CN104263518A - Extraction method of phoenix tree flower volatile oil - Google Patents
Extraction method of phoenix tree flower volatile oil Download PDFInfo
- Publication number
- CN104263518A CN104263518A CN201410550343.5A CN201410550343A CN104263518A CN 104263518 A CN104263518 A CN 104263518A CN 201410550343 A CN201410550343 A CN 201410550343A CN 104263518 A CN104263518 A CN 104263518A
- Authority
- CN
- China
- Prior art keywords
- phoenix tree
- volatile oil
- flower
- extraction method
- raw material
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
Abstract
The invention relates to an extraction method of phoenix tree flower volatile oil. The extraction method comprises the following processing steps: drying phoenix tree flowers in the shade, and smashing and screening through a 20-mesh sieve; adding biological enzyme with raw material mass of 1 to 3 percent, spraying an acetic acid/sodium acetate buffer solution which is equivalent to 0.5 to 1.0 time of the raw material and has a pH value of 4.0 to 5.0, packing by using a thin film, and carrying out fermentation at a temperature of 40 to 50 degrees for 3 to 5 days; extracting by using an ultrasound-microwave extraction method, and then carrying out steps of filtering and extracting, vacuum concentrating and the like to obtain the phoenix tree flower volatile oil. The extraction method provided by the invention can effectively improve the extraction ratio of the phoenix tree flower volatile oil, the solvent using amount is reduced, the process is simple, reaction conditions are mild and product quality is good.
Description
Technical field
The present invention relates to a kind of extracting method of Flower of Phoenix Tree volatile oil, belong to active ingredient of natural product extractive technique field.
Background technology
Chinese parasol tree, has another name called blue or green paulownia, belongs to Sterculiaceae deciduous tree.Its root, skin, leaf and Huadu have certain pharmaceutical use.Flower of Phoenix Tree, nature and flavor are sweet flat nontoxic, people liver, kidney, lung three warp, have clearing heat and detoxicating, dispel rheumatism, the effect such as inducing diuresis to remove edema.Cure mainly the illnesss such as oedema, the favus of the scalp, burn and scald.At present, the domestic pharmacological action to Semen Firmianae, leaf and pollen all has research, but rarely has report about the extracting method of volatile oil in Flower of Phoenix Tree.Research shows, Flower of Phoenix Tree chemical composition of volatile oil is more, and containing a large amount of alkanes and haematoporphyrin and yew Paclitaxe, in the last few years, many scholars had carried out large quantifier elimination to these two kinds of compounds, finds that haematoporphyrin is mainly used to treatment malignant tumour etc.; The growth of yew Paclitaxe to glioma cell has obvious restraining effect.Therefore, Flower of Phoenix Tree volatile oil has good using value, can be applicable to the industry such as medicine, healthcare products.
At present, only see the report to Leaf of Phoenix Tree Analysis of Essential Oil Components, and have no the research about its extracting method.Extraction now for volatile oil generally adopts steam distillation and supercritical CO
2extraction process etc.Steam distillation temperature is higher, takes longer, easily makes to change to damp and hot instability and oxidizable composition; And supercritical CO
2extraction process, although have, yield is high, product concentration is high, the advantage of no solvent residue, its apparatus expensive, and maintenance difficult, is not suitable for suitability for industrialized production.
Summary of the invention
The object of the present invention is to provide that a kind of technique is simple, yield is high and the method extracting Flower of Phoenix Tree volatile oil from Flower of Phoenix Tree that product quality is good.
The present invention includes following steps:
Flower of Phoenix Tree dries in the shade, and pulverizes, and crosses 20 mesh sieves; Add the biological enzyme of raw materials quality 1 ~ 3%, spray the acetic acid/sodium acetate buffer being equivalent to pH4.0 ~ 5.0 of raw material 0.5 ~ 1.0 times, film wrapped, in 40 ~ 50 DEG C of fermentations 3 ~ 5 days; Raw material after fermentation is added the ethanolic soln of 3 ~ 5 times 50 ~ 60%, be placed in ultrasonic-microwave extraction device to extract, control ultrasonic wave 500W often to open, microwave power 600 ~ 800W extracts 2 ~ 3h continuously, filters, and filtrate is through organic solvent extraction 2 ~ 3 times, combining extraction liquid, anhydrous sodium sulfate drying, concentrating under reduced pressure, obtains Flower of Phoenix Tree volatile oil.
Biological enzyme of the present invention is cellulase and the hemicellulase of mass ratio 2:1.
Organic solvent of the present invention is the one in sherwood oil or ether.
