CN104203899A - 获得碳酸二烷基酯和亚烷基二醇的方法 - Google Patents

获得碳酸二烷基酯和亚烷基二醇的方法 Download PDF

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Publication number
CN104203899A
CN104203899A CN201280069004.4A CN201280069004A CN104203899A CN 104203899 A CN104203899 A CN 104203899A CN 201280069004 A CN201280069004 A CN 201280069004A CN 104203899 A CN104203899 A CN 104203899A
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CN
China
Prior art keywords
carbonate
stream
alkylene
alkylene glycol
dialkyl carbonate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
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CN201280069004.4A
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English (en)
Chinese (zh)
Inventor
A·施密特
M·伯克
R·罗特格尔
R·鲍曼
A·弗兰克
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BASF SE
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BASF SE
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Application filed by BASF SE filed Critical BASF SE
Publication of CN104203899A publication Critical patent/CN104203899A/zh
Pending legal-status Critical Current

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/141—Fractional distillation or use of a fractionation or rectification column where at least one distillation column contains at least one dividing wall
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/36—Azeotropic distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/86—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C68/00—Preparation of esters of carbonic or haloformic acids
    • C07C68/06—Preparation of esters of carbonic or haloformic acids from organic carbonates
    • C07C68/065—Preparation of esters of carbonic or haloformic acids from organic carbonates from alkylene carbonates
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C68/00—Preparation of esters of carbonic or haloformic acids
    • C07C68/08—Purification; Separation; Stabilisation
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CN201280069004.4A 2011-12-05 2012-12-05 获得碳酸二烷基酯和亚烷基二醇的方法 Pending CN104203899A (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP11191894.2 2011-12-05
EP11191894 2011-12-05
PCT/EP2012/074478 WO2013083618A1 (de) 2011-12-05 2012-12-05 Verfahren zur gewinnung eines dialkylcarbonats und eines alkylenglykols

Publications (1)

Publication Number Publication Date
CN104203899A true CN104203899A (zh) 2014-12-10

Family

ID=47351616

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201280069004.4A Pending CN104203899A (zh) 2011-12-05 2012-12-05 获得碳酸二烷基酯和亚烷基二醇的方法

Country Status (7)

Country Link
EP (1) EP2788315A1 (enExample)
JP (1) JP2015504855A (enExample)
KR (1) KR20140113931A (enExample)
CN (1) CN104203899A (enExample)
BR (1) BR112014013557A2 (enExample)
IN (1) IN2014CN04151A (enExample)
WO (1) WO2013083618A1 (enExample)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109661259A (zh) * 2016-09-08 2019-04-19 伊士曼化工公司 用于分离具有非均相共沸物的三元组合物的热集成蒸馏系统和使用其的方法
CN114555553A (zh) * 2019-10-03 2022-05-27 国际壳牌研究有限公司 用于制备碳酸二烷基酯和链烷二醇的方法

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPWO2013150989A1 (ja) * 2012-04-04 2015-12-17 旭硝子株式会社 ジオールおよびジブチルカーボネートの分離方法、精製方法、ならびに製造方法
DK3368104T3 (da) 2015-10-28 2021-11-15 Shl Medical Ag Medikamentbeholderfatning
CN108440297A (zh) * 2017-03-23 2018-08-24 秦燕雯 一种用于碳酸二甲酯装置节能降耗的装置
WO2021110627A1 (en) * 2019-12-06 2021-06-10 Shell Internationale Research Maatschappij B.V. Process for removing an ether alkanol impurity from an organic carbonate stream
EP3831805A1 (en) * 2019-12-06 2021-06-09 Shell Internationale Research Maatschappij B.V. Process for the preparation of a dialkyl carbonate and an alkanediol
CN115594585B (zh) * 2022-12-13 2023-04-07 江苏华盛锂电材料股份有限公司 一种一步合成并提纯甲基三氟乙基碳酸酯的方法

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3642858A (en) * 1969-02-12 1972-02-15 Dow Chemical Co Carbonate synthesis from alkylene carbonates
US6166240A (en) * 2000-02-22 2000-12-26 Mobil Oil Corporation Process for co-production of dialkyl carbonate and alkanediol
US20030078448A1 (en) * 2001-10-12 2003-04-24 Buchanan J. Scott Co-productiion of dialkyl carbonates and diols with treatment of hydroxy alkyl carbonate
CN101935280A (zh) * 2009-06-26 2011-01-05 拜尔材料科学股份公司 由碳酸亚烷基酯和醇来制备碳酸二烷基酯的方法

