorice medicinal materials after softening is spread out and slightly dries in the air, its transepidermal water is evaporated, after medicinal material water content is down to 25% ~ 35% and epidermis tightens up, carry out cutting operation.
Embodiment 12
Remove impurity, the silt of licorice medicinal materials, get the licorice medicinal materials that 250g trims and put into soft packaging bag, to in soft packaging bag fill licorice medicinal materials quality 0.45 times of water, the air in soft packaging bag is removed by air-extractor, make vacuum in soft packaging bag be less than 0.08Mpa, then soft packaging bag is sealed; Soft packaging bag after sealing is put into pressure vessel, being forced into 1.45Mpa to pressure vessel insufflation gas, to carry out pressurization softening, within every 3 hours, runs through inspection, within 30 hours, reach required softness number to pressure vessel pressure release with bending method to licorice medicinal materials; Soft packaging bag is taken out to pressure vessel pressure release, opens soft packaging bag, the licorice medicinal materials after softening is spread out and slightly dries in the air, its transepidermal water is evaporated, after medicinal material water content is down to 25% ~ 35% and epidermis tightens up, carry out cutting operation.
The effect that the method for table 3 comparative example 3 and embodiment 9 ~ 12 is softened licorice medicinal materials
By shown in table 3, softening method of the present invention softens licorice medicinal materials, softening water consumption is that traditional bubble profit method softens 1/5th of water consumption, softening consumes time is compared conventional method and is greatly shortened, its liquiritin of medicine materical crude slice after cutting, glycyrrhizic acid content are also high than conventional method, illustrate that the present invention decreases the loss of active ingredient in licorice medicinal materials in softening link.
Claims (2)
1. the softening method before Chinese medicine section, is characterized in that:
The Chinese medicine trimmed is put into soft packaging bag, in soft packaging bag, injects the water of Chinese medicine quality 0.1 ~ 0.8 times, then soft packaging bag sealing is vacuumized, make the little 0.08Mpa of vacuum in soft packaging bag; Soft packaging bag after sealing is put into pressure vessel, regulates pressure to 1.0 ~ 3.0 Mpa, maintain this pressure, treat that the moisture in soft packaging bag penetrates into Chinese medicine inside completely, soft packaging bag is taken out to pressure vessel pressure release.
2. the softening method as claimed in claim 1 before the section of a kind of Chinese medicine, it is characterized in that: after soft packaging bag is taken out, open soft packaging bag, and the Chinese medicine after softening is spread out and slightly dries in the air, its transepidermal water is evaporated, after medicinal material water content is down to 25% ~ 35% and epidermis tightens up, carry out cutting operation.
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| CN201410580504.5A CN104289156B (en) | 2014-10-27 | 2014-10-27 | Method for softening traditional Chinese medicinal material before slicing |
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| CN201410580504.5A CN104289156B (en) | 2014-10-27 | 2014-10-27 | Method for softening traditional Chinese medicinal material before slicing |
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| CN104289156B CN104289156B (en) | 2017-02-01 |
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Cited By (3)
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| CN107582617A (en) * | 2017-10-13 | 2018-01-16 | 河南省三禾药业有限公司 | Radix glycyrrhizae is cut into slices and radix glycyrrhizae fresh-cut technique |
| CN109893447A (en) * | 2019-04-04 | 2019-06-18 | 亳州华宇中药饮片有限公司 | A kind of softening method before Chinese medicine cutting |
| CN111067132A (en) * | 2019-12-12 | 2020-04-28 | 位希望 | Non-tobacco cigarette and preparation method thereof |
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| CN111067132A (en) * | 2019-12-12 | 2020-04-28 | 位希望 | Non-tobacco cigarette and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN104289156B (en) | 2017-02-01 |
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