The invention has the advantages that: utilize fermented by biological enzyme method process raw material, destroy the cell wall structure of raw material, be convenient to the outflow of effective constituent; Again in conjunction with ultrasonic-microwave radiation exaraction, accelerate the leaching of volatile oil in Flower of Phoenix Tree, reaction conditions is gentle, avoids and makes heat-sensitive ingredients or chemically unstable composition volatilize, decompose because temperature is too high, extraction time is long; The method increase production efficiency, extraction yield is high, product quality is good.
Further illustrate the present invention below in conjunction with embodiment, but the scope of protection of present invention is not limited to following embodiments.
embodiment:
Embodiment 1:
Flower of Phoenix Tree dries in the shade, and pulverizes, and crosses 20 mesh sieves, gets 1000g; Add the biological enzyme (cellulase of mass ratio 2:1 and hemicellulase) of raw materials quality 1%, spray the acetic acid/sodium acetate buffer being equivalent to the pH4.0 of raw material 0.5 times, film wrapped, in 40 DEG C of fermentations 3 days; Raw material after fermentation is added the ethanolic soln of 3 times 50%, be placed in ultrasonic-microwave extraction device to extract, control ultrasonic wave 500W often to open, microwave power 600W extracts 2h continuously, filters, and filtrate is through petroleum ether extraction 2 times, combining extraction liquid, anhydrous sodium sulfate drying, concentrating under reduced pressure, obtains the Flower of Phoenix Tree volatile oil 14.67mL of yellow transparent.
Embodiment 2:
Flower of Phoenix Tree dries in the shade, and pulverizes, and crosses 20 mesh sieves, gets 1000g; Add the biological enzyme (cellulase of mass ratio 2:1 and hemicellulase) of raw materials quality 2%, spray the acetic acid/sodium acetate buffer being equivalent to the pH4.5 of raw material 1 times, film wrapped, in 50 DEG C of fermentations 5 days; Raw material after fermentation is added the ethanolic soln of 5 times 60%, be placed in ultrasonic-microwave extraction device to extract, control ultrasonic wave 500W often to open, microwave power 700W extracts 3h continuously, filters, and filtrate is through petroleum ether extraction 3 times, combining extraction liquid, anhydrous sodium sulfate drying, concentrating under reduced pressure, obtains the Flower of Phoenix Tree volatile oil 17.36mL of yellow transparent.
Embodiment 3:
Flower of Phoenix Tree dries in the shade, and pulverizes, and crosses 20 mesh sieves, gets 1000g; Add the biological enzyme (cellulase of mass ratio 2:1 and hemicellulase) of raw materials quality 3%, spray the acetic acid/sodium acetate buffer being equivalent to the pH5.0 of raw material 0.8 times, film wrapped, in 45 DEG C of fermentations 4 days; Raw material after fermentation is added the ethanolic soln of 4 times 55%, be placed in ultrasonic-microwave extraction device to extract, control ultrasonic wave 500W often to open, microwave power 800W extracts 3h continuously, filters, and filtrate is through extracted with diethyl ether 2 times, combining extraction liquid, anhydrous sodium sulfate drying, concentrating under reduced pressure, obtains the Flower of Phoenix Tree volatile oil 12.54mL of yellow transparent.
Claims (3)
1. an extracting method for Flower of Phoenix Tree volatile oil, is characterized in that, comprises the following steps: Flower of Phoenix Tree dries in the shade, and pulverizes, and crosses 20 mesh sieves; Add the biological enzyme of raw materials quality 1 ~ 3%, spray the acetic acid/sodium acetate buffer being equivalent to pH4.0 ~ 5.0 of raw material 0.5 ~ 1.0 times, film wrapped, in 40 ~ 50 DEG C of fermentations 3 ~ 5 days; Raw material after fermentation is added the ethanolic soln of 3 ~ 5 times 50 ~ 60%, be placed in ultrasonic-microwave extraction device to extract, control ultrasonic wave 500W often to open, microwave power 600 ~ 800W extracts 2 ~ 3h continuously, filters, and filtrate is through organic solvent extraction 2 ~ 3 times, combining extraction liquid, anhydrous sodium sulfate drying, concentrating under reduced pressure, obtains Flower of Phoenix Tree volatile oil.
2. the extracting method of a kind of Flower of Phoenix Tree volatile oil according to claim 1, is characterized in that, described biological enzyme is cellulase and the hemicellulase of mass ratio 2:1.