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US5489703A (en) 1995-05-19 1996-02-06 Amoco Corporation Reaction extraction of alkyl carbonate
EP0889025B1 (en) 1995-12-22 2002-04-03 Asahi Kasei Kabushiki Kaisha Process for continuously preparing dialkyl carbonates and diols
CN1145600C (zh) 1998-06-10 2004-04-14 旭化成株式会社 连续生产碳酸二烷基酯和二醇的方法
WO2000051954A1 (en) 1999-03-03 2000-09-08 Asahi Kasei Kabushiki Kaisha Process for continuously producing dialkyl carbonate and diol
JP2003300918A (ja) * 2002-04-11 2003-10-21 Mitsui Chemicals Inc ジアルキルカーボネートとグリコールの連続同時製造方法
US6620959B1 (en) 2002-04-16 2003-09-16 Exxonmobil Chemical Patents Inc. Process for the production of unsymmetric and/or symmetric dialkyl carbonates and diols
JP4000912B2 (ja) * 2002-05-30 2007-10-31 三菱化学株式会社 ジメチルカーボネートの製造方法
JP4424898B2 (ja) * 2002-10-08 2010-03-03 旭化成ケミカルズ株式会社 ジアルキルカーボネートおよびジオールを製造する方法
JP2006023065A (ja) 2004-06-10 2006-01-26 Mitsubishi Electric Corp 換気機能付き空気調和機及び換気機能付き空気調和機の換気装置及び換気機能付き空気調和機の換気方法
JP2006206497A (ja) * 2005-01-28 2006-08-10 Asahi Kasei Chemicals Corp ジアルキルカーボネートおよびジオールを製造する方法
CN101326146B (zh) 2005-12-12 2011-12-28 旭化成化学株式会社 碳酸二烷基酯和二醇类的工业制备方法
TW200732291A (en) 2005-12-14 2007-09-01 Asahi Kasei Chemicals Corp Process for production of dialkyl carbonate and diol in industrial scale and with high yield
TWI383976B (zh) 2006-02-22 2013-02-01 Shell Int Research 製備碳酸二烷酯及烷二醇的方法
JP5094459B2 (ja) 2007-03-09 2012-12-12 ローム アンド ハース カンパニー アルカンを不飽和カルボン酸に変換するための改良法
DE102009053370A1 (de) 2009-11-14 2011-05-19 Bayer Materialscience Ag Verfahren zur Reinigung von Dialkylcarbonaten
TWI473786B (zh) 2009-11-16 2015-02-21 Shell Int Research 製備烷二醇及碳酸二烷酯的方法

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3642858A (en) * 1969-02-12 1972-02-15 Dow Chemical Co Carbonate synthesis from alkylene carbonates
US6166240A (en) * 2000-02-22 2000-12-26 Mobil Oil Corporation Process for co-production of dialkyl carbonate and alkanediol
US20030078448A1 (en) * 2001-10-12 2003-04-24 Buchanan J. Scott Co-productiion of dialkyl carbonates and diols with treatment of hydroxy alkyl carbonate
CN101935280A (zh) * 2009-06-26 2011-01-05 拜尔材料科学股份公司 由碳酸亚烷基酯和醇来制备碳酸二烷基酯的方法

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109661259A (zh) * 2016-09-08 2019-04-19 伊士曼化工公司 用于分离具有非均相共沸物的三元组合物的热集成蒸馏系统和使用其的方法
CN109661259B (zh) * 2016-09-08 2021-10-01 伊士曼化工公司 用于分离具有非均相共沸物的三元组合物的热集成蒸馏系统和使用其的方法
CN114555553A (zh) * 2019-10-03 2022-05-27 国际壳牌研究有限公司 用于制备碳酸二烷基酯和链烷二醇的方法
CN114555553B (zh) * 2019-10-03 2024-04-05 国际壳牌研究有限公司 用于制备碳酸二烷基酯和链烷二醇的方法

Also Published As

Publication number Publication date
JP2015504855A (ja) 2015-02-16
WO2013083618A1 (de) 2013-06-13
BR112014013557A2 (pt) 2017-06-13
KR20140113931A (ko) 2014-09-25
IN2014CN04151A (enExample) 2015-07-17
EP2788315A1 (de) 2014-10-15

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Application publication date: 20141210