3. the extracting method of a kind of Flower of Phoenix Tree volatile oil according to claim 1, is characterized in that, described organic solvent is the one in sherwood oil or ether.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410550343.5A CN104263518A (en) | 2014-10-17 | 2014-10-17 | Extraction method of phoenix tree flower volatile oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410550343.5A CN104263518A (en) | 2014-10-17 | 2014-10-17 | Extraction method of phoenix tree flower volatile oil |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104263518A true CN104263518A (en) | 2015-01-07 |
Family
ID=52155103
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410550343.5A Pending CN104263518A (en) | 2014-10-17 | 2014-10-17 | Extraction method of phoenix tree flower volatile oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104263518A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105062676A (en) * | 2015-07-29 | 2015-11-18 | 湖北中烟工业有限责任公司 | Acacia farnesiana perfume for tobacco and preparation method thereof |
| CN106323719A (en) * | 2016-11-08 | 2017-01-11 | 四川农业大学 | Huidouba volatile component extraction method |
| CN106906042A (en) * | 2017-03-10 | 2017-06-30 | 刘海春 | A kind of Phoenix Tree Seed edible oil with rush digestion, guarantor's stomach, raising intelligence and immunity |
| CN113230175A (en) * | 2021-05-28 | 2021-08-10 | 潍坊职业学院 | A cosmetic containing Sterculia procumbens extract and its extraction method |
-
2014
- 2014-10-17 CN CN201410550343.5A patent/CN104263518A/en active Pending
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105062676A (en) * | 2015-07-29 | 2015-11-18 | 湖北中烟工业有限责任公司 | Acacia farnesiana perfume for tobacco and preparation method thereof |
| CN105062676B (en) * | 2015-07-29 | 2018-11-23 | 湖北中烟工业有限责任公司 | A kind of Acacia tobacco aromaticss and preparation method thereof |
| CN106323719A (en) * | 2016-11-08 | 2017-01-11 | 四川农业大学 | Huidouba volatile component extraction method |
| CN106323719B (en) * | 2016-11-08 | 2019-12-10 | 四川农业大学 | Extraction method of volatile components of Huidouba |
| CN106906042A (en) * | 2017-03-10 | 2017-06-30 | 刘海春 | A kind of Phoenix Tree Seed edible oil with rush digestion, guarantor's stomach, raising intelligence and immunity |
| CN113230175A (en) * | 2021-05-28 | 2021-08-10 | 潍坊职业学院 | A cosmetic containing Sterculia procumbens extract and its extraction method |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101781606B (en) | Extraction method of rosa rugosa essential oil | |
| CN104263518A (en) | Extraction method of phoenix tree flower volatile oil | |
| CN104194917A (en) | Method for extracting folium artemisiae argyi essential oil | |
| CN104666430A (en) | Method for optimized extraction of total flavonoids of jasmine employing response surface method | |
| CN102453601A (en) | Extraction method of Cinnamomum camphora seed oil by ultrasound-assisted compound enzyme | |
| CN104173398A (en) | Method for extracting notopterygium root volatile oil | |
| CN104164303A (en) | Method for extracting piperis longi volatile oil | |
| CN106176878A (en) | The extracting method of Radix Codonopsis extract | |
| Charpe et al. | Effect of ethanol concentration in ultrasound assisted extraction of glycyrrhizic acid from licorice root | |
| CN106467855A (en) | Peony seed oil supercritical CO 2 extraction technology | |
| CN103349850B (en) | A kind of method for extracting active ingredient in wax-apple | |
| CN106561743A (en) | Plant source medicament for preventing and treating mycetophilids | |
| CN104277916A (en) | Extracting method of blackberry lily essential oil | |
| CN105884737A (en) | Purification technology of sweetberry honeysuckle anthocyanin | |
| CN106187978A (en) | A kind of method extracting pitaya peel procyanidins | |
| CN106117056A (en) | A kind of preparation method of chlorogenic acid extracting from tobacco waste | |
| CN101029276B (en) | Fast method for continuouslly extracting nim oil and nimbin raw medicine from nim seed | |
| CN107285818A (en) | A kind of tea seed cake extract and preparation method thereof | |
| CN106892993A (en) | A kind of preparation method of honey raisin tree slag Thick many candies | |
| CN112608312A (en) | Optimized process for supercritical extraction of matrine | |
| CN104099180A (en) | Extraction method for Stemmacantha uniflora volatile oil | |
| CN106279455B (en) | A kind of comprehensive method for extracting cordycepin and Cordyceps sinensis polysaccharide in Cordyceps militaris of aqueous two-phase | |
| CN104208156A (en) | Method for simultaneously extracting schisandra chinensis volatile oil and lignans | |
| CN104069178A (en) | Extracting method for machilus salicina volatile oil | |
| CN105713937A (en) | Method for obtaining raphanin from broccoli hairy root culture system |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20150107 |
|
| WD01 | Invention patent application deemed withdrawn after publication |